CA3014623C - Lithium recovery from phosphate minerals - Google Patents

Lithium recovery from phosphate minerals Download PDF

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Publication number
CA3014623C
CA3014623C CA3014623A CA3014623A CA3014623C CA 3014623 C CA3014623 C CA 3014623C CA 3014623 A CA3014623 A CA 3014623A CA 3014623 A CA3014623 A CA 3014623A CA 3014623 C CA3014623 C CA 3014623C
Authority
CA
Canada
Prior art keywords
lithium
phosphate
impurity removal
impurity
removal step
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CA3014623A
Other languages
English (en)
French (fr)
Other versions
CA3014623A1 (en
Inventor
Gary Donald Johnson
Mark Daniel Urbani
Nicholas John VINES
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Li Technology Pty Ltd
Original Assignee
Li Technology Pty Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from AU2016900582A external-priority patent/AU2016900582A0/en
Application filed by Li Technology Pty Ltd filed Critical Li Technology Pty Ltd
Publication of CA3014623A1 publication Critical patent/CA3014623A1/en
Application granted granted Critical
Publication of CA3014623C publication Critical patent/CA3014623C/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B26/00—Obtaining alkali, alkaline earth metals or magnesium
    • C22B26/10—Obtaining alkali metals
    • C22B26/12—Obtaining lithium
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B1/00—Preliminary treatment of ores or scrap
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/04—Extraction of metal compounds from ores or concentrates by wet processes by leaching
    • C22B3/06—Extraction of metal compounds from ores or concentrates by wet processes by leaching in inorganic acid solutions, e.g. with acids generated in situ; in inorganic salt solutions other than ammonium salt solutions
    • C22B3/08—Sulfuric acid, other sulfurated acids or salts thereof
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/44—Treatment or purification of solutions, e.g. obtained by leaching by chemical processes
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00—Technologies related to metal processing
    • Y02P10/20—Recycling

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Organic Chemistry (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Manufacturing & Machinery (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Metallurgy (AREA)
  • Environmental & Geological Engineering (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Removal Of Specific Substances (AREA)
CA3014623A 2016-02-18 2017-02-17 Lithium recovery from phosphate minerals Active CA3014623C (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
AU2016900582 2016-02-18
AU2016900582A AU2016900582A0 (en) 2016-02-18 Lithium Recovery Process
PCT/AU2017/050142 WO2017139852A1 (en) 2016-02-18 2017-02-17 Lithium recovery from phosphate minerals

Publications (2)

Publication Number Publication Date
CA3014623A1 CA3014623A1 (en) 2017-08-24
CA3014623C true CA3014623C (en) 2023-08-22

Family

ID=59624689

Family Applications (1)

Application Number Title Priority Date Filing Date
CA3014623A Active CA3014623C (en) 2016-02-18 2017-02-17 Lithium recovery from phosphate minerals

Country Status (8)

Country Link
US (1) US10894997B2 (enExample)
EP (1) EP3417082B1 (enExample)
JP (1) JP6964084B2 (enExample)
AU (1) AU2017220394B2 (enExample)
CA (1) CA3014623C (enExample)
ES (1) ES2929719T3 (enExample)
PT (1) PT3417082T (enExample)
WO (1) WO2017139852A1 (enExample)

Families Citing this family (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108640131A (zh) * 2018-04-28 2018-10-12 四川思达能环保科技有限公司 锂矿石制备碳酸锂的方法及系统
US11180860B2 (en) 2018-05-18 2021-11-23 California Institute Of Technology Process to convert reduced sulfur species and water into hydrogen and sulfuric acid
WO2019220003A1 (en) * 2018-05-18 2019-11-21 Outotec (Finland) Oy Method for recovering lithium hydroxide
AU2019277206B2 (en) 2018-05-30 2025-06-26 Australian Nuclear Science And Technology Organisation Process for recovering lithium values
EP3802892B1 (en) * 2018-05-30 2023-08-30 Lithium Australia NL Process for recovering lithium phosphate and lithium sulfate from lithium-bearing silicates
CN109052436B (zh) * 2018-09-21 2022-01-07 深圳市德方纳米科技股份有限公司 一种由锂磷铝石制备含锂化合物的方法
CN113825848A (zh) * 2019-03-29 2021-12-21 锂业美洲公司 从沉积粘土中提取锂的方法
WO2021030529A1 (en) 2019-08-13 2021-02-18 California Institute Of Technology Process to make calcium oxide or ordinary portland cement from calcium bearing rocks and minerals
CN110817829A (zh) * 2019-12-13 2020-02-21 九江天赐高新材料有限公司 一种由含铝磷的固体原料制备高纯无水正磷酸铝的方法
US10995014B1 (en) 2020-07-10 2021-05-04 Northvolt Ab Process for producing crystallized metal sulfates
JP2023551108A (ja) * 2020-11-03 2023-12-07 ハッチ リミテッド 金属硫酸塩を結晶化するための処理方法
US20220340438A1 (en) * 2021-04-22 2022-10-27 Ut-Battelle, Llc Selective extraction of lithium from lithium sulfate aqueous solution
CN114032388B (zh) * 2021-09-17 2023-08-22 江西金德锂新能源科技有限公司 一种从锂云母原料中提取金属盐的工艺
CN114751434B (zh) * 2022-04-28 2023-11-24 中国地质科学院郑州矿产综合利用研究所 一种沉积型锂资源的综合回收利用方法
CN115652109B (zh) * 2022-11-18 2024-03-12 广东邦普循环科技有限公司 一种废旧锂电池浸出液的处理方法
US20240228310A1 (en) * 2023-01-06 2024-07-11 Lithium Nevada Corporation Magnesium removal process
WO2024163813A2 (en) * 2023-02-01 2024-08-08 US Metals Refining Group, Inc. Selective separation of metals from mineral-rich concentrates
CN116986615B (zh) * 2023-05-08 2025-10-24 四川顺应锂材料科技有限公司 一种磷铝锂矿中磷铝锂元素综合利用的方法
CN116514147A (zh) * 2023-05-08 2023-08-01 四川顺应锂材料科技有限公司 一种从磷锂铝矿中回收磷、锂、铝资源的方法
CN116730369A (zh) * 2023-06-20 2023-09-12 深圳市翼能新材料科技有限公司 一种锂磷铝石矿综合利用的方法
CN117385176B (zh) * 2023-10-16 2026-03-24 云南云铝润鑫铝业有限公司 一种从铝电解固废水处理渣中提取有价锂元素的系统
KR20260098263A (ko) * 2024-12-19 2026-06-26 포스코홀딩스 주식회사 황산리튬 용액을 정제하는 방법

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1591196A (en) 1923-12-12 1926-07-06 Allied Process Corp Process of recovering lithium salts from phosphate minerals containing lithium
GB424757A (en) 1933-07-13 1935-02-27 Hans Heinrich Huette Ges Mit B Process for the treatment of originating materials containing lithium phosphate
US2040573A (en) 1933-07-13 1936-05-12 American Lurgi Corp Process for the production of lithium salts
US2024026A (en) * 1933-11-17 1935-12-10 Warner Chemical Company Recovering lithium compounds
US8431005B1 (en) * 2010-06-24 2013-04-30 Western Lithium Corporation Production of lithium and potassium compounds
CN102285673B (zh) * 2011-06-03 2013-11-06 广东邦普循环科技股份有限公司 一种从电动汽车磷酸铁锂动力电池中回收锂和铁的方法
AU2013201833B2 (en) * 2012-08-13 2014-07-17 Reed Advanced Materials Pty Ltd Processing of Lithium Containing Ore
KR102445712B1 (ko) * 2013-10-23 2022-09-20 네마스카 리튬 인코포레이션 리튬 카보네이트의 제조방법
PT3204528T (pt) * 2014-10-10 2020-07-15 Li Tech Pty Ltd Processo de recuperação

Also Published As

Publication number Publication date
EP3417082A4 (en) 2019-08-28
JP6964084B2 (ja) 2021-11-10
PT3417082T (pt) 2022-11-08
ES2929719T3 (es) 2022-12-01
AU2017220394B2 (en) 2021-12-23
EP3417082B1 (en) 2022-10-26
JP2019508587A (ja) 2019-03-28
CA3014623A1 (en) 2017-08-24
AU2017220394A1 (en) 2018-08-23
WO2017139852A1 (en) 2017-08-24
EP3417082A1 (en) 2018-12-26
US10894997B2 (en) 2021-01-19
US20190185963A1 (en) 2019-06-20

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