CA2858403A1 - A method of making a hydrogen separation composite membrane - Google Patents

A method of making a hydrogen separation composite membrane Download PDF

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Publication number
CA2858403A1
CA2858403A1 CA2858403A CA2858403A CA2858403A1 CA 2858403 A1 CA2858403 A1 CA 2858403A1 CA 2858403 A CA2858403 A CA 2858403A CA 2858403 A CA2858403 A CA 2858403A CA 2858403 A1 CA2858403 A1 CA 2858403A1
Authority
CA
Canada
Prior art keywords
support
particulate material
coated
gas
particle size
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
CA2858403A
Other languages
English (en)
French (fr)
Inventor
John Charles Saukaitis
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shell Internationale Research Maatschappij BV
Original Assignee
Shell Internationale Research Maatschappij BV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shell Internationale Research Maatschappij BV filed Critical Shell Internationale Research Maatschappij BV
Publication of CA2858403A1 publication Critical patent/CA2858403A1/en
Abandoned legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
    • B01D69/10—Supported membranes; Membrane supports
    • B01D69/108—Inorganic support material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/22—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by diffusion
    • B01D53/228—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by diffusion characterised by specific membranes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
    • B01D67/0039—Inorganic membrane manufacture
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
    • B01D67/0039—Inorganic membrane manufacture
    • B01D67/0046—Inorganic membrane manufacture by slurry techniques, e.g. die or slip-casting
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
    • B01D67/0039—Inorganic membrane manufacture
    • B01D67/0069—Inorganic membrane manufacture by deposition from the liquid phase, e.g. electrochemical deposition
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
    • B01D67/0039—Inorganic membrane manufacture
    • B01D67/0076—Pretreatment of inorganic membrane material prior to membrane formation, e.g. coating of metal powder
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
    • B01D67/0081—After-treatment of organic or inorganic membranes
    • B01D67/0095—Drying
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
    • B01D69/02—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor characterised by their properties
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
    • B01D69/10—Supported membranes; Membrane supports
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
    • B01D69/12—Composite membranes; Ultra-thin membranes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
    • B01D69/12—Composite membranes; Ultra-thin membranes
    • B01D69/1213—Laminated layers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D71/00—Semi-permeable membranes for separation processes or apparatus characterised by the material; Manufacturing processes specially adapted therefor
    • B01D71/02—Inorganic material
    • B01D71/022—Metals
    • B01D71/0223—Group 8, 9 or 10 metals
    • B01D71/02231—Palladium
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen; Reversible storage of hydrogen
    • C01B3/50—Separation of hydrogen or hydrogen-containing gases from gaseous mixtures, e.g. purification
    • C01B3/501—Separation of hydrogen or hydrogen-containing gases from gaseous mixtures, e.g. purification by diffusion
    • C01B3/503—Separation of hydrogen or hydrogen-containing gases from gaseous mixtures, e.g. purification by diffusion characterised by membranes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2256/00—Main component in the product gas stream after treatment
    • B01D2256/16—Hydrogen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2323/00—Details relating to membrane preparation
    • B01D2323/08—Specific temperatures applied
    • B01D2323/081—Heating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2323/00—Details relating to membrane preparation
    • B01D2323/10—Specific pressure applied
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2325/00—Details relating to properties of membranes
    • B01D2325/02—Details relating to pores or porosity of the membranes
    • B01D2325/0283—Pore size
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2325/00—Details relating to properties of membranes
    • B01D2325/06—Surface irregularities
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2325/00—Details relating to properties of membranes
    • B01D2325/22—Thermal or heat-resistance properties

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Electrochemistry (AREA)
  • Combustion & Propulsion (AREA)
  • Analytical Chemistry (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
  • Hydrogen, Water And Hydrids (AREA)
CA2858403A 2011-12-19 2012-12-17 A method of making a hydrogen separation composite membrane Abandoned CA2858403A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201161577479P 2011-12-19 2011-12-19
US61/577,479 2011-12-19
PCT/US2012/070064 WO2013096183A1 (en) 2011-12-19 2012-12-17 A method of making a hydrogen separation composite membrane

Publications (1)

Publication Number Publication Date
CA2858403A1 true CA2858403A1 (en) 2013-06-27

Family

ID=47505346

Family Applications (1)

Application Number Title Priority Date Filing Date
CA2858403A Abandoned CA2858403A1 (en) 2011-12-19 2012-12-17 A method of making a hydrogen separation composite membrane

Country Status (8)

Country Link
US (1) US20130156945A1 (enExample)
EP (1) EP2794066B1 (enExample)
JP (1) JP2015507533A (enExample)
KR (1) KR20140108642A (enExample)
CN (1) CN104010713B (enExample)
CA (1) CA2858403A1 (enExample)
TW (1) TW201336577A (enExample)
WO (1) WO2013096183A1 (enExample)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101475679B1 (ko) * 2012-12-14 2014-12-23 한국에너지기술연구원 이산화탄소 포집용 수소 분리막 모듈
US20150290591A1 (en) * 2014-04-10 2015-10-15 Shell Oil Company Method of making a supported gas separation membrane
JP6787790B2 (ja) * 2014-04-10 2020-11-18 シエル・インターナシヨナル・リサーチ・マートスハツペイ・ベー・ヴエー 担持されたガス分離膜を作製する方法
US20210308630A1 (en) * 2020-04-07 2021-10-07 Ralph Aaron Bauer Support for Nano-Thickness Membranes
CN111686586B (zh) * 2020-06-29 2022-06-07 山东理工大学 一种用于在氧化铝中空纤维膜内表面制备钯膜的真空流动化学镀法
JP7300023B1 (ja) * 2022-01-31 2023-06-28 東邦チタニウム株式会社 チタン多孔質体及び、チタン多孔質体の製造方法

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20030190486A1 (en) * 2002-04-03 2003-10-09 Fernando Roa Process for Preparing Palladium Alloy Composite Membranes for Use in Hydrogen Separation, Palladium Alloy Composite Membranes and Products Incorporating or Made from the Membranes
CA2519774A1 (en) 2003-03-21 2004-10-07 Worcester Polytechnic Institute Method for fabricating composite gas separation modules
JP4379684B2 (ja) * 2003-07-09 2009-12-09 株式会社豊田中央研究所 流体分離フィルタおよびその製造方法と燃料電池システム
EP1723999B1 (en) * 2004-03-12 2017-06-07 NGK Insulators, Ltd. Carbon film laminate and method for production thereof, and voc removing device
JP2005262082A (ja) * 2004-03-18 2005-09-29 National Institute Of Advanced Industrial & Technology 水素分離膜、その製造方法並びに水素の分離方法
US7727596B2 (en) 2004-07-21 2010-06-01 Worcester Polytechnic Institute Method for fabricating a composite gas separation module
JP2008513337A (ja) * 2004-09-21 2008-05-01 ウスター ポリテクニック インスティチュート 膜増強反応器
JP2007000858A (ja) * 2005-05-23 2007-01-11 Kobe Steel Ltd 水素透過部材およびその製造方法
CN101351263B (zh) * 2006-07-20 2012-09-05 日本碍子株式会社 陶瓷过滤器
US7744675B2 (en) 2006-11-08 2010-06-29 Shell Oil Company Gas separation membrane comprising a substrate with a layer of coated inorganic oxide particles and an overlayer of a gas-selective material, and its manufacture and use
US7959711B2 (en) 2006-11-08 2011-06-14 Shell Oil Company Gas separation membrane system and method of making thereof using nanoscale metal material
US8048199B2 (en) * 2007-02-20 2011-11-01 Shell Oil Company Method of making a leak stable gas separation membrane system
CA2678274A1 (en) * 2007-02-20 2008-10-02 Shell Internationale Research Maatschappij B.V. A gas separation membrane system and a method of preparing or reconditioning and the use thereof
US20080255811A1 (en) * 2007-04-13 2008-10-16 Zi Qiang Sheng System and Method for Determining Surface Roughness
US20090277331A1 (en) * 2008-05-09 2009-11-12 Membrane Reactor Technologies Ltd. Hydrogen separation composite membrane module and the method of production thereof
JP5354516B2 (ja) * 2008-08-15 2013-11-27 日本碍子株式会社 水素分離体
JP5526387B2 (ja) * 2010-03-29 2014-06-18 独立行政法人産業技術総合研究所 無欠陥化水素分離膜、無欠陥化水素分離膜の製造方法及び水素分離方法

Also Published As

Publication number Publication date
US20130156945A1 (en) 2013-06-20
JP2015507533A (ja) 2015-03-12
WO2013096183A1 (en) 2013-06-27
EP2794066B1 (en) 2019-08-14
TW201336577A (zh) 2013-09-16
KR20140108642A (ko) 2014-09-12
EP2794066A1 (en) 2014-10-29
CN104010713B (zh) 2016-06-01
CN104010713A (zh) 2014-08-27

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Legal Events

Date Code Title Description
FZDE Discontinued

Effective date: 20161219