CA2829481A1 - Methods of producing biofuels, chlorophylls and carotenoids - Google Patents

Methods of producing biofuels, chlorophylls and carotenoids Download PDF

Info

Publication number
CA2829481A1
CA2829481A1 CA2829481A CA2829481A CA2829481A1 CA 2829481 A1 CA2829481 A1 CA 2829481A1 CA 2829481 A CA2829481 A CA 2829481A CA 2829481 A CA2829481 A CA 2829481A CA 2829481 A1 CA2829481 A1 CA 2829481A1
Authority
CA
Canada
Prior art keywords
extraction
fraction
algal
biomass
solvent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
CA2829481A
Other languages
English (en)
French (fr)
Inventor
Aniket Kale
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Heliae Development LLC
Original Assignee
Heliae Development LLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US13/081,221 external-priority patent/US8084038B2/en
Priority claimed from US13/149,595 external-priority patent/US8115022B2/en
Application filed by Heliae Development LLC filed Critical Heliae Development LLC
Publication of CA2829481A1 publication Critical patent/CA2829481A1/en
Abandoned legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00Refining fats or fatty oils
    • C11B3/10Refining fats or fatty oils by adsorption
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12PFERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00Preparation of oxygen-containing organic compounds
    • C12P7/64Fats; Fatty oils; Ester-type waxes; Higher fatty acids, i.e. having at least seven carbon atoms in an unbroken chain bound to a carboxyl group; Oxidised oils or fats
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10LFUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00Liquid carbonaceous fuels
    • C10L1/02Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only
    • C10L1/026Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only for compression ignition
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10LFUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00Liquid carbonaceous fuels
    • C10L1/04Liquid carbonaceous fuels essentially based on blends of hydrocarbons
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10LFUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00Liquid carbonaceous fuels
    • C10L1/04Liquid carbonaceous fuels essentially based on blends of hydrocarbons
    • C10L1/08Liquid carbonaceous fuels essentially based on blends of hydrocarbons for compression ignition
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/02Pretreatment
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/10Production of fats or fatty oils from raw materials by extracting
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00Refining fats or fatty oils
    • C11B3/008Refining fats or fatty oils by filtration, e.g. including ultra filtration, dialysis
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11CFATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/003Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12PFERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00Preparation of oxygen-containing organic compounds
    • C12P7/64Fats; Fatty oils; Ester-type waxes; Higher fatty acids, i.e. having at least seven carbon atoms in an unbroken chain bound to a carboxyl group; Oxidised oils or fats
    • C12P7/6436Fatty acid esters
    • C12P7/6445Glycerides
    • C12P7/6458Glycerides by transesterification, e.g. interesterification, ester interchange, alcoholysis or acidolysis
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12PFERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00Preparation of oxygen-containing organic compounds
    • C12P7/64Fats; Fatty oils; Ester-type waxes; Higher fatty acids, i.e. having at least seven carbon atoms in an unbroken chain bound to a carboxyl group; Oxidised oils or fats
    • C12P7/6436Fatty acid esters
    • C12P7/6445Glycerides
    • C12P7/6472Glycerides containing polyunsaturated fatty acid [PUFA] residues, i.e. having two or more double bonds in their backbone
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00Technologies for the production of fuel of non-fossil origin
    • Y02E50/10Biofuels, e.g. bio-diesel

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Zoology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • General Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Biotechnology (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Liquid Carbonaceous Fuels (AREA)
  • Fats And Perfumes (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Micro-Organisms Or Cultivation Processes Thereof (AREA)
CA2829481A 2011-04-06 2012-03-02 Methods of producing biofuels, chlorophylls and carotenoids Abandoned CA2829481A1 (en)

Applications Claiming Priority (6)

Application Number Priority Date Filing Date Title
US13/081,221 US8084038B2 (en) 2010-04-06 2011-04-06 Methods of and systems for isolating nutraceutical products from algae
US13/081,221 2011-04-06
US13/149,595 US8115022B2 (en) 2010-04-06 2011-05-31 Methods of producing biofuels, chlorophylls and carotenoids
US13/149,595 2011-05-31
US13/274,201 2011-10-14
PCT/US2012/027537 WO2012138438A1 (en) 2011-04-06 2012-03-02 Methods of producing biofuels, chlorophylls and carotenoids

Publications (1)

Publication Number Publication Date
CA2829481A1 true CA2829481A1 (en) 2012-10-11

Family

ID=46969499

Family Applications (1)

Application Number Title Priority Date Filing Date
CA2829481A Abandoned CA2829481A1 (en) 2011-04-06 2012-03-02 Methods of producing biofuels, chlorophylls and carotenoids

Country Status (10)

Country Link
EP (1) EP2675877A1 (es)
JP (1) JP2014514924A (es)
KR (1) KR20140010972A (es)
CN (1) CN103492541A (es)
AU (1) AU2012240608A1 (es)
BR (1) BR112013025609A2 (es)
CA (1) CA2829481A1 (es)
MX (1) MX2013011520A (es)
SG (1) SG193373A1 (es)
WO (1) WO2012138438A1 (es)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104168761A (zh) * 2012-02-29 2014-11-26 埃克森美孚研究工程公司 从藻类中溶剂萃取产物

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8308951B1 (en) 2010-04-06 2012-11-13 Heliae Development, Llc Extraction of proteins by a two solvent method
US8115022B2 (en) 2010-04-06 2012-02-14 Heliae Development, Llc Methods of producing biofuels, chlorophylls and carotenoids
US8475660B2 (en) 2010-04-06 2013-07-02 Heliae Development, Llc Extraction of polar lipids by a two solvent method
US8273248B1 (en) 2010-04-06 2012-09-25 Heliae Development, Llc Extraction of neutral lipids by a two solvent method
CA2793695A1 (en) 2010-04-06 2011-10-13 Heliae Development, Llc Selective extraction of proteins from freshwater algae
WO2013052598A1 (en) * 2011-10-04 2013-04-11 Heliae Development, Llc Method of producing biofuels from algal cell culture
US9200236B2 (en) 2011-11-17 2015-12-01 Heliae Development, Llc Omega 7 rich compositions and methods of isolating omega 7 fatty acids
CN103058462B (zh) * 2013-01-14 2013-12-18 江苏省农业科学院 一种双体系串联净化染料废水的方法
CN104628734B (zh) * 2014-12-25 2017-06-30 中国科学院南海海洋研究所 一种微藻叶绿素的脱除方法
CN107874253A (zh) * 2016-09-30 2018-04-06 国家开发投资公司 一种富含γ‑亚麻酸的螺旋藻糖脂制备方法
JP2021521882A (ja) * 2018-04-20 2021-08-30 ナノ アルジー ソリューションズ アーゲー エイコサペンタエン酸オイル組成物を提供するための新規なプロセス

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5008227A (en) * 1989-05-16 1991-04-16 Engelhard Corporation Process for making acid activated bleaching earth using high susceptibility source clay and novel bleaching earth product
DE4219360C2 (de) * 1992-06-12 1994-07-28 Milupa Ag Verfahren zur Gewinnung von Lipiden mit einem hohen Anteil von langkettig-hochungesättigten Fettsäuren
JP3128712B2 (ja) * 1992-10-02 2001-01-29 東和化成工業株式会社 クロロフィル類組成物の新規製造法
CA2113409A1 (en) * 1993-02-12 1994-08-13 Robert S. Nebergall Process for regenerating, and optionally carbonizing, spent acid-activated smectite clays
JPH07252493A (ja) * 1994-03-16 1995-10-03 Kawasaki Steel Corp 海洋性微細藻類からのドコサヘキサエン酸エステルの分離精製方法
JP4545235B2 (ja) * 1996-03-28 2010-09-15 ディーエスエム アイピー アセッツ ビー.ブイ. 顆粒状微生物バイオマスの製造法とそのバイオマスからの貴重化合物の単離法
ES2175409T5 (es) * 1996-05-15 2007-05-01 Dsm Ip Assets B.V. Extraccion de esterol con un disolvente polar para dar un aceite microbiano bajo en esterol.
US7045607B2 (en) 1999-05-18 2006-05-16 The Board Of Trustees Of The University Of Illinois Method and system for extraction of zein from corn
FR2904773B1 (fr) * 2006-08-11 2008-11-07 Lvmh Rech Composition cosmetique amincissante contenant un extrait de biomasse de l'algue neochloris oleoabundans
US8088614B2 (en) * 2006-11-13 2012-01-03 Aurora Algae, Inc. Methods and compositions for production and purification of biofuel from plants and microalgae
KR100896327B1 (ko) * 2008-09-09 2009-05-07 다이아텍코리아 주식회사 스피루리나로부터 클로로필 a 및 클로린을 제조하는 방법
KR100950441B1 (ko) * 2009-09-30 2010-04-02 주식회사 아큐텍 스피루리나로부터 클로로필 a 및 포토디타진을 제조하는 방법

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104168761A (zh) * 2012-02-29 2014-11-26 埃克森美孚研究工程公司 从藻类中溶剂萃取产物

Also Published As

Publication number Publication date
MX2013011520A (es) 2014-01-08
NZ615225A (en) 2015-11-27
KR20140010972A (ko) 2014-01-27
WO2012138438A1 (en) 2012-10-11
JP2014514924A (ja) 2014-06-26
AU2012240608A1 (en) 2013-09-19
CN103492541A (zh) 2014-01-01
BR112013025609A2 (pt) 2016-12-27
EP2675877A1 (en) 2013-12-25
SG193373A1 (en) 2013-10-30

Similar Documents

Publication Publication Date Title
US8569531B2 (en) Isolation of chlorophylls from intact algal cells
AU2011237695B2 (en) Sequential solvent extraction of oil and proteinaceous material from oleaginous material by using solvents of decreasing polarity
CA2829577A1 (en) Extraction of neutral lipids by a two solvent method
CA2828957A1 (en) Extraction of polar lipids by a two solvent method
CA2830183A1 (en) Extraction of proteins from algae
CA2829481A1 (en) Methods of producing biofuels, chlorophylls and carotenoids

Legal Events

Date Code Title Description
FZDE Discontinued

Effective date: 20180302