CA2405963C - Synthetic platy magadiite and octasilicate - Google Patents
Synthetic platy magadiite and octasilicate Download PDFInfo
- Publication number
- CA2405963C CA2405963C CA002405963A CA2405963A CA2405963C CA 2405963 C CA2405963 C CA 2405963C CA 002405963 A CA002405963 A CA 002405963A CA 2405963 A CA2405963 A CA 2405963A CA 2405963 C CA2405963 C CA 2405963C
- Authority
- CA
- Canada
- Prior art keywords
- magadiite
- synthetic
- platy
- silica
- mole ratio
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 241000276425 Xiphophorus maculatus Species 0.000 title claims abstract description 47
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 120
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 40
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 39
- 239000007788 liquid Substances 0.000 claims abstract description 34
- 239000008119 colloidal silica Substances 0.000 claims abstract description 28
- 239000000725 suspension Substances 0.000 claims abstract description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 19
- 229910001868 water Inorganic materials 0.000 claims abstract description 18
- 238000000034 method Methods 0.000 claims abstract description 11
- 238000010438 heat treatment Methods 0.000 claims abstract description 5
- 238000004519 manufacturing process Methods 0.000 claims abstract description 5
- -1 hydrogen ions Chemical class 0.000 claims description 6
- 229910001415 sodium ion Inorganic materials 0.000 claims description 5
- 229910052739 hydrogen Inorganic materials 0.000 claims description 4
- 239000001257 hydrogen Substances 0.000 claims description 4
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 3
- KKCBUQHMOMHUOY-UHFFFAOYSA-N sodium oxide Chemical compound [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 abstract description 20
- 239000006185 dispersion Substances 0.000 abstract description 13
- 229910001948 sodium oxide Inorganic materials 0.000 abstract description 11
- 239000002253 acid Substances 0.000 abstract description 5
- 239000000463 material Substances 0.000 abstract description 3
- OISDCQBZXBRXIA-UHFFFAOYSA-N dotriacontasodium octasilicate Chemical compound [Si]([O-])([O-])([O-])[O-].[Si]([O-])([O-])([O-])[O-].[Si]([O-])([O-])([O-])[O-].[Si]([O-])([O-])([O-])[O-].[Si]([O-])([O-])([O-])[O-].[Si]([O-])([O-])([O-])[O-].[Si]([O-])([O-])([O-])[O-].[Si]([O-])([O-])([O-])[O-].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+] OISDCQBZXBRXIA-UHFFFAOYSA-N 0.000 abstract description 2
- 239000004115 Sodium Silicate Substances 0.000 description 9
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 9
- 229910052911 sodium silicate Inorganic materials 0.000 description 9
- 229910052681 coesite Inorganic materials 0.000 description 8
- 229910052906 cristobalite Inorganic materials 0.000 description 8
- 229920000642 polymer Polymers 0.000 description 8
- 229910052682 stishovite Inorganic materials 0.000 description 8
- 229910052905 tridymite Inorganic materials 0.000 description 8
- 239000000945 filler Substances 0.000 description 4
- 238000002156 mixing Methods 0.000 description 4
- 239000002114 nanocomposite Substances 0.000 description 4
- 229910002027 silica gel Inorganic materials 0.000 description 3
- 239000000741 silica gel Substances 0.000 description 3
- 235000012239 silicon dioxide Nutrition 0.000 description 3
- 239000012190 activator Substances 0.000 description 2
- ANBBXQWFNXMHLD-UHFFFAOYSA-N aluminum;sodium;oxygen(2-) Chemical compound [O-2].[O-2].[Na+].[Al+3] ANBBXQWFNXMHLD-UHFFFAOYSA-N 0.000 description 2
- 239000007900 aqueous suspension Substances 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- 229910001388 sodium aluminate Inorganic materials 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 238000007711 solidification Methods 0.000 description 2
- 230000008023 solidification Effects 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 229910006283 Si—O—H Inorganic materials 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 239000002734 clay mineral Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000001493 electron microscopy Methods 0.000 description 1
- 239000000499 gel Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 239000005445 natural material Substances 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 229910052814 silicon oxide Inorganic materials 0.000 description 1
- 238000003746 solid phase reaction Methods 0.000 description 1
- 238000010671 solid-state reaction Methods 0.000 description 1
- 238000000527 sonication Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/20—Silicates
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/20—Silicates
- C01B33/36—Silicates having base-exchange properties but not having molecular sieve properties
- C01B33/38—Layered base-exchange silicates, e.g. clays, micas or alkali metal silicates of kenyaite or magadiite type
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/16—Preparation of silica xerogels
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Silicon Compounds (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US19725000P | 2000-04-14 | 2000-04-14 | |
| US60/197,250 | 2000-04-14 | ||
| PCT/US2001/011978 WO2001083370A2 (en) | 2000-04-14 | 2001-04-12 | Synthetic platy magadiite and octasilicate |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CA2405963A1 CA2405963A1 (en) | 2001-11-08 |
| CA2405963C true CA2405963C (en) | 2009-12-22 |
Family
ID=22728634
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA002405963A Expired - Fee Related CA2405963C (en) | 2000-04-14 | 2001-04-12 | Synthetic platy magadiite and octasilicate |
Country Status (9)
| Country | Link |
|---|---|
| EP (1) | EP1289884B1 (enExample) |
| JP (1) | JP2003531801A (enExample) |
| KR (1) | KR20030007518A (enExample) |
| AU (1) | AU2001257026A1 (enExample) |
| BR (1) | BR0110297A (enExample) |
| CA (1) | CA2405963C (enExample) |
| MX (1) | MXPA02010131A (enExample) |
| WO (1) | WO2001083370A2 (enExample) |
| ZA (1) | ZA200208268B (enExample) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7166265B2 (en) * | 2002-11-27 | 2007-01-23 | Board Of Trustees Of Michigan State University | Process for the assembly of ultrastable mesostructured organofunctional silica compositions |
| WO2004111118A1 (en) * | 2003-06-12 | 2004-12-23 | Dow Global Technologies Inc. | Fire retardant composition |
| JP4670033B2 (ja) * | 2003-11-19 | 2011-04-13 | 独立行政法人産業技術総合研究所 | 層状ケイ酸塩化合物の製造方法 |
| JP2007031172A (ja) * | 2005-07-22 | 2007-02-08 | Inst Fr Petrole | アミノアルコール型有機構造化剤からラメラ固体を合成する方法 |
| KR102655710B1 (ko) * | 2019-02-20 | 2024-04-09 | 주식회사 엘지화학 | 층상 실리케이트 합성방법 및 이로부터 합성된 층상 실리케이트 |
| JP7819025B2 (ja) * | 2022-05-06 | 2026-02-24 | 東ソ－・エスジ－エム株式会社 | シリカガラスの製造方法 |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DD220585A1 (de) * | 1984-01-09 | 1985-04-03 | Univ Halle Wittenberg | Verfahren zur herstellung von natriumoctosilikaten mit schichtstruktur |
| DD221723A1 (de) * | 1984-01-09 | 1985-05-02 | Genthin Waschmittelwerk | Verfahren zur herstellung von magadiit |
| DE3669490D1 (de) * | 1985-06-13 | 1990-04-19 | Hoechst Ag | Verfahren zur herstellung von kristallinen alkalischichtsilikaten. |
| US4626421A (en) * | 1985-06-28 | 1986-12-02 | Chevron Research Company | Preparation of magadiite |
| US5236882A (en) * | 1991-01-22 | 1993-08-17 | Mobil Oil Corp. | Catalyst comprising a hydrogenation metal and a delaminated layered silicate |
| JPH06104564B2 (ja) * | 1991-06-12 | 1994-12-21 | 工業技術院長 | 膜状層間化合物及びその製造法 |
| DE4308063A1 (de) * | 1993-03-13 | 1994-09-15 | Hoechst Ag | Verfahren zur Herstellung von Gemischen aus synthetischem, kristallinem Magadiit und sauerstoffabspaltenden Salzen sowie deren Verwendung |
| JP3364147B2 (ja) * | 1998-01-20 | 2003-01-08 | 科学技術振興事業団 | 層状ケイ酸塩のフルオロアルキルシリル化複合体 |
-
2001
- 2001-04-12 CA CA002405963A patent/CA2405963C/en not_active Expired - Fee Related
- 2001-04-12 WO PCT/US2001/011978 patent/WO2001083370A2/en not_active Ceased
- 2001-04-12 BR BR0110297-4A patent/BR0110297A/pt not_active Application Discontinuation
- 2001-04-12 KR KR1020027013767A patent/KR20030007518A/ko not_active Withdrawn
- 2001-04-12 JP JP2001580807A patent/JP2003531801A/ja active Pending
- 2001-04-12 EP EP01930495A patent/EP1289884B1/en not_active Expired - Lifetime
- 2001-04-12 AU AU2001257026A patent/AU2001257026A1/en not_active Abandoned
- 2001-04-12 MX MXPA02010131A patent/MXPA02010131A/es unknown
-
2002
- 2002-10-14 ZA ZA200208268A patent/ZA200208268B/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| AU2001257026A1 (en) | 2001-11-12 |
| WO2001083370A3 (en) | 2002-08-15 |
| CA2405963A1 (en) | 2001-11-08 |
| MXPA02010131A (es) | 2003-03-10 |
| EP1289884A2 (en) | 2003-03-12 |
| JP2003531801A (ja) | 2003-10-28 |
| EP1289884B1 (en) | 2012-08-22 |
| BR0110297A (pt) | 2003-01-07 |
| KR20030007518A (ko) | 2003-01-23 |
| WO2001083370A2 (en) | 2001-11-08 |
| ZA200208268B (en) | 2003-10-14 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EEER | Examination request | ||
| MKLA | Lapsed |
Effective date: 20130412 |