CA2368872A1 - Method for separating lignocellulose-containing biomass - Google Patents

Method for separating lignocellulose-containing biomass Download PDF

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Publication number
CA2368872A1
CA2368872A1 CA002368872A CA2368872A CA2368872A1 CA 2368872 A1 CA2368872 A1 CA 2368872A1 CA 002368872 A CA002368872 A CA 002368872A CA 2368872 A CA2368872 A CA 2368872A CA 2368872 A1 CA2368872 A1 CA 2368872A1
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CA
Canada
Prior art keywords
lignin
alkanolamine
containing biomass
cellulose
lignocellulose
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CA002368872A
Other languages
French (fr)
Other versions
CA2368872C (en
Inventor
Ties Karstens
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Zylum Beteiligungs GmbH and Co Patente II KG
Original Assignee
Rhodia Acetow Gmbh
Ties Karstens
Zylum Beteiligungsgesellschaft Mbh & Co. Patente Ii Kg
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Rhodia Acetow Gmbh, Ties Karstens, Zylum Beteiligungsgesellschaft Mbh & Co. Patente Ii Kg filed Critical Rhodia Acetow Gmbh
Publication of CA2368872A1 publication Critical patent/CA2368872A1/en
Application granted granted Critical
Publication of CA2368872C publication Critical patent/CA2368872C/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Classifications

    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C1/00—Pretreatment of the finely-divided materials before digesting
    • D21C1/02—Pretreatment of the finely-divided materials before digesting with water or steam
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C3/00—Pulping cellulose-containing materials
    • D21C3/003—Pulping cellulose-containing materials with organic compounds

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  • Paper (AREA)
  • Polysaccharides And Polysaccharide Derivatives (AREA)
  • Treatment Of Sludge (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Processing Of Solid Wastes (AREA)
  • Compounds Of Unknown Constitution (AREA)

Abstract

The invention relates to a method for separating lignocellulose-containing biomass, especially wood, into the essential components in the form of lignin, hemicellulose and cellulose, with the following steps:
a) pre-hydrolyzing the lignocellulose-containing biomass by treating it with water or steam; b) extracting the hydrolyzed hemicellulose obtained by pre-hydrolyzation with an aqueous medium; c) extracting the process-modified lignin that remains in the residue with an alkanolamine, isolating the lignin, recovering the alkanolamine, whereby the alkanolamine is not substituted by alkyl groups at the nitrogen atom, and d) obtaining a cellulose raw material. The inventive method is characterized in that hemicelluloses and lignin can be specifically separated from the cellulose in two different process steps. For this purpose, simple and commercially available system components can be used that facilitate an economical operation also with small installations.
CA002368872A 1999-04-12 2000-04-11 Method for separating lignocellulose-containing biomass Expired - Fee Related CA2368872C (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE19916347A DE19916347C1 (en) 1999-04-12 1999-04-12 Process for separating biomass containing lignocellulose
DE19916347.2 1999-04-12
PCT/EP2000/003212 WO2000061858A1 (en) 1999-04-12 2000-04-11 Method for separating lignocellulose-containing biomass

Publications (2)

Publication Number Publication Date
CA2368872A1 true CA2368872A1 (en) 2000-10-19
CA2368872C CA2368872C (en) 2005-11-29

Family

ID=7904218

Family Applications (1)

Application Number Title Priority Date Filing Date
CA002368872A Expired - Fee Related CA2368872C (en) 1999-04-12 2000-04-11 Method for separating lignocellulose-containing biomass

Country Status (18)

Country Link
EP (1) EP1190137B1 (en)
JP (1) JP2002541355A (en)
CN (1) CN1208514C (en)
AT (1) ATE255187T1 (en)
AU (1) AU756976B2 (en)
BR (1) BR0011169B1 (en)
CA (1) CA2368872C (en)
CZ (1) CZ298831B6 (en)
DE (2) DE19916347C1 (en)
ES (1) ES2213011T3 (en)
NO (1) NO20014939L (en)
NZ (1) NZ515051A (en)
PL (1) PL203363B1 (en)
PT (1) PT1190137E (en)
RU (1) RU2220245C2 (en)
SK (1) SK14392001A3 (en)
WO (1) WO2000061858A1 (en)
ZA (1) ZA200108406B (en)

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WO2009086265A3 (en) * 2007-12-26 2009-09-11 University Of Maine System Board Of Trustees Pre-extraction and solvent pulping of lignocellulosic material
WO2010121366A1 (en) * 2009-04-23 2010-10-28 Greenfield Ethanol Inc. Separation of reactive cellulose from lignocellulosic biomass with high lignin content
WO2011057413A1 (en) * 2009-11-13 2011-05-19 Fpinnovations Biomass fractionation process for bioproducts
US8182650B2 (en) 2005-05-24 2012-05-22 International Paper Company Modified Kraft fibers
US8475627B2 (en) 2006-12-18 2013-07-02 University Of Maine System Board Of Trustees Process of treating a lignocellulosic material
WO2014009604A1 (en) * 2012-07-11 2014-01-16 Von Schoultz Sebastian Method for extracting biomass
CN104313930A (en) * 2014-09-22 2015-01-28 洛阳华高轴承科技有限公司 Process method for papermaking pulping by utilizing waste corn stalks
US8945245B2 (en) 2009-08-24 2015-02-03 The Michigan Biotechnology Institute Methods of hydrolyzing pretreated densified biomass particulates and systems related thereto
US8968515B2 (en) 2006-05-01 2015-03-03 Board Of Trustees Of Michigan State University Methods for pretreating biomass
US9011640B2 (en) 2009-04-09 2015-04-21 Zylum Beteiligungsgesellschaft Mbh & Co Patente Ii Kg Method for obtaining cellulose from biomass comprising lignocellulose
US9039792B2 (en) 2009-08-24 2015-05-26 Board Of Trustees Of Michigan State University Methods for producing and using densified biomass products containing pretreated biomass fibers
WO2015104460A1 (en) * 2014-01-10 2015-07-16 Ab Bln-Woods Ltd Method for extracting lignin
US9187862B2 (en) 2010-11-05 2015-11-17 Greenfield Specialty Alcohols Inc. Bagasse fractionation for cellulosic ethanol and chemical production
US9206446B2 (en) 2006-05-01 2015-12-08 Board Of Trustees Of Michigan State University Extraction of solubles from plant biomass for use as microbial growth stimulant and methods related thereto
US9650657B2 (en) 2010-04-19 2017-05-16 Board Of Trustees Of Michigan State University Methods for producing extracted and digested products from pretreated lignocellulosic biomass
US9932707B2 (en) 2010-11-05 2018-04-03 Greenfield Specialty Alcohols Inc. Bagasse fractionation for cellulosic ethanol and chemical production
US10202660B2 (en) 2012-03-02 2019-02-12 Board Of Trustees Of Michigan State University Methods for increasing sugar yield with size-adjusted lignocellulosic biomass particles
US10457810B2 (en) 2009-08-24 2019-10-29 Board Of Trustees Of Michigan State University Densified biomass products containing pretreated biomass fibers
US10612059B2 (en) 2015-04-10 2020-04-07 Comet Biorefining Inc. Methods and compositions for the treatment of cellulosic biomass and products produced thereby
US10633461B2 (en) 2018-05-10 2020-04-28 Comet Biorefining Inc. Compositions comprising glucose and hemicellulose and their use
EP3990692A4 (en) * 2019-06-26 2023-05-24 Valmet Ab Method for extracting hemicellulose from lignocellulosic material

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DE10049340C1 (en) * 2000-10-05 2002-04-25 Rhodia Acetow Gmbh Process for the production of holocellulose by delignifying biomass containing lignocellulose
DE10109502A1 (en) 2001-02-28 2002-09-12 Rhodia Acetow Gmbh Removal of hemicellulose from biomaterial, especially wood pulp, involves extraction by treatment with an aqueous solution of metal complex, e.g. nickel tris-2-aminoethyl-amine di-hydroxide
DE10145338C1 (en) * 2001-09-14 2003-04-17 Rhodia Acetow Gmbh Process for the separation of hemicelluloses from hemicellulose-containing biomass
DE10158120A1 (en) * 2001-11-27 2003-06-18 Ties Karstens Process for separating xylose from xylan-rich lignocelluloses, especially wood
CN100487059C (en) * 2005-01-20 2009-05-13 中国科学院过程工程研究所 Method for preparing degradable material using stalk
CN1806945B (en) * 2005-01-20 2010-05-12 中国科学院过程工程研究所 Method for complete enzymolysis of straw cellulose by utilizing pretreatment and enzymolysis process
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JP5209597B2 (en) * 2006-03-29 2013-06-12 バージニア テック インテレクチュアル プロパティーズ インク Lignocellulose fractionation and reagent recycle based on cellulose solvent under mild reaction conditions
WO2007130337A1 (en) 2006-05-01 2007-11-15 Michigan State University Process for the treatment of lignocellulosic biomass
JP2008054640A (en) * 2006-09-04 2008-03-13 Univ Of Tokyo Method for treating biomass raw material, method for producing saccharide using the same and method for producing ethanol
JP5411846B2 (en) * 2007-04-19 2014-02-12 マスコマ コーポレイション Combined thermochemical pretreatment and refining of lignocellulose biomass
JP5520822B2 (en) * 2007-06-20 2014-06-11 ナーガルジュナ エナジー プライベート リミテッド Biomass component separation process
US7819976B2 (en) * 2007-08-22 2010-10-26 E. I. Du Pont De Nemours And Company Biomass treatment method
CN101821320B (en) * 2007-09-07 2013-01-09 科学与工业研究委员会 Process for fractionating sugarcane bagasse into high a-cellulose pulp, xylan and lignin
CN101143881B (en) * 2007-10-11 2011-03-16 孔延华 Method for synchronously extracting hemicellulose, cellulose and lignin and reclaiming phenolic acid compounds
CN101440108B (en) * 2007-11-23 2011-04-06 中国科学院过程工程研究所 Normal atmosphere degreasing crude glycerine pretreatment method for separating wood fiber biomass components
CN101210033B (en) * 2007-12-21 2011-09-07 武汉工程大学 Comprehensive utilization technique for plants fibrous raw material
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CA2726443C (en) * 2008-06-04 2017-08-01 Inbicon A/S Devices and methods for discharging pretreated biomass from higher to lower pressure regions
KR101657100B1 (en) * 2008-10-29 2016-09-19 삼성전자주식회사 Method and Apparatus for Fractionating Lignocellulose-based Biomass
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KR101554934B1 (en) * 2009-07-13 2015-09-22 베타 리뉴와블레스 에스.페.아. High temperature lignin separation process
EP2333151A1 (en) * 2009-12-11 2011-06-15 Nederlandse Organisatie voor toegepast -natuurwetenschappelijk onderzoek TNO Novel method for processing lignocellulose containing material
WO2011091044A1 (en) 2010-01-19 2011-07-28 Sriya Innovations, Inc. Production of fermentable sugars and lignin from biomass using supercritical fluids
MX2012008945A (en) * 2010-02-03 2012-11-30 Archer Daniels Midland Co Improved process for fractionation of lignocellulosic biomass.
US9034620B2 (en) 2010-03-19 2015-05-19 Poet Research, Inc. System for the treatment of biomass to facilitate the production of ethanol
EP3594354A1 (en) 2010-03-19 2020-01-15 Poet Research Incorporated Method for producing a fermentation product from biomass
JP5687693B2 (en) * 2010-05-12 2015-03-18 本田技研工業株式会社 Method for producing pre-saccharification product of lignocellulosic biomass and pre-saccharification treatment apparatus used therefor
AU2010354974A1 (en) * 2010-06-10 2013-01-24 Department Of Biotechnology Process for fractionation of biomass
IT1402202B1 (en) 2010-09-29 2013-08-28 Chemtex Italia S R L Ora Chemtex Italia S P A IMPROVED PROCEDURE TO RECOVER SUGAR FROM A LIGNOCELLULOSIC BIOMASS PRETREATMENT FLOW
US20120125551A1 (en) * 2010-11-23 2012-05-24 E. I. Du Pont De Nemours And Company Biomass pretreatment process for a packed bed reactor
US20120125548A1 (en) * 2010-11-23 2012-05-24 E. I. Du Pont De Nemours And Company Continuously fed biomass pretreatment process for a packed bed reactor
CN103547677B (en) 2011-01-18 2016-10-12 波特研究公司 System and method for biomass by hydrolyzation
US8663800B2 (en) * 2011-05-04 2014-03-04 Renmatix, Inc. Lignin production from lignocellulosic biomass
WO2013000074A1 (en) * 2011-06-30 2013-01-03 Nano-Green Biorefineries Inc. Catalytic biomass conversion
MX2014000245A (en) 2011-07-07 2014-09-15 Poet Res Inc Systems and methods for acid recycle.
AU2012286490B2 (en) * 2011-07-15 2016-08-11 Greenfield Specialty Alcohols Inc. Conditioning of biomass for improved C5/C6 sugar release prior to fermentation
US8759498B2 (en) 2011-12-30 2014-06-24 Renmatix, Inc. Compositions comprising lignin
JP2013143918A (en) * 2012-01-13 2013-07-25 Jx Nippon Oil & Energy Corp Method for producing raw material for enzymatic saccharification, method for producing sugar, and method for producing ethanol
AU2013256049B2 (en) * 2012-05-03 2017-02-16 Virdia, Inc. Methods for treating lignocellulosic materials
CN102660884B (en) * 2012-05-11 2014-06-11 南开大学 Method for producing hemicellulose by treating straw by ammonia water steam explosion technology
CN102864668B (en) * 2012-09-18 2015-03-11 北京林业大学 Preprocessing method for lignocellulose raw material
SE537929C2 (en) * 2014-02-11 2015-11-24 Daprox Ab Refiner and a method for refining cellulose materials
US10240006B2 (en) * 2014-05-01 2019-03-26 Renmatix, Inc. Upgrading lignin from lignin-containing residues through reactive extraction
EP3186326B1 (en) 2014-09-26 2024-02-21 Renmatix, Inc. Adhesive compositions comprising type-ii cellulose
EP3029010B1 (en) * 2014-12-01 2017-03-08 S2P AG Straw - Pulp & Paper Method for producing a fertilizer from black liquours
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CN105780569A (en) * 2016-05-19 2016-07-20 黄德辉 Physical preparation method of non-wood-fiber industrial raw material
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Cited By (34)

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US8182650B2 (en) 2005-05-24 2012-05-22 International Paper Company Modified Kraft fibers
US8328983B2 (en) 2005-05-24 2012-12-11 International Paper Company Modified kraft fibers
US9644222B2 (en) 2006-05-01 2017-05-09 Board Of Trustees Of Michigan State University Methods for pretreating biomass
US9206446B2 (en) 2006-05-01 2015-12-08 Board Of Trustees Of Michigan State University Extraction of solubles from plant biomass for use as microbial growth stimulant and methods related thereto
US8968515B2 (en) 2006-05-01 2015-03-03 Board Of Trustees Of Michigan State University Methods for pretreating biomass
WO2008017145A1 (en) * 2006-08-07 2008-02-14 Emicellex Energy Corporation Process for recovery of holocellulose and near-native lignin from biomass
US8475627B2 (en) 2006-12-18 2013-07-02 University Of Maine System Board Of Trustees Process of treating a lignocellulosic material
WO2009086265A3 (en) * 2007-12-26 2009-09-11 University Of Maine System Board Of Trustees Pre-extraction and solvent pulping of lignocellulosic material
US9011640B2 (en) 2009-04-09 2015-04-21 Zylum Beteiligungsgesellschaft Mbh & Co Patente Ii Kg Method for obtaining cellulose from biomass comprising lignocellulose
WO2010121366A1 (en) * 2009-04-23 2010-10-28 Greenfield Ethanol Inc. Separation of reactive cellulose from lignocellulosic biomass with high lignin content
US8603295B2 (en) 2009-04-23 2013-12-10 Greenfield Specialty Alcohols Inc. Separation of reactive cellulose from lignocellulosic biomass with high lignin content
US10457810B2 (en) 2009-08-24 2019-10-29 Board Of Trustees Of Michigan State University Densified biomass products containing pretreated biomass fibers
US9039792B2 (en) 2009-08-24 2015-05-26 Board Of Trustees Of Michigan State University Methods for producing and using densified biomass products containing pretreated biomass fibers
US9458482B2 (en) 2009-08-24 2016-10-04 The Michigan Biotechnology Institute Methods of hydrolyzing pretreated densified biomass particulates and systems related thereto
US8945245B2 (en) 2009-08-24 2015-02-03 The Michigan Biotechnology Institute Methods of hydrolyzing pretreated densified biomass particulates and systems related thereto
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US9650657B2 (en) 2010-04-19 2017-05-16 Board Of Trustees Of Michigan State University Methods for producing extracted and digested products from pretreated lignocellulosic biomass
US9187862B2 (en) 2010-11-05 2015-11-17 Greenfield Specialty Alcohols Inc. Bagasse fractionation for cellulosic ethanol and chemical production
US9932707B2 (en) 2010-11-05 2018-04-03 Greenfield Specialty Alcohols Inc. Bagasse fractionation for cellulosic ethanol and chemical production
US10202660B2 (en) 2012-03-02 2019-02-12 Board Of Trustees Of Michigan State University Methods for increasing sugar yield with size-adjusted lignocellulosic biomass particles
WO2014009604A1 (en) * 2012-07-11 2014-01-16 Von Schoultz Sebastian Method for extracting biomass
US11377790B2 (en) 2012-07-11 2022-07-05 Ch-Bioforce Oy Method for extracting biomass
WO2015104460A1 (en) * 2014-01-10 2015-07-16 Ab Bln-Woods Ltd Method for extracting lignin
CN104313930A (en) * 2014-09-22 2015-01-28 洛阳华高轴承科技有限公司 Process method for papermaking pulping by utilizing waste corn stalks
US10612059B2 (en) 2015-04-10 2020-04-07 Comet Biorefining Inc. Methods and compositions for the treatment of cellulosic biomass and products produced thereby
US11692211B2 (en) 2015-04-10 2023-07-04 Comet Biorefining Inc. Methods and compositions for the treatment of cellulosic biomass and products produced thereby
US10633461B2 (en) 2018-05-10 2020-04-28 Comet Biorefining Inc. Compositions comprising glucose and hemicellulose and their use
US11525016B2 (en) 2018-05-10 2022-12-13 Comet Biorefining Inc. Compositions comprising glucose and hemicellulose and their use
EP3990692A4 (en) * 2019-06-26 2023-05-24 Valmet Ab Method for extracting hemicellulose from lignocellulosic material

Also Published As

Publication number Publication date
SK14392001A3 (en) 2002-04-04
NO20014939D0 (en) 2001-10-10
AU4399500A (en) 2000-11-14
ZA200108406B (en) 2002-12-24
CN1208514C (en) 2005-06-29
PL203363B1 (en) 2009-09-30
DE19916347C1 (en) 2000-11-09
CN1352716A (en) 2002-06-05
JP2002541355A (en) 2002-12-03
DE50004573D1 (en) 2004-01-08
AU756976B2 (en) 2003-01-30
CA2368872C (en) 2005-11-29
CZ298831B6 (en) 2008-02-20
ES2213011T3 (en) 2004-08-16
CZ20013627A3 (en) 2003-10-15
BR0011169A (en) 2002-02-19
EP1190137B1 (en) 2003-11-26
PL351393A1 (en) 2003-04-07
PT1190137E (en) 2004-04-30
WO2000061858A1 (en) 2000-10-19
BR0011169B1 (en) 2011-02-22
ATE255187T1 (en) 2003-12-15
RU2220245C2 (en) 2003-12-27
EP1190137A1 (en) 2002-03-27
NO20014939L (en) 2001-12-04
NZ515051A (en) 2003-03-28

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