CA2230019C - A method for reactivating sorbent to enable the reuse thereof - Google Patents
A method for reactivating sorbent to enable the reuse thereof Download PDFInfo
- Publication number
- CA2230019C CA2230019C CA002230019A CA2230019A CA2230019C CA 2230019 C CA2230019 C CA 2230019C CA 002230019 A CA002230019 A CA 002230019A CA 2230019 A CA2230019 A CA 2230019A CA 2230019 C CA2230019 C CA 2230019C
- Authority
- CA
- Canada
- Prior art keywords
- cao
- ash particulates
- particulates containing
- combustor
- fossil fuel
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000002594 sorbent Substances 0.000 title claims abstract description 122
- 238000000034 method Methods 0.000 title claims abstract description 69
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims abstract description 56
- 239000000920 calcium hydroxide Substances 0.000 claims abstract description 56
- 229910001861 calcium hydroxide Inorganic materials 0.000 claims abstract description 56
- 235000011116 calcium hydroxide Nutrition 0.000 claims abstract description 56
- 239000002803 fossil fuel Substances 0.000 claims abstract description 41
- 238000002485 combustion reaction Methods 0.000 claims abstract description 34
- 238000006243 chemical reaction Methods 0.000 claims abstract description 25
- 230000000694 effects Effects 0.000 claims abstract description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 22
- 238000011065 in-situ storage Methods 0.000 claims description 7
- 230000006872 improvement Effects 0.000 claims description 5
- 239000002956 ash Substances 0.000 description 73
- 239000002245 particle Substances 0.000 description 42
- 239000007787 solid Substances 0.000 description 36
- RAHZWNYVWXNFOC-UHFFFAOYSA-N sulfur dioxide Inorganic materials O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 35
- 230000007420 reactivation Effects 0.000 description 16
- 238000009792 diffusion process Methods 0.000 description 15
- 230000008569 process Effects 0.000 description 13
- 239000003546 flue gas Substances 0.000 description 12
- 239000011575 calcium Substances 0.000 description 10
- 239000011148 porous material Substances 0.000 description 10
- 230000009467 reduction Effects 0.000 description 10
- 235000019738 Limestone Nutrition 0.000 description 9
- 239000006028 limestone Substances 0.000 description 9
- 239000011593 sulfur Substances 0.000 description 9
- 229910052717 sulfur Inorganic materials 0.000 description 9
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 8
- 229910052925 anhydrite Inorganic materials 0.000 description 8
- 238000005670 sulfation reaction Methods 0.000 description 8
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 7
- 239000007789 gas Substances 0.000 description 7
- 230000036571 hydration Effects 0.000 description 7
- 238000006703 hydration reaction Methods 0.000 description 7
- 239000000203 mixture Substances 0.000 description 7
- 238000002347 injection Methods 0.000 description 6
- 239000007924 injection Substances 0.000 description 6
- 230000004048 modification Effects 0.000 description 6
- 238000012986 modification Methods 0.000 description 6
- 230000019635 sulfation Effects 0.000 description 6
- 239000012535 impurity Substances 0.000 description 5
- 230000001965 increasing effect Effects 0.000 description 5
- 230000004913 activation Effects 0.000 description 4
- 238000000354 decomposition reaction Methods 0.000 description 4
- 238000002156 mixing Methods 0.000 description 4
- XTQHKBHJIVJGKJ-UHFFFAOYSA-N sulfur monoxide Chemical compound S=O XTQHKBHJIVJGKJ-UHFFFAOYSA-N 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 3
- 239000007795 chemical reaction product Substances 0.000 description 3
- 239000010410 layer Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 229910052815 sulfur oxide Inorganic materials 0.000 description 3
- 239000002699 waste material Substances 0.000 description 3
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 238000001354 calcination Methods 0.000 description 2
- 229910052791 calcium Inorganic materials 0.000 description 2
- 229910000019 calcium carbonate Inorganic materials 0.000 description 2
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 description 2
- JGIATAMCQXIDNZ-UHFFFAOYSA-N calcium sulfide Chemical compound [Ca]=S JGIATAMCQXIDNZ-UHFFFAOYSA-N 0.000 description 2
- 239000003245 coal Substances 0.000 description 2
- 239000000567 combustion gas Substances 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- 230000003467 diminishing effect Effects 0.000 description 2
- 239000010419 fine particle Substances 0.000 description 2
- 239000010881 fly ash Substances 0.000 description 2
- 239000000446 fuel Substances 0.000 description 2
- 230000007246 mechanism Effects 0.000 description 2
- 230000035515 penetration Effects 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 1
- LHJQIRIGXXHNLA-UHFFFAOYSA-N calcium peroxide Chemical compound [Ca+2].[O-][O-] LHJQIRIGXXHNLA-UHFFFAOYSA-N 0.000 description 1
- 235000019402 calcium peroxide Nutrition 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 238000006477 desulfuration reaction Methods 0.000 description 1
- 230000023556 desulfurization Effects 0.000 description 1
- 230000009977 dual effect Effects 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 238000005243 fluidization Methods 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000003134 recirculating effect Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 238000005549 size reduction Methods 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000002344 surface layer Substances 0.000 description 1
- 230000009897 systematic effect Effects 0.000 description 1
- 230000007723 transport mechanism Effects 0.000 description 1
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
- F23L—SUPPLYING AIR OR NON-COMBUSTIBLE LIQUIDS OR GASES TO COMBUSTION APPARATUS IN GENERAL ; VALVES OR DAMPERS SPECIALLY ADAPTED FOR CONTROLLING AIR SUPPLY OR DRAUGHT IN COMBUSTION APPARATUS; INDUCING DRAUGHT IN COMBUSTION APPARATUS; TOPS FOR CHIMNEYS OR VENTILATING SHAFTS; TERMINALS FOR FLUES
- F23L7/00—Supplying non-combustible liquids or gases, other than air, to the fire, e.g. oxygen, steam
- F23L7/002—Supplying water
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
- B01D53/77—Liquid phase processes
- B01D53/79—Injecting reactants
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/46—Removing components of defined structure
- B01D53/48—Sulfur compounds
- B01D53/50—Sulfur oxides
- B01D53/508—Sulfur oxides by treating the gases with solids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/96—Regeneration, reactivation or recycling of reactants
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/04—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium
- B01J20/041—Oxides or hydroxides
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/34—Regenerating or reactivating
- B01J20/3433—Regenerating or reactivating of sorbents or filter aids other than those covered by B01J20/3408 - B01J20/3425
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/34—Regenerating or reactivating
- B01J20/345—Regenerating or reactivating using a particular desorbing compound or mixture
- B01J20/3458—Regenerating or reactivating using a particular desorbing compound or mixture in the gas phase
- B01J20/3466—Regenerating or reactivating using a particular desorbing compound or mixture in the gas phase with steam
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
- F23C—METHODS OR APPARATUS FOR COMBUSTION USING FLUID FUEL OR SOLID FUEL SUSPENDED IN A CARRIER GAS OR AIR
- F23C10/00—Fluidised bed combustion apparatus
- F23C10/02—Fluidised bed combustion apparatus with means specially adapted for achieving or promoting a circulating movement of particles within the bed or for a recirculation of particles entrained from the bed
- F23C10/04—Fluidised bed combustion apparatus with means specially adapted for achieving or promoting a circulating movement of particles within the bed or for a recirculation of particles entrained from the bed the particles being circulated to a section, e.g. a heat-exchange section or a return duct, at least partially shielded from the combustion zone, before being reintroduced into the combustion zone
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
- F23C—METHODS OR APPARATUS FOR COMBUSTION USING FLUID FUEL OR SOLID FUEL SUSPENDED IN A CARRIER GAS OR AIR
- F23C10/00—Fluidised bed combustion apparatus
- F23C10/02—Fluidised bed combustion apparatus with means specially adapted for achieving or promoting a circulating movement of particles within the bed or for a recirculation of particles entrained from the bed
- F23C10/04—Fluidised bed combustion apparatus with means specially adapted for achieving or promoting a circulating movement of particles within the bed or for a recirculation of particles entrained from the bed the particles being circulated to a section, e.g. a heat-exchange section or a return duct, at least partially shielded from the combustion zone, before being reintroduced into the combustion zone
- F23C10/08—Fluidised bed combustion apparatus with means specially adapted for achieving or promoting a circulating movement of particles within the bed or for a recirculation of particles entrained from the bed the particles being circulated to a section, e.g. a heat-exchange section or a return duct, at least partially shielded from the combustion zone, before being reintroduced into the combustion zone characterised by the arrangement of separation apparatus, e.g. cyclones, for separating particles from the flue gases
- F23C10/10—Fluidised bed combustion apparatus with means specially adapted for achieving or promoting a circulating movement of particles within the bed or for a recirculation of particles entrained from the bed the particles being circulated to a section, e.g. a heat-exchange section or a return duct, at least partially shielded from the combustion zone, before being reintroduced into the combustion zone characterised by the arrangement of separation apparatus, e.g. cyclones, for separating particles from the flue gases the separation apparatus being located outside the combustion chamber
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
- F23C—METHODS OR APPARATUS FOR COMBUSTION USING FLUID FUEL OR SOLID FUEL SUSPENDED IN A CARRIER GAS OR AIR
- F23C2206/00—Fluidised bed combustion
- F23C2206/10—Circulating fluidised bed
- F23C2206/103—Cooling recirculating particles
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
- F23J—REMOVAL OR TREATMENT OF COMBUSTION PRODUCTS OR COMBUSTION RESIDUES; FLUES
- F23J2215/00—Preventing emissions
- F23J2215/20—Sulfur; Compounds thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Analytical Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Environmental & Geological Engineering (AREA)
- Combustion & Propulsion (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Biomedical Technology (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Inorganic Chemistry (AREA)
- Sustainable Development (AREA)
- Life Sciences & Earth Sciences (AREA)
- Fluidized-Bed Combustion And Resonant Combustion (AREA)
- Processing Of Solid Wastes (AREA)
- Treating Waste Gases (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US51748695A | 1995-08-21 | 1995-08-21 | |
| US08/517,486 | 1995-08-21 | ||
| PCT/IB1996/000930 WO1997006889A1 (en) | 1995-08-21 | 1996-07-29 | A method for reactivating sorbent to enable the reuse thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CA2230019A1 CA2230019A1 (en) | 1997-02-27 |
| CA2230019C true CA2230019C (en) | 2002-01-22 |
Family
ID=24060013
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA002230019A Expired - Fee Related CA2230019C (en) | 1995-08-21 | 1996-07-29 | A method for reactivating sorbent to enable the reuse thereof |
Country Status (10)
| Country | Link |
|---|---|
| KR (1) | KR100312360B1 (zh) |
| CN (1) | CN1104946C (zh) |
| CA (1) | CA2230019C (zh) |
| CZ (1) | CZ51098A3 (zh) |
| FI (1) | FI980394A (zh) |
| IN (1) | IN188644B (zh) |
| PL (1) | PL325057A1 (zh) |
| SE (1) | SE9800396D0 (zh) |
| TW (1) | TW397706B (zh) |
| WO (1) | WO1997006889A1 (zh) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6290921B1 (en) * | 1999-11-03 | 2001-09-18 | Foster Wheeler Enegeria Oy | Method and apparatus for binding pollutants in flue gas |
| ES2365199T3 (es) * | 2003-11-14 | 2011-09-26 | Her Majesty The Queen In Right Of Canada As Represented By The Minister Of Natural Resources | Pre-tratamiento de absorbentes basados en cal usando hidratación. |
| KR100699519B1 (ko) * | 2005-11-15 | 2007-03-23 | 한국에너지기술연구원 | 폐기물과 알피에프 연소 전용 순환유동층 보일러 |
| CN102307646B (zh) * | 2008-11-19 | 2014-08-27 | 俄亥俄州立大学研究基金会 | 使用高可再生的吸附剂进行co2捕获的碳酸化煅烧反应方法 |
| US9074767B2 (en) * | 2010-02-11 | 2015-07-07 | Alstom Technology Ltd | Rotary bottom ash regeneration system |
| US9657937B2 (en) * | 2010-08-23 | 2017-05-23 | Saudi Arabian Oil Company | Steam generation system having multiple combustion chambers and dry flue gas cleaning |
| FI123704B (fi) | 2011-02-04 | 2013-09-30 | Foster Wheeler Energia Oy | Menetelmä happipolttokiertoleijupetikattilan käyttämiseksi |
| SE538327C2 (sv) * | 2012-08-31 | 2016-05-17 | Marketing I Konsulting Per Anders Brattemo | Förfarande för att rena avgaser |
| CN103446875B (zh) * | 2013-07-29 | 2016-03-30 | 浙江大学 | 循环流化床燃烧系统的脱硫剂强化脱硫的方法及其系统 |
| EP2884163B1 (en) * | 2013-12-16 | 2017-04-05 | Doosan Lentjes GmbH | Fluidized bed apparatus with a fluidized bed heat exchanger |
| JP2017120151A (ja) * | 2015-12-28 | 2017-07-06 | 川崎重工業株式会社 | 燃焼設備 |
| TWI849370B (zh) * | 2021-12-23 | 2024-07-21 | 興展技術開發股份有限公司 | 用來降低氟化鈣汙泥中硫含量的方法 |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4312280A (en) * | 1980-03-13 | 1982-01-26 | The United States Of America As Represented By The United States Department Of Energy | Method of increasing the sulfation capacity of alkaline earth sorbents |
| SE457014B (sv) * | 1987-03-25 | 1988-11-21 | Abb Stal Ab | Saett att foerbaettra utnyttjningen av svavelabsorbent vid foerbraenning i en fluidiserad baedd och en kraftanlaeggning med foerbraenning i fluidiserad baedd |
| US5345883A (en) * | 1992-12-31 | 1994-09-13 | Combustion Engineering, Inc. | Reactivation of sorbent in a fluid bed boiler |
-
1996
- 1996-03-26 IN IN548CA1996 patent/IN188644B/en unknown
- 1996-07-29 CZ CZ98510A patent/CZ51098A3/cs unknown
- 1996-07-29 WO PCT/IB1996/000930 patent/WO1997006889A1/en not_active Application Discontinuation
- 1996-07-29 CN CN96197493A patent/CN1104946C/zh not_active Expired - Lifetime
- 1996-07-29 CA CA002230019A patent/CA2230019C/en not_active Expired - Fee Related
- 1996-07-29 KR KR1019980701332A patent/KR100312360B1/ko not_active IP Right Cessation
- 1996-07-29 PL PL96325057A patent/PL325057A1/xx unknown
- 1996-08-08 TW TW085109637A patent/TW397706B/zh not_active IP Right Cessation
-
1998
- 1998-02-11 SE SE9800396A patent/SE9800396D0/xx unknown
- 1998-02-20 FI FI980394A patent/FI980394A/fi unknown
Also Published As
| Publication number | Publication date |
|---|---|
| FI980394A (fi) | 1998-04-20 |
| KR19990044099A (ko) | 1999-06-25 |
| SE9800396L (sv) | 1998-02-11 |
| IN188644B (zh) | 2002-10-26 |
| CZ51098A3 (cs) | 1998-07-15 |
| KR100312360B1 (ko) | 2002-02-28 |
| CA2230019A1 (en) | 1997-02-27 |
| PL325057A1 (en) | 1998-07-06 |
| WO1997006889A1 (en) | 1997-02-27 |
| CN1199353A (zh) | 1998-11-18 |
| TW397706B (en) | 2000-07-11 |
| FI980394A0 (fi) | 1998-02-20 |
| CN1104946C (zh) | 2003-04-09 |
| SE9800396D0 (sv) | 1998-02-11 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EEER | Examination request | ||
| MKLA | Lapsed |