CA2007460A1 - Methode et appareil de fabrication de cristaux de carbure de bore - Google Patents
Methode et appareil de fabrication de cristaux de carbure de boreInfo
- Publication number
- CA2007460A1 CA2007460A1 CA002007460A CA2007460A CA2007460A1 CA 2007460 A1 CA2007460 A1 CA 2007460A1 CA 002007460 A CA002007460 A CA 002007460A CA 2007460 A CA2007460 A CA 2007460A CA 2007460 A1 CA2007460 A1 CA 2007460A1
- Authority
- CA
- Canada
- Prior art keywords
- hot zone
- boron carbide
- furnace
- nitrogen
- mixture
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
- 229910052580 B4C Inorganic materials 0.000 title claims abstract description 35
- INAHAJYZKVIDIZ-UHFFFAOYSA-N boron carbide Chemical compound B12B3B4C32B41 INAHAJYZKVIDIZ-UHFFFAOYSA-N 0.000 title claims abstract description 35
- 239000013078 crystal Substances 0.000 title claims abstract description 28
- 238000000034 method Methods 0.000 title claims abstract description 13
- 239000000203 mixture Substances 0.000 claims abstract description 36
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229910011255 B2O3 Inorganic materials 0.000 claims abstract description 13
- 150000001722 carbon compounds Chemical class 0.000 claims abstract description 10
- -1 boric oxide compound Chemical class 0.000 claims abstract description 9
- 229910052757 nitrogen Inorganic materials 0.000 claims abstract description 8
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 7
- 238000004519 manufacturing process Methods 0.000 claims description 6
- 239000012809 cooling fluid Substances 0.000 claims description 5
- JKWMSGQKBLHBQQ-UHFFFAOYSA-N diboron trioxide Chemical compound O=BOB=O JKWMSGQKBLHBQQ-UHFFFAOYSA-N 0.000 claims description 5
- 239000006229 carbon black Substances 0.000 claims description 2
- 150000001875 compounds Chemical class 0.000 claims description 2
- 238000002844 melting Methods 0.000 claims description 2
- 230000008018 melting Effects 0.000 claims description 2
- 239000011261 inert gas Substances 0.000 claims 1
- 238000002156 mixing Methods 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 abstract description 8
- 239000002245 particle Substances 0.000 abstract description 5
- 230000000977 initiatory effect Effects 0.000 abstract description 2
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 12
- 229910052786 argon Inorganic materials 0.000 description 6
- 238000001816 cooling Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 238000010926 purge Methods 0.000 description 4
- 239000007789 gas Substances 0.000 description 3
- 229910002804 graphite Inorganic materials 0.000 description 3
- 239000010439 graphite Substances 0.000 description 3
- 239000007858 starting material Substances 0.000 description 3
- 230000008901 benefit Effects 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 230000008878 coupling Effects 0.000 description 2
- 238000010168 coupling process Methods 0.000 description 2
- 238000005859 coupling reaction Methods 0.000 description 2
- 210000004907 gland Anatomy 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 238000009413 insulation Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 229910052582 BN Inorganic materials 0.000 description 1
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 1
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 description 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- 239000004593 Epoxy Substances 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 229910021538 borax Inorganic materials 0.000 description 1
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 1
- 239000004327 boric acid Substances 0.000 description 1
- 229910052796 boron Inorganic materials 0.000 description 1
- 229910002091 carbon monoxide Inorganic materials 0.000 description 1
- 229910010293 ceramic material Inorganic materials 0.000 description 1
- 230000002844 continuous effect Effects 0.000 description 1
- 239000011363 dried mixture Substances 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000006233 lamp black Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000004570 mortar (masonry) Substances 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 235000002020 sage Nutrition 0.000 description 1
- 238000005488 sandblasting Methods 0.000 description 1
- 239000004328 sodium tetraborate Substances 0.000 description 1
- 235000010339 sodium tetraborate Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
- C01B3/02—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
- C01B3/32—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air
- C01B3/34—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents
- C01B3/36—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents using oxygen or mixtures containing oxygen as gasifying agents
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/90—Carbides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/90—Carbides
- C01B32/914—Carbides of single elements
- C01B32/991—Boron carbide
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Combustion & Propulsion (AREA)
- Carbon And Carbon Compounds (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
- Ceramic Products (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US29568289A | 1989-01-11 | 1989-01-11 | |
| US295,682 | 1989-01-11 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA2007460A1 true CA2007460A1 (fr) | 1990-07-11 |
Family
ID=23138787
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA002007460A Abandoned CA2007460A1 (fr) | 1989-01-11 | 1990-01-10 | Methode et appareil de fabrication de cristaux de carbure de bore |
Country Status (8)
| Country | Link |
|---|---|
| EP (1) | EP0429557A4 (fr) |
| JP (1) | JPH03503158A (fr) |
| KR (1) | KR910700196A (fr) |
| AU (1) | AU621989B2 (fr) |
| CA (1) | CA2007460A1 (fr) |
| FI (1) | FI904446A0 (fr) |
| IL (1) | IL93018A0 (fr) |
| WO (1) | WO1990008102A1 (fr) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110357106A (zh) * | 2019-08-26 | 2019-10-22 | 燕山大学 | 一种制备纳米孪晶碳化硼粉体的方法 |
| CN114506846A (zh) * | 2022-02-15 | 2022-05-17 | 厦门金鹭特种合金有限公司 | 一种超细碳化物的生产方法及生产装置 |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NO20010929D0 (no) * | 2001-02-23 | 2001-02-23 | Norsk Hydro As | FremgangsmÕte for utøvelse av termiske reaksjoner mellom reaktanter samt en ovn for samme |
| CN106810261A (zh) * | 2017-04-12 | 2017-06-09 | 郑州嵩山硼业科技有限公司 | 一种使用中频炉冶炼碳化硼的方法 |
| CN113880093A (zh) * | 2021-11-24 | 2022-01-04 | 郑州嵩山硼业科技有限公司 | 一种碳化硼生产工艺 |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1897214A (en) * | 1930-05-14 | 1933-02-14 | Norton Co | Boron carbide and method of making the same |
| US2155682A (en) * | 1935-11-21 | 1939-04-25 | Norton Co | Method of making abrasive metal carbides |
| US3377141A (en) * | 1964-08-26 | 1968-04-09 | Cabot Corp | Process for producing metal carbides utilizing a solution treatment prior to reaction |
| US3379647A (en) * | 1966-05-04 | 1968-04-23 | Carborundum Co | Metal carbide and boride production |
| US3535080A (en) * | 1969-02-18 | 1970-10-20 | Norton Co | Apparatus and method for the continuous furnacing of borides,carbides and silicides |
| US4017587A (en) * | 1969-10-03 | 1977-04-12 | The United States Of America As Represented By The Secretary Of The Navy | Boron carbide |
| US4137295A (en) * | 1977-04-20 | 1979-01-30 | Tamers Murry A | Carbide production using molten metals as heat source |
| JPS55113609A (en) * | 1979-02-21 | 1980-09-02 | Ibiden Co Ltd | Manufacturing apparatus for beta crystallbase silicon carbide |
| JPS5825044B2 (ja) * | 1979-05-23 | 1983-05-25 | 安藤 義則 | 炭化物の超微粉末製造方法およびその装置 |
| US4529575A (en) * | 1982-08-27 | 1985-07-16 | Ibiden Kabushiki Kaisha | Process for producing ultrafine silicon carbide powder |
| US4804525A (en) * | 1986-04-14 | 1989-02-14 | The Dow Chemical Company | Producing boron carbide |
| JPS63166709A (ja) * | 1986-12-26 | 1988-07-09 | Ibiden Co Ltd | 炭化物の製造方法 |
-
1989
- 1989-12-27 EP EP19900902739 patent/EP0429557A4/en not_active Withdrawn
- 1989-12-27 WO PCT/US1989/005871 patent/WO1990008102A1/fr not_active Application Discontinuation
- 1989-12-27 KR KR1019900701997A patent/KR910700196A/ko not_active Application Discontinuation
- 1989-12-27 AU AU50364/90A patent/AU621989B2/en not_active Ceased
- 1989-12-27 JP JP90503055A patent/JPH03503158A/ja active Pending
-
1990
- 1990-01-09 IL IL93018A patent/IL93018A0/xx unknown
- 1990-01-10 CA CA002007460A patent/CA2007460A1/fr not_active Abandoned
- 1990-09-10 FI FI904446A patent/FI904446A0/fi not_active IP Right Cessation
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110357106A (zh) * | 2019-08-26 | 2019-10-22 | 燕山大学 | 一种制备纳米孪晶碳化硼粉体的方法 |
| CN110357106B (zh) * | 2019-08-26 | 2022-07-29 | 燕山大学 | 一种制备纳米孪晶碳化硼粉体的方法 |
| CN114506846A (zh) * | 2022-02-15 | 2022-05-17 | 厦门金鹭特种合金有限公司 | 一种超细碳化物的生产方法及生产装置 |
| CN114506846B (zh) * | 2022-02-15 | 2023-06-06 | 厦门金鹭特种合金有限公司 | 一种超细碳化物的生产方法及生产装置 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH03503158A (ja) | 1991-07-18 |
| KR910700196A (ko) | 1991-03-14 |
| FI904446A0 (fi) | 1990-09-10 |
| EP0429557A4 (en) | 1992-04-22 |
| AU5036490A (en) | 1990-08-13 |
| IL93018A0 (en) | 1990-11-05 |
| EP0429557A1 (fr) | 1991-06-05 |
| WO1990008102A1 (fr) | 1990-07-26 |
| AU621989B2 (en) | 1992-03-26 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FZDE | Discontinued |