CA1171616A - Method and apparatus for rapidly freezing molten metals and metalloids in particulate form - Google Patents
Method and apparatus for rapidly freezing molten metals and metalloids in particulate formInfo
- Publication number
- CA1171616A CA1171616A CA000396619A CA396619A CA1171616A CA 1171616 A CA1171616 A CA 1171616A CA 000396619 A CA000396619 A CA 000396619A CA 396619 A CA396619 A CA 396619A CA 1171616 A CA1171616 A CA 1171616A
- Authority
- CA
- Canada
- Prior art keywords
- disc
- coolant
- center
- metalloids
- rotation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 229910052751 metal Inorganic materials 0.000 title claims abstract description 12
- 239000002184 metal Substances 0.000 title claims abstract description 12
- 229910052752 metalloid Inorganic materials 0.000 title claims abstract description 11
- 150000002738 metalloids Chemical class 0.000 title claims abstract description 11
- 150000002739 metals Chemical class 0.000 title claims abstract description 11
- 238000000034 method Methods 0.000 title claims abstract description 8
- 230000008014 freezing Effects 0.000 title claims abstract description 6
- 238000007710 freezing Methods 0.000 title claims abstract description 6
- 239000002826 coolant Substances 0.000 claims abstract description 28
- 239000000463 material Substances 0.000 claims abstract description 27
- 239000007788 liquid Substances 0.000 claims abstract description 25
- 238000009834 vaporization Methods 0.000 claims abstract description 7
- 230000008016 vaporization Effects 0.000 claims abstract description 7
- 239000012768 molten material Substances 0.000 claims description 7
- 239000000155 melt Substances 0.000 claims 2
- 239000007787 solid Substances 0.000 claims 2
- 230000002093 peripheral effect Effects 0.000 claims 1
- 238000001816 cooling Methods 0.000 abstract description 7
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 11
- 229910001868 water Inorganic materials 0.000 description 10
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 9
- 229910052710 silicon Inorganic materials 0.000 description 9
- 239000010703 silicon Substances 0.000 description 9
- 239000007789 gas Substances 0.000 description 8
- 239000002245 particle Substances 0.000 description 7
- 239000010949 copper Substances 0.000 description 6
- 229910045601 alloy Inorganic materials 0.000 description 5
- 239000000956 alloy Substances 0.000 description 5
- 238000001704 evaporation Methods 0.000 description 5
- 229910052802 copper Inorganic materials 0.000 description 4
- 230000008020 evaporation Effects 0.000 description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 3
- 238000010276 construction Methods 0.000 description 3
- 229910002804 graphite Inorganic materials 0.000 description 3
- 239000010439 graphite Substances 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 239000005300 metallic glass Substances 0.000 description 3
- 239000010453 quartz Substances 0.000 description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 3
- 229910052718 tin Inorganic materials 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 230000001788 irregular Effects 0.000 description 2
- NJPPVKZQTLUDBO-UHFFFAOYSA-N novaluron Chemical compound C1=C(Cl)C(OC(F)(F)C(OC(F)(F)F)F)=CC=C1NC(=O)NC(=O)C1=C(F)C=CC=C1F NJPPVKZQTLUDBO-UHFFFAOYSA-N 0.000 description 2
- 238000012935 Averaging Methods 0.000 description 1
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 229910001315 Tool steel Inorganic materials 0.000 description 1
- 238000005299 abrasion Methods 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- 229910052796 boron Inorganic materials 0.000 description 1
- 239000001273 butane Substances 0.000 description 1
- 239000000110 cooling liquid Substances 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 239000011888 foil Substances 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- 230000006698 induction Effects 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 229910001092 metal group alloy Inorganic materials 0.000 description 1
- -1 metallic alloys Chemical class 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 description 1
- OFBQJSOFQDEBGM-UHFFFAOYSA-N n-pentane Natural products CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 1
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 description 1
- 229910010271 silicon carbide Inorganic materials 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F9/00—Making metallic powder or suspensions thereof
- B22F9/02—Making metallic powder or suspensions thereof using physical processes
- B22F9/06—Making metallic powder or suspensions thereof using physical processes starting from liquid material
- B22F9/08—Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F9/00—Making metallic powder or suspensions thereof
- B22F9/02—Making metallic powder or suspensions thereof using physical processes
- B22F9/06—Making metallic powder or suspensions thereof using physical processes starting from liquid material
- B22F9/08—Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying
- B22F9/10—Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying using centrifugal force
Landscapes
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
- Glanulating (AREA)
- Processing Of Solid Wastes (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US239,306 | 1981-03-02 | ||
| US06/239,306 US4347199A (en) | 1981-03-02 | 1981-03-02 | Method and apparatus for rapidly freezing molten metals and metalloids in particulate form |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1171616A true CA1171616A (en) | 1984-07-31 |
Family
ID=22901584
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA000396619A Expired CA1171616A (en) | 1981-03-02 | 1982-02-19 | Method and apparatus for rapidly freezing molten metals and metalloids in particulate form |
Country Status (12)
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4419060A (en) * | 1983-03-14 | 1983-12-06 | Dow Corning Corporation | Apparatus for rapidly freezing molten metals and metalloids in particulate form |
| US4559187A (en) * | 1983-12-14 | 1985-12-17 | Battelle Development Corporation | Production of particulate or powdered metals and alloys |
| US4687606A (en) * | 1984-10-15 | 1987-08-18 | Ford Motor Company | Metalloid precursor powder and method of making same |
| US4701289A (en) * | 1985-11-08 | 1987-10-20 | Dow Corning Corporation | Method and apparatus for the rapid solidification of molten material in particulate form |
| FR2595595B1 (fr) * | 1986-03-17 | 1989-07-28 | Aubert & Duval Acieries | Procede de refroidissement et de collecte de poudres metalliques produites par atomisation de metal liquide |
| US5071332A (en) * | 1986-03-21 | 1991-12-10 | Petroleo Brasileiro S.A. | Sulphur granulator |
| DE3730147A1 (de) * | 1987-09-09 | 1989-03-23 | Leybold Ag | Verfahren zur herstellung von pulvern aus geschmolzenen stoffen |
| NO165288C (no) * | 1988-12-08 | 1991-01-23 | Elkem As | Silisiumpulver og fremgangsmaate for fremstilling av silisiumpulver. |
| NO166032C (no) * | 1988-12-08 | 1991-05-22 | Elkem As | Fremgangsmaate ved fremstilling av triklormonosilan. |
| NO174165C (no) * | 1992-01-08 | 1994-03-23 | Elkem Aluminium | Fremgangsmåte ved kornforfining av aluminium samt kornforfiningslegering for utförelse av fremgangsmåten |
| US6352426B1 (en) | 1998-03-19 | 2002-03-05 | Advanced Plastics Technologies, Ltd. | Mold for injection molding multilayer preforms |
| DE19830057C1 (de) * | 1998-06-29 | 2000-03-16 | Juergen Schulze | Verfahren und Vorrichtung zum drucklosen Herstellen von Weichlotpulver |
| RU2141392C1 (ru) * | 1998-08-18 | 1999-11-20 | Открытое акционерное общество "Чепецкий механический завод" | Способ получения металлического порошка и устройство для его осуществления |
| EP1313587A1 (en) * | 2000-09-01 | 2003-05-28 | FRY'S METALS, INC. d/b/a ALPHA METALS, INC. | Rapid surface cooling of solder droplets by flash evaporation |
| CA2569639A1 (en) | 2004-06-10 | 2005-12-29 | Advanced Plastics Technologies Luxembourg S.A. | Methods and systems for cooling molds |
| JP2007084905A (ja) * | 2005-08-26 | 2007-04-05 | Sanki Dengyo Kk | 金属粉末の製造装置および製造方法 |
| US7717697B2 (en) | 2005-08-30 | 2010-05-18 | Sharon Hutchinson | Methods and systems for controlling mold temperatures |
| WO2016031692A1 (ja) * | 2014-08-28 | 2016-03-03 | 日本ゼオン株式会社 | アトマイザ、噴霧乾燥装置及び複合粒子の製造方法 |
| JP2019530803A (ja) * | 2016-09-23 | 2019-10-24 | オーロラ ラブス リミテッド | 粉末形成用装置および粉末形成用プロセス |
| CN115605622A (zh) | 2021-04-28 | 2023-01-13 | Neo新材料技术（新加坡）私人有限公司（Sg） | 生产磁性材料的方法和系统 |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2304130A (en) * | 1937-12-01 | 1942-12-08 | Chemical Marketing Company Inc | Process for the conversion of metals into finely divided form |
| US2305172A (en) * | 1938-05-05 | 1942-12-15 | Chemical Marketing Company Inc | Process for the conversion of liquid substances into finely divided form |
| US2356599A (en) * | 1938-05-05 | 1944-08-22 | Landgraf Otto | Process and apparatus for comminuting liquid substances |
| US2880456A (en) * | 1956-04-09 | 1959-04-07 | Kuzela Jan | Device for the production of a light filling from blast furnace, boiler and other slag |
| US3346673A (en) * | 1965-11-19 | 1967-10-10 | George A Last | Formation of submicorn uranium carbide particles in metallic uranium |
| US4127158A (en) * | 1973-10-15 | 1978-11-28 | Toyo Kohan Co., Ltd. | Process for preparing hollow metallic bodies |
| SE7414810L (sv) * | 1974-11-26 | 1976-05-28 | Skf Nova Ab | Metallflingeprodukt lempad for framstellning av metallpulver for pulvermetallurgiska endamal samt sett att tillverka produkter |
| US4069045A (en) * | 1974-11-26 | 1978-01-17 | Skf Nova Ab | Metal powder suited for powder metallurgical purposes, and a process for manufacturing the metal powder |
| JPS6044363B2 (ja) * | 1976-07-12 | 1985-10-03 | 大同特殊鋼株式会社 | 遠心噴霧法における金属粉末の製造法 |
-
1981
- 1981-03-02 US US06/239,306 patent/US4347199A/en not_active Expired - Lifetime
-
1982
- 1982-02-11 AU AU82704/82A patent/AU543455B2/en not_active Ceased
- 1982-02-11 WO PCT/US1982/000175 patent/WO1982003024A1/en unknown
- 1982-02-11 BR BR8206647A patent/BR8206647A/pt unknown
- 1982-02-11 JP JP57501035A patent/JPS58500202A/ja active Granted
- 1982-02-19 CA CA000396619A patent/CA1171616A/en not_active Expired
- 1982-02-25 DE DE8282300968T patent/DE3265709D1/de not_active Expired
- 1982-02-25 EP EP82300968A patent/EP0059607B1/en not_active Expired
- 1982-02-26 AR AR288585A patent/AR228389A1/es active
- 1982-02-26 ZA ZA821291A patent/ZA821291B/xx unknown
- 1982-03-01 MX MX191624A patent/MX156694A/es unknown
- 1982-03-02 KR KR8200918A patent/KR890004629B1/ko not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| ZA821291B (en) | 1983-03-30 |
| JPS58500202A (ja) | 1983-02-10 |
| EP0059607B1 (en) | 1985-08-28 |
| US4347199A (en) | 1982-08-31 |
| DE3265709D1 (en) | 1985-10-03 |
| BR8206647A (pt) | 1983-03-01 |
| AU543455B2 (en) | 1985-04-18 |
| JPH026804B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1990-02-14 |
| WO1982003024A1 (en) | 1982-09-16 |
| EP0059607A1 (en) | 1982-09-08 |
| KR830008772A (ko) | 1983-12-14 |
| KR890004629B1 (ko) | 1989-11-21 |
| MX156694A (es) | 1988-09-27 |
| AR228389A1 (es) | 1983-02-28 |
| AU8270482A (en) | 1982-09-28 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKEC | Expiry (correction) | ||
| MKEX | Expiry |