BRPI0409316A - processos para a retirada de água de ácido cianìdrico por destilação e para a hidrocianação de olefinas ou dienos - Google Patents
processos para a retirada de água de ácido cianìdrico por destilação e para a hidrocianação de olefinas ou dienosInfo
- Publication number
- BRPI0409316A BRPI0409316A BRPI0409316-0A BRPI0409316A BRPI0409316A BR PI0409316 A BRPI0409316 A BR PI0409316A BR PI0409316 A BRPI0409316 A BR PI0409316A BR PI0409316 A BRPI0409316 A BR PI0409316A
- Authority
- BR
- Brazil
- Prior art keywords
- distilling
- dienes
- olefins
- acid water
- hydrocyanation
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
- C01C3/00—Cyanogen; Compounds thereof
- C01C3/02—Preparation, separation or purification of hydrogen cyanide
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C253/00—Preparation of carboxylic acid nitriles
- C07C253/08—Preparation of carboxylic acid nitriles by addition of hydrogen cyanide or salts thereof to unsaturated compounds
- C07C253/10—Preparation of carboxylic acid nitriles by addition of hydrogen cyanide or salts thereof to unsaturated compounds to compounds containing carbon-to-carbon double bonds
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
- C01C3/00—Cyanogen; Compounds thereof
- C01C3/02—Preparation, separation or purification of hydrogen cyanide
- C01C3/0295—Purification
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
- C01C3/00—Cyanogen; Compounds thereof
- C01C3/06—Stabilisation of hydrogen cyanide
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00105—Controlling the temperature by indirect heating or cooling employing heat exchange fluids part or all of the reactants being heated or cooled outside the reactor while recycling
- B01J2219/0011—Controlling the temperature by indirect heating or cooling employing heat exchange fluids part or all of the reactants being heated or cooled outside the reactor while recycling involving reactant liquids
Abstract
"PROCESSOS PARA A RETIRADA DE áGUA DE áCIDO CIANìDRICO POR DESTILAçãO E PARA A HIDROCIANAçãO DE OLEFINAS OU DIENOS". A invenção refere-se a um processo para a retirada de água de ácido cianídrico por destilação, que compreende a destilação de ácido cianídrico bruto contendo de 50 a 99,9% em peso de HCN, de 0,1 a 40% em peso de água, de 0 a 15% em peso de óxidos de carbono e opcionalmente de 0,01 a 1% em peso de um estabilizante não volátil, em uma pressão de 1 bar a 2,5 bar, uma temperatura de fundo de 100<198>C a 130<198>C e uma temperatura de topo de 25<198>C a 54<198>C, na ausência de um estabilizante volátil, em uma coluna de destilação para obter uma corrente de retirada de topo contendo ácido cianídrico anidro purificado e óxidos de carbono e uma corrente de retirada de fundo compreendendo água e, quando apropriado, o estabilizante não volátil.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE10317929A DE10317929A1 (de) | 2003-04-17 | 2003-04-17 | Verfahren zur Aufreinigung von Blausäure |
PCT/EP2004/003973 WO2004092068A1 (de) | 2003-04-17 | 2004-04-15 | Verfahren zur aufreinigung von blausäure |
Publications (2)
Publication Number | Publication Date |
---|---|
BRPI0409316A true BRPI0409316A (pt) | 2006-04-25 |
BRPI0409316B1 BRPI0409316B1 (pt) | 2013-10-15 |
Family
ID=33154295
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BRPI0409316-0B1A BRPI0409316B1 (pt) | 2003-04-17 | 2004-04-15 | Processos para a retirada de água de ácido cianídrico por destilação e para a hidrocianação de olefinas ou dienos |
Country Status (16)
Country | Link |
---|---|
US (1) | US7462263B2 (pt) |
EP (1) | EP1618068B1 (pt) |
JP (1) | JP4406635B2 (pt) |
KR (1) | KR101093377B1 (pt) |
CN (1) | CN100340487C (pt) |
AR (1) | AR044023A1 (pt) |
AT (1) | ATE336464T1 (pt) |
BR (1) | BRPI0409316B1 (pt) |
CA (1) | CA2522520C (pt) |
DE (2) | DE10317929A1 (pt) |
ES (1) | ES2270376T3 (pt) |
MX (1) | MXPA05010572A (pt) |
MY (1) | MY138553A (pt) |
PL (1) | PL1618068T3 (pt) |
TW (1) | TW200505792A (pt) |
WO (1) | WO2004092068A1 (pt) |
Families Citing this family (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE102009001699A1 (de) | 2008-03-26 | 2009-10-15 | Basf Se | Verfahren zur Erhöhung der Verfügbarkeit von Anlagen, in denen Blausäure gehandhabt wird |
ES2442927T3 (es) | 2010-07-07 | 2014-02-14 | Invista Technologies S.A R.L. | Procedimiento de producción de nitrilos |
CN103936033B (zh) * | 2012-12-18 | 2017-08-11 | 英威达科技公司 | 从Andrussow工艺的氨解吸塔中回收热量的方法 |
JP2016508522A (ja) * | 2013-02-28 | 2016-03-22 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | So2不含のシアン化水素を使用したedaの製造法 |
CN106103405B (zh) | 2014-03-13 | 2019-03-19 | 巴斯夫欧洲公司 | 蒸馏提纯eda的方法 |
CN104724725B (zh) * | 2014-11-21 | 2017-05-24 | 重庆紫光化工股份有限公司 | 氢氰酸气体分离纯化系统及方法 |
WO2017011428A1 (en) * | 2015-07-14 | 2017-01-19 | The Chemours Company Fc, Llc | Method for removing nitriles from hydrogen cyanide |
CN105366692B (zh) * | 2015-12-04 | 2018-03-30 | 中国天辰工程有限公司 | 一种制取高纯液态氰化氢工艺及系统 |
CN106365178B (zh) * | 2016-08-29 | 2018-07-27 | 重庆紫光化工股份有限公司 | 一种氢氰酸的提纯方法 |
CN106495186A (zh) * | 2016-11-02 | 2017-03-15 | 中国天辰工程有限公司 | 一种高效回收氰化氢的方法 |
EP3604222A1 (en) | 2018-07-30 | 2020-02-05 | Evonik Operations GmbH | Process for the purification of hydrogen cyanide |
CN110627091A (zh) * | 2019-10-24 | 2019-12-31 | 重庆工商大学 | 一种采用化学法提纯用于制备己二腈的氢氰酸的方法 |
TW202335966A (zh) | 2021-10-29 | 2023-09-16 | 德商羅伊姆公司 | 生產及分離氰化氫之最佳化方法以及將其轉化為甲基丙烯酸(mas)及/或甲基丙烯酸烷酯之方法 |
CN114618181B (zh) * | 2022-03-17 | 2023-12-08 | 北京道思克矿山装备技术有限公司 | 一种戊烯腈合成反应中回收氢氰酸的系统和方法 |
Family Cites Families (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US1934838A (en) * | 1930-04-14 | 1933-11-14 | Ig Farbenindustrie Ag | Production of hydrocyanic acid |
US2571099A (en) * | 1950-01-07 | 1951-10-16 | Du Pont | Process for hydrocyanation of conjugated diolefinic compounds |
NL302210A (pt) | 1963-01-16 | |||
FR1377939A (fr) * | 1963-01-16 | 1964-11-06 | Knapsack Ag | Procédé pour la séparation de l'acrylonitrile et de l'acide cyanhydrique à partir de mélanges par distillation |
DE1205064B (de) * | 1963-05-04 | 1965-11-18 | Basf Ag | Verfahren und Vorrichtung zur Gewinnung von weitgehend wasserfreier Blausaeure durch Destillation von blausaeure- und wasserhaltigen Gasen oder Fluessigkeiten |
US3357900A (en) * | 1965-05-17 | 1967-12-12 | American Cyanamid Co | Series flash distillation for recovery of hcn from aqueous cu-containing slurries |
FR2198895B1 (pt) * | 1972-09-07 | 1977-02-25 | Du Pont | |
US3920721A (en) * | 1974-09-18 | 1975-11-18 | Du Pont | Hydrocyanation of olefins |
DE3334321A1 (de) * | 1983-09-22 | 1985-04-11 | Lentia GmbH Chem. u. pharm. Erzeugnisse - Industriebedarf, 8000 München | Verfahren zur reinigung von rohem acetonitril unter gewinnung von reiner blausaeure |
AU3131897A (en) * | 1996-05-30 | 1998-01-05 | E.I. Du Pont De Nemours And Company | An improved process for preparing anhydrous hcn |
ES2166953T3 (es) * | 1996-09-25 | 2002-05-01 | Mitsubishi Rayon Co | Procedimiento de amoxidacion en reactor de lecho fluidificado. |
DE19647527C1 (de) * | 1996-11-16 | 1998-03-12 | Degussa | Verfahren zur Herstellung von Cyanoverbindungen durch Ammonoxidation |
DE10034193A1 (de) * | 2000-07-13 | 2002-03-28 | Roehm Gmbh | Verfahren zur Herstellung von Cyanwasserstoff |
-
2003
- 2003-04-17 DE DE10317929A patent/DE10317929A1/de not_active Withdrawn
-
2004
- 2004-04-12 MY MYPI20041332A patent/MY138553A/en unknown
- 2004-04-13 TW TW093110266A patent/TW200505792A/zh unknown
- 2004-04-15 AR ARP040101272A patent/AR044023A1/es unknown
- 2004-04-15 US US10/553,537 patent/US7462263B2/en not_active Expired - Fee Related
- 2004-04-15 BR BRPI0409316-0B1A patent/BRPI0409316B1/pt not_active IP Right Cessation
- 2004-04-15 AT AT04727522T patent/ATE336464T1/de not_active IP Right Cessation
- 2004-04-15 WO PCT/EP2004/003973 patent/WO2004092068A1/de active IP Right Grant
- 2004-04-15 EP EP04727522A patent/EP1618068B1/de not_active Expired - Lifetime
- 2004-04-15 CN CNB2004800095152A patent/CN100340487C/zh not_active Expired - Fee Related
- 2004-04-15 JP JP2006500091A patent/JP4406635B2/ja not_active Expired - Fee Related
- 2004-04-15 CA CA2522520A patent/CA2522520C/en not_active Expired - Fee Related
- 2004-04-15 MX MXPA05010572A patent/MXPA05010572A/es active IP Right Grant
- 2004-04-15 DE DE502004001216T patent/DE502004001216D1/de not_active Expired - Lifetime
- 2004-04-15 KR KR1020057019448A patent/KR101093377B1/ko not_active IP Right Cessation
- 2004-04-15 PL PL04727522T patent/PL1618068T3/pl unknown
- 2004-04-15 ES ES04727522T patent/ES2270376T3/es not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
AR044023A1 (es) | 2005-08-24 |
TW200505792A (en) | 2005-02-16 |
DE502004001216D1 (de) | 2006-09-28 |
US7462263B2 (en) | 2008-12-09 |
CN1771197A (zh) | 2006-05-10 |
JP2006523590A (ja) | 2006-10-19 |
CA2522520C (en) | 2011-11-08 |
WO2004092068A1 (de) | 2004-10-28 |
MY138553A (en) | 2009-06-30 |
BRPI0409316B1 (pt) | 2013-10-15 |
PL1618068T3 (pl) | 2006-12-29 |
EP1618068A1 (de) | 2006-01-25 |
KR20050120801A (ko) | 2005-12-23 |
JP4406635B2 (ja) | 2010-02-03 |
CN100340487C (zh) | 2007-10-03 |
EP1618068B1 (de) | 2006-08-16 |
US20060201798A1 (en) | 2006-09-14 |
MXPA05010572A (es) | 2005-11-23 |
DE10317929A1 (de) | 2004-11-11 |
ATE336464T1 (de) | 2006-09-15 |
CA2522520A1 (en) | 2004-10-28 |
KR101093377B1 (ko) | 2011-12-14 |
ES2270376T3 (es) | 2007-04-01 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
B06A | Patent application procedure suspended [chapter 6.1 patent gazette] | ||
B06A | Patent application procedure suspended [chapter 6.1 patent gazette] | ||
B07A | Application suspended after technical examination (opinion) [chapter 7.1 patent gazette] | ||
B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
B07B | Technical examination (opinion): publication cancelled [chapter 7.2 patent gazette] |
Free format text: ANULADA A PUBLICACAO DO ITEM 7.1 DA RPI 2222 DE 06/08/2013 POR TER SIDO INDEVIDA. |
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B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] |
Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 15/04/2004, OBSERVADAS AS CONDICOES LEGAIS. |
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B21F | Lapse acc. art. 78, item iv - on non-payment of the annual fees in time |
Free format text: REFERENTE A 11A ANUIDADE. |
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B24J | Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12) |
Free format text: EM VIRTUDE DA EXTINCAO PUBLICADA NA RPI 2343 DE 01-12-2015 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDA A EXTINCAO DA PATENTE E SEUS CERTIFICADOS, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013. |