BR9812595A - Processo para purificar 4-amino-piperidinas 2,2,6,6-tetrasubstituìdas - Google Patents
Processo para purificar 4-amino-piperidinas 2,2,6,6-tetrasubstituìdasInfo
- Publication number
- BR9812595A BR9812595A BR9812595-8A BR9812595A BR9812595A BR 9812595 A BR9812595 A BR 9812595A BR 9812595 A BR9812595 A BR 9812595A BR 9812595 A BR9812595 A BR 9812595A
- Authority
- BR
- Brazil
- Prior art keywords
- amino
- tetrasubstituted
- piperidines
- purifying
- purify
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 3
- BCIIMDOZSUCSEN-UHFFFAOYSA-N piperidin-4-amine Chemical class NC1CCNCC1 BCIIMDOZSUCSEN-UHFFFAOYSA-N 0.000 title abstract 3
- -1 2,2,6,6-tetrasubstituted 4-amino-piperidines Chemical class 0.000 abstract 1
- VRJHQPZVIGNGMX-UHFFFAOYSA-N 4-piperidinone Chemical class O=C1CCNCC1 VRJHQPZVIGNGMX-UHFFFAOYSA-N 0.000 abstract 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 238000004821 distillation Methods 0.000 abstract 1
- 230000000887 hydrating effect Effects 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D211/00—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings
- C07D211/04—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D211/06—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having no double bonds between ring members or between ring members and non-ring members
- C07D211/36—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having no double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D211/56—Nitrogen atoms
- C07D211/58—Nitrogen atoms attached in position 4
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D211/00—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings
- C07D211/04—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D211/06—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having no double bonds between ring members or between ring members and non-ring members
- C07D211/36—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having no double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D211/40—Oxygen atoms
- C07D211/44—Oxygen atoms attached in position 4
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Hydrogenated Pyridines (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
"PROCESSO PARA PURIFICAR 4-AMINO-PIPERIDINAS 2,2,6,6-TETRASUBSTITUìDAS". A invenção está relacionada a um processo para purificar 4-amino-piperidinas 2,2,6,6-tetrasubstituídas produzidas das correspondentes piperidin-4-onas, e subsequente destilação. De acordo com a invenção, a 4-amino-piperidina 2,2,6,6-tetrasubstituída destilada é reagida com hidrogênio na presença de um catalisador hidratante ou deshidratante e a 4-amino piperidina é então separada da mistura de reação.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19743433A DE19743433C1 (de) | 1997-10-01 | 1997-10-01 | Verfahren zur Reinigung von 4-Amino-piperidinen |
PCT/EP1998/006117 WO1999016749A1 (de) | 1997-10-01 | 1998-09-25 | Verfahren zur reinigung von 4-amino-piperidinen |
Publications (1)
Publication Number | Publication Date |
---|---|
BR9812595A true BR9812595A (pt) | 2000-08-01 |
Family
ID=7844311
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BR9812595-8A BR9812595A (pt) | 1997-10-01 | 1998-09-25 | Processo para purificar 4-amino-piperidinas 2,2,6,6-tetrasubstituìdas |
Country Status (16)
Country | Link |
---|---|
EP (1) | EP1025084A1 (pt) |
JP (1) | JP2001518465A (pt) |
KR (1) | KR20010030840A (pt) |
CN (1) | CN1272843A (pt) |
AU (1) | AU9746998A (pt) |
BR (1) | BR9812595A (pt) |
CA (1) | CA2305282A1 (pt) |
CO (1) | CO4770994A1 (pt) |
DE (1) | DE19743433C1 (pt) |
HU (1) | HUP0004584A2 (pt) |
ID (1) | ID23897A (pt) |
NZ (1) | NZ503565A (pt) |
PL (1) | PL339578A1 (pt) |
SK (1) | SK4262000A3 (pt) |
TW (1) | TW377345B (pt) |
WO (1) | WO1999016749A1 (pt) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE102008040045A1 (de) | 2008-02-01 | 2009-08-06 | Evonik Degussa Gmbh | Verfahren zur Herstellung von 4-Amino-2,2,6,6-tetramethylpiperidin |
EP2085384A1 (de) | 2008-02-01 | 2009-08-05 | Evonik Degussa GmbH | Verfahren zur Herstellung von 4-Amino-2,2,6,6-tetramethylpiperidin |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3003843A1 (de) * | 1980-02-02 | 1981-08-13 | Chemische Werke Hüls AG, 4370 Marl | Verfahren zur herstellung von 4-amino-2,2,6,6-tetramethylpiperidin |
CH664361A5 (de) * | 1985-06-13 | 1988-02-29 | Ni Institutkhimikatov Dlya Pol | Verfahren zur herstellung von 4-amino-2,2,6,6-tetramethylpiperidin. |
US4766247A (en) * | 1986-09-26 | 1988-08-23 | Air Products And Chemicals, Inc. | Color reduction of polyamines by mild catalytic hydrogenation |
JP2718179B2 (ja) * | 1989-05-26 | 1998-02-25 | 三井化学株式会社 | 2,2,6,6‐テトラアルキル‐4‐ピペリジノンの精製方法 |
DE19622269A1 (de) * | 1996-06-03 | 1997-12-04 | Basf Ag | Verfahren zur Reinigung von sterisch gehinderten 4-Aminopiperidinen |
-
1997
- 1997-10-01 DE DE19743433A patent/DE19743433C1/de not_active Expired - Lifetime
-
1998
- 1998-09-25 NZ NZ503565A patent/NZ503565A/en unknown
- 1998-09-25 KR KR1020007003498A patent/KR20010030840A/ko not_active Application Discontinuation
- 1998-09-25 HU HU0004584A patent/HUP0004584A2/hu unknown
- 1998-09-25 SK SK426-2000A patent/SK4262000A3/sk unknown
- 1998-09-25 PL PL98339578A patent/PL339578A1/xx unknown
- 1998-09-25 WO PCT/EP1998/006117 patent/WO1999016749A1/de not_active Application Discontinuation
- 1998-09-25 JP JP2000513835A patent/JP2001518465A/ja not_active Withdrawn
- 1998-09-25 CA CA002305282A patent/CA2305282A1/en not_active Abandoned
- 1998-09-25 CN CN98809761A patent/CN1272843A/zh active Pending
- 1998-09-25 AU AU97469/98A patent/AU9746998A/en not_active Abandoned
- 1998-09-25 ID IDW20000612D patent/ID23897A/id unknown
- 1998-09-25 EP EP98951469A patent/EP1025084A1/de not_active Withdrawn
- 1998-09-25 BR BR9812595-8A patent/BR9812595A/pt not_active Application Discontinuation
- 1998-09-30 CO CO98056932A patent/CO4770994A1/es unknown
- 1998-09-30 TW TW087116216A patent/TW377345B/zh active
Also Published As
Publication number | Publication date |
---|---|
EP1025084A1 (de) | 2000-08-09 |
AU9746998A (en) | 1999-04-23 |
CO4770994A1 (es) | 1999-04-30 |
ID23897A (id) | 2000-05-25 |
JP2001518465A (ja) | 2001-10-16 |
HUP0004584A2 (hu) | 2001-04-28 |
SK4262000A3 (en) | 2000-10-09 |
CN1272843A (zh) | 2000-11-08 |
TW377345B (en) | 1999-12-21 |
CA2305282A1 (en) | 1999-04-08 |
KR20010030840A (ko) | 2001-04-16 |
NZ503565A (en) | 2001-09-28 |
PL339578A1 (en) | 2000-12-18 |
WO1999016749A1 (de) | 1999-04-08 |
DE19743433C1 (de) | 1999-04-22 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
FA10 | Dismissal: dismissal - article 33 of industrial property law | ||
B11Y | Definitive dismissal - extension of time limit for request of examination expired [chapter 11.1.1 patent gazette] |