BR112020002577A2 - processo de centrifugação dupla para purificação de óleo nutritivo - Google Patents
processo de centrifugação dupla para purificação de óleo nutritivo Download PDFInfo
- Publication number
- BR112020002577A2 BR112020002577A2 BR112020002577-1A BR112020002577A BR112020002577A2 BR 112020002577 A2 BR112020002577 A2 BR 112020002577A2 BR 112020002577 A BR112020002577 A BR 112020002577A BR 112020002577 A2 BR112020002577 A2 BR 112020002577A2
- Authority
- BR
- Brazil
- Prior art keywords
- oil
- centrifugation
- product
- yield
- light phase
- Prior art date
Links
- 238000005119 centrifugation Methods 0.000 title claims abstract description 63
- 235000008935 nutritious Nutrition 0.000 title claims abstract description 17
- 238000000746 purification Methods 0.000 title description 7
- 238000000034 method Methods 0.000 claims abstract description 56
- 238000000855 fermentation Methods 0.000 claims abstract description 38
- 230000004151 fermentation Effects 0.000 claims abstract description 38
- 239000000203 mixture Substances 0.000 claims description 21
- 235000020777 polyunsaturated fatty acids Nutrition 0.000 claims description 14
- 239000000839 emulsion Substances 0.000 claims description 8
- 230000000717 retained effect Effects 0.000 claims description 4
- GNFTZDOKVXKIBK-UHFFFAOYSA-N 3-(2-methoxyethoxy)benzohydrazide Chemical compound COCCOC1=CC=CC(C(=O)NN)=C1 GNFTZDOKVXKIBK-UHFFFAOYSA-N 0.000 claims description 2
- 230000015572 biosynthetic process Effects 0.000 claims description 2
- 238000005086 pumping Methods 0.000 claims description 2
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims 3
- FGUUSXIOTUKUDN-IBGZPJMESA-N C1(=CC=CC=C1)N1C2=C(NC([C@H](C1)NC=1OC(=NN=1)C1=CC=CC=C1)=O)C=CC=C2 Chemical compound C1(=CC=CC=C1)N1C2=C(NC([C@H](C1)NC=1OC(=NN=1)C1=CC=CC=C1)=O)C=CC=C2 FGUUSXIOTUKUDN-IBGZPJMESA-N 0.000 claims 1
- 102000004190 Enzymes Human genes 0.000 claims 1
- 108090000790 Enzymes Proteins 0.000 claims 1
- 235000016709 nutrition Nutrition 0.000 claims 1
- 238000000605 extraction Methods 0.000 abstract description 3
- 239000003921 oil Substances 0.000 description 106
- 239000012071 phase Substances 0.000 description 85
- 239000000047 product Substances 0.000 description 37
- 238000000926 separation method Methods 0.000 description 15
- 238000004519 manufacturing process Methods 0.000 description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
- 238000002347 injection Methods 0.000 description 7
- 239000007924 injection Substances 0.000 description 7
- 238000004458 analytical method Methods 0.000 description 6
- 239000008346 aqueous phase Substances 0.000 description 6
- 230000003647 oxidation Effects 0.000 description 5
- 238000007254 oxidation reaction Methods 0.000 description 5
- 230000008901 benefit Effects 0.000 description 4
- 230000001413 cellular effect Effects 0.000 description 4
- 238000002955 isolation Methods 0.000 description 4
- 208000016444 Benign adult familial myoclonic epilepsy Diseases 0.000 description 3
- 230000000052 comparative effect Effects 0.000 description 3
- 238000010924 continuous production Methods 0.000 description 3
- 208000016427 familial adult myoclonic epilepsy Diseases 0.000 description 3
- 235000019387 fatty acid methyl ester Nutrition 0.000 description 3
- ZGNITFSDLCMLGI-UHFFFAOYSA-N flubendiamide Chemical compound CC1=CC(C(F)(C(F)(F)F)C(F)(F)F)=CC=C1NC(=O)C1=CC=CC(I)=C1C(=O)NC(C)(C)CS(C)(=O)=O ZGNITFSDLCMLGI-UHFFFAOYSA-N 0.000 description 3
- 244000005700 microbiome Species 0.000 description 3
- 239000006227 byproduct Substances 0.000 description 2
- 238000004364 calculation method Methods 0.000 description 2
- 239000003995 emulsifying agent Substances 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000000813 microbial effect Effects 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 238000004064 recycling Methods 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 241000251468 Actinopterygii Species 0.000 description 1
- 241000195493 Cryptophyta Species 0.000 description 1
- 239000004614 Process Aid Substances 0.000 description 1
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 238000003287 bathing Methods 0.000 description 1
- 230000006037 cell lysis Effects 0.000 description 1
- 210000002421 cell wall Anatomy 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000009089 cytolysis Effects 0.000 description 1
- 230000037213 diet Effects 0.000 description 1
- 235000005911 diet Nutrition 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- 102000038379 digestive enzymes Human genes 0.000 description 1
- 108091007734 digestive enzymes Proteins 0.000 description 1
- 230000009977 dual effect Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 230000008821 health effect Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000008240 homogeneous mixture Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 239000012074 organic phase Substances 0.000 description 1
- 239000003380 propellant Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 235000019640 taste Nutrition 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P7/00—Preparation of oxygen-containing organic compounds
- C12P7/64—Fats; Fatty oils; Ester-type waxes; Higher fatty acids, i.e. having at least seven carbon atoms in an unbroken chain bound to a carboxyl group; Oxidised oils or fats
- C12P7/6409—Fatty acids
- C12P7/6427—Polyunsaturated fatty acids [PUFA], i.e. having two or more double bonds in their backbone
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
- A23D9/04—Working-up
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/115—Fatty acids or derivatives thereof; Fats or oils
- A23L33/12—Fatty acids or derivatives thereof
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D21/00—Separation of suspended solid particles from liquids by sedimentation
- B01D21/26—Separation of sediment aided by centrifugal force or centripetal force
- B01D21/262—Separation of sediment aided by centrifugal force or centripetal force by using a centrifuge
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P7/00—Preparation of oxygen-containing organic compounds
- C12P7/64—Fats; Fatty oils; Ester-type waxes; Higher fatty acids, i.e. having at least seven carbon atoms in an unbroken chain bound to a carboxyl group; Oxidised oils or fats
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Zoology (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Genetics & Genomics (AREA)
- General Chemical & Material Sciences (AREA)
- Biotechnology (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Microbiology (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Mycology (AREA)
- Nutrition Science (AREA)
- Fats And Perfumes (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Edible Oils And Fats (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201762543659P | 2017-08-10 | 2017-08-10 | |
| US62/543,659 | 2017-08-10 | ||
| PCT/US2018/046081 WO2019032880A1 (en) | 2017-08-10 | 2018-08-09 | DOUBLE CENTRIFUGATION PROCESS FOR THE PURIFICATION OF NUTRITIVE OIL |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BR112020002577A2 true BR112020002577A2 (pt) | 2020-08-04 |
Family
ID=65271572
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BR112020002577-1A BR112020002577A2 (pt) | 2017-08-10 | 2018-08-09 | processo de centrifugação dupla para purificação de óleo nutritivo |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US11725221B2 (es) |
| EP (1) | EP3665296B1 (es) |
| CN (1) | CN111032878B (es) |
| BR (1) | BR112020002577A2 (es) |
| CA (1) | CA3072451A1 (es) |
| DK (1) | DK3665296T3 (es) |
| ES (1) | ES2916462T3 (es) |
| RU (1) | RU2769461C2 (es) |
| WO (1) | WO2019032880A1 (es) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DK180016B1 (da) | 2014-10-02 | 2020-01-22 | Evonik Degussa Gmbh | Feedstuff of high abrasion resistance and good stability in water, containing PUFAs |
| US11324234B2 (en) | 2014-10-02 | 2022-05-10 | Evonik Operations Gmbh | Method for raising animals |
| JP6998935B2 (ja) | 2016-07-13 | 2022-01-18 | エボニック オペレーションズ ゲーエムベーハー | 溶解された脂質含有バイオマスから脂質を分離する方法 |
| ES2872009T3 (es) | 2016-12-27 | 2021-11-02 | Evonik Degussa Gmbh | Método de aislamiento de lípidos a partir de una biomasa que contiene lípidos |
| EP3470502A1 (en) | 2017-10-13 | 2019-04-17 | Evonik Degussa GmbH | Method of separating lipids from a lysed lipids containing biomass |
| EP3527664A1 (en) | 2018-02-15 | 2019-08-21 | Evonik Degussa GmbH | Method of isolating lipids from a lipids containing biomass |
| US11976253B2 (en) | 2018-05-15 | 2024-05-07 | Evonik Operations Gmbh | Method of isolating lipids from a lysed lipids containing biomass by emulsion inversion |
| CA3101855C (en) | 2018-05-15 | 2023-06-20 | Evonik Operations Gmbh | Method of isolating lipids from a lipids containing biomass with aid of hydrophobic silica |
| EP3933016A1 (en) | 2020-06-30 | 2022-01-05 | Evonik Operations GmbH | Method of isolating lipids from a lipids containing biomass |
| FR3111912A1 (fr) | 2020-06-24 | 2021-12-31 | Fermentalg | Procédé de culture de microorganismes pour l’accumulation de lipides |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1178118A1 (en) * | 2000-08-02 | 2002-02-06 | Dsm N.V. | Isolation of microbial oils |
| JP2005529621A (ja) * | 2002-06-19 | 2005-10-06 | デーエスエム イーペー アセッツ ベスローテン フェンノートシャップ | 微生物細胞及び微生物油の低温殺菌方法 |
| EP2145942A1 (de) * | 2008-07-15 | 2010-01-20 | Lonza Ltd. | Verfahren zur Isolierung von Ölen aus Zellen und Biomasse |
| FR2949348B1 (fr) * | 2009-09-03 | 2012-11-02 | Rhodia Operations | Procede de separation en continu |
| CA2787344C (en) * | 2010-01-19 | 2018-03-20 | Dsm Ip Assets B.V. | Eicosapentaenoic acid-producing microorganisms, fatty acid compositions, and methods of making and uses thereof |
| FR2975705B1 (fr) * | 2011-05-27 | 2014-12-26 | Roquette Freres | Procede d'extraction du squalene a partir de microalgues |
| FR2991337B1 (fr) * | 2012-05-29 | 2016-09-02 | Roquette Freres | Procede continu d'enrichissement en esters ethyliques de dha d'une huile produite par des microalgues |
| US11124736B2 (en) * | 2013-12-20 | 2021-09-21 | Dsm Ip Assets B.V. | Processes for obtaining microbial oil from microbial cells |
| WO2015113864A1 (en) * | 2014-01-30 | 2015-08-06 | Evonik Degussa Gmbh | Process for making ethanol by fermentation |
| CN106811285B (zh) * | 2017-02-23 | 2020-04-17 | 湖北福星生物科技有限公司 | 一种从dha发酵液中物理提取dha油脂的方法 |
-
2018
- 2018-08-09 RU RU2020109893A patent/RU2769461C2/ru active
- 2018-08-09 CN CN201880052028.6A patent/CN111032878B/zh active Active
- 2018-08-09 CA CA3072451A patent/CA3072451A1/en active Pending
- 2018-08-09 EP EP18844409.5A patent/EP3665296B1/en active Active
- 2018-08-09 US US16/636,940 patent/US11725221B2/en active Active
- 2018-08-09 BR BR112020002577-1A patent/BR112020002577A2/pt unknown
- 2018-08-09 WO PCT/US2018/046081 patent/WO2019032880A1/en unknown
- 2018-08-09 DK DK18844409.5T patent/DK3665296T3/da active
- 2018-08-09 ES ES18844409T patent/ES2916462T3/es active Active
Also Published As
| Publication number | Publication date |
|---|---|
| EP3665296A1 (en) | 2020-06-17 |
| EP3665296B1 (en) | 2022-04-20 |
| US20200362373A1 (en) | 2020-11-19 |
| CN111032878A (zh) | 2020-04-17 |
| US11725221B2 (en) | 2023-08-15 |
| RU2020109893A3 (es) | 2021-11-11 |
| EP3665296A4 (en) | 2021-04-28 |
| RU2020109893A (ru) | 2021-09-14 |
| WO2019032880A1 (en) | 2019-02-14 |
| CN111032878B (zh) | 2024-03-08 |
| ES2916462T3 (es) | 2022-07-01 |
| CA3072451A1 (en) | 2019-02-14 |
| RU2769461C2 (ru) | 2022-03-31 |
| DK3665296T3 (da) | 2022-07-11 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| BR112020002577A2 (pt) | processo de centrifugação dupla para purificação de óleo nutritivo | |
| JP6266681B2 (ja) | 細胞からの脂質の抽出およびそれに由来する生産物 | |
| US20170298288A1 (en) | Solventless Extraction Process | |
| US6166231A (en) | Two phase extraction of oil from biomass | |
| DK2697345T3 (en) | A process for the isolation of a phospholipid | |
| US20110124034A1 (en) | Enrichment of process feedstock | |
| JP2019521685A (ja) | 油糧微生物を含む発酵ブロスから多価不飽和脂肪酸を含む微生物油を抽出するための方法 | |
| BR112016014262B1 (pt) | Método para recuperar lipídeos de uma população de micro-organismos | |
| WO2012109642A1 (en) | Aqueous extraction methods for high lipid microorganisms | |
| CN107523417A (zh) | 提取微生物油脂的方法 | |
| EP2988759A1 (fr) | Procédé d'extraction de solides organiques et d'huile d'organismes marins enrichis en astaxanthine | |
| CN106318985A (zh) | 微生物油脂 | |
| CN103820204A (zh) | 金枪鱼肝油的制备方法 | |
| Tabtabaei et al. | Biodiesel feedstock from emulsions produced by aqueous processing of yellow mustard | |
| RU2683559C1 (ru) | Способ получения топленого жира страуса | |
| CN103666743B (zh) | 一种利用木瓜蛋白酶从大鲵尾部脂肪提取粗鲵油的方法 | |
| US20140039212A1 (en) | Refining of edible oil | |
| CN116391850B (zh) | 一种具有高抗氧化活性的蛋黄油微乳液及其制备方法与应用 | |
| RU2619986C2 (ru) | Способ комплексной переработки малоценного рыбного сырья | |
| BR102014027320A2 (pt) | processo para extração de óleo vegetal | |
| BR102018074782A2 (pt) | processo de obtenção de matéria-prima para produção de tocoferóis / fitoesteróis / esqualeno / carotenóides e tocotrienóis | |
| CN116355698A (zh) | 一种利用二氯甲烷安全高效地提取土壤磷脂脂肪酸的方法 | |
| Adeoti et al. | LITERATURE REVIEW A REVIEW OF LIPID EXTRACTION FROM FISH PROCESSING BY-PRODUCT FOR USE AS A BIOFUEL |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| B350 | Update of information on the portal [chapter 15.35 patent gazette] |