BR112016028808A2 - ?usina e processo para executar reações de fase gasosa heterogeneamente catalisadas? - Google Patents

?usina e processo para executar reações de fase gasosa heterogeneamente catalisadas?

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Publication number
BR112016028808A2
BR112016028808A2 BR112016028808A BR112016028808A BR112016028808A2 BR 112016028808 A2 BR112016028808 A2 BR 112016028808A2 BR 112016028808 A BR112016028808 A BR 112016028808A BR 112016028808 A BR112016028808 A BR 112016028808A BR 112016028808 A2 BR112016028808 A2 BR 112016028808A2
Authority
BR
Brazil
Prior art keywords
gas phase
reactor
line
reagent
leading
Prior art date
Application number
BR112016028808A
Other languages
English (en)
Other versions
BR112016028808B1 (pt
BR112016028808B8 (pt
Inventor
Walter Thomas
Hammon Ulrich
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of BR112016028808A2 publication Critical patent/BR112016028808A2/pt
Publication of BR112016028808B1 publication Critical patent/BR112016028808B1/pt
Publication of BR112016028808B8 publication Critical patent/BR112016028808B8/pt

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B01J8/065—Feeding reactive fluids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/0278—Feeding reactive fluids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B01J8/067—Heating or cooling the reactor
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/28—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation of CHx-moieties
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/32—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
    • C07C45/33—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties
    • C07C45/34—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties in unsaturated compounds
    • C07C45/35—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties in unsaturated compounds in propene or isobutene
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/25—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
    • C07C51/252—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring of propene, butenes, acrolein or methacrolein
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00176—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles outside the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/0053—Controlling multiple zones along the direction of flow, e.g. pre-heating and after-cooling
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796—Details of the reactor or of the particulate material
    • B01J2208/00893—Feeding means for the reactants
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

a invenção refere-se a um sistema (1) para realizar reações catalíticas heterogêneas de fase gasosa que compreende: um reator (3); pelo menos uma linha (11), que leva ao reator (3), para introduzir reagentes no reator (3); pelo menos uma primeira alimentação (5), que leva à linha (11), para prover pelo menos um primeiro reagente a; pelo menos uma segunda alimentação (7), que leva à linha (11), para prover pelo menos um segundo reagente b; pelo menos uma terceira alimentação (9), que leva à linha (11), para prover um gás de circuito g; uma unidade de controle de temperatura (13), arranjada a montante do reator (3) na linha (11), para controlar a temperatura do primeiro reagente a e/ou segundo reagente b e/ou o gás de circuito g antes de entrar no reator (3); e pelo menos uma saída (15) para produtos, subprodutos e/ou reagentes não reagidos da reação de fase gasosa. a invenção também se refere a um método para realizar reações catalíticas heterogêneas de fase gasosa.
BR112016028808A 2014-06-12 2015-06-09 Usina e processo para executar reações de fase gasosa heterogeneamente catalisadas, e, uso de uma unidade de controle de temperatura em uma usina BR112016028808B8 (pt)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US201462011067P 2014-06-12 2014-06-12
DE102014108272.9A DE102014108272A1 (de) 2014-06-12 2014-06-12 Anlage und Verfahren zur Durchführung von heterogen katalysierten Gasphasen-Reaktionen
DE102014108272.9 2014-06-12
US62/011,067 2014-06-12
PCT/EP2015/062857 WO2015189221A1 (de) 2014-06-12 2015-06-09 Anlage und verfahren zur durchführung von heterogen katalysierten gasphasen-reaktionen

Publications (3)

Publication Number Publication Date
BR112016028808A2 true BR112016028808A2 (pt) 2017-08-22
BR112016028808B1 BR112016028808B1 (pt) 2021-09-21
BR112016028808B8 BR112016028808B8 (pt) 2021-11-23

Family

ID=54706241

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112016028808A BR112016028808B8 (pt) 2014-06-12 2015-06-09 Usina e processo para executar reações de fase gasosa heterogeneamente catalisadas, e, uso de uma unidade de controle de temperatura em uma usina

Country Status (8)

Country Link
US (1) US9636651B2 (pt)
EP (1) EP3154672A1 (pt)
JP (2) JP6751354B2 (pt)
CN (1) CN106457189A (pt)
BR (1) BR112016028808B8 (pt)
DE (1) DE102014108272A1 (pt)
RU (1) RU2688858C2 (pt)
WO (1) WO2015189221A1 (pt)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102014114193A1 (de) 2014-09-30 2015-08-13 Basf Se Verfahren und Anlage zur Rückgewinnung von Acrylsäure
JP2024055688A (ja) * 2022-10-07 2024-04-18 日立造船株式会社 生成装置及び生成方法

Family Cites Families (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3904652A (en) * 1972-11-16 1975-09-09 Standard Oil Co Indiana Recycle process for oxidation of n-butane to maleic anhydride
DE2513405C2 (de) * 1975-03-26 1982-10-21 Basf Ag, 6700 Ludwigshafen Verfahren zur Herstellung von Acrylsäure durch Oxidation von Propylen mit Sauerstoff enthaltenden Gasen in zwei getrennten Katalysatorstufen, die in einem Röhrenreaktor hintereinander angeordnet sind
US4087471A (en) * 1977-05-20 1978-05-02 Petro-Tex Chemical Corporation Fixed bed process for the production of t-butanol
DE4023239A1 (de) 1990-07-21 1992-01-23 Basf Ag Verfahren zur katalytischen gasphasenoxidation von propen oder iso-buten zu acrolein oder methacrolein
DE4132263A1 (de) 1991-09-27 1993-04-01 Basf Ag Verfahren zur katalytischen gasphasenoxidation von acrolein zu acrylsaeure
JP4659988B2 (ja) * 2001-02-06 2011-03-30 株式会社日本触媒 機器の冷却方法
CN100379776C (zh) * 2002-02-06 2008-04-09 株式会社日本触媒 在非稳定状态下冷却加热用换热器的方法
JP4325146B2 (ja) 2002-03-11 2009-09-02 三菱化学株式会社 （メタ）アクリル酸類の製造方法
KR100450234B1 (ko) 2002-07-10 2004-09-24 주식회사 엘지화학 개선된 열교환 시스템을 갖는 촉매 산화 반응기
US7414149B2 (en) * 2004-11-22 2008-08-19 Rohm And Haas Company Non-routine reactor shutdown method
BRPI0609864B1 (pt) * 2005-04-29 2016-09-06 Altaca Insaat Ve Dis Ticaret A S processo para conversão de um material orgânico em combustíveis hidrocarbonetos
DE102006051899A1 (de) * 2006-10-31 2008-05-15 Bayer Technology Services Gmbh Verfahren und Vorrichtung zur katalytischen Oxidation von SO2-haltigen Gasen mit Sauerstoff
DE102007004961A1 (de) 2007-01-26 2008-07-31 Basf Se Verfahren zur Herstellung von Katalysatorformkörpern, deren Aktivmasse ein Multielementoxid ist
EP2114562B1 (de) 2007-01-19 2017-11-01 Basf Se Verfahren zur herstellung von katalysatorformkörpern, deren aktivmasse ein multielementoxid ist
DE102010048405A1 (de) 2010-10-15 2011-05-19 Basf Se Verfahren zum Langzeitbetrieb einer heterogen katalysierten partiellen Gasphasenoxidation von Proben zu Acrolein
DE102013218628A1 (de) 2013-09-17 2014-03-06 Basf Se Katalysator zur Herstellung einer ungesättigten Carbonsäure durch Gasphasenoxidationeines ungesättigten Aldehyds
JP6407278B2 (ja) 2013-11-11 2018-10-17 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ アルケンを気相酸化して不飽和アルデヒド及び／又は不飽和カルボン酸にするための、機械的に安定な中空円筒形触媒成形体
DE102013226428A1 (de) 2013-12-18 2015-06-18 Basf Se Extraktionskolonne und Verfahren zum Extrahieren eines Bestandteils aus einem Fluid

Also Published As

Publication number Publication date
JP2017520397A (ja) 2017-07-27
EP3154672A1 (de) 2017-04-19
DE102014108272A1 (de) 2015-12-17
US9636651B2 (en) 2017-05-02
BR112016028808B1 (pt) 2021-09-21
CN106457189A (zh) 2017-02-22
US20150360191A1 (en) 2015-12-17
JP6732972B2 (ja) 2020-07-29
JP6751354B2 (ja) 2020-09-02
JP2019069444A (ja) 2019-05-09
RU2688858C2 (ru) 2019-05-22
BR112016028808B8 (pt) 2021-11-23
WO2015189221A1 (de) 2015-12-17
RU2017100551A3 (pt) 2018-12-11
RU2017100551A (ru) 2018-07-12

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Legal Events

Date Code Title Description
B06U Preliminary requirement: requests with searches performed by other patent offices: procedure suspended [chapter 6.21 patent gazette]
B07A Application suspended after technical examination (opinion) [chapter 7.1 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 09/06/2015, OBSERVADAS AS CONDICOES LEGAIS.

B09W Correction of the decision to grant [chapter 9.1.4 patent gazette]

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B16C Correction of notification of the grant [chapter 16.3 patent gazette]

Free format text: REFERENTE AO DESPACHO 16.1 PUBLICADO NA RPI 2646, QUANTO AO RELATORIO DESCRITIVO E AS REIVINDICACOES