BR112015014084A2 - dispositivo e método para a separação de um diéster cíclico de massas poliméricas fundidas - Google Patents
dispositivo e método para a separação de um diéster cíclico de massas poliméricas fundidasInfo
- Publication number
- BR112015014084A2 BR112015014084A2 BR112015014084A BR112015014084A BR112015014084A2 BR 112015014084 A2 BR112015014084 A2 BR 112015014084A2 BR 112015014084 A BR112015014084 A BR 112015014084A BR 112015014084 A BR112015014084 A BR 112015014084A BR 112015014084 A2 BR112015014084 A2 BR 112015014084A2
- Authority
- BR
- Brazil
- Prior art keywords
- cyclic diester
- separation
- polymer melts
- separating
- diester
- Prior art date
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D7/00—Sublimation
- B01D7/02—Crystallisation directly from the vapour phase
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D319/00—Heterocyclic compounds containing six-membered rings having two oxygen atoms as the only ring hetero atoms
- C07D319/10—1,4-Dioxanes; Hydrogenated 1,4-dioxanes
- C07D319/12—1,4-Dioxanes; Hydrogenated 1,4-dioxanes not condensed with other rings
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/10—Vacuum distillation
- B01D3/101—Recirculation of the fluid used as fluid working medium in a vacuum creating device
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/10—Vacuum distillation
- B01D3/105—Vacuum distillation with the use of an ejector for creating the vacuum, the ejector being placed between evaporator or distillation devices
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
- B01D5/0003—Condensation of vapours; Recovering volatile solvents by condensation by using heat-exchange surfaces for indirect contact between gases or vapours and the cooling medium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
- B01D5/0033—Other features
- B01D5/0045—Vacuum condensation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/02—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
- C08G63/06—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from hydroxycarboxylic acids
- C08G63/08—Lactones or lactides
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/78—Preparation processes
- C08G63/785—Preparation processes characterised by the apparatus used
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/88—Post-polymerisation treatment
- C08G63/90—Purification; Drying
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Crystallography & Structural Chemistry (AREA)
- Polyesters Or Polycarbonates (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Heterocyclic Compounds That Contain Two Or More Ring Oxygen Atoms (AREA)
- Separation, Recovery Or Treatment Of Waste Materials Containing Plastics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
resumo dispositivo e método para a separação de um diéster cíclico de massas poliméricas fundidas a presente invenção se refere a um dispositivo e também a um método para a separação e recuperação de um diéster cíclico, em particular, dilactídeo ou glicolídeo a partir de massas poliméricas fundidas que incluem o diéster cíclico como impureza. o dispositivo e também o método de acordo com a invenção permite a recuperação do diéster cíclico com um rendimento elevado e, ao mesmo tempo, alta pureza. 1/1
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP12197885.2 | 2012-12-18 | ||
EP12197885.2A EP2746313B1 (de) | 2012-12-18 | 2012-12-18 | Vorrichtung und Verfahren zur Abtrennung eines cyclischen Diesters aus Polymerschmelzen |
PCT/EP2013/071674 WO2014095116A1 (de) | 2012-12-18 | 2013-10-17 | Vorrichtung und verfahren zur abtrennung eines cyclischen diesters aus polymerschmelzen |
Publications (2)
Publication Number | Publication Date |
---|---|
BR112015014084A2 true BR112015014084A2 (pt) | 2017-07-11 |
BR112015014084B1 BR112015014084B1 (pt) | 2021-08-31 |
Family
ID=47561144
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BR112015014084-0A BR112015014084B1 (pt) | 2012-12-18 | 2013-10-17 | Dispositivo e método para a separação e recuperação de um diéster cíclico |
Country Status (11)
Country | Link |
---|---|
US (1) | US10322358B2 (pt) |
EP (1) | EP2746313B1 (pt) |
KR (1) | KR101982543B1 (pt) |
CN (2) | CN104995233B (pt) |
BR (1) | BR112015014084B1 (pt) |
EA (1) | EA028421B1 (pt) |
ES (1) | ES2649369T3 (pt) |
IN (1) | IN2015DN02401A (pt) |
MX (1) | MX366117B (pt) |
TW (1) | TWI609009B (pt) |
WO (1) | WO2014095116A1 (pt) |
Families Citing this family (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2746313B1 (de) | 2012-12-18 | 2017-08-30 | Uhde Inventa-Fischer GmbH | Vorrichtung und Verfahren zur Abtrennung eines cyclischen Diesters aus Polymerschmelzen |
RU2621342C1 (ru) * | 2016-07-29 | 2017-06-02 | Федеральное государственное автономное образовательное учреждение высшего образования "Национальный исследовательский Томский государственный университет" (ТГУ, НИ ТГУ) | Приемник вакуумного камерного реактора синтеза гликолида и лактида |
EP3318590B1 (de) | 2016-11-08 | 2020-08-05 | thyssenkrupp AG | Verfahren zur abtrennung von flüchtigen verbindungen aus viskosen produkten mit einem dünnschichtverdampfer |
US10358540B2 (en) * | 2017-06-09 | 2019-07-23 | GM Global Technology Operations LLC | Process and system for reducing volatile compound emissions from a product |
US10266512B2 (en) | 2017-08-10 | 2019-04-23 | Novus International, Inc. | Processes for preparing heteroatom containing cyclic dimers |
DE102018120988C5 (de) | 2018-08-28 | 2023-01-12 | Technip Zimmer Gmbh | Verfahren und Vorrichtung zur Herstellung von extraktarmem Polyamid 6 |
CN112892147B (zh) * | 2021-01-30 | 2022-05-13 | 成都易态科技有限公司 | 混合气体的处理方法 |
CN112892097B (zh) * | 2021-01-30 | 2022-05-13 | 成都易态科技有限公司 | 混合气体的处理方法 |
CN112807921B (zh) * | 2021-01-30 | 2022-05-13 | 成都易态科技有限公司 | 混合气体的处理系统 |
CN114146442A (zh) * | 2021-12-14 | 2022-03-08 | 中国船舶重工集团公司第七0三研究所 | 真空旋流交换装置及其控制方法 |
Family Cites Families (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5023350A (en) * | 1990-05-24 | 1991-06-11 | E. I. Du Pont De Nemours And Company | Process for the purification of cyclic esters |
US5136017A (en) | 1991-02-22 | 1992-08-04 | Polysar Financial Services S.A. | Continuous lactide polymerization |
US5770682A (en) | 1995-07-25 | 1998-06-23 | Shimadzu Corporation | Method for producing polylactic acid |
JP3330284B2 (ja) * | 1996-07-03 | 2002-09-30 | 株式会社神戸製鋼所 | ポリ乳酸の製造方法 |
KR100543541B1 (ko) | 1997-02-14 | 2006-01-20 | 하이프럭스 아이피 리소시스 피티이. 엘티디. | 폴리락티드로부터 락티드를 분리하고 회수하는 방법 |
DE10020898B4 (de) | 2000-04-20 | 2004-02-05 | Inventa-Fischer Gmbh | Verfahren zur Herstellung von Polymilchsäure und Vorrichtung hierzu |
EP2030679A1 (de) | 2007-09-03 | 2009-03-04 | Uhde Inventa-Fischer GmbH | Polymerisationsreaktor, Polymerisationsvorrichtung, Verfahren zur Herstellung von bioabbaubarem Polyester sowie Verwendungen |
EP2055730B1 (en) | 2007-10-29 | 2013-02-27 | Hitachi Plant Technologies, Ltd. | Polymer producing method and apparatus and polymer degassing method and apparatus |
JP4670901B2 (ja) | 2008-05-27 | 2011-04-13 | 株式会社日立プラントテクノロジー | ポリ乳酸の製造装置およびその方法 |
WO2012110117A1 (en) * | 2011-02-18 | 2012-08-23 | Sulzer Chemtech Ag | Method for the manufacture of a polyhydroxy-carboxylic acid |
CN202052518U (zh) * | 2011-03-19 | 2011-11-30 | 友邦(江苏)聚氨酯新材料有限公司 | 生产聚醚多元醇的真空系统 |
EP2559725B1 (de) | 2011-08-19 | 2024-05-08 | Uhde Inventa-Fischer GmbH | Verfahren und Vorrichtung zur Rückgewinnung von Lactid aus Polylactid bzw. Glycolid aus Polyglycolid |
EP2725048B1 (de) | 2012-10-29 | 2016-07-20 | Uhde Inventa-Fischer GmbH | Verfahren zur Herstellung eines hochmolekularen Polyesters oder Copolyesters sowie diese enthaltende Polymerblends |
EP2746313B1 (de) | 2012-12-18 | 2017-08-30 | Uhde Inventa-Fischer GmbH | Vorrichtung und Verfahren zur Abtrennung eines cyclischen Diesters aus Polymerschmelzen |
-
2012
- 2012-12-18 EP EP12197885.2A patent/EP2746313B1/de active Active
- 2012-12-18 ES ES12197885.2T patent/ES2649369T3/es active Active
-
2013
- 2013-10-17 BR BR112015014084-0A patent/BR112015014084B1/pt active IP Right Grant
- 2013-10-17 WO PCT/EP2013/071674 patent/WO2014095116A1/de active Application Filing
- 2013-10-17 IN IN2401DEN2015 patent/IN2015DN02401A/en unknown
- 2013-10-17 MX MX2015007606A patent/MX366117B/es active IP Right Grant
- 2013-10-17 EA EA201590365A patent/EA028421B1/ru not_active IP Right Cessation
- 2013-10-17 CN CN201380062630.5A patent/CN104995233B/zh active Active
- 2013-10-17 US US14/652,617 patent/US10322358B2/en active Active
- 2013-10-17 KR KR1020157008915A patent/KR101982543B1/ko active IP Right Grant
- 2013-10-17 CN CN201710402721.9A patent/CN106977492B/zh active Active
- 2013-12-04 TW TW102144317A patent/TWI609009B/zh active
Also Published As
Publication number | Publication date |
---|---|
ES2649369T3 (es) | 2018-01-11 |
EA201590365A1 (ru) | 2015-09-30 |
TWI609009B (zh) | 2017-12-21 |
US10322358B2 (en) | 2019-06-18 |
CN104995233B (zh) | 2017-05-10 |
US20150329516A1 (en) | 2015-11-19 |
EP2746313A1 (de) | 2014-06-25 |
KR20150118083A (ko) | 2015-10-21 |
CN106977492B (zh) | 2019-10-18 |
CN104995233A (zh) | 2015-10-21 |
IN2015DN02401A (pt) | 2015-09-04 |
BR112015014084B1 (pt) | 2021-08-31 |
EP2746313B1 (de) | 2017-08-30 |
CN106977492A (zh) | 2017-07-25 |
TW201434823A (zh) | 2014-09-16 |
EA028421B1 (ru) | 2017-11-30 |
MX2015007606A (es) | 2015-10-22 |
WO2014095116A1 (de) | 2014-06-26 |
MX366117B (es) | 2019-06-27 |
KR101982543B1 (ko) | 2019-05-27 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
BR112015014084A2 (pt) | dispositivo e método para a separação de um diéster cíclico de massas poliméricas fundidas | |
WO2014100213A3 (en) | High temperature melt integrity battery separators via spinning | |
PL2864302T3 (pl) | Sposób wytwarzania oczyszczonego dialkilofurano-2,5-dikarboksylanu poprzez rozdzielanie fizyczne i rozdzielanie fazy stałej i ciekłej | |
MX2016013557A (es) | Produccion de 4-metil-tetrahidropiranos 2-sustituidos a partir de materiales de partida con contenido de 2-alquil-4,4-dimetil-1,3-di oxanos. | |
PE20180555A1 (es) | Procedimiento para la preparacion de (4s)-4-(4-ciano-2-metoxifenilo)-5-etoxi-2,8-dimetil-1,4-dihidro-1,6-naftiridina-3-carboxamida y para la recuperacion de (4s)-4-(4-ciano-2-metoxifenilo)-5-etoxi-2,8-dimetil-1,4-dihidro-1,6-naftiridina-3-carboxamida por medio de metodos electroquimicos | |
FR3007412B1 (fr) | Procede de recuperation de fibres organiques a partir d'un materiau composite | |
Chatrchyan et al. | Search for third-generation leptoquarks and scalar bottom quarks in pp collisions at $\sqrt {s}= 7\; TeV$ | |
PH12015500644B1 (en) | Novel rig-i ligands and methods for producing them | |
BR112015020883A2 (pt) | processo e aparelho para purificação de uma corrente contendo um éster cíclico de um ácido alfa-hidroxicarboxílico | |
MX2016013555A (es) | Produccion de 4-hidroxi-4-metil-tetrahidropiranos 2-sustituidos a partir de materiales de partida que contienen 2-alquil-4,4-dimetil-1,3-dioxanos. | |
BRPI0702959A (pt) | processo para extrair polióis de polìmeros | |
BR112016018347A2 (pt) | Método para a produção de composições enriquecidas em vitamina e, especialmente enriquecidas em tocotrienol, a partir de óleos naturais | |
SG11201501585SA (en) | Process for separating methylcyclopentanone from cyclohexanone | |
AR102062A1 (es) | Proceso para la separación mejorada de etilbenceno | |
BR112015027931A2 (pt) | processo para recuperar e aperfeiçoar a produção de meso-lactida a partir de um fluxo que contém bruta | |
MY164790A (en) | Purification of bio-based acrylic acid to crude and glacial acrylic acid | |
FR2986229B1 (fr) | Nouveaux monergols ioniques a base de n2o pour la propulsion spatiale | |
MX2018004009A (es) | Proceso para la recuperacion de una mezcla que comprende un derivado de acido (tio) fosforico. | |
BR112014000848A2 (pt) | processo de separação | |
WO2014102834A3 (en) | Process for lurasidone | |
BR112015012026A2 (pt) | método para isolamento de ácido chiquímico a partir do material residual do dendezeiro | |
CO7141428A2 (es) | Proceso para la elaboración de undecapéptidos cíclicos | |
IN2013MU03508A (pt) | ||
BR112015011204A8 (pt) | processo para a produção e separação de manitol e sorbitol de uma mistura a qual foi obtida pela hidrogenação de um precursor | |
MX2015005343A (es) | Sistema y metodo de extraccion de solvente de una planta de licor madre puro. |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
B06F | Objections, documents and/or translations needed after an examination request according [chapter 6.6 patent gazette] | ||
B06F | Objections, documents and/or translations needed after an examination request according [chapter 6.6 patent gazette] | ||
B06I | Publication of requirement cancelled [chapter 6.9 patent gazette] |
Free format text: ANULADA A PUBLICACAO CODIGO 6.6.1 NA RPI NO 2462 DE 13/03/2018 POR TER SIDO INDEVIDA. |
|
B06U | Preliminary requirement: requests with searches performed by other patent offices: procedure suspended [chapter 6.21 patent gazette] | ||
B06A | Patent application procedure suspended [chapter 6.1 patent gazette] | ||
B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] |
Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 17/10/2013, OBSERVADAS AS CONDICOES LEGAIS. |