BR112013025996A2 - processo para isolamento de micronutrientes - Google Patents

processo para isolamento de micronutrientes

Info

Publication number
BR112013025996A2
BR112013025996A2 BR112013025996A BR112013025996A BR112013025996A2 BR 112013025996 A2 BR112013025996 A2 BR 112013025996A2 BR 112013025996 A BR112013025996 A BR 112013025996A BR 112013025996 A BR112013025996 A BR 112013025996A BR 112013025996 A2 BR112013025996 A2 BR 112013025996A2
Authority
BR
Brazil
Prior art keywords
feedstock
micronutrient
fatty acid
glycerides
acyl
Prior art date
Application number
BR112013025996A
Other languages
English (en)
Inventor
Bent Sarup
Susanne Jonsson
Original Assignee
Alfa Laval Corp Ab
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Alfa Laval Corp Ab filed Critical Alfa Laval Corp Ab
Publication of BR112013025996A2 publication Critical patent/BR112013025996A2/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D311/00—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings
    • C07D311/02—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings ortho- or peri-condensed with carbocyclic rings or ring systems
    • C07D311/04—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring
    • C07D311/58—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring other than with oxygen or sulphur atoms in position 2 or 4
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G3/00—Production of liquid hydrocarbon mixtures from oxygen-containing organic materials, e.g. fatty oils, fatty acids
    • C10G3/42—Catalytic treatment
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B13/00—Recovery of fats, fatty oils or fatty acids from waste materials
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C1/00—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
    • C11C1/08—Refining
    • C11C1/10—Refining by distillation
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/003—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/02—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with glycerol
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/04—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fats or fatty oils
    • C11C3/06—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fats or fatty oils with glycerol
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/04—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fats or fatty oils
    • C11C3/10—Ester interchange
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/10—Biofuels, e.g. bio-diesel
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P30/00—Technologies relating to oil refining and petrochemical industry
    • Y02P30/20—Technologies relating to oil refining and petrochemical industry using bio-feedstock
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00—Technologies for solid waste management
    • Y02W30/50—Reuse, recycling or recovery technologies
    • Y02W30/74—Recovery of fats, fatty oils, fatty acids or other fatty substances, e.g. lanolin or waxes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Wood Science & Technology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Fats And Perfumes (AREA)
  • Liquid Carbonaceous Fuels (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

processo para isolamento de micronutrientes a presente invenção se refere a um processo para o isolamento de micronutrientes a partir do destilado desodorizador que compreende ácidos graxos livres, o processo compreende as seguintes etapas: (i) tratar o destilado desodorizador em uma etapa de esterificação com glicerol, na qual a etapa de esterificação é autocatalisada, produzinto uma carga de alimentação de glicerídeos de acila e excesso de descarga de glicerol e água produzida; (ii) transferir a carga de alimentação dos glicerídeos de acila tendo um teor de água menor do que 1500 ppm e um teor de ácido graxo livre menor do que 3% em peso a uma etapa de transesterificação e tratar a carga de alimentação dos glicerídeos de acila com metanol para produzir um produto biodiesel bruto; (iii) refinar o produto biodiesel bruto em uma etapa de destilação e separar o produto biodiesel bruto nas três frações 1) éster metílico do ácido graxo, 2) produto rico em micronutriente que compreende tocoferol e 3) hidrocarbonetos leves.
BR112013025996A 2011-04-14 2012-04-12 processo para isolamento de micronutrientes BR112013025996A2 (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
SE1100281 2011-04-14
PCT/EP2012/056630 WO2012140111A1 (en) 2011-04-14 2012-04-12 A process for autocatalytic esterification of fatty acids

Publications (1)

Publication Number Publication Date
BR112013025996A2 true BR112013025996A2 (pt) 2016-12-27

Family

ID=45976920

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112013025996A BR112013025996A2 (pt) 2011-04-14 2012-04-12 processo para isolamento de micronutrientes

Country Status (12)

Country Link
US (1) US9085547B2 (pt)
EP (1) EP2697348B1 (pt)
JP (1) JP5808479B2 (pt)
CN (1) CN103502410A (pt)
AR (1) AR086082A1 (pt)
BR (1) BR112013025996A2 (pt)
ES (1) ES2556788T3 (pt)
MY (1) MY163129A (pt)
PL (1) PL2697348T3 (pt)
PT (1) PT2697348E (pt)
RU (1) RU2558364C2 (pt)
WO (1) WO2012140111A1 (pt)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2920288B1 (en) * 2012-11-13 2019-04-03 Rrip, Llc Method to recover free fatty acids from fats and oils
HUE049020T2 (hu) * 2013-06-11 2020-08-28 Renewable Energy Group Inc Eljárás biodízel és az abból nyert termékek elõállítására
WO2015164106A1 (en) * 2014-04-24 2015-10-29 The Procter & Gamble Company Method for converting odor containing fatty acids to deodorized glycerides
US9643163B2 (en) 2014-10-10 2017-05-09 Crystaphase Products, Inc. Heterogeneous catalyst for transesterification and method of preparing same
WO2016168697A1 (en) 2015-04-17 2016-10-20 Crystaphase Products, Inc. Heterogeneous catalyst for transesterification and method of preparing same
TR201720807A1 (tr) * 2017-12-19 2019-07-22 Maysa Yag Sanayi Anonim Sirketi Yüksek asi̇tli̇ yağlardan (high ffa oils&fats), yağ asi̇tleri̇nden (fatty acid), yağlarin rafi̇nasyon yan ürünü sülfürlü asi̇tli̇ yağlardan (acidoil) en14214 normunda bi̇yodi̇zel (meti̇l ester) üreti̇m yöntemi̇
AU2019262044B2 (en) * 2018-05-03 2024-05-30 Renewable Energy Group, Inc. Methods and devices for producing biodiesel, diesel-range hydrocarbons, and products obtained therefrom
WO2020223208A1 (en) * 2019-04-29 2020-11-05 Regents Of The University Of Minnesota Systems and methods for assessing and treating hemorrhage and other conditions
FI129823B (en) * 2019-08-30 2022-09-15 Neste Oyj Purification procedure for biological input material
IT201900023979A1 (it) * 2019-12-13 2021-06-13 Sepe S R L Procedimento per la produzione di olio vegetale puro (ppo) da oli acidi
IL286349A (en) * 2021-09-13 2023-04-01 Univice M E Ltd Processes for the production of biodiesel from fatty waste

Family Cites Families (13)

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Publication number Priority date Publication date Assignee Title
JPS5716878A (en) 1980-07-04 1982-01-28 Nisshin Oil Mills Ltd:The Production of tocopherol concentrate
DE4228476C2 (de) 1992-08-27 2002-05-02 Cognis Deutschland Gmbh Verfahren zum Gewinnen von Tocopherol und/oder Sterin
US5424457A (en) * 1994-05-27 1995-06-13 Eastman Chemical Company Process for the production of sterol and tocopherol concentrates
US6750359B1 (en) 2001-09-04 2004-06-15 Ip Holdings, L.L.C. Methods for treating deodorizer distillate
UA78066C2 (en) 2002-06-19 2007-02-15 Process for recovery of plant sterols and tocopherols from deodorized distillates
CN1292670C (zh) 2002-07-04 2007-01-03 北京市粮食科学研究所 一种液态低热量油脂——混合的甘油三酯
US6822105B1 (en) 2003-08-12 2004-11-23 Stepan Company Method of making alkyl esters using glycerin
ATE525344T1 (de) * 2006-07-10 2011-10-15 A & A F Lli Parodi S R L Verfahren zur herstellung von biodiesel
CN101657543A (zh) 2007-04-11 2010-02-24 诺维信公司 用于产生生物柴油的方法
GB2451580A (en) 2007-08-01 2009-02-04 Smet Ballestra Engineering S A Esterification process
EP2028260A1 (en) 2007-08-01 2009-02-25 N.V. Desmet Ballestra Engineering S.A. Esterification process
CN101173176A (zh) 2007-08-07 2008-05-07 崔明林 利用动植物废油连续生产生物柴油的工艺方法
CN101451071A (zh) * 2007-12-05 2009-06-10 青岛生物能源与过程研究所 一种生物柴油制备方法及其可移动式生产装置

Also Published As

Publication number Publication date
JP5808479B2 (ja) 2015-11-10
RU2013150594A (ru) 2015-05-20
PT2697348E (pt) 2016-01-20
US20140039206A1 (en) 2014-02-06
EP2697348A1 (en) 2014-02-19
US9085547B2 (en) 2015-07-21
AR086082A1 (es) 2013-11-20
WO2012140111A1 (en) 2012-10-18
MY163129A (en) 2017-08-15
RU2558364C2 (ru) 2015-08-10
CN103502410A (zh) 2014-01-08
ES2556788T3 (es) 2016-01-20
PL2697348T3 (pl) 2016-03-31
JP2014510823A (ja) 2014-05-01
EP2697348B1 (en) 2015-10-21

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Legal Events

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B08F Application fees: dismissal - article 86 of industrial property law
B08K Lapse as no evidence of payment of the annual fee has been furnished to inpi (acc. art. 87)