BR0317047A - Processo contìnuo de preparo de lactato de etila - Google Patents
Processo contìnuo de preparo de lactato de etilaInfo
- Publication number
- BR0317047A BR0317047A BR0317047-0A BR0317047A BR0317047A BR 0317047 A BR0317047 A BR 0317047A BR 0317047 A BR0317047 A BR 0317047A BR 0317047 A BR0317047 A BR 0317047A
- Authority
- BR
- Brazil
- Prior art keywords
- ethyl lactate
- mixture
- ethanol
- continuous process
- lactic acid
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
- C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
- C07C69/66—Esters of carboxylic acids having esterified carboxylic groups bound to acyclic carbon atoms and having any of the groups OH, O—metal, —CHO, keto, ether, acyloxy, groups, groups, or in the acid moiety
- C07C69/67—Esters of carboxylic acids having esterified carboxylic groups bound to acyclic carbon atoms and having any of the groups OH, O—metal, —CHO, keto, ether, acyloxy, groups, groups, or in the acid moiety of saturated acids
- C07C69/675—Esters of carboxylic acids having esterified carboxylic groups bound to acyclic carbon atoms and having any of the groups OH, O—metal, —CHO, keto, ether, acyloxy, groups, groups, or in the acid moiety of saturated acids of saturated hydroxy-carboxylic acids
- C07C69/68—Lactic acid esters
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
"PROCESSO CONTìNUO DE PREPARO DE LACTATO DE ETILA". A invenção se refere a um processo contínuo de preparo de lactato de etila por esterificação de ácido láctico por meio do etanol, em presença de um catalisador que consiste em extrair em contínuo, do meio reacional de esterificação a uma taxa de conversão parcial do ácido láctico, uma mistura que compreende lactato de etila, etanol, água e diversos produtos pesados, depois de se submeter essa mistura a uma separação flash, sob pressão reduzida, da qual sai um fluxo de cabeça, compreendendo uma mistura de lactato de etila, de etanol e de água, mistura essa que alimenta, em sua parte baixa, uma coluna de destilação fracionada.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR0215348A FR2848209B1 (fr) | 2002-12-05 | 2002-12-05 | Procede continu de preparation de lactate d'ethyle |
PCT/FR2003/003598 WO2004052825A2 (fr) | 2002-12-05 | 2003-12-05 | Procede continu de preparation de lactate d'ethyle |
Publications (1)
Publication Number | Publication Date |
---|---|
BR0317047A true BR0317047A (pt) | 2005-10-25 |
Family
ID=32320010
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BR0317047-0A BR0317047A (pt) | 2002-12-05 | 2003-12-05 | Processo contìnuo de preparo de lactato de etila |
Country Status (11)
Country | Link |
---|---|
US (1) | US20060041165A1 (pt) |
EP (1) | EP1569891A2 (pt) |
JP (1) | JP2006509024A (pt) |
KR (1) | KR100762773B1 (pt) |
CN (1) | CN1720215A (pt) |
AU (1) | AU2003298421B2 (pt) |
BR (1) | BR0317047A (pt) |
CA (1) | CA2508125A1 (pt) |
FR (1) | FR2848209B1 (pt) |
MX (1) | MXPA05005962A (pt) |
WO (1) | WO2004052825A2 (pt) |
Families Citing this family (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN100427453C (zh) * | 2004-08-27 | 2008-10-22 | 清华大学 | 催化精馏法合成乳酸乙酯工艺 |
US20110160480A1 (en) * | 2008-07-30 | 2011-06-30 | Galactic Sa | Continuous Process for Obtaining a Lactic Ester |
BE1019021A3 (fr) * | 2009-07-01 | 2012-01-10 | Galactic Sa | Procede de preparation de lactate d'alkyle c1-c4 de grande purete par putrification des lactates d'alkyle c1-c4 bruts. |
KR101140649B1 (ko) * | 2009-09-30 | 2012-05-03 | 한국화학연구원 | 암모늄락테이트로부터 알킬락테이트를 직접 제조하는 방법 |
KR101198866B1 (ko) | 2010-12-02 | 2012-11-07 | 한국화학연구원 | 고순도 알킬락테이트 및 젖산의 회수 방법 |
CN102381973B (zh) * | 2011-09-19 | 2014-01-29 | 南京大学 | 一种超高纯度(电子级)乳酸酯类产品的生产工艺 |
WO2013159347A1 (zh) | 2012-04-27 | 2013-10-31 | 孝感市易生新材料有限公司 | 一种连续生产高含量和高光学纯度乳酸酯的方法 |
WO2015058118A1 (en) | 2013-10-17 | 2015-04-23 | Cargill, Incorporated | Method for producing alkyl hydroxyalkanoates |
RU2017101543A (ru) * | 2014-07-10 | 2018-08-10 | Арчер Дэниелс Мидлэнд Компани | Новый способ извлечения молочной кислоты |
US10239819B2 (en) | 2014-10-17 | 2019-03-26 | Cargill, Incorporated | Methods for producing an ester of an alpha, beta-unsaturated carboxylic acid |
PL229904B1 (pl) | 2015-01-08 | 2018-09-28 | Wroclawskie Centrum Badan Eit Spolka Z Ograniczona Odpowiedzialnoscia | Sposób otrzymywania estrów kwasu mlekowego i mleczanomlekowego w reakcji alkoholizy poliestru alifatycznego |
CN104876819A (zh) * | 2015-05-14 | 2015-09-02 | 安徽中草香料有限公司 | 一种乳酸异丙酯的制备方法 |
CN107032984A (zh) * | 2016-02-03 | 2017-08-11 | 天津中福工程技术有限公司 | 一种连续催化精馏制备乳酸乙酯的方法 |
KR102019037B1 (ko) | 2017-05-26 | 2019-09-06 | 지에스칼텍스 주식회사 | 알킬 카르복실산 에스테르의 제조 방법 |
KR102151747B1 (ko) | 2018-11-23 | 2020-09-03 | 지에스칼텍스 주식회사 | 알킬 카르복실산 에스테르의 제조 방법 및 알킬 카르복실산 에스테르의 제조 장치 |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2406648A (en) * | 1942-12-08 | 1946-08-27 | Sealtest Inc | Process of preparing water-soluble alkyl lactates |
US2465772A (en) * | 1944-02-17 | 1949-03-29 | Nat Dairy Res Lab Inc | Preparation of alkyl lactates |
DD206373A1 (de) * | 1982-03-16 | 1984-01-25 | Joachim Franke | Verfahren und vorrichtung zur abtrennung von milchsaeure aus rohloesungen |
US5210296A (en) * | 1990-11-19 | 1993-05-11 | E. I. Du Pont De Nemours And Company | Recovery of lactate esters and lactic acid from fermentation broth |
US5723639A (en) * | 1995-10-16 | 1998-03-03 | University Of Chicago | Esterification of fermentation-derived acids via pervaporation |
US6664413B1 (en) * | 1998-11-19 | 2003-12-16 | A. E. Staley Manufacturing Co. | Process for production of esters |
-
2002
- 2002-12-05 FR FR0215348A patent/FR2848209B1/fr not_active Expired - Fee Related
-
2003
- 2003-12-05 WO PCT/FR2003/003598 patent/WO2004052825A2/fr active Application Filing
- 2003-12-05 MX MXPA05005962A patent/MXPA05005962A/es unknown
- 2003-12-05 EP EP03796169A patent/EP1569891A2/fr not_active Withdrawn
- 2003-12-05 US US10/537,422 patent/US20060041165A1/en not_active Abandoned
- 2003-12-05 CA CA002508125A patent/CA2508125A1/fr not_active Abandoned
- 2003-12-05 AU AU2003298421A patent/AU2003298421B2/en not_active Ceased
- 2003-12-05 BR BR0317047-0A patent/BR0317047A/pt not_active IP Right Cessation
- 2003-12-05 JP JP2004558173A patent/JP2006509024A/ja active Pending
- 2003-12-05 KR KR1020057010224A patent/KR100762773B1/ko not_active IP Right Cessation
- 2003-12-05 CN CNA2003801049176A patent/CN1720215A/zh active Pending
Also Published As
Publication number | Publication date |
---|---|
FR2848209B1 (fr) | 2006-10-13 |
FR2848209A1 (fr) | 2004-06-11 |
US20060041165A1 (en) | 2006-02-23 |
CN1720215A (zh) | 2006-01-11 |
MXPA05005962A (es) | 2006-02-08 |
AU2003298421B2 (en) | 2008-04-24 |
WO2004052825A2 (fr) | 2004-06-24 |
CA2508125A1 (fr) | 2004-06-24 |
JP2006509024A (ja) | 2006-03-16 |
KR20050084179A (ko) | 2005-08-26 |
WO2004052825A3 (fr) | 2004-07-15 |
AU2003298421A1 (en) | 2004-06-30 |
EP1569891A2 (fr) | 2005-09-07 |
WO2004052825A8 (fr) | 2005-09-15 |
KR100762773B1 (ko) | 2007-10-04 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
B08F | Application fees: application dismissed [chapter 8.6 patent gazette] |
Free format text: REFERENTE AS 7A E 8A ANUIDADES. |
|
B08K | Patent lapsed as no evidence of payment of the annual fee has been furnished to inpi [chapter 8.11 patent gazette] |
Free format text: REFERENTE AO DESPACHO 8.6 PUBLICADO NA RPI 2160 DE 29/05/2012. |