BR0317047A - Processo contìnuo de preparo de lactato de etila - Google Patents

Processo contìnuo de preparo de lactato de etila

Info

Publication number
BR0317047A
BR0317047A BR0317047-0A BR0317047A BR0317047A BR 0317047 A BR0317047 A BR 0317047A BR 0317047 A BR0317047 A BR 0317047A BR 0317047 A BR0317047 A BR 0317047A
Authority
BR
Brazil
Prior art keywords
ethyl lactate
mixture
ethanol
continuous process
lactic acid
Prior art date
Application number
BR0317047-0A
Other languages
English (en)
Inventor
Serge Tretjak
Remy Teissier
Original Assignee
Arkema
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Arkema filed Critical Arkema
Publication of BR0317047A publication Critical patent/BR0317047A/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/66—Esters of carboxylic acids having esterified carboxylic groups bound to acyclic carbon atoms and having any of the groups OH, O—metal, —CHO, keto, ether, acyloxy, groups, groups, or in the acid moiety
    • C07C69/67—Esters of carboxylic acids having esterified carboxylic groups bound to acyclic carbon atoms and having any of the groups OH, O—metal, —CHO, keto, ether, acyloxy, groups, groups, or in the acid moiety of saturated acids
    • C07C69/675—Esters of carboxylic acids having esterified carboxylic groups bound to acyclic carbon atoms and having any of the groups OH, O—metal, —CHO, keto, ether, acyloxy, groups, groups, or in the acid moiety of saturated acids of saturated hydroxy-carboxylic acids
    • C07C69/68—Lactic acid esters

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

"PROCESSO CONTìNUO DE PREPARO DE LACTATO DE ETILA". A invenção se refere a um processo contínuo de preparo de lactato de etila por esterificação de ácido láctico por meio do etanol, em presença de um catalisador que consiste em extrair em contínuo, do meio reacional de esterificação a uma taxa de conversão parcial do ácido láctico, uma mistura que compreende lactato de etila, etanol, água e diversos produtos pesados, depois de se submeter essa mistura a uma separação flash, sob pressão reduzida, da qual sai um fluxo de cabeça, compreendendo uma mistura de lactato de etila, de etanol e de água, mistura essa que alimenta, em sua parte baixa, uma coluna de destilação fracionada.
BR0317047-0A 2002-12-05 2003-12-05 Processo contìnuo de preparo de lactato de etila BR0317047A (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR0215348A FR2848209B1 (fr) 2002-12-05 2002-12-05 Procede continu de preparation de lactate d'ethyle
PCT/FR2003/003598 WO2004052825A2 (fr) 2002-12-05 2003-12-05 Procede continu de preparation de lactate d'ethyle

Publications (1)

Publication Number Publication Date
BR0317047A true BR0317047A (pt) 2005-10-25

Family

ID=32320010

Family Applications (1)

Application Number Title Priority Date Filing Date
BR0317047-0A BR0317047A (pt) 2002-12-05 2003-12-05 Processo contìnuo de preparo de lactato de etila

Country Status (11)

Country Link
US (1) US20060041165A1 (pt)
EP (1) EP1569891A2 (pt)
JP (1) JP2006509024A (pt)
KR (1) KR100762773B1 (pt)
CN (1) CN1720215A (pt)
AU (1) AU2003298421B2 (pt)
BR (1) BR0317047A (pt)
CA (1) CA2508125A1 (pt)
FR (1) FR2848209B1 (pt)
MX (1) MXPA05005962A (pt)
WO (1) WO2004052825A2 (pt)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100427453C (zh) * 2004-08-27 2008-10-22 清华大学 催化精馏法合成乳酸乙酯工艺
US20110160480A1 (en) * 2008-07-30 2011-06-30 Galactic Sa Continuous Process for Obtaining a Lactic Ester
BE1019021A3 (fr) * 2009-07-01 2012-01-10 Galactic Sa Procede de preparation de lactate d'alkyle c1-c4 de grande purete par putrification des lactates d'alkyle c1-c4 bruts.
KR101140649B1 (ko) * 2009-09-30 2012-05-03 한국화학연구원 암모늄락테이트로부터 알킬락테이트를 직접 제조하는 방법
KR101198866B1 (ko) 2010-12-02 2012-11-07 한국화학연구원 고순도 알킬락테이트 및 젖산의 회수 방법
CN102381973B (zh) * 2011-09-19 2014-01-29 南京大学 一种超高纯度（电子级）乳酸酯类产品的生产工艺
WO2013159347A1 (zh) 2012-04-27 2013-10-31 孝感市易生新材料有限公司 一种连续生产高含量和高光学纯度乳酸酯的方法
WO2015058116A1 (en) 2013-10-17 2015-04-23 Cargill, Incorporated Methods for producing alkyl hydroxyalkanoates
EP3166920A4 (en) * 2014-07-10 2018-03-07 Archer Daniels Midland Company Novel lactic acid recovery process
US10239819B2 (en) 2014-10-17 2019-03-26 Cargill, Incorporated Methods for producing an ester of an alpha, beta-unsaturated carboxylic acid
PL229904B1 (pl) 2015-01-08 2018-09-28 Wroclawskie Centrum Badan Eit Spolka Z Ograniczona Odpowiedzialnoscia Sposób otrzymywania estrów kwasu mlekowego i mleczanomlekowego w reakcji alkoholizy poliestru alifatycznego
CN104876819A (zh) * 2015-05-14 2015-09-02 安徽中草香料有限公司 一种乳酸异丙酯的制备方法
CN107032984A (zh) * 2016-02-03 2017-08-11 天津中福工程技术有限公司 一种连续催化精馏制备乳酸乙酯的方法
KR102019037B1 (ko) * 2017-05-26 2019-09-06 지에스칼텍스 주식회사 알킬 카르복실산 에스테르의 제조 방법
KR102151747B1 (ko) * 2018-11-23 2020-09-03 지에스칼텍스 주식회사 알킬 카르복실산 에스테르의 제조 방법 및 알킬 카르복실산 에스테르의 제조 장치

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2406648A (en) * 1942-12-08 1946-08-27 Sealtest Inc Process of preparing water-soluble alkyl lactates
US2465772A (en) * 1944-02-17 1949-03-29 Nat Dairy Res Lab Inc Preparation of alkyl lactates
DD206373A1 (de) * 1982-03-16 1984-01-25 Joachim Franke Verfahren und vorrichtung zur abtrennung von milchsaeure aus rohloesungen
US5210296A (en) * 1990-11-19 1993-05-11 E. I. Du Pont De Nemours And Company Recovery of lactate esters and lactic acid from fermentation broth
US5723639A (en) * 1995-10-16 1998-03-03 University Of Chicago Esterification of fermentation-derived acids via pervaporation
US6664413B1 (en) * 1998-11-19 2003-12-16 A. E. Staley Manufacturing Co. Process for production of esters

Also Published As

Publication number Publication date
WO2004052825A8 (fr) 2005-09-15
AU2003298421B2 (en) 2008-04-24
WO2004052825A3 (fr) 2004-07-15
WO2004052825A2 (fr) 2004-06-24
KR100762773B1 (ko) 2007-10-04
FR2848209A1 (fr) 2004-06-11
CA2508125A1 (fr) 2004-06-24
CN1720215A (zh) 2006-01-11
JP2006509024A (ja) 2006-03-16
US20060041165A1 (en) 2006-02-23
MXPA05005962A (es) 2006-02-08
KR20050084179A (ko) 2005-08-26
FR2848209B1 (fr) 2006-10-13
EP1569891A2 (fr) 2005-09-07
AU2003298421A1 (en) 2004-06-30

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Legal Events

Date Code Title Description
B08F Application fees: application dismissed [chapter 8.6 patent gazette]

Free format text: REFERENTE AS 7A E 8A ANUIDADES.

B08K Patent lapsed as no evidence of payment of the annual fee has been furnished to inpi [chapter 8.11 patent gazette]

Free format text: REFERENTE AO DESPACHO 8.6 PUBLICADO NA RPI 2160 DE 29/05/2012.