BG32112A3 - Метод за получаване на ортометалилоксифонол - Google Patents
Метод за получаване на ортометалилоксифонолInfo
- Publication number
- BG32112A3 BG32112A3 BG045757A BG4575779A BG32112A3 BG 32112 A3 BG32112 A3 BG 32112A3 BG 045757 A BG045757 A BG 045757A BG 4575779 A BG4575779 A BG 4575779A BG 32112 A3 BG32112 A3 BG 32112A3
- Authority
- BG
- Bulgaria
- Prior art keywords
- zone
- pyrocatechin
- ortometalyl
- oxyphenol
- obtaining
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 2
- 229930195143 oxyphenol Natural products 0.000 title 1
- OHXAOPZTJOUYKM-UHFFFAOYSA-N 3-Chloro-2-methylpropene Chemical compound CC(=C)CCl OHXAOPZTJOUYKM-UHFFFAOYSA-N 0.000 abstract 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 3
- YCIMNLLNPGFGHC-UHFFFAOYSA-N catechol Chemical compound OC1=CC=CC=C1O YCIMNLLNPGFGHC-UHFFFAOYSA-N 0.000 abstract 3
- RDOXTESZEPMUJZ-UHFFFAOYSA-N anisole Chemical compound COC1=CC=CC=C1 RDOXTESZEPMUJZ-UHFFFAOYSA-N 0.000 abstract 2
- 239000007788 liquid Substances 0.000 abstract 2
- 239000007791 liquid phase Substances 0.000 abstract 2
- NHGXDBSUJJNIRV-UHFFFAOYSA-M tetrabutylammonium chloride Chemical compound [Cl-].CCCC[N+](CCCC)(CCCC)CCCC NHGXDBSUJJNIRV-UHFFFAOYSA-M 0.000 abstract 2
- 239000003153 chemical reaction reagent Substances 0.000 abstract 1
- UZKWTJUDCOPSNM-UHFFFAOYSA-N methoxybenzene Substances CCCCOC=C UZKWTJUDCOPSNM-UHFFFAOYSA-N 0.000 abstract 1
- 239000012074 organic phase Substances 0.000 abstract 1
- 239000012071 phase Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
- C07C41/01—Preparation of ethers
- C07C41/16—Preparation of ethers by reaction of esters of mineral or organic acids with hydroxy or O-metal groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Measurement Of Radiation (AREA)
- Picture Signal Circuits (AREA)
- Transforming Electric Information Into Light Information (AREA)
Abstract
Метод за получаване на ортометалилоксифенол от пирокатехин и металилхлорид, характеризиращ се с това, че в първа зона се намира течна среда, образувана от две течни фази, едната органична, другата водна, които две фази се смесват една с друга и течната среда се получава чрез смесване на пирокатехин, металилхлорид, анизол, тетрабутиламониев хлорид и натриева основа, като температурата на първата зона е от 15 до 30'с, общата концентрация на реагентите е от 22 до 41% и съотношението на металилхлорида към пирокатехина е от 0,6 до 2,22 см3/г, като органична фаза се отделя от течната фаза в първата зона и втората зона се загрява до температура от 90 до 100'с. Патентните претенции са формулирани в 1 точка
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7834297A FR2442822A1 (fr) | 1978-11-30 | 1978-11-30 | Procede de preparation d'ethers insatures |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BG32112A3 true BG32112A3 (bg) | 1982-05-14 |
Family
ID=9215726
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BG045757A BG32112A3 (bg) | 1978-11-30 | 1979-11-30 | Метод за получаване на ортометалилоксифонол |
Country Status (20)
| Country | Link |
|---|---|
| US (1) | US4263462A (bg) |
| EP (1) | EP0013250B1 (bg) |
| JP (1) | JPS5576833A (bg) |
| AT (1) | ATE6632T1 (bg) |
| BG (1) | BG32112A3 (bg) |
| BR (1) | BR7907798A (bg) |
| CA (1) | CA1148978A (bg) |
| DD (1) | DD147536A5 (bg) |
| DE (1) | DE2966807D1 (bg) |
| DK (1) | DK171294B1 (bg) |
| ES (1) | ES8100239A1 (bg) |
| FR (1) | FR2442822A1 (bg) |
| GB (1) | GB2035322B (bg) |
| IE (1) | IE49216B1 (bg) |
| IL (1) | IL58662A (bg) |
| PL (1) | PL126599B1 (bg) |
| PT (1) | PT70524A (bg) |
| RO (1) | RO79087A (bg) |
| SU (1) | SU934907A3 (bg) |
| YU (1) | YU41353B (bg) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4465868A (en) * | 1981-07-17 | 1984-08-14 | Otsuka Kagaku Yakuhin Kabushiki Kaisha | Process for preparing o-methallyloxyphenol |
| US4613703A (en) * | 1982-04-05 | 1986-09-23 | The Dow Chemical Company | Process for allylating hydroxyaromatic compounds |
| IT1151718B (it) * | 1982-04-19 | 1986-12-24 | Brichima Spa | Procedimento per la preparazione del 2,3-diidro-2,2-dimetilbenzofuran-7-olo |
| IT1196002B (it) * | 1984-01-20 | 1988-11-10 | Brichima Spa | Procedimento per la sintesi di o-isopropossifenolo |
| JPH01503541A (ja) * | 1987-06-01 | 1989-11-30 | ザ ダウ ケミカル カンパニー | ヒドロキシ芳香族化合物のプロパルギルエーテルの製造方法 |
| US4982012A (en) * | 1987-12-18 | 1991-01-01 | Fmc Corporation | Two phase process for preparing 2-methallyloxyphenol from catechol |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2378698A (en) * | 1943-05-01 | 1945-06-19 | Goodrich Co B F | Partial ethers of alkenyl substituted polyhydroxybenzenes |
| GB1227144A (bg) * | 1967-04-05 | 1971-04-07 | ||
| US3927118A (en) * | 1973-12-21 | 1975-12-16 | Crown Zellerbach Corp | Process for monoetherification of polyhydric benzenes |
-
1978
- 1978-11-30 FR FR7834297A patent/FR2442822A1/fr active Granted
-
1979
- 1979-11-07 US US06/092,415 patent/US4263462A/en not_active Expired - Lifetime
- 1979-11-07 IL IL58662A patent/IL58662A/xx unknown
- 1979-11-13 ES ES485895A patent/ES8100239A1/es not_active Expired
- 1979-11-23 IE IE2248/79A patent/IE49216B1/en not_active IP Right Cessation
- 1979-11-23 GB GB7940667A patent/GB2035322B/en not_active Expired
- 1979-11-23 CA CA000340551A patent/CA1148978A/en not_active Expired
- 1979-11-26 YU YU2891/79A patent/YU41353B/xx unknown
- 1979-11-28 EP EP79420063A patent/EP0013250B1/fr not_active Expired
- 1979-11-28 DE DE7979420063T patent/DE2966807D1/de not_active Expired
- 1979-11-28 AT AT79420063T patent/ATE6632T1/de not_active IP Right Cessation
- 1979-11-29 RO RO7999393A patent/RO79087A/ro unknown
- 1979-11-29 PT PT70524A patent/PT70524A/pt not_active IP Right Cessation
- 1979-11-29 SU SU792847446A patent/SU934907A3/ru active
- 1979-11-29 JP JP15493579A patent/JPS5576833A/ja active Granted
- 1979-11-29 DK DK507279A patent/DK171294B1/da not_active IP Right Cessation
- 1979-11-29 PL PL1979219995A patent/PL126599B1/pl unknown
- 1979-11-30 BR BR7907798A patent/BR7907798A/pt not_active IP Right Cessation
- 1979-11-30 DD DD79217283A patent/DD147536A5/de not_active IP Right Cessation
- 1979-11-30 BG BG045757A patent/BG32112A3/bg unknown
Also Published As
| Publication number | Publication date |
|---|---|
| SU934907A3 (ru) | 1982-06-07 |
| CA1148978A (en) | 1983-06-28 |
| ES485895A0 (es) | 1980-05-16 |
| IL58662A (en) | 1983-10-31 |
| GB2035322A (en) | 1980-06-18 |
| FR2442822A1 (fr) | 1980-06-27 |
| EP0013250B1 (fr) | 1984-03-14 |
| DK507279A (da) | 1980-05-31 |
| PL219995A1 (bg) | 1980-08-25 |
| JPS6223730B2 (bg) | 1987-05-25 |
| DE2966807D1 (en) | 1984-04-19 |
| BR7907798A (pt) | 1980-08-26 |
| FR2442822B1 (bg) | 1981-06-12 |
| RO79087A (ro) | 1982-10-26 |
| IE792248L (en) | 1980-05-30 |
| IL58662A0 (en) | 1980-02-29 |
| JPS5576833A (en) | 1980-06-10 |
| DK171294B1 (da) | 1996-08-26 |
| IE49216B1 (en) | 1985-08-21 |
| PT70524A (fr) | 1979-12-01 |
| EP0013250A1 (fr) | 1980-07-09 |
| YU289179A (en) | 1982-08-31 |
| YU41353B (en) | 1987-02-28 |
| ATE6632T1 (de) | 1984-03-15 |
| PL126599B1 (en) | 1983-08-31 |
| GB2035322B (en) | 1983-03-09 |
| US4263462A (en) | 1981-04-21 |
| ES8100239A1 (es) | 1980-05-16 |
| DD147536A5 (de) | 1981-04-08 |
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