BE781567A - Procede de preparation en continu d'acide terephtalique de haute puret - Google Patents
Procede de preparation en continu d'acide terephtalique de haute puretInfo
- Publication number
- BE781567A BE781567A BE781567A BE781567A BE781567A BE 781567 A BE781567 A BE 781567A BE 781567 A BE781567 A BE 781567A BE 781567 A BE781567 A BE 781567A BE 781567 A BE781567 A BE 781567A
- Authority
- BE
- Belgium
- Prior art keywords
- puret
- preparation
- terephthalic acid
- continuous process
- continuous
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/02—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
- C08G63/12—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from polycarboxylic acids and polyhydroxy compounds
- C08G63/40—Polyesters derived from ester-forming derivatives of polycarboxylic acids or of polyhydroxy compounds, other than from esters thereof
- C08G63/42—Cyclic ethers; Cyclic carbonates; Cyclic sulfites; Cyclic orthoesters
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
- B01J19/1862—Stationary reactors having moving elements inside placed in series
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
- C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
- C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
- C07C51/265—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/487—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/02—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
- C08G63/12—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from polycarboxylic acids and polyhydroxy compounds
- C08G63/16—Dicarboxylic acids and dihydroxy compounds
- C08G63/18—Dicarboxylic acids and dihydroxy compounds the acids or hydroxy compounds containing carbocyclic rings
- C08G63/181—Acids containing aromatic rings
- C08G63/183—Terephthalic acids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00054—Controlling or regulating the heat exchange system
- B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
- B01J2219/00067—Liquid level measurement
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00101—Reflux columns
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00182—Controlling or regulating processes controlling the level of reactants in the reactor vessel
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2042571A JPS5518698B1 (it) | 1971-04-03 | 1971-04-03 |
Publications (1)
Publication Number | Publication Date |
---|---|
BE781567A true BE781567A (fr) | 1972-07-17 |
Family
ID=12026669
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BE781567A BE781567A (fr) | 1971-04-03 | 1972-03-31 | Procede de preparation en continu d'acide terephtalique de haute puret |
Country Status (7)
Country | Link |
---|---|
US (1) | US3859344A (it) |
JP (1) | JPS5518698B1 (it) |
BE (1) | BE781567A (it) |
FR (1) | FR2132363B1 (it) |
GB (1) | GB1350874A (it) |
IT (1) | IT952505B (it) |
NL (1) | NL7204330A (it) |
Families Citing this family (23)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4208352A (en) * | 1975-12-15 | 1980-06-17 | Phillips Petroleum Company | Oxidation process for alkylaromatics |
JPS5278846A (en) * | 1975-12-25 | 1977-07-02 | Matsuyama Sekyu Kagaku Kk | Continuous production of high purity telephthalic acid |
US4185073A (en) * | 1976-07-26 | 1980-01-22 | Standard Oil Company (Indiana) | Apparatus for iso- or terephthalic acid production in and recovery from benzoic acid-water solvent system |
US4081464A (en) * | 1976-07-26 | 1978-03-28 | Standard Oil Company | Iso- or terephthalic acid production in and recovery from benzoic acid-water solvent system |
DE2714985C2 (de) * | 1977-04-04 | 1982-05-06 | Chemische Werke Hüls AG, 4370 Marl | Verfahren zur Reinigung von Terephthalsäure |
JPS5555138A (en) * | 1978-10-19 | 1980-04-22 | Mitsubishi Chem Ind Ltd | Preparation of highly pure terephthalic acid |
DE3063298D1 (en) | 1979-07-02 | 1983-07-07 | Ici Plc | Process for the preparation of terephthalic acid |
US4550198A (en) * | 1982-11-04 | 1985-10-29 | Georgia Tech Research Institute | Purification of terephthalic acid by supercritical fluid extraction |
JPS59104345A (ja) * | 1982-12-03 | 1984-06-16 | Kuraray Yuka Kk | 直接重合用に適したテレフタル酸の製造方法 |
US5030749A (en) * | 1985-12-04 | 1991-07-09 | Amoco Corporation | Method for producing purified trimesic acid |
US5132450A (en) * | 1990-06-25 | 1992-07-21 | Mitsubishi Gas Chemical Company, Inc. | Process for producing high purity isophthalic acid |
KR970000136B1 (ko) * | 1993-09-28 | 1997-01-04 | 브이.피. 유리예프 | 고순도 벤젠디카르복실산 이성질체의 제조방법 |
US6013835A (en) * | 1995-06-07 | 2000-01-11 | Hfm International, Inc. | Method and apparatus for preparing purified terephthalic acid |
US5767311A (en) * | 1995-06-07 | 1998-06-16 | Glitsch International, Inc. | Method and apparatus for preparing purified terephtalic acid |
US5929274A (en) * | 1995-06-07 | 1999-07-27 | Hfm International, Inc. | Method to reduce carboxybenzaldehyde isomers in terephthalic acid or isophthalic acid |
US6054610A (en) * | 1995-06-07 | 2000-04-25 | Hfm International, Inc. | Method and apparatus for preparing purified terephthalic acid and isophthalic acid from mixed xylenes |
US6527018B2 (en) * | 2000-06-07 | 2003-03-04 | Fuji Photo Film Co., Ltd. | Method and system for optimizing batch process of preparing solution |
KR20060038405A (ko) * | 2003-07-02 | 2006-05-03 | 이 아이 듀폰 디 네모아 앤드 캄파니 | 가압된 고온 중합 방법 |
US7615663B2 (en) * | 2004-09-02 | 2009-11-10 | Eastman Chemical Company | Optimized production of aromatic dicarboxylic acids |
EP1777001A1 (en) * | 2005-10-21 | 2007-04-25 | Saudi Basic Industries Corporation | Bubble column reactor with level measuring device and method for level measurement therein |
CN110944972A (zh) * | 2017-06-29 | 2020-03-31 | Bp北美公司 | 制造芳族羧酸的方法 |
CN108484888A (zh) * | 2018-01-23 | 2018-09-04 | 浙江省现代纺织工业研究院 | 一种无机改性对二甲苯的制备方法 |
CN114053978A (zh) * | 2021-11-25 | 2022-02-18 | 上海师范大学 | 一种含金属废料提纯装置 |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3064044A (en) * | 1957-08-15 | 1962-11-13 | Standard Oil Co | Multistage oxidation system for preparing dicarboxylic acid |
US3170768A (en) * | 1959-04-22 | 1965-02-23 | Standard Oil Co | System for continuous preparation of terephthalic acid |
FR1272209A (fr) * | 1960-10-14 | 1961-09-22 | Standard Oil Co | Perfectionnements apportés à la production en continu d'acides carboxyliques par oxydation |
FR1504431A (fr) * | 1965-11-09 | 1967-12-08 | Inst Francais Du Petrole | Procédé d'oxydation du paraxylène en deux étapes |
-
1971
- 1971-04-03 JP JP2042571A patent/JPS5518698B1/ja active Pending
-
1972
- 1972-03-30 GB GB1523672A patent/GB1350874A/en not_active Expired
- 1972-03-30 NL NL7204330A patent/NL7204330A/xx not_active Application Discontinuation
- 1972-03-31 FR FR7211596A patent/FR2132363B1/fr not_active Expired
- 1972-03-31 IT IT49397/72A patent/IT952505B/it active
- 1972-03-31 BE BE781567A patent/BE781567A/xx unknown
- 1972-04-03 US US240520A patent/US3859344A/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
FR2132363B1 (it) | 1977-04-01 |
IT952505B (it) | 1973-07-30 |
FR2132363A1 (it) | 1972-11-17 |
GB1350874A (en) | 1974-04-24 |
NL7204330A (it) | 1972-10-05 |
JPS5518698B1 (it) | 1980-05-21 |
DE2216208A1 (de) | 1972-10-26 |
DE2216208B2 (de) | 1977-02-10 |
US3859344A (en) | 1975-01-07 |
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