BE563320A - - Google Patents
Info
- Publication number
- BE563320A BE563320A BE563320DA BE563320A BE 563320 A BE563320 A BE 563320A BE 563320D A BE563320D A BE 563320DA BE 563320 A BE563320 A BE 563320A
- Authority
- BE
- Belgium
- Prior art keywords
- dextrose
- sep
- liquor
- starch
- mother liquor
- Prior art date
Links
- 239000008121 dextrose Substances 0.000 claims description 79
- 229920002472 Starch Polymers 0.000 claims description 69
- 235000019698 starch Nutrition 0.000 claims description 69
- 239000008107 starch Substances 0.000 claims description 66
- 108090000790 Enzymes Proteins 0.000 claims description 46
- 102000004190 Enzymes Human genes 0.000 claims description 46
- 238000000034 method Methods 0.000 claims description 45
- 239000012452 mother liquor Substances 0.000 claims description 44
- 229940088598 Enzyme Drugs 0.000 claims description 36
- 239000006188 syrup Substances 0.000 claims description 24
- 235000020357 syrup Nutrition 0.000 claims description 24
- 238000002425 crystallisation Methods 0.000 claims description 20
- 230000005712 crystallization Effects 0.000 claims description 20
- 238000006243 chemical reaction Methods 0.000 claims description 17
- 239000012535 impurity Substances 0.000 claims description 17
- 239000003456 ion exchange resin Substances 0.000 claims description 16
- 229920003303 ion-exchange polymer Polymers 0.000 claims description 16
- 108010073178 Glucan 1,4-alpha-Glucosidase Proteins 0.000 claims description 15
- 239000002253 acid Substances 0.000 claims description 14
- 229920002245 Dextrose equivalent Polymers 0.000 claims description 13
- 239000000203 mixture Substances 0.000 claims description 13
- 239000007787 solid Substances 0.000 claims description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 12
- 125000004122 cyclic group Chemical group 0.000 claims description 8
- 235000019749 Dry matter Nutrition 0.000 claims description 6
- 239000003463 adsorbent Substances 0.000 claims description 6
- 102000004139 alpha-Amylases Human genes 0.000 claims description 4
- 108090000637 alpha-Amylases Proteins 0.000 claims description 4
- 229940024171 alpha-amylase Drugs 0.000 claims description 4
- 229910052500 inorganic mineral Inorganic materials 0.000 claims description 4
- 239000011707 mineral Substances 0.000 claims description 4
- 241000228245 Aspergillus niger Species 0.000 claims description 3
- 241000233866 Fungi Species 0.000 claims description 3
- 238000011081 inoculation Methods 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 241000228251 Aspergillus phoenicis Species 0.000 claims description 2
- 229920001098 polystyrene-block-poly(ethylene/propylene) Polymers 0.000 description 132
- WQZGKKKJIJFFOK-VFUOTHLCSA-N β-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 71
- 229960001031 Glucose Drugs 0.000 description 70
- 239000000047 product Substances 0.000 description 19
- 239000011780 sodium chloride Substances 0.000 description 17
- 150000003839 salts Chemical class 0.000 description 16
- 238000007670 refining Methods 0.000 description 14
- 229920001888 polyacrylic acid Polymers 0.000 description 13
- 238000004519 manufacturing process Methods 0.000 description 10
- VEXZGXHMUGYJMC-UHFFFAOYSA-N HCl Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 8
- 239000011347 resin Substances 0.000 description 8
- 229920005989 resin Polymers 0.000 description 8
- 238000009825 accumulation Methods 0.000 description 6
- 150000001720 carbohydrates Chemical class 0.000 description 6
- 235000014633 carbohydrates Nutrition 0.000 description 6
- OKTJSMMVPCPJKN-UHFFFAOYSA-N carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 6
- 239000000706 filtrate Substances 0.000 description 6
- WSFSSNUMVMOOMR-UHFFFAOYSA-N formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 6
- 239000002994 raw material Substances 0.000 description 6
- SPFMQWBKVUQXJV-BTVCFUMJSA-N (2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanal;hydrate Chemical compound O.OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C=O SPFMQWBKVUQXJV-BTVCFUMJSA-N 0.000 description 5
- 230000015572 biosynthetic process Effects 0.000 description 5
- 239000003795 chemical substances by application Substances 0.000 description 5
- 238000006460 hydrolysis reaction Methods 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- 240000005020 Acaciella glauca Species 0.000 description 4
- 239000003957 anion exchange resin Substances 0.000 description 4
- 239000003729 cation exchange resin Substances 0.000 description 4
- 238000001311 chemical methods and process Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 238000002360 preparation method Methods 0.000 description 4
- 235000003499 redwood Nutrition 0.000 description 4
- 238000005406 washing Methods 0.000 description 4
- 229940077731 Carbohydrate nutrients Drugs 0.000 description 3
- 229920002261 Corn starch Polymers 0.000 description 3
- 239000006227 byproduct Substances 0.000 description 3
- -1 i.e. Proteins 0.000 description 3
- 238000010899 nucleation Methods 0.000 description 3
- 229920000642 polymer Polymers 0.000 description 3
- LSNNMFCWUKXFEE-UHFFFAOYSA-N sulfonic acid Chemical compound OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 description 3
- 238000003786 synthesis reaction Methods 0.000 description 3
- 230000002194 synthesizing Effects 0.000 description 3
- MYRTYDVEIRVNKP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene Chemical compound C=CC1=CC=CC=C1C=C MYRTYDVEIRVNKP-UHFFFAOYSA-N 0.000 description 2
- HUMNYLRZRPPJDN-UHFFFAOYSA-N Benzaldehyde Chemical compound O=CC1=CC=CC=C1 HUMNYLRZRPPJDN-UHFFFAOYSA-N 0.000 description 2
- 210000000988 Bone and Bones Anatomy 0.000 description 2
- 229920001353 Dextrin Polymers 0.000 description 2
- 239000004375 Dextrin Substances 0.000 description 2
- GUBGYTABKSRVRQ-YOLKTULGSA-N Maltose Natural products O([C@@H]1[C@H](O)[C@@H](O)[C@H](O)O[C@H]1CO)[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 GUBGYTABKSRVRQ-YOLKTULGSA-N 0.000 description 2
- 240000007594 Oryza sativa Species 0.000 description 2
- 235000007164 Oryza sativa Nutrition 0.000 description 2
- GHMLBKRAJCXXBS-UHFFFAOYSA-N Resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 description 2
- 240000001016 Solanum tuberosum Species 0.000 description 2
- 235000002595 Solanum tuberosum Nutrition 0.000 description 2
- 240000006394 Sorghum bicolor Species 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 240000008529 Triticum aestivum Species 0.000 description 2
- 238000005903 acid hydrolysis reaction Methods 0.000 description 2
- 150000001299 aldehydes Chemical class 0.000 description 2
- 150000001412 amines Chemical class 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 229940023913 cation exchange resins Drugs 0.000 description 2
- 239000003086 colorant Substances 0.000 description 2
- 238000004040 coloring Methods 0.000 description 2
- 229920001577 copolymer Polymers 0.000 description 2
- 239000008120 corn starch Substances 0.000 description 2
- 238000005115 demineralization Methods 0.000 description 2
- 230000002328 demineralizing Effects 0.000 description 2
- 230000001627 detrimental Effects 0.000 description 2
- 235000019425 dextrin Nutrition 0.000 description 2
- 229960000673 dextrose monohydrate Drugs 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 238000005755 formation reaction Methods 0.000 description 2
- 239000012458 free base Substances 0.000 description 2
- 239000000543 intermediate Substances 0.000 description 2
- 150000004682 monohydrates Chemical class 0.000 description 2
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 2
- 235000012015 potatoes Nutrition 0.000 description 2
- 238000004064 recycling Methods 0.000 description 2
- 235000009566 rice Nutrition 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L sodium carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- PPBRXRYQALVLMV-UHFFFAOYSA-N styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
- 235000000346 sugar Nutrition 0.000 description 2
- 150000008163 sugars Chemical class 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- 235000021307 wheat Nutrition 0.000 description 2
- 101700023572 AGL Proteins 0.000 description 1
- 206010067484 Adverse reaction Diseases 0.000 description 1
- 229940089206 Anhydrous Dextrose Drugs 0.000 description 1
- 241000228212 Aspergillus Species 0.000 description 1
- 101710012512 CPM1 Proteins 0.000 description 1
- 241000193403 Clostridium Species 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 229940018564 M-PHENYLENEDIAMINE Drugs 0.000 description 1
- WZCQRUWWHSTZEM-UHFFFAOYSA-N M-Phenylenediamine Chemical compound NC1=CC=CC(N)=C1 WZCQRUWWHSTZEM-UHFFFAOYSA-N 0.000 description 1
- 101700010794 MAL12 Proteins 0.000 description 1
- 101700025925 MAL32 Proteins 0.000 description 1
- 101700012066 MAL62 Proteins 0.000 description 1
- 101710026950 MGAM Proteins 0.000 description 1
- 102100008175 MGAM Human genes 0.000 description 1
- 235000019759 Maize starch Nutrition 0.000 description 1
- 101710011129 Mal-B1 Proteins 0.000 description 1
- 240000003183 Manihot esculenta Species 0.000 description 1
- 235000016735 Manihot esculenta subsp esculenta Nutrition 0.000 description 1
- 229920000881 Modified starch Polymers 0.000 description 1
- 241000235395 Mucor Species 0.000 description 1
- 241000235527 Rhizopus Species 0.000 description 1
- 235000011684 Sorghum saccharatum Nutrition 0.000 description 1
- 240000008042 Zea mays Species 0.000 description 1
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 1
- 239000003377 acid catalyst Substances 0.000 description 1
- 230000002378 acidificating Effects 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 238000007792 addition Methods 0.000 description 1
- 101700023638 aglA Proteins 0.000 description 1
- 238000005349 anion exchange Methods 0.000 description 1
- 150000004982 aromatic amines Chemical class 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 229940095076 benzaldehyde Drugs 0.000 description 1
- 235000019658 bitter taste Nutrition 0.000 description 1
- 238000004061 bleaching Methods 0.000 description 1
- 230000024881 catalytic activity Effects 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000003776 cleavage reaction Methods 0.000 description 1
- 235000005822 corn Nutrition 0.000 description 1
- 235000005824 corn Nutrition 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 230000002939 deleterious Effects 0.000 description 1
- 229940079919 digestives Enzyme preparations Drugs 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000002349 favourable Effects 0.000 description 1
- 238000005243 fluidization Methods 0.000 description 1
- 238000003306 harvesting Methods 0.000 description 1
- 230000003301 hydrolyzing Effects 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 238000011068 load Methods 0.000 description 1
- 101700009216 malA Proteins 0.000 description 1
- RXVWSYJTUUKTEA-CGQAXDJHSA-N maltotriose Chemical compound O[C@@H]1[C@@H](O)[C@@H](O[C@H]([C@H](O)CO)[C@H](O)[C@@H](O)C=O)O[C@H](CO)[C@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 RXVWSYJTUUKTEA-CGQAXDJHSA-N 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 235000019713 millet Nutrition 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000006011 modification reaction Methods 0.000 description 1
- 235000019426 modified starch Nutrition 0.000 description 1
- 230000001264 neutralization Effects 0.000 description 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 1
- 238000006396 nitration reaction Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 235000011837 pasties Nutrition 0.000 description 1
- 229920000768 polyamine Polymers 0.000 description 1
- 230000002035 prolonged Effects 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 235000019643 salty taste Nutrition 0.000 description 1
- 239000001187 sodium carbonate Substances 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 229920001059 synthetic polymer Polymers 0.000 description 1
- 235000019640 taste Nutrition 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P19/00—Preparation of compounds containing saccharide radicals
- C12P19/20—Preparation of compounds containing saccharide radicals produced by the action of an exo-1,4 alpha-glucosidase, e.g. dextrose
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P19/00—Preparation of compounds containing saccharide radicals
- C12P19/14—Preparation of compounds containing saccharide radicals produced by the action of a carbohydrase (EC 3.2.x), e.g. by alpha-amylase, e.g. by cellulase, hemicellulase
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K1/00—Glucose; Glucose-containing syrups
- C13K1/06—Glucose; Glucose-containing syrups obtained by saccharification of starch or raw materials containing starch
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Zoology (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- General Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Microbiology (AREA)
- General Chemical & Material Sciences (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Genetics & Genomics (AREA)
- Emergency Medicine (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BE563320A true BE563320A (de) |
Family
ID=184606
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BE563320D BE563320A (de) |
Country Status (1)
| Country | Link |
|---|---|
| BE (1) | BE563320A (de) |
-
0
- BE BE563320D patent/BE563320A/fr unknown
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US5177008A (en) | Process for manufacturing ethanol and for recovering glycerol, succinic acid, lactic acid, betaine, potassium sulfate, and free flowing distiller's dry grain and solubles or a solid fertilizer therefrom | |
| FI96122B (fi) | Menetelmä etanolin valmistamiseksi ja glyserolin talteenottamiseksi sivutuotteena | |
| EP0421882B1 (de) | Verfahren zur Gewinnung von Xylit und an Xylit reichen Produkten | |
| US3039935A (en) | Production of crystalline glucose | |
| JP2016520093A (ja) | 前処理ありのフェルラ酸の最適化抽出方法 | |
| CN105821095A (zh) | 葡萄糖结晶的优化方法 | |
| US4168988A (en) | Process for the winning of xylose by hydrolysis of residues of annuals | |
| CA2248439C (fr) | Procede de fabrication d'un sirop riche en maltose | |
| US5112407A (en) | Process to prepare maltose powder | |
| WO2024119730A1 (zh) | 利用玉米芯联产优级木糖和高端焦糖色素的系统及方法 | |
| JP2000308499A (ja) | 高いデキストロース含有量を有するデンプン加水分解物の生産法 | |
| FR2559490A1 (fr) | Procede de production d'oligoglucosylfructosides tres purs | |
| BE563320A (de) | ||
| JP2024507514A (ja) | キシリトール発酵液の精製システム及びその方法 | |
| EP1041161B1 (de) | Vefahren zur Herstellung von hochreiner alphakristalliner wasserfreier Dextrose | |
| CA2145411C (fr) | Compositions liquides visqueuses de xylitol et leur procede de preparation | |
| CN112479813A (zh) | 一种木糖醇的生产工艺 | |
| US4888060A (en) | Enrichment of fructose syrups | |
| JPH01312997A (ja) | 加水分解によってとうもろこし粒外皮から選択された単糖類を製造するためのコンビネーション方法 | |
| CN117701782A (zh) | 一种用竹材制备木糖的方法 | |
| BE834292R (fr) | Hydrolyse enzymatique de l'amidon granulaire | |
| CN112626281A (zh) | 一种利用木糖二蒸液生产木糖醇及联产l-阿拉伯糖的方法 | |
| EP0237442A2 (de) | Verfahren zur Herstellung von kristallisierter Dextrose aus Saccharose und Vorrichtungen für deren Herstellung | |
| HU210627B (en) | Process for manufacturing glycerol and betaine | |
| RU2015165C1 (ru) | Способ выделения глицерина и сопутствующих продуктов при производстве этанола |