BE511437A - - Google Patents
Info
- Publication number
- BE511437A BE511437A BE511437DA BE511437A BE 511437 A BE511437 A BE 511437A BE 511437D A BE511437D A BE 511437DA BE 511437 A BE511437 A BE 511437A
- Authority
- BE
- Belgium
- Prior art keywords
- acid
- nitrile
- formaldehyde
- acrylic acid
- hydrochloric acid
- Prior art date
Links
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 12
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims description 10
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 6
- 238000000034 method Methods 0.000 claims description 6
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 239000003054 catalyst Substances 0.000 claims description 3
- 238000006243 chemical reaction Methods 0.000 claims description 3
- AWKUJKPNTJGGJP-UHFFFAOYSA-N 2,2-dichlorobut-3-enamide Chemical compound C=CC(C(=O)N)(Cl)Cl AWKUJKPNTJGGJP-UHFFFAOYSA-N 0.000 claims description 2
- YZYDPPZYDIRSJT-UHFFFAOYSA-K boron phosphate Chemical compound [B+3].[O-]P([O-])([O-])=O YZYDPPZYDIRSJT-UHFFFAOYSA-K 0.000 claims description 2
- 229910000149 boron phosphate Inorganic materials 0.000 claims description 2
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 claims description 2
- -1 nitrile derivatives of acrylic acid Chemical class 0.000 claims description 2
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 claims description 2
- 238000006467 substitution reaction Methods 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims 1
- 125000002560 nitrile group Chemical group 0.000 claims 1
- 150000002825 nitriles Chemical class 0.000 description 8
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- SZTBMYHIYNGYIA-UHFFFAOYSA-N 2-chloroacrylic acid Chemical compound OC(=O)C(Cl)=C SZTBMYHIYNGYIA-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 150000001408 amides Chemical class 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- RZKHESYDFDVNRS-UHFFFAOYSA-N 2,2-dichlorobut-3-enoic acid Chemical compound OC(=O)C(Cl)(Cl)C=C RZKHESYDFDVNRS-UHFFFAOYSA-N 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- LDHQCZJRKDOVOX-NSCUHMNNSA-N crotonic acid Chemical compound C\C=C\C(O)=O LDHQCZJRKDOVOX-NSCUHMNNSA-N 0.000 description 1
- 239000012043 crude product Substances 0.000 description 1
- 150000004985 diamines Chemical class 0.000 description 1
- 239000008098 formaldehyde solution Substances 0.000 description 1
- 239000013067 intermediate product Substances 0.000 description 1
- HZVOZRGWRWCICA-UHFFFAOYSA-N methanediyl Chemical class [CH2] HZVOZRGWRWCICA-UHFFFAOYSA-N 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- NNFCIKHAZHQZJG-UHFFFAOYSA-N potassium cyanide Chemical compound [K+].N#[C-] NNFCIKHAZHQZJG-UHFFFAOYSA-N 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- LDHQCZJRKDOVOX-UHFFFAOYSA-N trans-crotonic acid Natural products CC=CC(O)=O LDHQCZJRKDOVOX-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C231/00—Preparation of carboxylic acid amides
- C07C231/06—Preparation of carboxylic acid amides from nitriles by transformation of cyano groups into carboxamide groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BE511437A true BE511437A (show.php) |
Family
ID=150209
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BE511437D BE511437A (show.php) |
Country Status (1)
| Country | Link |
|---|---|
| BE (1) | BE511437A (show.php) |
-
0
- BE BE511437D patent/BE511437A/fr unknown
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Markó et al. | Radical mediated oxidations in organic chemistry. 3. An efficient and versatile transformation of aldehydes into amides¥. | |
| Thompson | The diacylation of amides by acyl chloride—pyridine compounds | |
| Mitchell et al. | Intermediates in the synthesis of orotic acid from oxalacetic ester and urea | |
| BE511437A (show.php) | ||
| JPS58126826A (ja) | 純粋なネオヘキサノ−ルの製造方法 | |
| Konev et al. | Fluoroaziridines as novel substrates in the modified Petasis reaction: synthesis of monofluorinated propargyl amines | |
| Walton et al. | An efficient, simple synthesis of 4-azidobenzaldehyde | |
| FR2553761A1 (fr) | Procede continu pour la preparation de bisfluoroxydifluoromethane | |
| CA1247634A (en) | Process for preparing aromatic bromine compounds | |
| US3019264A (en) | 2-(2, 2, 3-trimethylcyclobutyl)-hepta-2, 4-dien-6-one | |
| JPS61229852A (ja) | １−メチル−５−ヒドロキシピラゾ−ルの製造法 | |
| FR2549039A1 (fr) | Procede de preparation de 3,3,3-trifluoro-2-trifluoro-mehylpropene | |
| Stack et al. | Formation of a new bis-organocopper reagent from the reaction of 2, 3-dichloropropene and highly active zero valent copper derived from a CuCN· 2LiCl complex | |
| US3448139A (en) | Process for the preparation of gamma-(nitrophenyl)butyronitriles | |
| HU213374B (en) | Process for producing 4-amino-5-hexenoic acid | |
| FR2602766A1 (fr) | Composes dichlorotrifluoromethylnitrotoluenes et procede de preparation d'aminotrifluoromethyltoluenes a partir de ces composes | |
| US4588837A (en) | Process for the preparation of fluorocarboxylic acids | |
| Hashimoto et al. | Nitriles. II. Synthesis of. beta.,. beta.-dichloroacrylonitrile and its reactions with some nucleophilic reagents | |
| US3322816A (en) | Process for preparing dicyanoacetylene | |
| US3019263A (en) | Process for preparing 1-acetyl-2, 2, 3-trimethylcyclobutane | |
| BE817776Q (fr) | Nouveaux derives de 5-phenyl-tetrazoles | |
| IL123990A (en) | Process for the preparation of 3-bromoanizole from nitrobenzene | |
| US3338968A (en) | Process for the preparation of primary 1, 1-dihydropolyfloroalkyl amines | |
| Sauers et al. | Further studies in pentacycloundecan-8-one photochemistry | |
| EP0308325A1 (fr) | Procédé de préparation du di-N-propylacétonitrile |