AU636887B2 - Finely powdered magnesium hydroxide and method for preparing it - Google Patents

Finely powdered magnesium hydroxide and method for preparing it

Info

Publication number
AU636887B2
AU636887B2 AU55281/90A AU5528190A AU636887B2 AU 636887 B2 AU636887 B2 AU 636887B2 AU 55281/90 A AU55281/90 A AU 55281/90A AU 5528190 A AU5528190 A AU 5528190A AU 636887 B2 AU636887 B2 AU 636887B2
Authority
AU
Australia
Prior art keywords
ppm
magnesium hydroxide
water
preparing
finely powdered
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn - After Issue
Application number
AU55281/90A
Other versions
AU5528190A (en
Inventor
Michael Grill
Andreas Meier
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Veitscher Magnesitwerke AG
Original Assignee
Veitscher Magnesitwerke AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Veitscher Magnesitwerke AG filed Critical Veitscher Magnesitwerke AG
Publication of AU5528190A publication Critical patent/AU5528190A/en
Application granted granted Critical
Publication of AU636887B2 publication Critical patent/AU636887B2/en
Anticipated expiration legal-status Critical
Withdrawn - After Issue legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01FCOMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F5/00Compounds of magnesium
    • C01F5/02Magnesia
    • C01F5/06Magnesia by thermal decomposition of magnesium compounds
    • C01F5/10Magnesia by thermal decomposition of magnesium compounds by thermal decomposition of magnesium chloride with water vapour
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01FCOMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F5/00Compounds of magnesium
    • C01F5/14Magnesium hydroxide
    • C01F5/16Magnesium hydroxide by treating magnesia, e.g. calcined dolomite, with water or solutions of salts not containing magnesium
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/18Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20Oxides; Hydroxides
    • C08K3/22Oxides; Hydroxides of metals
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/61Micrometer sized, i.e. from 1-100 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/62Submicrometer sized, i.e. from 0.1-1 micrometer

Abstract

Finely powdered magnesium hydroxide, in particular for use as a flame retardant filler for plastic compounds, in which the particles may have a thin coating of a surface active substance. The particle size of the magnesium hydroxide, as determined by laser diffraction, is less than 10 mu m and the mean particle size is greater than 0.8 mu m but not more than 3 mu m. The magnesium hydroxide has a water-soluble ionic impurities content, i.e., Ca<++>, Na<+>, K<+>, SO4<--> and Cl<->, below the following limits (in parts by mass): Ca<++> < 1000 ppm, Na<+> < 20 ppm, K<+> < 20 ppm, SO4<--> < 1500 ppm and Cl<-> < 1000 ppm, and Mn, Ni and Cu contents below the following limits (in parts by mass): MnO < 100 ppm, NiO < 100 ppm and CuO < 10 ppm. In the method for preparing the magnesium hydroxide, magnesium oxide obtained by spray roasting a magnesium chloride solution free of impurities is hydrated by mixing with water, the resultant magnesium hydroxide is filtered off and the filter cake material is then washed with water.
AU55281/90A 1989-05-05 1990-05-02 Finely powdered magnesium hydroxide and method for preparing it Withdrawn - After Issue AU636887B2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
AT1073/89 1989-05-05
AT1073/89A AT392774B (en) 1989-05-05 1989-05-05 FINE POWDERED MAGNESIUM HYDROXIDE AND METHOD FOR THE PRODUCTION THEREOF

Publications (2)

Publication Number Publication Date
AU5528190A AU5528190A (en) 1990-11-29
AU636887B2 true AU636887B2 (en) 1993-05-13

Family

ID=3506013

Family Applications (1)

Application Number Title Priority Date Filing Date
AU55281/90A Withdrawn - After Issue AU636887B2 (en) 1989-05-05 1990-05-02 Finely powdered magnesium hydroxide and method for preparing it

Country Status (16)

Country Link
EP (1) EP0427817B1 (en)
JP (1) JPH03505863A (en)
KR (1) KR920700162A (en)
CN (1) CN1046878A (en)
AT (2) AT392774B (en)
AU (1) AU636887B2 (en)
BR (1) BR9006763A (en)
CA (1) CA2032470C (en)
CZ (1) CZ219790A3 (en)
DD (1) DD294234A5 (en)
DE (1) DE59004217D1 (en)
HU (1) HUT56795A (en)
IL (1) IL94273A (en)
SK (1) SK219790A3 (en)
WO (1) WO1990013516A1 (en)
ZA (1) ZA903359B (en)

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IL112385A (en) * 1994-01-21 1998-08-16 Flamemag International Gie Process for preparing a flame retardant magnesium hydroxide
JP3836649B2 (en) 1999-11-22 2006-10-25 協和化学工業株式会社 Semiconductor sealing resin composition and molded product thereof
KR20000049740A (en) * 2000-04-26 2000-08-05 김철우 Making process of magnesia powder by spray roasting method
WO2001083620A1 (en) * 2000-05-02 2001-11-08 Kyowa Chemical Industry Co., Ltd. Resin composition for electric and electronic appliances
JP2002371198A (en) * 2001-04-11 2002-12-26 Sakai Chem Ind Co Ltd Flame retardant resin composition blended with high purity zinc borate
CN100375778C (en) * 2005-09-23 2008-03-19 清华大学 Liquid amonia pressurized precipitation and hydrothermal modification process for preparing magnesium hydroxide fire retardant
JP4201792B2 (en) * 2005-10-25 2008-12-24 神島化学工業株式会社 Flame retardant, flame retardant resin composition and molded article
KR101380184B1 (en) * 2006-02-01 2014-04-01 스미또모 가가꾸 가부시키가이샤 Micropore forming agent for porous resin film and composition for porous resin film containing the agent
KR20080114779A (en) * 2006-03-31 2008-12-31 알베마를 코포레이션 Magnesium hydroxide with improved compounding and viscosity performance
RU2008143217A (en) * 2006-03-31 2010-05-10 Альбемарл Корпорейшн (Us) MAGNESIUM HYDROXIDE HAVING IMPROVED MIXTURE AND VISCOSITY CHARACTERISTICS
WO2008120746A1 (en) * 2007-03-30 2008-10-09 Ube Material Industries, Ltd. Magnesium hydroxide powder and method for producing the same
WO2009153936A1 (en) * 2008-06-18 2009-12-23 丸尾カルシウム株式会社 Magnesium hydrate composition and manufacturing method thereof, and resin composition and molded article thereof
JP2020045349A (en) * 2011-08-16 2020-03-26 ピュラック バイオケム ビー. ブイ. Recovery of carboxylic acids from magnesium salts thereof through precipitation using hydrochloric acid, useful for fermentation broth processing
WO2015051482A1 (en) * 2013-10-11 2015-04-16 河北联合大学 Method for manufacturing sheet monodisperse nano-magnesium hydroxide by using magnesite
CN104925838B (en) * 2015-07-15 2016-12-28 后英集团海城市高新技术产品有限公司 A kind of efficient oxidation magnesium prepares magnesium hydroxide technique
EP3575267A1 (en) * 2018-06-01 2019-12-04 Omya International AG Development of surface-treated magnesium hydroxide-comprising material
GR20180100313A (en) * 2018-07-12 2020-03-18 Τερνα Λευκολιθοι Ανωνυμος Μεταλλευτικη, Εμπορικη, Τεχνικη, Βιομηχανικη Εταιρεια Α.Μ.Ε. Τ.Β.Ε Magnesium hydroxide production method
CN110182832A (en) * 2019-05-25 2019-08-30 邢台镁熙环保材料有限公司 A kind of petroleum catalyst special magnesium oxide production technology
CN115893459A (en) * 2022-12-20 2023-04-04 山东沃特斯德新材料科技有限公司 Preparation method of multifunctional water-soluble nano magnesium hydroxide stock solution

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AT335973B (en) * 1975-03-12 1977-04-12 Oesterr Amerikan Magnesit PROCESS FOR THE PREPARATION OF AQUATIC SOLUTIONS OF MAGNESIUM CHLORIDE
AT356630B (en) * 1978-12-13 1980-05-12 Ruthner Industrieanlagen Ag METHOD FOR PRODUCING MAGNESIUM OXYD SINTER
DD205412A1 (en) * 1982-07-02 1983-12-28 Kali Veb K PROCESS FOR CLEANING CHLORIDE-CONTAINING MAGNESIUM OXIDE
US4695445A (en) * 1985-08-14 1987-09-22 Asahi Glass Company Ltd. Magnesium hydroxide and process for its production
AT388392B (en) * 1987-06-26 1989-06-12 Veitscher Magnesitwerke Ag METHOD FOR THE PRODUCTION OF PURE MAGNESIUM OXIDE, IN PARTICULAR FOR THE PRODUCTION OF REFRACTORY-RESISTANT PRODUCTS

Also Published As

Publication number Publication date
IL94273A0 (en) 1991-03-10
ATA107389A (en) 1990-11-15
DE59004217D1 (en) 1994-02-24
SK278418B6 (en) 1997-05-07
JPH03505863A (en) 1991-12-19
KR920700162A (en) 1992-02-19
DD294234A5 (en) 1991-09-26
HU903640D0 (en) 1991-07-29
CZ219790A3 (en) 1998-04-15
BR9006763A (en) 1991-08-13
SK219790A3 (en) 1997-05-07
AU5528190A (en) 1990-11-29
CA2032470A1 (en) 1990-11-06
ATE100070T1 (en) 1994-01-15
WO1990013516A1 (en) 1990-11-15
AT392774B (en) 1991-06-10
ZA903359B (en) 1991-02-27
CA2032470C (en) 2000-09-05
EP0427817A1 (en) 1991-05-22
HUT56795A (en) 1991-10-28
EP0427817B1 (en) 1994-01-12
IL94273A (en) 1995-03-30
CN1046878A (en) 1990-11-14

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