AU2018101776A4 - Stabilizer methyl cellulose production plant - Google Patents
Stabilizer methyl cellulose production plant Download PDFInfo
- Publication number
- AU2018101776A4 AU2018101776A4 AU2018101776A AU2018101776A AU2018101776A4 AU 2018101776 A4 AU2018101776 A4 AU 2018101776A4 AU 2018101776 A AU2018101776 A AU 2018101776A AU 2018101776 A AU2018101776 A AU 2018101776A AU 2018101776 A4 AU2018101776 A4 AU 2018101776A4
- Authority
- AU
- Australia
- Prior art keywords
- tank
- pump
- methyl cellulose
- production plant
- feedstock
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B11/00—Preparation of cellulose ethers
- C08B11/02—Alkyl or cycloalkyl ethers
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Materials Engineering (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
Stabilizer methyl cellulose production plant Abstract 5 Stabilizer methyl cellulose production plant, including: opener (LIO), steeping press (L102), feedstock pump (J101), feedstock pump (J104), feedstock pump (JI05), smash reactor (DI01), transfer pump (J102), transfer pump (J103), transfer pump (J106), etherification kettle (D102), purification kettle (D103), tank (F101), tank (F102), dryer (L103), conveyer (ViO); among them, tank (FlOl) is used to store 10 methyl chloride, tank (F102) is used to store oxalic acid; among them, impeller diameter of feedstock pump (J104) is 130-135 mm. Figure 1 A -4 Figre-
Description
FIELD OF THE INVENTION
The present invention relates to a kind of pharmaceutical synthesis plant, more particularly, relates to stabilizer methyl cellulose production plant.
GENERAL BACKGROUND
Methyl cellulose is mainly used as adhesive, tackifier and latex stabilizer. It is used as adhesive, suspending agent, flocculation reducer in building materials and ceramics. It is commonly used as water-retaining agent in slurry. It can also be used as 10 a fertilizer adhesive in agriculture. Methyl cellulose is widely used in the construction industry, such as cement, mortar, sealant and other joints compound. In the cosmetics, pharmaceuticals and food industry, it is used as film-forming adhesive. Methyl cellulose is also used as weaving dyeing sizing agent, synthetic resin dispersant, paint filming agent and thickener. Methyl fiber is a very stable material, with acid-resisting, 15 alkali-resisting, microorganisms-resisting, heat-resisting and so on. Most of the existing production plant processes are complex. Thus, as a stabilizer, the advantages and disadvantages of production equipment of methyl cellulose have a great economic significant for improving product quality and reducing the by-product contents.
SUMMARY
The purpose of the present invention is to provide stabilizer methyl cellulose production plant, including: opener (L101), steeping press (L102), feedstock pump (JI01), feedstock pump (JI04), feedstock pump (JI05), smash reactor (DI01), transfer pump (JI02), transfer pump (JI03), transfer pump (JI06), etherification kettle (DI02), purification kettle (DI03), tank (Fl01), tank (Fl02), dryer (L103), conveyer (V101);
among them, tank (Fl01) is used to store methyl chloride, tank (Fl02) is used to store oxalic acid; among them, impeller diameter of feedstock pump (JI 04) is 130-135 mm, inner pot diameter of purification kettle (DI03) is 600-700 mm, cylinder diameter of tank (F102) is 1200-1300 mm.
Stabilizer methyl cellulose production plant, the production process is: opened the refined cotton pulp and added into steeping press L101, added alkali solution to make the cellulose fully alkalize at a temperature of 40-43 °C, pressed by presser L102, controlled the press ratio at 3.3-3.6, then aged in smash reactor D101 for 1-2 h at 45-47 °C, added the above-mentioned alkali cellulose into etherification kettle DI02, added purified methyl chloride under stirring in vacuum condition, the pressure in the autoclave is 0.4-0.5 MPa and the temperature is 30-32 °C. With the etherification reaction, jacket hot water circulation temperature is 60-65 °C, the pressure is 18.1-18.3 kg/cm2, the etherification time is 2-3 h. Discharged under stirring and adding hot water, added into washing autoclave DI03 for purification, put the wet purified product into rake dryer LI03 to obtain the finished product. The advantages of this invention are that the reaction time is reduced and the reaction rate is improved.
DESCRIPTION OF THE DRAWINGS
Figure 1 stabilizer methyl cellulose production plant.
Include: opener (LI01), steeping press (LI02), feedstock pump (JI01), feedstock pump (JI04), feedstock pump (JI05), smash reactor (DI01), transfer pump (JI02), transfer pump (JI03), transfer pump (JI06), etherification kettle (DI02), purification kettle (DI03), tank (Fl01), tank (Fl02), dryer (LI03), conveyer (V101);
DETAILED DESCRIPTION OF PREFERRED EMBODIMENTS
The following examples with reference to specific embodiments of the present invention are further illustrated:
Embodiment 1
Raw materials and dosages
| Refined cotton pulp | Commercial product | 150 | Glacial acetic acid | Industrial grade | 15 |
| Methyl chloride | Industrial grade | 450 | Oxalic acid | Industrial grade | 10 |
| Caustic soda | Industrial grade, 35% | 220 |
2018101776 19 Nov 2018
Stabilizer methyl cellulose production plant, including: opener (L101), steeping press (LI02), feedstock pump (JI01), feedstock pump (JI04), feedstock pump (JI05), smash reactor (DI01), transfer pump (JI02), transfer pump (JI03), transfer pump (JI06), etherification kettle (DI02), purification kettle (DI03), tank (Fl01), tank 5 (Fl02), dryer (LI03), conveyer (V101); among them, tank (Fl01) is used to store methyl chloride, tank (Fl02) is used to store oxalic acid; among them, impeller diameter of feedstock pump (JI04) is 130 mm, inner pot diameter of purification kettle (DI 03) is 600 mm, cylinder diameter of tank (Fl 02) is 1200 mm.
Stabilizer methyl cellulose production plant, the production process is: opened the refined cotton pulp and added into steeping press L101, added alkali solution to make the cellulose fully alkalize at a temperature of 40 °C, pressed by presser L102, controlled the press ratio at 3.3, then aged in smash reactor D101 for 1 h at 45 °C, added the above-mentioned alkali cellulose into etherification kettle DI02, added purified methyl chloride under stirring in vacuum condition, the pressure in the autoclave is 0.4 MPa and the temperature is 30 °C. With the etherification reaction, jacket hot water circulation temperature is 60 °C, the pressure is 18.1 kg/cm2, the etherification time is 2 h. Discharged under stirring and adding hot water, added into washing autoclave DI03 for purification, put the wet purified product into rake dryer LI03 to obtain the finished product.
The qualities of the product are as follows:
| Exterior | Fibrous solid | pH value | 6.6 |
| Solid content | 52% |
Embodiment 2
Raw materials and dosages
| Refined cotton pulp | Commercial product | 170 | Glacial acetic acid | Industrial grade | 20 |
| Methyl chloride | Industrial grade | 480 | Oxalic acid | Industrial grade | 13 |
| Caustic soda | Industrial | 250 |
2018101776 19 Nov 2018
| grade, 35% |
Stabilizer methyl cellulose production plant, including: opener (L101), steeping press (LI02), feedstock pump (JI01), feedstock pump (JI04), feedstock pump (JI05), smash reactor (DI01), transfer pump (JI02), transfer pump (JI03), transfer pump (JI06), etherification kettle (DI02), purification kettle (DI03), tank (Fl01), tank 5 (Fl02), dryer (LI03), conveyer (V101); among them, tank (Fl01) is used to store methyl chloride, tank (Fl02) is used to store oxalic acid; among them, impeller diameter of feedstock pump (JI04) is 135 mm, inner pot diameter of purification kettle (D103) is 700 mm, cylinder diameter of tank (F102) is 1300 mm.
Stabilizer methyl cellulose production plant, the production process is: opened the refined cotton pulp and added into steeping press L101, added alkali solution to make the cellulose fully alkalize at a temperature of 43 °C, pressed by presser L102, controlled the press ratio at 3.6, then aged in smash reactor D101 for 2 h at 47 °C, added the above-mentioned alkali cellulose into etherification kettle DI02, added purified methyl chloride under stirring in vacuum condition, the pressure in the autoclave is 0.5 MPa and the temperature is 32 °C. With the etherification reaction, jacket hot water circulation temperature is 65 °C, the pressure is 18.3 kg/cm2, the etherification time is 3 h. Discharged under stirring and adding hot water, added into washing autoclave DI03 for purification, put the wet purified product into rake dryer LI03 to obtain the finished product.
The qualities of the product are as follows:
| Exterior | Fibrous solid | pH value | 6.8 |
| Solid content | 55% |
The embodiments of the present invention are merely preferred embodiments of the present invention, but the range of the present invention is not limited this, and any person who is familiar with those skilled in the arts, within the technical range of the present invention. It is intended that the technical solution and its inventive concept be replaced or modified equivalently with reference to the range of the invention.
Claims (3)
- Claims1. Stabilizer methyl cellulose production plant, including: opener (L101), steeping press (LI02), feedstock pump (JI01), feedstock pump (JI04), feedstock5 pump (JI05), smash reactor (DI01), transfer pump (JI02), transfer pump (JI03), transfer pump (JI06), etherification kettle (DI02), purification kettle (DI03), tank (Fl01), tank (Fl02), dryer (LI03), conveyer (V101); among them, tank (Fl01) is used to store methyl chloride, tank (Fl02) is used to store oxalic acid; among them, impeller diameter of feedstock pump (JI 04) is 130-135 mm.10
- 2. Stabilizer methyl cellulose production plant according to claim 1 wherein inner pot diameter of purification kettle (DI 03) is 600-700 mm.
- 3. Stabilizer methyl cellulose production plant according to claim 1 wherein cylinder diameter of tank (F102) is 1200-1300 mm.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2017112534183 | 2017-12-02 | ||
| CN201711253418.3A CN108239152A (en) | 2017-12-02 | 2017-12-02 | The process units of stabilizer methylcellulose |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| AU2018101776A4 true AU2018101776A4 (en) | 2019-01-03 |
Family
ID=61158154
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AU2018101776A Ceased AU2018101776A4 (en) | 2017-12-02 | 2018-11-19 | Stabilizer methyl cellulose production plant |
Country Status (3)
| Country | Link |
|---|---|
| CN (1) | CN108239152A (en) |
| AU (1) | AU2018101776A4 (en) |
| GB (1) | GB201722005D0 (en) |
-
2017
- 2017-12-02 CN CN201711253418.3A patent/CN108239152A/en not_active Withdrawn
- 2017-12-28 GB GBGB1722005.4A patent/GB201722005D0/en not_active Ceased
-
2018
- 2018-11-19 AU AU2018101776A patent/AU2018101776A4/en not_active Ceased
Also Published As
| Publication number | Publication date |
|---|---|
| GB201722005D0 (en) | 2018-02-14 |
| CN108239152A (en) | 2018-07-03 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| AU2018101776A4 (en) | Stabilizer methyl cellulose production plant | |
| CN101659635A (en) | Preparation method of methyl p-tolyl sulfone | |
| CN1271087C (en) | Process for preparing high substituted degree hydroxyalkyl starch | |
| IE20180437U1 (en) | Stabilizer methyl cellulose production plant | |
| CN110804103A (en) | Gas-solid method production process of cellulose mixed ether | |
| AU2018101966A4 (en) | Viscosity reducer sodium humate production plant | |
| IES20180437A2 (en) | Stabilizer methyl cellulose production plant | |
| CN108047336A (en) | The etherification technology of medicinal HPMC | |
| AU2018101964A4 (en) | Dispersant sodium carboxymethyl starch production plant | |
| AU2018101727A4 (en) | Polyvinyl acetate coating production plant | |
| AU2018101968A4 (en) | 2-hydroxy-3-sulfopropyl propyl starch ether production plant | |
| AU2018101833A4 (en) | Polybutylene succinate-MDI hot melt adhesive production plant | |
| AU2018101985A4 (en) | Dye dispersant sodium cellulose sulfate production plant | |
| IE20180479U1 (en) | Dispersant carboxymethyl cellulose production plant | |
| AU2018101997A4 (en) | Dimethylol dihydroxy ethylene urea resin production plant | |
| AU2018101739A4 (en) | Neoprene paint production plant | |
| AU2018101818A4 (en) | Anaerobic sealing adhesive production plant | |
| AU2018101735A4 (en) | Emulsified asphalt waterproof coating production plant | |
| AU2018101811A4 (en) | Polyvinyl formal production plant | |
| AU2018101413A4 (en) | Water treatment agent sodium tungstate production plant | |
| AU2018101770A4 (en) | Dispersant sodium lignosulphonate production plant | |
| AU2018101736A4 (en) | Compound modification polystyrene emulsion coating production plant | |
| AU2018101907A4 (en) | Cellulose super absorbent resin production plant | |
| AU2018101834A4 (en) | High temperature inorganic adhesive production plant | |
| CN205603494U (en) | Paint industry emulsifier midbody alcohol ether carboxylate surfactant apparatus for producing |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FGI | Letters patent sealed or granted (innovation patent) | ||
| MK22 | Patent ceased section 143a(d), or expired - non payment of renewal fee or expiry |