AU2018101834A4 - High temperature inorganic adhesive production plant - Google Patents
High temperature inorganic adhesive production plant Download PDFInfo
- Publication number
- AU2018101834A4 AU2018101834A4 AU2018101834A AU2018101834A AU2018101834A4 AU 2018101834 A4 AU2018101834 A4 AU 2018101834A4 AU 2018101834 A AU2018101834 A AU 2018101834A AU 2018101834 A AU2018101834 A AU 2018101834A AU 2018101834 A4 AU2018101834 A4 AU 2018101834A4
- Authority
- AU
- Australia
- Prior art keywords
- tank
- high temperature
- reactor
- production plant
- inorganic adhesive
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J1/00—Adhesives based on inorganic constituents
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
Landscapes
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Organic Chemistry (AREA)
- Adhesives Or Adhesive Processes (AREA)
Abstract
High temperature inorganic adhesive production plant Abstract 5 High temperature inorganic adhesive production plant, including: tank (F101), tank (FI02), reactor (Di01), feedstock pump (Ji01, J102, J104), transfer pump (JI03, J105), filter (LiO), dryer (LI02), conveyor (Viol, V102), muffle furnace (LI03), sifter (LI04), reactor (DI02), tank (FI03); among them, tank (FiOl) is used to store sodium hydroxide solution, tank (FI02) is used to store copper sulfate solution, tank 10 (FI03) is used to store phosphoric acid; among them, nominal volume of tank (FI02) is 1.6-1.9 in3 . Figure 1 f/I -~ a I -~ p-z2~> / \ -r 'II N- V __- ft Figure
Description
High temperature inorganic adhesive production plant
FIELD OF THE INVENTION
The present invention relates to a kind of pharmaceutical synthesis plant, more particularly, relates to high temperature inorganic adhesive production plant.
GENERAL BACKGROUND
High temperature inorganic adhesive is for bonding and repairing of a variety of high temperature mechanical parts. Application temperature can up to 600-800 °C. It can also be used for ceramic and other refractories bonding. Most of the existing production plant processes are complex. Thus, as a special adhesive, the advantages and disadvantages of production equipment of high temperature inorganic adhesive have a great economic significant for improving product quality and reducing the by-product contents.
SUMMARY
The purpose of the present invention is to provide high temperature inorganic adhesive production plant, including: tank (F101), tank (F102), reactor (D101), feedstock pump (JI01, JI02, JI04), transfer pump (JI03, JI05), filter (LI01), dryer (LI02), conveyor (V101, V102), muffle furnace (LI03), sifter (LI04), reactor (DI02), tank (Fl03); among them, tank (Fl01) is used to store sodium hydroxide solution, tank (Fl02) is used to store copper sulfate solution, tank (Fl03) is used to store phosphoric acid; among them, nominal volume of tank (F102) is 1.6-1.9 m3, inlet diameter of feedstock pump (J101) is 255-260 mm, jacket capacity of reactor (D102) is 230-240 mm.
High temperature inorganic adhesive production plant, the production process is:
added sodium hydroxide solution with a mass fraction of 12-14% from F101 into reactor D101, heated to 70-75 °C, then pumped 16-19% copper sulfate solution while stirring, gradually precipitated black solid material of copper oxide, finally heated to boil for 40-50 min so that precipitated all copper oxide. Separated the copper oxide precipitate by filtration L101, repeatedly washed with boiling water to remove SO®.
2018101834 27 Nov 2018
Dried the washed filter cake of copper oxide in drying oven L102 at 130-135 °C for 2-3 h. Coarsely crushed the dried copper oxide and put into muffle furnace LI03, heated to 700-760°C, the copper oxide is silver black and black lump after calcining.
Finely crushed copper oxide, sieved 200 mesh, and finally dried, sealed, which is A 5 component. Added 110 parts ofFfiPCfi and 6 parts of AI(OH)3to reactor D102, stirred and heated to 180-190 °C to dissolve, cooled naturally, and obtained B component.
When used, compounded uniformly the prepared B component and A component in a ratio of 1:6 and got the finished product. The advantages of this invention are that the reaction time is reduced and the reaction rate is improved.
DESCRIPTION OF THE DRAWINGS
Figure 1 is high temperature inorganic adhesive production plant.
Include: tank (F101), tank (F102), reactor (D101), feedstock pump (J101, J102, JI04), transfer pump (JI03, JI05), filter (LI01), dryer (LI02), conveyor (V101, VI02), muffle furnace (LI03), sifter (LI04), reactor (D102), tank (Fl03);
DETAILED DESCRIPTION OF PREFERRED EMBODIMENTS
The following examples with reference to specific embodiments of the present invention are further illustrated:
Embodiment 1
Raw materials and dosages
| Copper sulfate | Industrial grade | 100 | Sodium hydroxide | Industrial grade | 60 |
| Phosphoric acid | Industrial grade | 200 |
High temperature inorganic adhesive production plant, including: tank (Fl01), tank (Fl02), reactor (D101), feedstock pump (JI01, JI02, JI04), transfer pump (JI03, J105), filter (L101), dryer (L102), conveyor (V101, V102), muffle furnace (L103), sifter (LI04), reactor (D102), tank (Fl03); among them, tank (Fl01) is used to store sodium hydroxide solution, tank (F102) is used to store copper sulfate solution, tank (F103) is used to store phosphoric acid; among them, nominal volume of tank (F102) is 1.6 m3, inlet diameter of feedstock pump (J101) is 255 mm, jacket capacity of reactor (D102) is 230 mm.
2018101834 27 Nov 2018
High temperature inorganic adhesive production plant, the production process is:
added sodium hydroxide solution with a mass fraction of 12% from Fl01 into reactor
D101, heated to 70 °C, then pumped 16% copper sulfate solution while stirring, gradually precipitated black solid material of copper oxide, finally heated to boil for
40-50 min so that precipitated all copper oxide. Separated the copper oxide precipitate by filtration L101, repeatedly washed with boiling water to remove SCfi2’. Dried the washed filter cake of copper oxide in drying oven L102 at 130 °C for 2 h. Coarsely crushed the dried copper oxide and put into muffle furnace LI03, heated to 700°C, the copper oxide is silver black and black lump after calcining. Finely crushed copper 10 oxide, sieved 200 mesh, and finally dried, sealed, which is A component. Added 110 parts of H3PO4 and 6 parts of AI(OH)3 to reactor D102, stirred and heated to 180 °C to dissolve, cooled naturally, and obtained B component. When used, compounded uniformly the prepared B component and A component in a ratio of 1:6 and got the finished product.
The qualities of the product are as follows:
| Exterior | A component is black powder | Hardness | HB57 |
| B component is colorless and transparent liquid | Adhesive strength | > 82 MPa |
Embodiment 2
Raw materials and dosages
| Copper sulfate | Industrial grade | 130 | Sodium hydroxide | Industrial grade | 85 |
| Phosphoric acid | Industrial grade | 220 |
High temperature inorganic adhesive production plant, including: tank (Fl01), tank (Fl02), reactor (DI01), feedstock pump (JI01, JI02, JI04), transfer pump (JI03,
J105), filter (L101), dryer (L102), conveyor (V101, V102), muffle furnace (L103), sifter (LI04), reactor (DI02), tank (Fl03); among them, tank (Fl01) is used to store sodium hydroxide solution, tank (F102) is used to store copper sulfate solution, tank (F103) is used to store phosphoric acid; among them, nominal volume of tank (F102)
2018101834 27 Nov 2018 is 1.9 m3, inlet diameter of feedstock pump (J101) is 260 mm, jacket capacity of reactor (DI02) is 240 mm.
High temperature inorganic adhesive production plant, the production process is: added sodium hydroxide solution with a mass fraction of 14% from Fl01 into reactor 5 D101, heated to 75 °C, then pumped 19% copper sulfate solution while stirring, gradually precipitated black solid material of copper oxide, finally heated to boil for 40-50 min so that precipitated all copper oxide. Separated the copper oxide precipitate by filtration L101, repeatedly washed with boiling water to remove SCff2’. Dried the washed filter cake of copper oxide in drying oven L102 at 135 °C for 3 h. Coarsely 10 crushed the dried copper oxide and put into muffle furnace LI03, heated to 760°C, the copper oxide is silver black and black lump after calcining. Finely crushed copper oxide, sieved 200 mesh, and finally dried, sealed, which is A component. Added 110 parts of H3PO4 and 6 parts of AI(OH)3 to reactor D102, stirred and heated to 190 °C to dissolve, cooled naturally, and obtained B component. When used, compounded 15 uniformly the prepared B component and A component in a ratio of 1:6 and got the finished product.
The qualities of the product are as follows:
| Exterior | A component is black powder | Hardness | HB 62 |
| B component is colorless and transparent liquid | Adhesive strength | > 86 MPa |
The embodiments of the present invention are merely preferred embodiments of the present invention, but the range of the present invention is not limited this, and any person who is familiar with those skilled in the arts, within the technical range of the present invention. It is intended that the technical solution and its inventive concept be replaced or modified equivalently with reference to the range of the invention.
Claims (3)
1. High temperature inorganic adhesive production plant, including: tank (Fl01), tank (Fl02), reactor (DI01), feedstock pump (JI01, JI02, JI04), transfer pump (JI03,
5 J105), filter (L101), dryer (L102), conveyor (V101, V102), muffle furnace (L103), sifter (L104), reactor (DI02), tank (Fl03); among them, tank (Fl01) is used to store sodium hydroxide solution, tank (F102) is used to store copper sulfate solution, tank (F103) is used to store phosphoric acid; among them, nominal volume of tank (F102) is 1.6-1.9 m3.
10
2. High temperature inorganic adhesive production plant according to claim 1 wherein inlet diameter of feedstock pump (JI 01) is 255-260 mm.
3. High temperature inorganic adhesive production plant according to claim 1 wherein jacket capacity of reactor (D102) is 230-240 mm.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711267984.XA CN108239485A (en) | 2017-12-05 | 2017-12-05 | The process units of high temperature resistant inorganic gluing agent |
| CN201711267984X | 2017-12-05 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| AU2018101834A4 true AU2018101834A4 (en) | 2019-01-17 |
Family
ID=61131638
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AU2018101834A Ceased AU2018101834A4 (en) | 2017-12-05 | 2018-11-27 | High temperature inorganic adhesive production plant |
Country Status (3)
| Country | Link |
|---|---|
| CN (1) | CN108239485A (en) |
| AU (1) | AU2018101834A4 (en) |
| GB (1) | GB201721959D0 (en) |
-
2017
- 2017-12-05 CN CN201711267984.XA patent/CN108239485A/en not_active Withdrawn
- 2017-12-27 GB GBGB1721959.3A patent/GB201721959D0/en not_active Ceased
-
2018
- 2018-11-27 AU AU2018101834A patent/AU2018101834A4/en not_active Ceased
Also Published As
| Publication number | Publication date |
|---|---|
| CN108239485A (en) | 2018-07-03 |
| GB201721959D0 (en) | 2018-02-07 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FGI | Letters patent sealed or granted (innovation patent) | ||
| MK22 | Patent ceased section 143a(d), or expired - non payment of renewal fee or expiry |