AU2015274247B2 - A process for the preparation of fatty acid alkyl esters - Google Patents

A process for the preparation of fatty acid alkyl esters Download PDF

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Publication number
AU2015274247B2
AU2015274247B2 AU2015274247A AU2015274247A AU2015274247B2 AU 2015274247 B2 AU2015274247 B2 AU 2015274247B2 AU 2015274247 A AU2015274247 A AU 2015274247A AU 2015274247 A AU2015274247 A AU 2015274247A AU 2015274247 B2 AU2015274247 B2 AU 2015274247B2
Authority
AU
Australia
Prior art keywords
fatty acid
mixture
alkyl esters
acid alkyl
amount
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
AU2015274247A
Other languages
English (en)
Other versions
AU2015274247A1 (en
Inventor
Reno Emilio Beltrame
Ketav KULKARNI
Patrick Perlmutter
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Southern Biofuel Technology Pty Ltd
Original Assignee
Southern Biofuel Tech Pty Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from AU2014902260A external-priority patent/AU2014902260A0/en
Application filed by Southern Biofuel Tech Pty Ltd filed Critical Southern Biofuel Tech Pty Ltd
Publication of AU2015274247A1 publication Critical patent/AU2015274247A1/en
Application granted granted Critical
Publication of AU2015274247B2 publication Critical patent/AU2015274247B2/en
Ceased legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/02—Preparation of carboxylic acid esters by interreacting ester groups, i.e. transesterification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/03—Preparation of carboxylic acid esters by reacting an ester group with a hydroxy group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/003—Esters of saturated alcohols having the esterified hydroxy group bound to an acyclic carbon atom
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/02—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only
    • C10L1/026—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only for compression ignition
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/02—Refining fats or fatty oils by chemical reaction
    • C11B3/04—Refining fats or fatty oils by chemical reaction with acids
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/02—Refining fats or fatty oils by chemical reaction
    • C11B3/08—Refining fats or fatty oils by chemical reaction with oxidising agents
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/003—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/04—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fats or fatty oils
    • C11C3/10—Ester interchange
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
    • C10L2200/00—Components of fuel compositions
    • C10L2200/04—Organic compounds
    • C10L2200/0461—Fractions defined by their origin
    • C10L2200/0469—Renewables or materials of biological origin
    • C10L2200/0476—Biodiesel, i.e. defined lower alkyl esters of fatty acids first generation biodiesel
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/10—Biofuels, e.g. bio-diesel

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • General Chemical & Material Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Microbiology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Fats And Perfumes (AREA)
  • Liquid Carbonaceous Fuels (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
AU2015274247A 2014-06-13 2015-06-12 A process for the preparation of fatty acid alkyl esters Ceased AU2015274247B2 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
AU2014902260 2014-06-13
AU2014902260A AU2014902260A0 (en) 2014-06-13 A process for the preparation of fatty acid alkyl esters
PCT/AU2015/050324 WO2015188233A1 (en) 2014-06-13 2015-06-12 A process for the preparation of fatty acid alkyl esters

Publications (2)

Publication Number Publication Date
AU2015274247A1 AU2015274247A1 (en) 2017-01-05
AU2015274247B2 true AU2015274247B2 (en) 2019-02-07

Family

ID=54832629

Family Applications (1)

Application Number Title Priority Date Filing Date
AU2015274247A Ceased AU2015274247B2 (en) 2014-06-13 2015-06-12 A process for the preparation of fatty acid alkyl esters

Country Status (6)

Country Link
US (2) US10233141B2 (enExample)
EP (1) EP3154935A4 (enExample)
JP (1) JP2017518377A (enExample)
AU (1) AU2015274247B2 (enExample)
CA (1) CA2950748A1 (enExample)
WO (1) WO2015188233A1 (enExample)

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2371284A (en) * 1945-03-13 Preparation of sulphated fatty
US3172905A (en) * 1965-03-09 Catalytic preparation of esters from tertiary olefins and carboxylic acids
US2467095A (en) * 1947-07-08 1949-04-12 Carbide & Carbon Chem Corp Acylation with enol esters
US3128294A (en) * 1961-06-09 1964-04-07 Alexander J Stirton Salts of alpha-sulfonated fatty acid esters
JPH09278739A (ja) * 1996-04-11 1997-10-28 Lion Corp 淡色α−スルホ脂肪酸アルキルエステル塩、脂肪酸アルキルエステルおよびその製造法
JP4230097B2 (ja) * 1999-06-25 2009-02-25 ライオン株式会社 α−スルホ脂肪酸アルキルエステル塩の製造方法
GB0505064D0 (en) * 2005-03-11 2005-04-20 Univ Belfast Production of bio-diesel
JP2008024672A (ja) * 2006-07-24 2008-02-07 Lion Corp α―スルホ脂肪酸アルキルエステル塩の製造方法
JP2009126847A (ja) * 2007-11-27 2009-06-11 Lion Corp 脂肪酸アルキルエステル中の微量グリセリンの除去方法
CN101343245B (zh) * 2008-08-22 2011-03-16 江南大学 一种先磺化后酯化工艺制造低二钠盐含量脂肪酸甲酯磺酸盐的方法
MY151440A (en) * 2009-10-29 2014-05-30 Malaysian Palm Oil Board Mpob A method of converting free fatty acid (ffa) from oil to methyl ester

Also Published As

Publication number Publication date
AU2015274247A1 (en) 2017-01-05
CA2950748A1 (en) 2015-12-17
WO2015188233A1 (en) 2015-12-17
JP2017518377A (ja) 2017-07-06
US20170113996A1 (en) 2017-04-27
EP3154935A4 (en) 2018-03-07
US10233141B2 (en) 2019-03-19
EP3154935A1 (en) 2017-04-19
US20190210953A1 (en) 2019-07-11

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MK14 Patent ceased section 143(a) (annual fees not paid) or expired