AU2013234971B2 - Collisional broadening compensation using real or near-real time validation in spectroscopic analyzers - Google Patents
Collisional broadening compensation using real or near-real time validation in spectroscopic analyzers Download PDFInfo
- Publication number
- AU2013234971B2 AU2013234971B2 AU2013234971A AU2013234971A AU2013234971B2 AU 2013234971 B2 AU2013234971 B2 AU 2013234971B2 AU 2013234971 A AU2013234971 A AU 2013234971A AU 2013234971 A AU2013234971 A AU 2013234971A AU 2013234971 B2 AU2013234971 B2 AU 2013234971B2
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- AU
- Australia
- Prior art keywords
- gas
- validation
- detector
- sample gas
- spectrometer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01J—MEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT, POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRARED, VISIBLE OR ULTRAVIOLET LIGHT; COLORIMETRY; RADIATION PYROMETRY
- G01J3/00—Spectrometry; Spectrophotometry; Monochromators; Measuring colours
- G01J3/02—Details
- G01J3/0297—Constructional arrangements for removing other types of optical noise or for performing calibration
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01J—MEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT, POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRARED, VISIBLE OR ULTRAVIOLET LIGHT; COLORIMETRY; RADIATION PYROMETRY
- G01J3/00—Spectrometry; Spectrophotometry; Monochromators; Measuring colours
- G01J3/28—Investigating the spectrum
- G01J3/42—Absorption spectrometry; Double beam spectrometry; Flicker spectrometry; Reflection spectrometry
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/01—Arrangements or apparatus for facilitating the optical investigation
- G01N21/03—Cuvette constructions
- G01N21/05—Flow-through cuvettes
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
- G01N21/27—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands using photo-electric detection ; circuits for computing concentration
- G01N21/274—Calibration, base line adjustment, drift correction
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
- G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
- G01N21/35—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
- G01N21/3504—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light for analysing gases, e.g. multi-gas analysis
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/01—Arrangements or apparatus for facilitating the optical investigation
- G01N21/03—Cuvette constructions
- G01N21/031—Multipass arrangements
- G01N2021/0314—Double pass, autocollimated path
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
- G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
- G01N21/39—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using tunable lasers
- G01N2021/396—Type of laser source
- G01N2021/399—Diode laser
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
- G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
- G01N21/39—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using tunable lasers
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2201/00—Features of devices classified in G01N21/00
- G01N2201/12—Circuits of general importance; Signal processing
- G01N2201/121—Correction signals
- G01N2201/1211—Correction signals for temperature
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2201/00—Features of devices classified in G01N21/00
- G01N2201/12—Circuits of general importance; Signal processing
- G01N2201/121—Correction signals
- G01N2201/1218—Correction signals for pressure variations
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2201/00—Features of devices classified in G01N21/00
- G01N2201/12—Circuits of general importance; Signal processing
- G01N2201/127—Calibration; base line adjustment; drift compensation
Landscapes
- Physics & Mathematics (AREA)
- Spectroscopy & Molecular Physics (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Mathematical Physics (AREA)
- Theoretical Computer Science (AREA)
- Investigating Or Analysing Materials By Optical Means (AREA)
- Investigating, Analyzing Materials By Fluorescence Or Luminescence (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US13/428,591 | 2012-03-23 | ||
| US13/428,591 US8976358B2 (en) | 2012-03-23 | 2012-03-23 | Collisional broadening compensation using real or near-real time validation in spectroscopic analyzers |
| PCT/US2013/033383 WO2013142737A1 (en) | 2012-03-23 | 2013-03-21 | Collisional broadening compensation using real or near-real time validation in spectroscopic analyzers |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| AU2013234971A1 AU2013234971A1 (en) | 2014-09-11 |
| AU2013234971B2 true AU2013234971B2 (en) | 2015-06-25 |
Family
ID=48096235
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AU2013234971A Ceased AU2013234971B2 (en) | 2012-03-23 | 2013-03-21 | Collisional broadening compensation using real or near-real time validation in spectroscopic analyzers |
Country Status (7)
| Country | Link |
|---|---|
| US (2) | US8976358B2 (enExample) |
| EP (1) | EP2828642A1 (enExample) |
| CN (1) | CN104364635B (enExample) |
| AU (1) | AU2013234971B2 (enExample) |
| CA (1) | CA2865649C (enExample) |
| IN (1) | IN2014MN02008A (enExample) |
| WO (1) | WO2013142737A1 (enExample) |
Families Citing this family (32)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8976358B2 (en) | 2012-03-23 | 2015-03-10 | Spectrasensors, Inc. | Collisional broadening compensation using real or near-real time validation in spectroscopic analyzers |
| US20140361172A1 (en) * | 2013-06-11 | 2014-12-11 | Jp3 Measurement, Llc | Detection of h2s in natural gas and hydrocarbon streams using a dual-path near-ir spectroscopy system |
| DE102014101915B4 (de) * | 2014-02-14 | 2024-08-01 | Avl Analytical Technologies Gmbh | Vorrichtung und Verfahren zur Bestimmung der Konzentration zumindest eines Gases in einem Probengasstrom mittels Infrarotabsorptionsspektroskopie |
| CN107250740A (zh) * | 2014-11-06 | 2017-10-13 | 光谱引擎股份公司 | 光学测量系统 |
| US10643008B2 (en) * | 2014-11-11 | 2020-05-05 | Spectrasensors, Inc. | Target analyte detection and quantification in sample gases with complex background compositions |
| CN104374712A (zh) * | 2014-11-19 | 2015-02-25 | 山东罗纳德分析仪器有限公司 | 一种光谱分析仪的谱型变化补偿方法及装置 |
| CN104713841B (zh) * | 2015-02-09 | 2017-05-24 | 中国石油大学(华东) | 一种自校准分析仪的设计方法及装置 |
| KR102109245B1 (ko) * | 2015-05-12 | 2020-05-11 | 코니카 미놀타 가부시키가이샤 | 식물 생육 지표 측정 장치 및 그의 방법 그리고 식물 생육 지표 측정 시스템 |
| US11953427B2 (en) * | 2015-08-03 | 2024-04-09 | Endress+Hauser Optical Analysis, Inc. | Reconstruction of frequency registration for quantitative spectroscopy |
| WO2017024046A2 (en) * | 2015-08-03 | 2017-02-09 | Spectrasensors, Inc. | Reconstruction of frequency registration deviations for quantitative spectroscopy |
| US9696204B2 (en) | 2015-08-03 | 2017-07-04 | Spectrasensors, Inc. | Determination and correction of frequency registration deviations for quantitative spectroscopy |
| JP2017129374A (ja) * | 2016-01-18 | 2017-07-27 | 株式会社堀場製作所 | 分析装置、及び、分析方法 |
| KR102497849B1 (ko) * | 2016-05-09 | 2023-02-07 | 삼성전자주식회사 | 분석물질 농도 예측 방법 및 장치 |
| US10677713B1 (en) * | 2016-08-04 | 2020-06-09 | Hrl Laboratories, Llc | Adaptive gas analyzer |
| CN106841035B (zh) * | 2017-01-25 | 2024-02-23 | 成都中信华瑞科技有限公司 | 检测方法及装置 |
| US10663344B2 (en) | 2017-04-26 | 2020-05-26 | Viavi Solutions Inc. | Calibration for an instrument (device, sensor) |
| US10824049B1 (en) | 2017-10-06 | 2020-11-03 | Hrl Laboratories, Llc | Optical-frequency up-converting spectrometric imager |
| EP3517937B1 (en) * | 2017-11-28 | 2021-10-20 | Cloudminds (Shenzhen) Holdings Co., Ltd. | Mixture detection method and device |
| US12044570B2 (en) | 2018-03-27 | 2024-07-23 | Viavi Solutions Inc. | Calibration for an instrument (device, sensor) |
| CN112804938B (zh) * | 2018-08-08 | 2024-08-13 | 布赖特斯佩克股份有限公司 | 用于低挥发性采样的方法和设备 |
| WO2020106557A1 (en) | 2018-11-21 | 2020-05-28 | Thermo Fisher Scientific Inc. | System and method for rapid and accurate trace gas measurement |
| JP7498545B2 (ja) * | 2019-05-09 | 2024-06-12 | 株式会社堀場エステック | 吸光分析システム、吸光分析システム用プログラム、吸光分析装置、及び、吸光度測定方法 |
| CN110208204A (zh) * | 2019-06-13 | 2019-09-06 | 苗春磊 | 一种基于dlp技术的傅里叶变换光谱仪 |
| US11079324B2 (en) | 2019-07-15 | 2021-08-03 | Spectrasensors, Inc. | Spectrometer with wide-scan tunable diode laser |
| US11719576B2 (en) * | 2019-11-01 | 2023-08-08 | California Institute Of Technology | Mid-wave and long-wave infrared point spectrometer |
| US12298232B2 (en) * | 2020-05-29 | 2025-05-13 | Horiba, Ltd. | Analysis device, program for analysis device, and analysis method |
| US11456577B2 (en) * | 2020-07-28 | 2022-09-27 | Raytheon Company | Monolithic quantum cascade laser (QCL)/avalanche photodiode (APD) infrared transceiver |
| US11639892B2 (en) * | 2021-04-02 | 2023-05-02 | Abb Schweiz Ag | Systems and methods for skewed basis set fitting |
| US12546709B2 (en) | 2022-12-30 | 2026-02-10 | Endress+Hauser Optical Analysis, Inc. | Quantification of target analyte based on multi-layer multi-variant spectra analysis for spectroscopic analyzers |
| DE102023115474A1 (de) * | 2023-06-14 | 2024-12-19 | Dräger Safety AG & Co. KGaA | Verfahren und Vorrichtung zum Überprüfen eines Gasdetektionsgeräts |
| CN117871436B (zh) * | 2023-12-01 | 2024-07-16 | 江苏南大光电材料股份有限公司 | 用于高纯特气痕量水分仪验证的渗透管分析装置及方法 |
| DE102023136103A1 (de) * | 2023-12-20 | 2025-06-26 | Endress+Hauser Group Services Ag | Messanordnungen und Verfahren zum Nachweis von Spurengasen in einem Messgas |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4110619A (en) * | 1975-11-21 | 1978-08-29 | H. Maihak Ag | Method of compensating for carrier-gas-composition dependence due to the collision-broadening effect in non-dispersive infrared photometers having a detector comprised of two absorption chambers arranged one behind the other |
| US4849636A (en) * | 1988-05-18 | 1989-07-18 | Mine Safety Appliances Company | Analyzer with compensation |
| US5900635A (en) * | 1995-09-29 | 1999-05-04 | Instrumentarium Oy | Correction of collision broadening in non-dispersive absorption measurement of gases |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4803370A (en) * | 1987-05-18 | 1989-02-07 | Li-Cor, Inc. | Infrared light generation |
| US5340987A (en) * | 1991-03-15 | 1994-08-23 | Li-Cor, Inc. | Apparatus and method for analyzing gas |
| FI101749B (fi) * | 1996-12-30 | 1998-08-14 | Instrumentarium Oy | Kaasukomponentin pitoisuuden tarkka mittaaminen kaasuseoksessa, jossa muut komponentit vaikuttavat pitoisuusmääritykseen |
| US6527398B1 (en) * | 2000-06-08 | 2003-03-04 | Gregory J. Fetzer | Tubular-waveguide gas sample chamber for optical spectrometer, and related methods |
| US6844554B2 (en) * | 2002-06-28 | 2005-01-18 | Instrumentarium Corp. | Method and arrangement for determining the concentration of a gas component in a gas mixture |
| US7508521B2 (en) | 2007-03-14 | 2009-03-24 | Spectrasensors, Inc. | Pressure-invariant trace gas detection |
| WO2008128114A1 (en) | 2007-04-11 | 2008-10-23 | Spectrasensors, Inc. | Reactive gas detection in complex backgrounds |
| US9267881B2 (en) * | 2008-11-06 | 2016-02-23 | Li-Cor, Inc. | Hybrid gas analyzer with thermally insulated flow cell |
| WO2010122990A1 (ja) * | 2009-04-20 | 2010-10-28 | ユニバーサル・バイオ・リサーチ株式会社 | 生体関連物質測定用チューブおよび定量システム |
| US8358417B2 (en) * | 2010-10-21 | 2013-01-22 | Spectrasensors, Inc. | Spectrometer with validation cell |
| US8178832B1 (en) * | 2011-05-31 | 2012-05-15 | Wong Jacob Y | Re-calibration methodology for NDIR gas sensors |
| US8976358B2 (en) | 2012-03-23 | 2015-03-10 | Spectrasensors, Inc. | Collisional broadening compensation using real or near-real time validation in spectroscopic analyzers |
-
2012
- 2012-03-23 US US13/428,591 patent/US8976358B2/en active Active
-
2013
- 2013-03-21 WO PCT/US2013/033383 patent/WO2013142737A1/en not_active Ceased
- 2013-03-21 EP EP13716562.7A patent/EP2828642A1/en not_active Ceased
- 2013-03-21 AU AU2013234971A patent/AU2013234971B2/en not_active Ceased
- 2013-03-21 CN CN201380015938.4A patent/CN104364635B/zh active Active
- 2013-03-21 CA CA2865649A patent/CA2865649C/en not_active Expired - Fee Related
- 2013-03-21 IN IN2008MUN2014 patent/IN2014MN02008A/en unknown
-
2015
- 2015-02-27 US US14/634,364 patent/US9618391B2/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4110619A (en) * | 1975-11-21 | 1978-08-29 | H. Maihak Ag | Method of compensating for carrier-gas-composition dependence due to the collision-broadening effect in non-dispersive infrared photometers having a detector comprised of two absorption chambers arranged one behind the other |
| US4849636A (en) * | 1988-05-18 | 1989-07-18 | Mine Safety Appliances Company | Analyzer with compensation |
| US5900635A (en) * | 1995-09-29 | 1999-05-04 | Instrumentarium Oy | Correction of collision broadening in non-dispersive absorption measurement of gases |
Non-Patent Citations (2)
| Title |
|---|
| SEVERINGHAUS et al., "Correction Factors for Infrared Carbon Dioxide Pressure Broadening by Nitrogen, Nitrous Oxide and Cyclopropane", Anethesiology, American Society of Anesthesiology (1961), vol. 22 pages 429 - 432. * |
| TANG et al., "A New Calibration Method that Compensates for the Effects of O2 and N2 on Infrared CO2 Analysers", Journal of Clinical Monitoring and Computing (2006), vol. 20 pages 75-59. * |
Also Published As
| Publication number | Publication date |
|---|---|
| US9618391B2 (en) | 2017-04-11 |
| EP2828642A1 (en) | 2015-01-28 |
| US8976358B2 (en) | 2015-03-10 |
| CA2865649A1 (en) | 2013-09-26 |
| US20130250301A1 (en) | 2013-09-26 |
| CN104364635A (zh) | 2015-02-18 |
| AU2013234971A1 (en) | 2014-09-11 |
| CA2865649C (en) | 2017-07-18 |
| IN2014MN02008A (enExample) | 2015-08-07 |
| WO2013142737A1 (en) | 2013-09-26 |
| US20160011047A1 (en) | 2016-01-14 |
| CN104364635B (zh) | 2017-05-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FGA | Letters patent sealed or granted (standard patent) | ||
| MK14 | Patent ceased section 143(a) (annual fees not paid) or expired |