ATE416165T1 - Verfahren zur herstellung von 4-ä(di)alkylaminoü- pyridin-verbindungen - Google Patents
Verfahren zur herstellung von 4-ä(di)alkylaminoü- pyridin-verbindungenInfo
- Publication number
- ATE416165T1 ATE416165T1 AT03027035T AT03027035T ATE416165T1 AT E416165 T1 ATE416165 T1 AT E416165T1 AT 03027035 T AT03027035 T AT 03027035T AT 03027035 T AT03027035 T AT 03027035T AT E416165 T1 ATE416165 T1 AT E416165T1
- Authority
- AT
- Austria
- Prior art keywords
- substituted
- tertiary
- pyridine
- aminopyridine
- reacting
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title 1
- -1 4-substituted pyridine Chemical class 0.000 abstract 2
- 150000003927 aminopyridines Chemical class 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 abstract 2
- JUJWROOIHBZHMG-UHFFFAOYSA-N pyridine Substances C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 abstract 2
- 150000003222 pyridines Chemical class 0.000 abstract 2
- ICSNLGPSRYBMBD-UHFFFAOYSA-N 2-aminopyridine Chemical compound NC1=CC=CC=N1 ICSNLGPSRYBMBD-UHFFFAOYSA-N 0.000 abstract 1
- 230000003213 activating effect Effects 0.000 abstract 1
- 125000003277 amino group Chemical group 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 abstract 1
- 239000012429 reaction media Substances 0.000 abstract 1
- 125000000467 secondary amino group Chemical class [H]N([*:1])[*:2] 0.000 abstract 1
- 238000006467 substitution reaction Methods 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
- B01J37/0063—Granulating
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/72—Nitrogen atoms
- C07D213/73—Unsubstituted amino or imino radicals
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
- B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
- B01J31/0234—Nitrogen-, phosphorus-, arsenic- or antimony-containing compounds
- B01J31/0235—Nitrogen containing compounds
- B01J31/0237—Amines
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
- B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
- B01J31/0234—Nitrogen-, phosphorus-, arsenic- or antimony-containing compounds
- B01J31/0235—Nitrogen containing compounds
- B01J31/0244—Nitrogen containing compounds with nitrogen contained as ring member in aromatic compounds or moieties, e.g. pyridine
-
- B01J35/40—
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/72—Nitrogen atoms
- C07D213/74—Amino or imino radicals substituted by hydrocarbon or substituted hydrocarbon radicals
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/78—Carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, e.g. ester or nitrile radicals
- C07D213/84—Nitriles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2231/00—Catalytic reactions performed with catalysts classified in B01J31/00
- B01J2231/40—Substitution reactions at carbon centres, e.g. C-C or C-X, i.e. carbon-hetero atom, cross-coupling, C-H activation or ring-opening reactions
- B01J2231/42—Catalytic cross-coupling, i.e. connection of previously not connected C-atoms or C- and X-atoms without rearrangement
- B01J2231/4205—C-C cross-coupling, e.g. metal catalyzed or Friedel-Crafts type
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US5508697P | 1997-08-01 | 1997-08-01 | |
| US5447397P | 1997-08-01 | 1997-08-01 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE416165T1 true ATE416165T1 (de) | 2008-12-15 |
Family
ID=26733072
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT98938244T ATE289993T1 (de) | 1997-08-01 | 1998-07-31 | Supernukleophile in 4-stellung substituierte pyridinkatalysatoren und verfahren die nützlich zu deren herstellung sind |
| AT03027035T ATE416165T1 (de) | 1997-08-01 | 1998-07-31 | Verfahren zur herstellung von 4-ä(di)alkylaminoü- pyridin-verbindungen |
Family Applications Before (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT98938244T ATE289993T1 (de) | 1997-08-01 | 1998-07-31 | Supernukleophile in 4-stellung substituierte pyridinkatalysatoren und verfahren die nützlich zu deren herstellung sind |
Country Status (12)
| Country | Link |
|---|---|
| US (4) | US6369230B1 (de) |
| EP (1) | EP1012141B1 (de) |
| JP (2) | JP4150497B2 (de) |
| KR (1) | KR20010022497A (de) |
| CN (3) | CN1159104C (de) |
| AT (2) | ATE289993T1 (de) |
| AU (1) | AU8681498A (de) |
| CA (1) | CA2298821C (de) |
| DE (2) | DE69829188T2 (de) |
| ES (2) | ES2236927T3 (de) |
| TW (1) | TW580408B (de) |
| WO (1) | WO1999006370A1 (de) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6369230B1 (en) * | 1997-08-01 | 2002-04-09 | Reilly Industries, Inc. | Supernucleophilic 4-substituted-pyridine catalysts, and processes useful for preparing same |
| WO2000043363A1 (en) * | 1999-01-21 | 2000-07-27 | Reilly Industries, Inc. | Low-dusting, flowable aminopyridine products |
| US8075812B2 (en) | 2007-04-04 | 2011-12-13 | Sabic Innovative Plastics Ip B.V. | Method of separating a poly(arylene ether) composition from a solvent, and poly(arylene ether) composition prepared thereby |
| CN101845015B (zh) * | 2010-06-04 | 2012-09-05 | 安徽省郎溪县联科实业有限公司 | 一种4-二甲氨基吡啶的精制分离及干燥方法 |
| IT1400395B1 (it) * | 2010-06-08 | 2013-05-31 | Procos Spa | Processo one-pot per la sintesi di dalfampridine. |
| CN103787963A (zh) * | 2013-12-20 | 2014-05-14 | 安徽国星生物化学有限公司 | 高效制备4-二甲氨基吡啶 |
| CN110655489A (zh) * | 2019-11-11 | 2020-01-07 | 安徽瑞邦生物科技有限公司 | 一种挥发再结晶提纯4-氰基吡啶的方法 |
| CN111592488A (zh) * | 2019-11-18 | 2020-08-28 | 河南郑大嘉源环保技术有限公司 | 一种高效制备4-二甲氨基吡啶的方法 |
| CN111454201B (zh) * | 2020-04-15 | 2022-01-04 | 杭州瑞思新材料有限公司 | 一种制备高效酰化催化剂材料的新方法 |
| CN111320572B (zh) * | 2020-04-15 | 2021-07-23 | 杭州瑞思新材料有限公司 | 一种取代吡啶的制备方法 |
Family Cites Families (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3452018A (en) | 1966-08-29 | 1969-06-24 | American Home Prod | 1 - (2 - substituted - 6 - arylsulfonamidopyrimidin - 4 - yl)pyridinium hydroxide inner salts |
| US3509165A (en) | 1967-03-24 | 1970-04-28 | Us Agriculture | Process for preparing pyridinium betaines and derivatives |
| US4012437A (en) * | 1972-02-07 | 1977-03-15 | Rohm And Haas Company | Method of producing betaines, monomers and polymers containing betaine-type units and novel and useful copolymers thereby obtained |
| US4013437A (en) | 1975-05-15 | 1977-03-22 | Owens-Illinois, Inc. | Method for forming glass bottles |
| US4120859A (en) | 1977-01-27 | 1978-10-17 | Cilag-Chemie A.G. | (N-Substituted-pyridyl)-alkyl sulfonic acid betaines as electroplating additives |
| US4150232A (en) | 1977-07-15 | 1979-04-17 | Cilag-Chemie A.G. | 1-Carboxymethyl-3-sulfoloweralkyl pyridinium betaine inner salts |
| US4158093A (en) * | 1977-12-15 | 1979-06-12 | Reilly Tar & Chemical Corporation | Process for substituting and dequaternizing pyridylethyl quaternary salts of pyridine and bypyridine bases |
| EP0012192B1 (de) | 1978-12-08 | 1983-01-12 | Santrade Ltd. | Vorrichtung zum Auspressen von fliessfähigen Massen aus einem Behälter |
| US4287338A (en) | 1980-03-10 | 1981-09-01 | The Upjohn Company | Sulfooxy-pyrimidinium, -pyridinium, and -triazinium hydroxide inner salts |
| JPS5890580A (ja) * | 1981-09-11 | 1983-05-30 | レイリー・インダストリーズ・インコーポレーテッド | ４−（４′−メチルピペリジノ）ピリジン |
| DE3215451A1 (de) | 1982-04-24 | 1983-10-27 | Hoechst Ag, 6230 Frankfurt | Betain-aminoxide, verfahren zu ihrer herstellung und ihre verwendung als tenside |
| US4591625A (en) * | 1984-11-26 | 1986-05-27 | University Of Southern Mississippi | Monomer and polymers containing 4-aminopyridine |
| US4672121A (en) * | 1985-01-16 | 1987-06-09 | Nepera Chemical Co. | Preparation of 4-substituted pyridines using quaternary pyridine salts |
| US4772713A (en) | 1985-01-16 | 1988-09-20 | Nepera, Inc. | Quaternary pyridine salts useful for preparation of 4-substituted pyridines |
| US4882405A (en) * | 1985-12-30 | 1989-11-21 | Exxon Research And Engineering Company | Terpolymers of acrylamide, alkylacrylamide and betaine monomers |
| US4742135A (en) | 1985-12-30 | 1988-05-03 | Exxon Research And Engineering Company | Terpolymers of acrylamide, alkylacrylamide and betaine monomers |
| US5234918A (en) | 1988-04-04 | 1993-08-10 | American Cyanamid Company | Certain phosphinyl-oxy-phenyl-methyl-pyridinium-hydroxide inner salts useful as antagonists of PAF |
| DE4013349A1 (de) | 1990-04-23 | 1991-10-24 | Schering Ag | 1-(2-sulfoaethyl)pyridiniumbetain, verfahren zu dessen herstellung sowie saure nickelbaeder enthaltend diese verbindung |
| US5006628A (en) * | 1990-08-15 | 1991-04-09 | Eastman Kodak Company | Melt phase polyarylate process |
| US5359139A (en) | 1991-03-18 | 1994-10-25 | Albemarle Corporation | Tertiary amine treatment |
| US5136092A (en) | 1991-03-18 | 1992-08-04 | Ethyl Corporation | Process for treating tertiary amines |
| NL9101702A (nl) * | 1991-10-11 | 1993-05-03 | Dsm Nv | Uithardingskatalysator voor de reaktie tussen carboxyl-functionele polymeren en epoxyfunctionele verbindingen als basis van poedercoatings. |
| WO1993008150A1 (en) * | 1991-10-15 | 1993-04-29 | Indiana University Foundation | Hydrolyzing esters using 4-aminopyridyl siloxane catalysts |
| DE4211190A1 (de) * | 1992-04-03 | 1993-10-07 | Hoechst Ag | Verfahren zur Herstellung von wäßrigen Betainlösungen |
| US5245036A (en) * | 1992-05-07 | 1993-09-14 | Dowelanco | Process for the preparation of 4-phenoxyquinoline compounds |
| DE4232157A1 (de) | 1992-09-25 | 1994-03-31 | Hoechst Ag | Verfahren zur Herstellung von reinen wäßrigen Betainlösungen |
| US6369230B1 (en) * | 1997-08-01 | 2002-04-09 | Reilly Industries, Inc. | Supernucleophilic 4-substituted-pyridine catalysts, and processes useful for preparing same |
-
1998
- 1998-07-31 US US09/463,902 patent/US6369230B1/en not_active Expired - Lifetime
- 1998-07-31 US US09/127,542 patent/US6046336A/en not_active Expired - Lifetime
- 1998-07-31 DE DE69829188T patent/DE69829188T2/de not_active Expired - Lifetime
- 1998-07-31 CN CNB02130226XA patent/CN1159104C/zh not_active Expired - Lifetime
- 1998-07-31 CN CNB021302286A patent/CN1239484C/zh not_active Expired - Lifetime
- 1998-07-31 AT AT98938244T patent/ATE289993T1/de active
- 1998-07-31 JP JP2000505129A patent/JP4150497B2/ja not_active Expired - Fee Related
- 1998-07-31 DE DE69840305T patent/DE69840305D1/de not_active Expired - Lifetime
- 1998-07-31 CN CNB988095661A patent/CN1280274C/zh not_active Expired - Lifetime
- 1998-07-31 AU AU86814/98A patent/AU8681498A/en not_active Abandoned
- 1998-07-31 ES ES98938244T patent/ES2236927T3/es not_active Expired - Lifetime
- 1998-07-31 KR KR1020007001083A patent/KR20010022497A/ko not_active Application Discontinuation
- 1998-07-31 CA CA002298821A patent/CA2298821C/en not_active Expired - Lifetime
- 1998-07-31 EP EP98938244A patent/EP1012141B1/de not_active Expired - Lifetime
- 1998-07-31 WO PCT/US1998/016024 patent/WO1999006370A1/en active IP Right Grant
- 1998-07-31 AT AT03027035T patent/ATE416165T1/de active
- 1998-07-31 ES ES03027035T patent/ES2318083T3/es not_active Expired - Lifetime
- 1998-08-01 TW TW087112697A patent/TW580408B/zh not_active IP Right Cessation
-
2001
- 2001-11-06 US US09/993,046 patent/US6603010B2/en not_active Expired - Lifetime
-
2003
- 2003-04-29 US US10/425,504 patent/US6958400B2/en not_active Expired - Lifetime
-
2007
- 2007-08-03 JP JP2007202584A patent/JP2008030037A/ja active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| WO1999006370A1 (en) | 1999-02-11 |
| CN1159104C (zh) | 2004-07-28 |
| JP4150497B2 (ja) | 2008-09-17 |
| JP2008030037A (ja) | 2008-02-14 |
| US20030232995A1 (en) | 2003-12-18 |
| US20020165087A1 (en) | 2002-11-07 |
| EP1012141B1 (de) | 2005-03-02 |
| US6046336A (en) | 2000-04-04 |
| DE69829188T2 (de) | 2005-12-29 |
| JP2001512102A (ja) | 2001-08-21 |
| US6603010B2 (en) | 2003-08-05 |
| CA2298821A1 (en) | 1999-02-11 |
| ES2236927T3 (es) | 2005-07-16 |
| US6958400B2 (en) | 2005-10-25 |
| US6369230B1 (en) | 2002-04-09 |
| KR20010022497A (ko) | 2001-03-15 |
| CN1239484C (zh) | 2006-02-01 |
| TW580408B (en) | 2004-03-21 |
| ATE289993T1 (de) | 2005-03-15 |
| CN1491943A (zh) | 2004-04-28 |
| CN1404923A (zh) | 2003-03-26 |
| CN1280274C (zh) | 2006-10-18 |
| CA2298821C (en) | 2007-11-20 |
| AU8681498A (en) | 1999-02-22 |
| DE69840305D1 (de) | 2009-01-15 |
| DE69829188D1 (de) | 2005-04-07 |
| EP1012141A4 (de) | 2000-12-27 |
| EP1012141A1 (de) | 2000-06-28 |
| CN1271344A (zh) | 2000-10-25 |
| ES2318083T3 (es) | 2009-05-01 |
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| Date | Code | Title | Description |
|---|---|---|---|
| UEP | Publication of translation of european patent specification |
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