ATE250616T1 - Reinigung einer metallorganischen verbindung durch umkristallisieren - Google Patents
Reinigung einer metallorganischen verbindung durch umkristallisierenInfo
- Publication number
- ATE250616T1 ATE250616T1 AT00932537T AT00932537T ATE250616T1 AT E250616 T1 ATE250616 T1 AT E250616T1 AT 00932537 T AT00932537 T AT 00932537T AT 00932537 T AT00932537 T AT 00932537T AT E250616 T1 ATE250616 T1 AT E250616T1
- Authority
- AT
- Austria
- Prior art keywords
- recrystallization
- purification
- metal compound
- organic metal
- solvent
- Prior art date
Links
- 238000001953 recrystallisation Methods 0.000 title abstract 2
- 150000002736 metal compounds Chemical class 0.000 title 1
- 238000000746 purification Methods 0.000 title 1
- 150000002902 organometallic compounds Chemical class 0.000 abstract 3
- 239000002904 solvent Substances 0.000 abstract 3
- 238000001816 cooling Methods 0.000 abstract 2
- JLTRXTDYQLMHGR-UHFFFAOYSA-N trimethylaluminium Chemical compound C[Al](C)C JLTRXTDYQLMHGR-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F5/00—Compounds containing elements of Groups 3 or 13 of the Periodic Table
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F5/00—Compounds containing elements of Groups 3 or 13 of the Periodic Table
- C07F5/06—Aluminium compounds
- C07F5/061—Aluminium compounds with C-aluminium linkage
- C07F5/062—Al linked exclusively to C
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Laminated Bodies (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US13537699P | 1999-05-21 | 1999-05-21 | |
PCT/US2000/013566 WO2000071551A2 (en) | 1999-05-21 | 2000-05-17 | Purification of an organometallic compound by recrystallization |
Publications (1)
Publication Number | Publication Date |
---|---|
ATE250616T1 true ATE250616T1 (de) | 2003-10-15 |
Family
ID=22467824
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
AT00932537T ATE250616T1 (de) | 1999-05-21 | 2000-05-17 | Reinigung einer metallorganischen verbindung durch umkristallisieren |
Country Status (8)
Country | Link |
---|---|
US (1) | US6482968B1 (de) |
EP (1) | EP1259516B1 (de) |
JP (1) | JP2003518007A (de) |
KR (1) | KR20020005751A (de) |
AT (1) | ATE250616T1 (de) |
DE (1) | DE60005565T2 (de) |
TW (1) | TW593325B (de) |
WO (1) | WO2000071551A2 (de) |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1624851B1 (de) * | 2003-05-16 | 2014-05-28 | Dow Corning Corporation | Haarpflegende anwendungen vom emulsionen, die elastomere silane oder siloxane mit stickstoffatomen enthalten |
JP2006001896A (ja) * | 2004-06-18 | 2006-01-05 | Shin Etsu Chem Co Ltd | 高純度トリメチルアルミニウム及びトリメチルアルミニウムの精製方法 |
JP4488186B2 (ja) | 2004-06-18 | 2010-06-23 | 信越化学工業株式会社 | トリメチルアルミニウムの精製方法 |
JP4470682B2 (ja) * | 2004-10-13 | 2010-06-02 | 住友化学株式会社 | トリメチルガリウムの製造方法 |
JP2006290889A (ja) * | 2005-04-12 | 2006-10-26 | Rohm & Haas Electronic Materials Llc | 金属含有化合物精製 |
JP2008024617A (ja) * | 2006-07-19 | 2008-02-07 | Ube Ind Ltd | 高純度トリアルキルアルミニウム及びその製法 |
CN118406074B (zh) * | 2024-07-03 | 2024-09-06 | 安徽亚格盛电子新材料股份有限公司 | 一种三甲基铝粗品的提纯方法 |
Family Cites Families (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3326954A (en) * | 1962-07-12 | 1967-06-20 | Ethyl Corp | Separation of aluminum alkyl compounds |
FR1595766A (de) * | 1967-12-08 | 1970-06-15 | ||
US4013421A (en) | 1974-12-30 | 1977-03-22 | Khachik Saakovich Bagdasarov | Apparatus for growing single crystals of high-melting oxides |
US4362560A (en) | 1980-11-28 | 1982-12-07 | Abrjutin Vladimir N | Process for producing high-purity gallium |
GB2123423B (en) | 1982-06-29 | 1985-11-27 | Secr Defence | Purification of trialkyl gallium |
EP0116319B1 (de) | 1983-02-09 | 1989-04-12 | Sumitomo Chemical Company, Limited | Verfahren zur Herstellung von sehr reinen Metallverbindungen |
US4720561A (en) | 1984-03-26 | 1988-01-19 | The Secretary Of State For Defence In Her Britannic Majesty's Government Of The United Kingdom Of Great Britain And Northern Ireland | Preparation of metal alkyls |
JPS62132888A (ja) | 1985-12-03 | 1987-06-16 | Sumitomo Chem Co Ltd | 有機金属化合物の精製方法 |
US4847399A (en) | 1987-01-23 | 1989-07-11 | Morton Thiokol, Inc. | Process for preparing or purifying Group III-A organometallic compounds |
GB2201418B (en) | 1987-02-27 | 1990-10-24 | Plessey Co Plc | Preparation of metal alkyls |
TW217415B (de) | 1991-11-19 | 1993-12-11 | Shell Internat Res Schappej B V | |
DE69421249T2 (de) | 1993-12-14 | 2000-07-13 | Sumitomo Chemical Co., Ltd. | Verfahren zur Entfernung von Sauerstoff-enthaltenden Verunreinigungen aus Organo-Gallium oder -Indium Verbindungen |
JP3221237B2 (ja) | 1994-06-30 | 2001-10-22 | 住友化学工業株式会社 | 有機金属化合物の精製方法 |
JP3525371B2 (ja) | 1996-06-25 | 2004-05-10 | 信越化学工業株式会社 | 有機金属化合物の精製方法 |
-
2000
- 2000-05-17 DE DE60005565T patent/DE60005565T2/de not_active Expired - Fee Related
- 2000-05-17 WO PCT/US2000/013566 patent/WO2000071551A2/en not_active Application Discontinuation
- 2000-05-17 AT AT00932537T patent/ATE250616T1/de not_active IP Right Cessation
- 2000-05-17 EP EP00932537A patent/EP1259516B1/de not_active Revoked
- 2000-05-17 JP JP2000619807A patent/JP2003518007A/ja active Pending
- 2000-05-17 US US09/980,044 patent/US6482968B1/en not_active Expired - Fee Related
- 2000-05-17 KR KR1020017014782A patent/KR20020005751A/ko not_active Application Discontinuation
- 2000-05-20 TW TW089109876A patent/TW593325B/zh not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
DE60005565D1 (de) | 2003-10-30 |
WO2000071551A2 (en) | 2000-11-30 |
US6482968B1 (en) | 2002-11-19 |
KR20020005751A (ko) | 2002-01-17 |
TW593325B (en) | 2004-06-21 |
WO2000071551A3 (en) | 2002-09-12 |
EP1259516B1 (de) | 2003-09-24 |
JP2003518007A (ja) | 2003-06-03 |
EP1259516A2 (de) | 2002-11-27 |
DE60005565T2 (de) | 2004-06-24 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
RER | Ceased as to paragraph 5 lit. 3 law introducing patent treaties |