ATE224904T1 - Herstellung von spirobis-phosphiten aus feingemahlenem pentaerythritol - Google Patents
Herstellung von spirobis-phosphiten aus feingemahlenem pentaerythritolInfo
- Publication number
- ATE224904T1 ATE224904T1 AT99912952T AT99912952T ATE224904T1 AT E224904 T1 ATE224904 T1 AT E224904T1 AT 99912952 T AT99912952 T AT 99912952T AT 99912952 T AT99912952 T AT 99912952T AT E224904 T1 ATE224904 T1 AT E224904T1
- Authority
- AT
- Austria
- Prior art keywords
- pentaerythritol
- particle size
- phosphites
- spirobis
- production
- Prior art date
Links
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 title abstract 6
- AQSJGOWTSHOLKH-UHFFFAOYSA-N phosphite(3-) Chemical compound [O-]P([O-])[O-] AQSJGOWTSHOLKH-UHFFFAOYSA-N 0.000 title 1
- 238000000034 method Methods 0.000 abstract 4
- 239000002245 particle Substances 0.000 abstract 4
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 abstract 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 abstract 3
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 abstract 2
- 229910052739 hydrogen Inorganic materials 0.000 abstract 2
- 239000001257 hydrogen Substances 0.000 abstract 2
- 125000004435 hydrogen atom Chemical group [H]* 0.000 abstract 2
- 239000002904 solvent Substances 0.000 abstract 2
- 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 abstract 2
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- BHEPBYXIRTUNPN-UHFFFAOYSA-N hydridophosphorus(.) (triplet) Chemical compound [PH] BHEPBYXIRTUNPN-UHFFFAOYSA-N 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- TVMXDCGIABBOFY-UHFFFAOYSA-N octane Chemical compound CCCCCCCC TVMXDCGIABBOFY-UHFFFAOYSA-N 0.000 abstract 1
- 150000002989 phenols Chemical class 0.000 abstract 1
- 150000008301 phosphite esters Chemical class 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
- 230000035484 reaction time Effects 0.000 abstract 1
- 239000008096 xylene Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
- C07F9/6564—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms
- C07F9/6571—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms having phosphorus and oxygen atoms as the only ring hetero atoms
- C07F9/6574—Esters of oxyacids of phosphorus
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
- C07F9/6564—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms
- C07F9/6571—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms having phosphorus and oxygen atoms as the only ring hetero atoms
- C07F9/6574—Esters of oxyacids of phosphorus
- C07F9/65746—Esters of oxyacids of phosphorus the molecule containing more than one cyclic phosphorus atom
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US09/061,292 US5917076A (en) | 1998-04-16 | 1998-04-16 | Process for the preparation of spiro bis-phosphites using finely ground pentaerythritol |
| PCT/US1999/007054 WO1999052916A1 (en) | 1998-04-16 | 1999-03-30 | Preparation of spiro bis-phosphites using finely ground pentaerythritol |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE224904T1 true ATE224904T1 (de) | 2002-10-15 |
Family
ID=22034839
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT99912952T ATE224904T1 (de) | 1998-04-16 | 1999-03-30 | Herstellung von spirobis-phosphiten aus feingemahlenem pentaerythritol |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US5917076A (de) |
| EP (1) | EP1071688B1 (de) |
| JP (1) | JP4542265B2 (de) |
| KR (1) | KR100622745B1 (de) |
| AT (1) | ATE224904T1 (de) |
| DE (1) | DE69903145T2 (de) |
| ES (1) | ES2184425T3 (de) |
| WO (1) | WO1999052916A1 (de) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100430407C (zh) * | 2005-06-22 | 2008-11-05 | 中国石油化工股份有限公司 | 二-2,4-二枯基苯基季戊四醇双亚磷酸酯的制备方法 |
| CN100460410C (zh) * | 2005-06-22 | 2009-02-11 | 中国石油化工股份有限公司 | 制备二-2,4-二枯基苯基季戊四醇双亚磷酸酯的方法 |
| TWI503326B (zh) * | 2014-05-14 | 2015-10-11 | Chitec Technology Co Ltd | 螺環雙亞磷酸酯系化合物及其應用 |
Family Cites Families (47)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3056823A (en) * | 1956-05-31 | 1962-10-02 | Hooker Chemical Corp | Transesterification process for making trialiphatic phosphite esters |
| US3281381A (en) * | 1958-06-17 | 1966-10-25 | Hooker Chemical Corp | Reaction products of pentaerythritol and phosphites as vinyl chloride stabilizer |
| US3039993A (en) * | 1960-05-10 | 1962-06-19 | Weston Chemical Corp | Polyethylene stabilizers |
| GB951670A (en) * | 1961-05-23 | 1964-03-11 | Boyer & Cie Sa | Process for the preparation of tetraesters of penta-erythritol |
| US3281506A (en) * | 1962-08-31 | 1966-10-25 | Hooker Chemical Corp | Secondary phosphites and process for manufacture thereof |
| US3415906A (en) * | 1964-05-29 | 1968-12-10 | Hooker Chemical Corp | Phosphite phospholane and phosphorinane compounds |
| US3342767A (en) * | 1964-06-10 | 1967-09-19 | Ferro Corp | Vinyl chloride resins containing cyclic phosphites |
| US3305526A (en) * | 1964-07-07 | 1967-02-21 | Weston Chemical Corp | Phenoxy phosphite polymers |
| US3467733A (en) * | 1965-11-26 | 1969-09-16 | Hooker Chemical Corp | Cyclic esters of phosphorus and a process for the preparation thereof |
| US3488407A (en) * | 1965-11-26 | 1970-01-06 | Hooker Chemical Corp | Cyclic esters of phosphorus |
| US3441633A (en) * | 1965-12-03 | 1969-04-29 | Weston Chemical Corp | Cyclic phosphites |
| US3558554A (en) * | 1966-06-09 | 1971-01-26 | Yoshitomi Pharmaceutical | Oxidatively stable polyolefin composition |
| US3482002A (en) * | 1966-07-27 | 1969-12-02 | Hooker Chemical Corp | Phosphorus acid-carboxylic acid anhydrides |
| US3845168A (en) * | 1970-01-16 | 1974-10-29 | Weston Chemical Corp | Trimethylol propane phosphite |
| US4024049A (en) * | 1975-01-07 | 1977-05-17 | Nalco Chemical Company | Mono and di organophosphite esters as crude oil antifoulants |
| NL7506988A (nl) * | 1975-06-12 | 1976-12-14 | Akzo Nv | Organische trifosfieten met verbeterde hydrolyti- sche stabiliteit. |
| US4067903A (en) * | 1975-10-04 | 1978-01-10 | Basf Aktiengesellschaft | Manufacture of arylamines |
| EP0000757B1 (de) * | 1977-08-08 | 1981-08-05 | Ciba-Geigy Ag | Verfahren zur Herstellung von Triarylphosphiten |
| US4440696A (en) * | 1977-08-08 | 1984-04-03 | Ciba-Geigy Corporation | Process for producing triarylphosphites |
| US4492661A (en) * | 1977-08-08 | 1985-01-08 | Ciba-Geigy Corporation | Process for producing triarylphosphites |
| US4196117A (en) * | 1978-01-03 | 1980-04-01 | Ciba-Geigy Corporation | Alkylated 1,1'-biphenyl-2,2'-diyl phosphites and stabilized compositions |
| US4276233A (en) * | 1978-11-02 | 1981-06-30 | General Electric Company | Hindered phenol phosphites |
| US4237075A (en) * | 1979-06-05 | 1980-12-02 | Mobil Oil Corporation | Formamide catalysts for reacting phosphorus halides with thiols |
| US4322530A (en) * | 1980-02-22 | 1982-03-30 | W. R. Grace & Co. | Alkylation of polyamines |
| JPS56152863A (en) * | 1980-04-28 | 1981-11-26 | Adeka Argus Chem Co Ltd | Synthetic resin composition |
| US4407765A (en) * | 1980-07-02 | 1983-10-04 | Stauffer Chemical Company | Synthesis of organic phosphate-phosphonates |
| DE3025377C2 (de) * | 1980-07-04 | 1983-06-23 | Bayer Ag, 5090 Leverkusen | Verfahren zur Herstellung von Benzolphosphonsäurediphenylester |
| US4318845A (en) * | 1980-11-24 | 1982-03-09 | Ciba-Geigy Corporation | Alkanolamine esters of 1,1'-biphenyl-2,2'-diyl-and alkylidene-1,1'-biphenyl-2,2'-diyl-cyclic phosphites |
| JPS60231687A (ja) * | 1984-04-17 | 1985-11-18 | チバ‐ガイギー アクチエンゲゼルシヤフト | ペンタエリスリトール亜燐酸エステルの製造方法 |
| DE3566260D1 (en) * | 1984-04-17 | 1988-12-22 | Ciba Geigy Ag | Process for preparing cyclic phosphorous-acid esters |
| US4656302A (en) * | 1985-03-08 | 1987-04-07 | Koppers Company, Inc. | Tris-(3-hydroxy-4,6-di-t-alkylphenyl) phosphites |
| JPS61225191A (ja) * | 1985-03-29 | 1986-10-06 | Adeka Argus Chem Co Ltd | ジアリ−ルペンタエリスリト−ルジホスフアイトの製造方法 |
| US4705879A (en) * | 1986-01-13 | 1987-11-10 | Koppers Company, Inc. | Long-chain alkylresorcinol phosphites |
| US4724056A (en) * | 1987-03-05 | 1988-02-09 | Stauffer Chemical Company | Pollution-free process for making trialkyl phosphites |
| US4786329A (en) * | 1987-09-09 | 1988-11-22 | The Dow Chemical Company | Asphalt compositions containing anti-stripping additives prepared from amines or polyamines and phosphonates |
| US4894481A (en) * | 1988-07-05 | 1990-01-16 | Ethyl Corporation | Method of making cyclic aryl chlorophosphites |
| AU3788189A (en) * | 1988-07-25 | 1990-01-25 | Borg-Warner Specialty Chemicals, Inc. | 3, 9-diphosphaspiroundecanes and process for making3, 9-diphosphaspiroundecanes |
| US4882374A (en) * | 1989-02-06 | 1989-11-21 | Eastman Kodak Company | Dioxaphosphorinane compounds and polyolefin compositions sabilized therewith |
| US5235086A (en) * | 1989-08-15 | 1993-08-10 | Ciba-Geigy Corporation | Process for the preparation of tris(2,4-ditert-butylphenyl)phosphite |
| US5254709A (en) * | 1989-12-08 | 1993-10-19 | Uniroyal Chemical Company, Inc. | Method for preparing stearically hindered aryl phosphites |
| DE3942787A1 (de) * | 1989-12-23 | 1991-06-27 | Hoechst Ag | Verfahren zur herstellung hydrolysestabiler organischer phosphite |
| US5141975A (en) * | 1991-06-07 | 1992-08-25 | General Electric Company | Thermoplastic compositions containing hydrolytically stable phosphites |
| ATE203044T1 (de) * | 1992-10-05 | 2001-07-15 | Ciba Sc Holding Ag | Verfahren zur stabilisierung dreiwertiger phosphorverbindungen mit aminen |
| EP0635514B1 (de) * | 1993-07-22 | 1999-05-12 | General Electric Company | Neo-Diol Phosphite als Polymer-Stabilisatoren |
| US5438086A (en) * | 1993-08-30 | 1995-08-01 | Stevenson; Donald R. | Hydrolytically stable pentaerythritol diphosphites |
| US5468895A (en) * | 1994-10-19 | 1995-11-21 | General Electric Company | Amine stabilized amorphous phosphite |
| US5919966A (en) * | 1998-03-26 | 1999-07-06 | General Electric Company | Process for the preparation of spiro bis-phosphites |
-
1998
- 1998-04-16 US US09/061,292 patent/US5917076A/en not_active Expired - Lifetime
-
1999
- 1999-03-30 ES ES99912952T patent/ES2184425T3/es not_active Expired - Lifetime
- 1999-03-30 WO PCT/US1999/007054 patent/WO1999052916A1/en active IP Right Grant
- 1999-03-30 AT AT99912952T patent/ATE224904T1/de not_active IP Right Cessation
- 1999-03-30 KR KR1020007011449A patent/KR100622745B1/ko not_active IP Right Cessation
- 1999-03-30 JP JP2000543472A patent/JP4542265B2/ja not_active Expired - Fee Related
- 1999-03-30 DE DE69903145T patent/DE69903145T2/de not_active Expired - Lifetime
- 1999-03-30 EP EP99912952A patent/EP1071688B1/de not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| US5917076A (en) | 1999-06-29 |
| JP2002511474A (ja) | 2002-04-16 |
| KR20010042726A (ko) | 2001-05-25 |
| WO1999052916A1 (en) | 1999-10-21 |
| DE69903145T2 (de) | 2003-05-08 |
| KR100622745B1 (ko) | 2006-09-13 |
| EP1071688A1 (de) | 2001-01-31 |
| JP4542265B2 (ja) | 2010-09-08 |
| EP1071688B1 (de) | 2002-09-25 |
| ES2184425T3 (es) | 2003-04-01 |
| DE69903145D1 (de) | 2002-10-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| RER | Ceased as to paragraph 5 lit. 3 law introducing patent treaties |