ATE269346T1 - Verfahren zur herstellung von spirobisphosphiten - Google Patents
Verfahren zur herstellung von spirobisphosphitenInfo
- Publication number
- ATE269346T1 ATE269346T1 AT99911278T AT99911278T ATE269346T1 AT E269346 T1 ATE269346 T1 AT E269346T1 AT 99911278 T AT99911278 T AT 99911278T AT 99911278 T AT99911278 T AT 99911278T AT E269346 T1 ATE269346 T1 AT E269346T1
- Authority
- AT
- Austria
- Prior art keywords
- producing
- vacuum
- spirobisphosphites
- bis
- mixture
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title 1
- 238000000034 method Methods 0.000 abstract 3
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 abstract 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 abstract 1
- 229910052753 mercury Inorganic materials 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 abstract 1
- 150000002989 phenols Chemical class 0.000 abstract 1
- 150000008301 phosphite esters Chemical class 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
- 125000003003 spiro group Chemical group 0.000 abstract 1
- 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
- C07F9/6564—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms
- C07F9/6571—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms having phosphorus and oxygen atoms as the only ring hetero atoms
- C07F9/6574—Esters of oxyacids of phosphorus
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
- C07F9/6564—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms
- C07F9/6571—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms having phosphorus and oxygen atoms as the only ring hetero atoms
- C07F9/6574—Esters of oxyacids of phosphorus
- C07F9/65746—Esters of oxyacids of phosphorus the molecule containing more than one cyclic phosphorus atom
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US09/048,369 US5919966A (en) | 1998-03-26 | 1998-03-26 | Process for the preparation of spiro bis-phosphites |
| PCT/US1999/005206 WO1999048900A1 (en) | 1998-03-26 | 1999-03-10 | Process for the preparation of spiro bisphosphites |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE269346T1 true ATE269346T1 (de) | 2004-07-15 |
Family
ID=21954204
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT99911278T ATE269346T1 (de) | 1998-03-26 | 1999-03-10 | Verfahren zur herstellung von spirobisphosphiten |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US5919966A (de) |
| EP (1) | EP1066299B1 (de) |
| JP (1) | JP4272814B2 (de) |
| KR (1) | KR100622744B1 (de) |
| AT (1) | ATE269346T1 (de) |
| DE (1) | DE69918077T2 (de) |
| ES (1) | ES2221369T3 (de) |
| WO (1) | WO1999048900A1 (de) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5917076A (en) * | 1998-04-16 | 1999-06-29 | General Electric Company | Process for the preparation of spiro bis-phosphites using finely ground pentaerythritol |
| US6426429B1 (en) | 2000-08-11 | 2002-07-30 | General Electric Company | Process for the preparation of hindered phosphites |
| US7442732B2 (en) * | 2005-03-29 | 2008-10-28 | Crompton Corporation | Hindered amine light stabilizers comprising neoalkanediol phosphites |
| CN1948321B (zh) * | 2005-10-11 | 2010-04-28 | 上海化学试剂研究所 | 双（2,4－二枯基苯基）季戊四醇双亚磷酸酯的制备方法 |
| CN102549004A (zh) * | 2009-10-01 | 2012-07-04 | 大八化学工业株式会社 | 环状亚烷基磷卤化物及环状磷酸酯的制造方法 |
| KR102684992B1 (ko) | 2018-10-11 | 2024-07-16 | 에스케이온 주식회사 | 리튬 이차전지 전해액 및 이를 포함하는 리튬 이차전지 |
| CN111606953A (zh) * | 2020-07-02 | 2020-09-01 | 浙江万盛股份有限公司 | 一种季戊四醇型双磷酸酯的制备方法 |
Family Cites Families (45)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3056823A (en) * | 1956-05-31 | 1962-10-02 | Hooker Chemical Corp | Transesterification process for making trialiphatic phosphite esters |
| US3281381A (en) * | 1958-06-17 | 1966-10-25 | Hooker Chemical Corp | Reaction products of pentaerythritol and phosphites as vinyl chloride stabilizer |
| US3039993A (en) * | 1960-05-10 | 1962-06-19 | Weston Chemical Corp | Polyethylene stabilizers |
| US3281506A (en) * | 1962-08-31 | 1966-10-25 | Hooker Chemical Corp | Secondary phosphites and process for manufacture thereof |
| US3364285A (en) * | 1963-05-18 | 1968-01-16 | Agfa Ag | Process for the production of spirocyclic phosphoric acid esters |
| US3415906A (en) * | 1964-05-29 | 1968-12-10 | Hooker Chemical Corp | Phosphite phospholane and phosphorinane compounds |
| US3342767A (en) * | 1964-06-10 | 1967-09-19 | Ferro Corp | Vinyl chloride resins containing cyclic phosphites |
| US3305526A (en) * | 1964-07-07 | 1967-02-21 | Weston Chemical Corp | Phenoxy phosphite polymers |
| US3467733A (en) * | 1965-11-26 | 1969-09-16 | Hooker Chemical Corp | Cyclic esters of phosphorus and a process for the preparation thereof |
| US3488407A (en) * | 1965-11-26 | 1970-01-06 | Hooker Chemical Corp | Cyclic esters of phosphorus |
| US3441633A (en) * | 1965-12-03 | 1969-04-29 | Weston Chemical Corp | Cyclic phosphites |
| US3558554A (en) * | 1966-06-09 | 1971-01-26 | Yoshitomi Pharmaceutical | Oxidatively stable polyolefin composition |
| US3482002A (en) * | 1966-07-27 | 1969-12-02 | Hooker Chemical Corp | Phosphorus acid-carboxylic acid anhydrides |
| US3714302A (en) * | 1969-07-08 | 1973-01-30 | Borg Warner | Preparation of neoalkyl phenyl phosphite |
| US3845168A (en) * | 1970-01-16 | 1974-10-29 | Weston Chemical Corp | Trimethylol propane phosphite |
| US4024049A (en) * | 1975-01-07 | 1977-05-17 | Nalco Chemical Company | Mono and di organophosphite esters as crude oil antifoulants |
| NL7506988A (nl) * | 1975-06-12 | 1976-12-14 | Akzo Nv | Organische trifosfieten met verbeterde hydrolyti- sche stabiliteit. |
| US4067903A (en) * | 1975-10-04 | 1978-01-10 | Basf Aktiengesellschaft | Manufacture of arylamines |
| DE2860898D1 (en) * | 1977-08-08 | 1981-11-05 | Ciba Geigy Ag | Process for the preparation of triarylphosphites |
| US4492661A (en) * | 1977-08-08 | 1985-01-08 | Ciba-Geigy Corporation | Process for producing triarylphosphites |
| US4440696A (en) * | 1977-08-08 | 1984-04-03 | Ciba-Geigy Corporation | Process for producing triarylphosphites |
| US4196117A (en) * | 1978-01-03 | 1980-04-01 | Ciba-Geigy Corporation | Alkylated 1,1'-biphenyl-2,2'-diyl phosphites and stabilized compositions |
| US4276233A (en) * | 1978-11-02 | 1981-06-30 | General Electric Company | Hindered phenol phosphites |
| CA1136152A (en) * | 1979-02-05 | 1982-11-23 | Ingenuin Hechenbleikner | Process for preparing aromatic polyphosphites |
| US4237075A (en) * | 1979-06-05 | 1980-12-02 | Mobil Oil Corporation | Formamide catalysts for reacting phosphorus halides with thiols |
| US4322530A (en) * | 1980-02-22 | 1982-03-30 | W. R. Grace & Co. | Alkylation of polyamines |
| JPS56152863A (en) * | 1980-04-28 | 1981-11-26 | Adeka Argus Chem Co Ltd | Synthetic resin composition |
| US4407765A (en) * | 1980-07-02 | 1983-10-04 | Stauffer Chemical Company | Synthesis of organic phosphate-phosphonates |
| DE3025377C2 (de) * | 1980-07-04 | 1983-06-23 | Bayer Ag, 5090 Leverkusen | Verfahren zur Herstellung von Benzolphosphonsäurediphenylester |
| US4318845A (en) * | 1980-11-24 | 1982-03-09 | Ciba-Geigy Corporation | Alkanolamine esters of 1,1'-biphenyl-2,2'-diyl-and alkylidene-1,1'-biphenyl-2,2'-diyl-cyclic phosphites |
| US4656302A (en) * | 1985-03-08 | 1987-04-07 | Koppers Company, Inc. | Tris-(3-hydroxy-4,6-di-t-alkylphenyl) phosphites |
| US4705879A (en) * | 1986-01-13 | 1987-11-10 | Koppers Company, Inc. | Long-chain alkylresorcinol phosphites |
| US4724056A (en) * | 1987-03-05 | 1988-02-09 | Stauffer Chemical Company | Pollution-free process for making trialkyl phosphites |
| US4786329A (en) * | 1987-09-09 | 1988-11-22 | The Dow Chemical Company | Asphalt compositions containing anti-stripping additives prepared from amines or polyamines and phosphonates |
| US4894481A (en) * | 1988-07-05 | 1990-01-16 | Ethyl Corporation | Method of making cyclic aryl chlorophosphites |
| US4882374A (en) * | 1989-02-06 | 1989-11-21 | Eastman Kodak Company | Dioxaphosphorinane compounds and polyolefin compositions sabilized therewith |
| US5235086A (en) * | 1989-08-15 | 1993-08-10 | Ciba-Geigy Corporation | Process for the preparation of tris(2,4-ditert-butylphenyl)phosphite |
| US5254709A (en) * | 1989-12-08 | 1993-10-19 | Uniroyal Chemical Company, Inc. | Method for preparing stearically hindered aryl phosphites |
| DE3942787A1 (de) * | 1989-12-23 | 1991-06-27 | Hoechst Ag | Verfahren zur herstellung hydrolysestabiler organischer phosphite |
| US5141975A (en) * | 1991-06-07 | 1992-08-25 | General Electric Company | Thermoplastic compositions containing hydrolytically stable phosphites |
| EP0592364B1 (de) * | 1992-10-05 | 2001-07-11 | Ciba SC Holding AG | Verfahren zur Stabilisierung dreiwertiger Phosphorverbindungen mit Aminen |
| ES2131162T3 (es) * | 1993-07-22 | 1999-07-16 | Gen Electric | Neodiolfosfitos como estabilizadores de polimeros. |
| AU7015294A (en) * | 1993-08-30 | 1995-03-22 | Dover Chemical Corporation | Hydrolytically stable pentaerythritol diphosphites |
| EP0702019A1 (de) * | 1994-09-16 | 1996-03-20 | General Electric Company | Flüssige Neo-Diol Phosphite als Polymer-Stabilisatoren |
| US5468895A (en) * | 1994-10-19 | 1995-11-21 | General Electric Company | Amine stabilized amorphous phosphite |
-
1998
- 1998-03-26 US US09/048,369 patent/US5919966A/en not_active Expired - Lifetime
-
1999
- 1999-03-10 JP JP2000537883A patent/JP4272814B2/ja not_active Expired - Fee Related
- 1999-03-10 KR KR1020007010619A patent/KR100622744B1/ko not_active IP Right Cessation
- 1999-03-10 WO PCT/US1999/005206 patent/WO1999048900A1/en active IP Right Grant
- 1999-03-10 AT AT99911278T patent/ATE269346T1/de not_active IP Right Cessation
- 1999-03-10 DE DE69918077T patent/DE69918077T2/de not_active Expired - Lifetime
- 1999-03-10 ES ES99911278T patent/ES2221369T3/es not_active Expired - Lifetime
- 1999-03-10 EP EP99911278A patent/EP1066299B1/de not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| DE69918077T2 (de) | 2004-10-14 |
| JP2002507620A (ja) | 2002-03-12 |
| ES2221369T3 (es) | 2004-12-16 |
| EP1066299A1 (de) | 2001-01-10 |
| JP4272814B2 (ja) | 2009-06-03 |
| KR20010034667A (ko) | 2001-04-25 |
| KR100622744B1 (ko) | 2006-09-13 |
| US5919966A (en) | 1999-07-06 |
| WO1999048900A1 (en) | 1999-09-30 |
| EP1066299B1 (de) | 2004-06-16 |
| DE69918077D1 (de) | 2004-07-22 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| RER | Ceased as to paragraph 5 lit. 3 law introducing patent treaties |