AT85948B - Process for the production of condensation products from coal tar and formaldehyde. - Google Patents
Process for the production of condensation products from coal tar and formaldehyde.Info
- Publication number
- AT85948B AT85948B AT85948DA AT85948B AT 85948 B AT85948 B AT 85948B AT 85948D A AT85948D A AT 85948DA AT 85948 B AT85948 B AT 85948B
- Authority
- AT
- Austria
- Prior art keywords
- coal tar
- formaldehyde
- condensation products
- production
- paraformaldehyde
- Prior art date
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
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Verfahren zur Herstellung von Kondensationsprodukten aus Steinkohlenteer und Formaldehyd.
Die Herstellung von Kondensationsprodukten aus Holzteer und. Formaldehyd ist bekannt.
Es ist aber bisher unbekannt, dass auch Steinkohlenteer bei entsprechender Behandlung'mit Formaldehyd Kondensationsprodukte gibt, die hellbraune, geruchlose Pulver darstellen, welche die therapeutisch wertvollen Eigenschaften des Steinkohlenteers besitzen.
Diese neuen Produkte sind in Alkali, Seife und Alkohol löslich.
Das neue Verfahren besteht darin, dass Steinkohlenteer mit Formalin oder Paraformaldehyd zweckmässig in Gegenwart eines Kondensationsmittels, wie H Cl oder Alkalilauge erwärmt wird, bis die Masse zähflüssig wird und beim Erkalten erstarrt. Durch Auflösen in Natronlauge und Ausfällen mit Salzsäure wird das Produkt gereinigt und in zarten hellbraunen Flocken erhalten, Beispiel li
So kg Steinkohlenteer werden mit 1 : 5 kg Paraformaldehyd auf dem Wasserbad erwärmt bis die Masse zähflüssig ist und beim Erkalten erstarrt. Hierauf wird in Alkalilauge gelöst in Wasser gegossen und mit Salzsäure gefällt.
Beispiel II.
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**WARNUNG** Ende DESC Feld kannt Anfang CLMS uberlappen**.
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Process for the production of condensation products from coal tar and formaldehyde.
The manufacture of condensation products from wood tar and. Formaldehyde is known.
However, it is hitherto unknown that coal tar, when appropriately treated with formaldehyde, also gives condensation products which are light brown, odorless powders which have the therapeutically valuable properties of coal tar.
These new products are soluble in alkali, soap and alcohol.
The new process consists in heating coal tar with formalin or paraformaldehyde in the presence of a condensing agent such as H Cl or alkali until the mass becomes viscous and solidifies when it cools. The product is purified by dissolving it in sodium hydroxide solution and precipitating it with hydrochloric acid and obtained in delicate light brown flakes, example left
So kg of coal tar are heated with 1: 5 kg of paraformaldehyde on a water bath until the mass is viscous and solidifies when it cools. It is then dissolved in alkali, poured into water and precipitated with hydrochloric acid.
Example II.
EMI1.1
** WARNING ** End of DESC field may overlap beginning of CLMS **.
Claims (1)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
AT85948T | 1920-02-07 |
Publications (1)
Publication Number | Publication Date |
---|---|
AT85948B true AT85948B (en) | 1921-10-25 |
Family
ID=3606894
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
AT85948D AT85948B (en) | 1920-02-07 | 1920-02-07 | Process for the production of condensation products from coal tar and formaldehyde. |
Country Status (1)
Country | Link |
---|---|
AT (1) | AT85948B (en) |
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1920
- 1920-02-07 AT AT85948D patent/AT85948B/en active
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