AT65917B - Process for the production of camphor from borneol or isoborneol. - Google Patents

Process for the production of camphor from borneol or isoborneol.

Info

Publication number
AT65917B
AT65917B AT65917DA AT65917B AT 65917 B AT65917 B AT 65917B AT 65917D A AT65917D A AT 65917DA AT 65917 B AT65917 B AT 65917B
Authority
AT
Austria
Prior art keywords
sep
camphor
isoborneol
borneol
production
Prior art date
Application number
Other languages
German (de)
Original Assignee
C Ruder & Co Dr
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by C Ruder & Co Dr filed Critical C Ruder & Co Dr
Application granted granted Critical
Publication of AT65917B publication Critical patent/AT65917B/en

Links

Description

  

   <Desc/Clms Page number 1> 
 
 EMI1.1 
 
 EMI1.2 
 

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 EMI2.1 
 
<tb> 
<tb> Bei <SEP> Beginn <SEP> ................ <SEP> 1 <SEP> cm3 <SEP> Benzol,
<tb> nach <SEP> einer <SEP> Stunde <SEP> .............. <SEP> 1 <SEP> ,, <SEP> ,,
<tb> ,, <SEP> weiteren. <SEP> Stunde.... <SEP> l <SEP> 
<tb> ,, <SEP> ,, <SEP> ,, <SEP> halben <SEP> Stunde <SEP> 1 <SEP> ,, <SEP> ,,
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<tb> zusammen <SEP> .. <SEP> 83 <SEP> cm3 <SEP> Benzol <SEP> = <SEP> etwa <SEP> 75 <SEP> g <SEP> Benzol.
<tb> 
 



   Nachdem alles Benzol   eingetragen ist, rührt   man noch eine Stunde lang. 



   Die   Benzol-Kampferlösung   wird dann von der   Chromlauge abgetrennt, mit Wasser und   Natronlauge bis zur vollständigen Entfärbung gewaschen, mit Kochsalz getrocknet und nach dem Filtrieren des Lösungsmittels abdestilliert. Es hinterbleiben 95 Teile Kampfer, der ohne weitere Reinigung bei 175 bis   1760 schmilzt.   



   Die in den Beispielen genannten Zusatzmengen en Benzol sind natürlich abhängig 
 EMI2.2 




   <Desc / Clms Page number 1>
 
 EMI1.1
 
 EMI1.2
 

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<tb>
<tb> At <SEP> start <SEP> ................ <SEP> 1 <SEP> cm3 <SEP> benzene,
<tb> after <SEP> one <SEP> hour <SEP> .............. <SEP> 1 <SEP> ,, <SEP> ,,
<tb> ,, <SEP> further. <SEP> hour .... <SEP> l <SEP>
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<tb> together <SEP> .. <SEP> 83 <SEP> cm3 <SEP> benzene <SEP> = <SEP> about <SEP> 75 <SEP> g <SEP> benzene.
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   After all the benzene has been added, the mixture is stirred for another hour.



   The benzene-camphor solution is then separated from the chromium hydroxide solution, washed with water and sodium hydroxide solution until completely discolored, dried with sodium chloride and, after the solvent has been filtered off, distilled off. 95 parts of camphor remain, which melts at 175 to 1760 without further purification.



   The amounts of benzene added in the examples are of course dependent
 EMI2.2
AT65917D 1911-12-06 1912-10-24 Process for the production of camphor from borneol or isoborneol. AT65917B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE65917X 1911-12-06

Publications (1)

Publication Number Publication Date
AT65917B true AT65917B (en) 1914-07-25

Family

ID=5633140

Family Applications (1)

Application Number Title Priority Date Filing Date
AT65917D AT65917B (en) 1911-12-06 1912-10-24 Process for the production of camphor from borneol or isoborneol.

Country Status (1)

Country Link
AT (1) AT65917B (en)

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