AR096156A1 - Adsorbentes zeolíticos que comprenden zeolita emt, su procedimiento de preparación y sus utilizaciones - Google Patents
Adsorbentes zeolíticos que comprenden zeolita emt, su procedimiento de preparación y sus utilizacionesInfo
- Publication number
- AR096156A1 AR096156A1 ARP140101787A ARP140101787A AR096156A1 AR 096156 A1 AR096156 A1 AR 096156A1 AR P140101787 A ARP140101787 A AR P140101787A AR P140101787 A ARP140101787 A AR P140101787A AR 096156 A1 AR096156 A1 AR 096156A1
- Authority
- AR
- Argentina
- Prior art keywords
- adsorbents
- potassium
- emt
- separation
- ions
- Prior art date
Links
Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
- B01J20/16—Alumino-silicates
- B01J20/18—Synthetic zeolitic molecular sieves
- B01J20/186—Chemical treatments in view of modifying the properties of the sieve, e.g. increasing the stability or the activity, also decreasing the activity
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
- B01J20/28002—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their physical properties
- B01J20/28004—Sorbent size or size distribution, e.g. particle size
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
- B01J20/28002—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their physical properties
- B01J20/28004—Sorbent size or size distribution, e.g. particle size
- B01J20/28007—Sorbent size or size distribution, e.g. particle size with size in the range 1-100 nanometers, e.g. nanosized particles, nanofibers, nanotubes, nanowires or the like
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
- B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
- B01J20/2803—Sorbents comprising a binder, e.g. for forming aggregated, agglomerated or granulated products
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/3028—Granulating, agglomerating or aggregating
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/3042—Use of binding agents; addition of materials ameliorating the mechanical properties of the produced sorbent
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/3071—Washing or leaching
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/3078—Thermal treatment, e.g. calcining or pyrolizing
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/3085—Chemical treatments not covered by groups B01J20/3007 - B01J20/3078
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
- B01J20/3202—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the carrier, support or substrate used for impregnation or coating
- B01J20/3204—Inorganic carriers, supports or substrates
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
- B01J20/3231—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the coating or impregnating layer
- B01J20/3234—Inorganic material layers
- B01J20/3236—Inorganic material layers containing metal, other than zeolites, e.g. oxides, hydroxides, sulphides or salts
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
- C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
- C07C37/70—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
- C07C37/82—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by solid-liquid treatment; by chemisorption
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C7/00—Purification; Separation; Use of additives
- C07C7/12—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers
- C07C7/13—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers by molecular-sieve technique
Abstract
La presente se refiere a adsorbentes zeoliticos a base de cristales aglomerados de zeolita EMT que comprende bario y/o potasio. Estos adsorbentes encuentran aplicaciones en la separación de cortes de isómeros aromáticos en C₈ y particularmente de los xilenos, en la separación de isómeros de tolueno sustituido tales como nitrotolueno, dietiltolueno, toluenodiamina, en la separación de los cresoles, y alcoholes polihídricos, tales como los azúcares. Reivindicación 12: Procedimiento de preparación de un adsorbente según cualquiera de las reivindicaciones precedentes, que comprende al menos las etapas de: a) aglomeración de un polvo de zeolita que comprende zeolita EMT, con un ligante y puesta en forma, luego secado y calcinación, b) intercambio catiónico del aglomerado por puesta en contacto con una solución de iones bario, o de iones potasio, o de iones bario y de iones potasio, c) Intercambio eventual con potasio, d) luego lavado y secado del producto así tratado, y e) activación del adsorbente zeolítico así obtenido.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR1353971A FR3004966B1 (fr) | 2013-04-30 | 2013-04-30 | Adsorbants zeolithiques comprenant de la zeolithe emt, leur procede de preparation et leurs utilisations |
Publications (1)
Publication Number | Publication Date |
---|---|
AR096156A1 true AR096156A1 (es) | 2015-12-09 |
Family
ID=48795747
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ARP140101787A AR096156A1 (es) | 2013-04-30 | 2014-04-30 | Adsorbentes zeolíticos que comprenden zeolita emt, su procedimiento de preparación y sus utilizaciones |
Country Status (7)
Country | Link |
---|---|
US (1) | US9707539B2 (es) |
EP (1) | EP2991760B1 (es) |
CN (1) | CN105339082B (es) |
AR (1) | AR096156A1 (es) |
FR (1) | FR3004966B1 (es) |
TW (1) | TW201509519A (es) |
WO (1) | WO2014177567A1 (es) |
Families Citing this family (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR3013236B1 (fr) * | 2013-11-20 | 2015-12-11 | Ceca Sa | Materiau granulaire zeolithique a structure connexe |
FR3038528B1 (fr) | 2015-07-09 | 2020-10-23 | Ifp Energies Now | Adsorbants zeolithiques, leur procede de preparation et leurs utilisations |
FR3038529B1 (fr) * | 2015-07-09 | 2020-10-23 | Ceca Sa | Adsorbants zeolithiques, leur procede de preparation et leurs utilisations |
EP4292707A3 (en) * | 2015-12-24 | 2024-02-21 | California Institute Of Technology | Molecular sieves mediated unsaturated hydrocarbon separation and related compositions, materials, methods and systems |
FR3052986B1 (fr) * | 2016-06-28 | 2021-04-09 | Ifp Energies Now | Adsorbant zeolithique sous forme d'agglomeres a faible tortuosite |
FR3059571B1 (fr) * | 2016-12-02 | 2018-11-16 | Arkema France | Materiau adsorbant zeolithique, procede de preparation et utilisation pour la separation non-cryogenique des gaz industriels |
DE102017207817A1 (de) * | 2017-05-09 | 2018-11-15 | Clariant International Ltd | Zeolithhaltiges Adsorbens zur selektiven Abtrennung von Isomeren aus aromatischen Kohlenwasserstoffgemischen, seine Herstellung und Verwendung |
CN107983176A (zh) * | 2017-12-04 | 2018-05-04 | 上海绿强新材料有限公司 | 一种用于c8芳烃异构体分离的emt分子筛膜的制备方法 |
FR3075792B1 (fr) * | 2017-12-22 | 2019-11-29 | Arkema France | Adsorbants zeolitiques contenant du strontium |
FR3112289B1 (fr) | 2020-07-10 | 2022-07-22 | Arkema France | Purification de liquides aromatiques |
Family Cites Families (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2985589A (en) | 1957-05-22 | 1961-05-23 | Universal Oil Prod Co | Continuous sorption process employing fixed bed of sorbent and moving inlets and outlets |
US3558730A (en) | 1968-06-24 | 1971-01-26 | Universal Oil Prod Co | Aromatic hydrocarbon separation by adsorption |
US3626020A (en) | 1969-03-12 | 1971-12-07 | Universal Oil Prod Co | Separation of paraxylene from mixture of c aromatic utilizing crystalline aluminosilicate adsorbent |
US3558732A (en) | 1969-05-12 | 1971-01-26 | Universal Oil Prod Co | Aromatic hydrocarbon separation by adsorption |
US3663638A (en) | 1970-08-31 | 1972-05-16 | Universal Oil Prod Co | Aromatic hydrocarbon separation by adsorption |
US3960774A (en) | 1973-05-02 | 1976-06-01 | Universal Oil Products Company | Zeolitic adsorbent for xylene separation |
US4402832A (en) | 1982-08-12 | 1983-09-06 | Uop Inc. | High efficiency continuous separation process |
US4498991A (en) | 1984-06-18 | 1985-02-12 | Uop Inc. | Serial flow continuous separation process |
TW200454B (es) | 1991-09-05 | 1993-02-21 | Inst Of France Petroleum | |
FR2750893B1 (fr) | 1996-07-12 | 1998-10-30 | Elf Aquitaine | Procede de synthese de zeolithe avec agitation homogene du milieu, dispositif et application |
NO304183B1 (no) | 1996-11-22 | 1998-11-09 | Nyfotek As | FremgangsmÕte for fremstilling av heksagonal faujasitt med lavt forbruk av organisk tilsetningsstoff, samt anvendelse av denne som katalysator ved alkylering |
FR2789914B1 (fr) | 1999-02-22 | 2001-04-06 | Ceca Sa | Adsorbants zeolitiques agglomeres a faible taux de liant inerte, leur procede d'obtention et leurs utilisations |
FR2903978B1 (fr) | 2006-07-19 | 2010-09-24 | Ceca Sa | Adsorbants zeolitiques agglomeres, leur procede de preparation et leurs utilisations |
US7820869B2 (en) * | 2008-06-30 | 2010-10-26 | Uop Llc | Binderless adsorbents and their use in the adsorptive separation of para-xylene |
JP2012218998A (ja) | 2011-04-13 | 2012-11-12 | Tosoh Corp | Emt構造を有する微結晶ゼオライト及びその製造方法 |
-
2013
- 2013-04-30 FR FR1353971A patent/FR3004966B1/fr active Active
-
2014
- 2014-04-29 CN CN201480024557.7A patent/CN105339082B/zh active Active
- 2014-04-29 WO PCT/EP2014/058732 patent/WO2014177567A1/fr active Application Filing
- 2014-04-29 EP EP14719802.2A patent/EP2991760B1/fr active Active
- 2014-04-29 US US14/888,309 patent/US9707539B2/en active Active
- 2014-04-30 AR ARP140101787A patent/AR096156A1/es unknown
- 2014-04-30 TW TW103115639A patent/TW201509519A/zh unknown
Also Published As
Publication number | Publication date |
---|---|
EP2991760B1 (fr) | 2022-04-06 |
CN105339082B (zh) | 2020-01-17 |
FR3004966A1 (fr) | 2014-10-31 |
FR3004966B1 (fr) | 2016-02-05 |
US9707539B2 (en) | 2017-07-18 |
US20160067673A1 (en) | 2016-03-10 |
CN105339082A (zh) | 2016-02-17 |
TW201509519A (zh) | 2015-03-16 |
EP2991760A1 (fr) | 2016-03-09 |
WO2014177567A1 (fr) | 2014-11-06 |
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