ZA931871B - Integrated process for producing crystalline fructose - Google Patents

Integrated process for producing crystalline fructose

Info

Publication number
ZA931871B
ZA931871B ZA931871A ZA931871A ZA931871B ZA 931871 B ZA931871 B ZA 931871B ZA 931871 A ZA931871 A ZA 931871A ZA 931871 A ZA931871 A ZA 931871A ZA 931871 B ZA931871 B ZA 931871B
Authority
ZA
South Africa
Prior art keywords
cooling
integrated process
producing crystalline
crystalline fructose
fructose
Prior art date
Application number
ZA931871A
Inventor
Donald W Lillard Jr
Robert V Schanefelt
Daniel K Tang
Gary A Day
Francis M Mallee
Larwrence R Schwab
Larry W Peckous
Original Assignee
Staley Mfg Co A E
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US07/747,764 external-priority patent/US5350456A/en
Priority to US07/747,764 priority Critical patent/US5350456A/en
Priority to US07/747,773 priority patent/US5230742A/en
Priority to US07/747,775 priority patent/US5234503A/en
Priority claimed from US07/747,773 external-priority patent/US5230742A/en
Priority claimed from US07/747,775 external-priority patent/US5234503A/en
Priority to DE69321456T priority patent/DE69321456T2/en
Priority to AT93301559T priority patent/ATE176503T1/en
Priority to EP93301560A priority patent/EP0613954B1/en
Priority to AT93301560T priority patent/ATE171982T1/en
Priority to EP93301559A priority patent/EP0613953B1/en
Priority to DE69323414T priority patent/DE69323414T2/en
Priority to ES93301560T priority patent/ES2124283T3/en
Priority to ES93301559T priority patent/ES2126627T3/en
Priority to AU33991/93A priority patent/AU662391B2/en
Application filed by Staley Mfg Co A E filed Critical Staley Mfg Co A E
Priority to CA002091706A priority patent/CA2091706A1/en
Priority to ZA931871A priority patent/ZA931871B/en
Priority to JP07412893A priority patent/JP3399576B2/en
Priority to HU9301156A priority patent/HUT67470A/en
Priority to BR9301098A priority patent/BR9301098A/en
Publication of ZA931871B publication Critical patent/ZA931871B/en
Priority to GR990400653T priority patent/GR3029569T3/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
    • C13K1/00—Glucose; Glucose-containing syrups
    • C13K1/10—Crystallisation
    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
    • C13K11/00—Fructose
    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
    • C13K3/00—Invert sugar; Separation of glucose or fructose from invert sugar

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • General Health & Medical Sciences (AREA)
  • Seasonings (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Saccharide Compounds (AREA)

Abstract

During fructose crystallization by cooling a fructose solution, the rate of cooling is first reduced and then increased again. The reduced cooling rate is preferably in the temperature band 46 +/- 3 DEG C and this controlled cooling results in an improved product. The process preferably uses the mother liquor remaining after crystallization for the preparation of a liquid phase sweetener.
ZA931871A 1987-02-02 1993-03-16 Integrated process for producing crystalline fructose ZA931871B (en)

Priority Applications (18)

Application Number Priority Date Filing Date Title
US07/747,764 US5350456A (en) 1987-02-02 1991-08-20 Integrated process for producing crystalline fructose and a high fructose, liquid-phase sweetener
US07/747,773 US5230742A (en) 1987-02-02 1991-08-20 Integrated process for producing crystalline fructose and high-fructose, liquid-phase sweetener
US07/747,775 US5234503A (en) 1987-02-02 1991-08-20 Integrated process for producing crystalline fructose and a high-fructose, liquid-phase sweetener
ES93301560T ES2124283T3 (en) 1991-08-20 1993-03-01 FRUCTOSE CRYSTALLIZATION.
ES93301559T ES2126627T3 (en) 1991-08-20 1993-03-01 LIQUID SWEETENER CONTAINING FRUCTOSE AND DEXTROSE.
AT93301559T ATE176503T1 (en) 1991-08-20 1993-03-01 LIQUID SWEETENER CONTAINING FRUCTOSE AND DEXTROSE
DE69323414T DE69323414T2 (en) 1991-08-20 1993-03-01 Liquid sweetener containing fructose and dextrose
EP93301560A EP0613954B1 (en) 1991-08-20 1993-03-01 Fructose crystallization
AT93301560T ATE171982T1 (en) 1991-08-20 1993-03-01 CRYSTALLIZATION OF FRUCTOSE
DE69321456T DE69321456T2 (en) 1991-08-20 1993-03-01 Crystallization of fructose
EP93301559A EP0613953B1 (en) 1991-08-20 1993-03-01 Fructose and dextrose containing liquid sweetener
AU33991/93A AU662391B2 (en) 1991-08-20 1993-03-04 Fructose and dextrose containing liquid sweetener
CA002091706A CA2091706A1 (en) 1991-08-20 1993-03-16 Integrated process for producing crystalline fructose
ZA931871A ZA931871B (en) 1991-08-20 1993-03-16 Integrated process for producing crystalline fructose
JP07412893A JP3399576B2 (en) 1991-08-20 1993-03-31 Integrated process for producing crystalline fructose
HU9301156A HUT67470A (en) 1991-08-20 1993-04-19 Integrated process for producing crystalline fructose
BR9301098A BR9301098A (en) 1991-08-20 1993-05-17 Integrated process for the production of crystalline fructose
GR990400653T GR3029569T3 (en) 1991-08-20 1999-03-04 Fructose and dextrose containing liquid sweetener.

Applications Claiming Priority (11)

Application Number Priority Date Filing Date Title
US07/747,764 US5350456A (en) 1987-02-02 1991-08-20 Integrated process for producing crystalline fructose and a high fructose, liquid-phase sweetener
US07/747,775 US5234503A (en) 1987-02-02 1991-08-20 Integrated process for producing crystalline fructose and a high-fructose, liquid-phase sweetener
US07/747,773 US5230742A (en) 1987-02-02 1991-08-20 Integrated process for producing crystalline fructose and high-fructose, liquid-phase sweetener
EP93301559A EP0613953B1 (en) 1991-08-20 1993-03-01 Fructose and dextrose containing liquid sweetener
EP93301560A EP0613954B1 (en) 1991-08-20 1993-03-01 Fructose crystallization
AU33991/93A AU662391B2 (en) 1991-08-20 1993-03-04 Fructose and dextrose containing liquid sweetener
ZA931871A ZA931871B (en) 1991-08-20 1993-03-16 Integrated process for producing crystalline fructose
CA002091706A CA2091706A1 (en) 1991-08-20 1993-03-16 Integrated process for producing crystalline fructose
JP07412893A JP3399576B2 (en) 1991-08-20 1993-03-31 Integrated process for producing crystalline fructose
HU9301156A HUT67470A (en) 1991-08-20 1993-04-19 Integrated process for producing crystalline fructose
BR9301098A BR9301098A (en) 1991-08-20 1993-05-17 Integrated process for the production of crystalline fructose

Publications (1)

Publication Number Publication Date
ZA931871B true ZA931871B (en) 1993-10-06

Family

ID=27581357

Family Applications (1)

Application Number Title Priority Date Filing Date
ZA931871A ZA931871B (en) 1987-02-02 1993-03-16 Integrated process for producing crystalline fructose

Country Status (11)

Country Link
EP (2) EP0613953B1 (en)
JP (1) JP3399576B2 (en)
AT (2) ATE176503T1 (en)
AU (1) AU662391B2 (en)
BR (1) BR9301098A (en)
CA (1) CA2091706A1 (en)
DE (2) DE69323414T2 (en)
ES (2) ES2124283T3 (en)
GR (1) GR3029569T3 (en)
HU (1) HUT67470A (en)
ZA (1) ZA931871B (en)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BR0103406A (en) 2001-08-15 2004-05-04 Getec Guanabara Quimica Ind S Process of producing high purity crystalline fructose using low fructose syrup originating from sucrose and product obtained
FI115919B (en) * 2002-06-27 2005-08-15 Danisco Sweeteners Oy Procedure for removing crystallization inhibitors from a solution containing monosaccharide sugar
KR101217137B1 (en) * 2012-03-05 2012-12-31 한국생산기술연구원 Method for manufacturing 5-hydroxymethyl-2-furfural from corn syrup containing fructose
KR20150070097A (en) * 2012-08-20 2015-06-24 나뚜랄리아 잉그레졍츠 에세.에레.엘레. Method of producing a sugar product from fruit
CN103146849B (en) * 2013-03-25 2014-01-08 保龄宝生物股份有限公司 Method for co-producing crystalline fructose and fructose corn syrup by taking wheat as raw material, and preparation method of wheat starch
KR102283524B1 (en) * 2015-02-24 2021-07-30 테이트 앤드 라일 인그리디언츠 어메리카즈 엘엘씨 allulose syrup
KR101695831B1 (en) * 2015-05-15 2017-01-12 주식회사 삼양사 Saccharide mixture containing psicose with improved sweetness quality and crystallization
EP3464606A1 (en) 2016-05-23 2019-04-10 Annikki GmbH Method for enzymatic conversion of d-glucose into d-fructose via d-sorbitol
KR102065155B1 (en) 2016-12-08 2020-02-11 주식회사 삼양사 Production of psciose
FR3061413B1 (en) 2017-01-05 2021-08-27 Roquette Freres PROCESS FOR MANUFACTURING D-ALLULOSE CRYSTALS
FR3061414B1 (en) 2017-01-05 2021-07-16 Roquette Freres D-ALLULOSE CRYSTALLIZABLE SYRUPS
KR102004940B1 (en) * 2017-06-30 2019-07-29 주식회사 삼양사 production of allulose as sweetener

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2007971A (en) * 1926-11-29 1935-07-16 Richard F Jackson Process of making sugar products
FR1534746A (en) * 1966-04-29 1968-08-02 Boehringer & Soehne Gmbh Process for obtaining fructose in the crystallized state
US3883365A (en) * 1972-01-04 1975-05-13 Suomen Sokeri Oy PH adjustment in fructose crystallization for increased yield
US3816175A (en) * 1972-07-03 1974-06-11 Suomen Sokeri Oy Process for formation of crystalline fructose-glucose blends
JPS5239901B2 (en) * 1973-02-12 1977-10-07
US4199373A (en) * 1979-04-13 1980-04-22 Chimicasa Gmbh Process for the manufacture of crystalline fructose
US4517021A (en) * 1983-10-28 1985-05-14 A. E. Staley Manufacturing Company Semi-crystalline fructose
US4634472A (en) * 1985-08-23 1987-01-06 A. E. Staley Manufacturing Company Enrichment of fructose syrups
US5047088A (en) * 1989-06-30 1991-09-10 A. E. Staley Manufacturing Company Method for crystallization of fructose

Also Published As

Publication number Publication date
DE69323414T2 (en) 1999-06-10
ES2126627T3 (en) 1999-04-01
HUT67470A (en) 1995-04-28
GR3029569T3 (en) 1999-06-30
EP0613954A1 (en) 1994-09-07
EP0613953B1 (en) 1999-02-03
AU3399193A (en) 1994-09-15
CA2091706A1 (en) 1994-09-17
JPH06277099A (en) 1994-10-04
BR9301098A (en) 1994-11-29
ES2124283T3 (en) 1999-02-01
EP0613953A1 (en) 1994-09-07
ATE171982T1 (en) 1998-10-15
DE69321456T2 (en) 1999-06-17
ATE176503T1 (en) 1999-02-15
AU662391B2 (en) 1995-08-31
HU9301156D0 (en) 1993-07-28
JP3399576B2 (en) 2003-04-21
DE69321456D1 (en) 1998-11-12
DE69323414D1 (en) 1999-03-18
EP0613954B1 (en) 1998-10-07

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