DE69323414T2 - Liquid sweetener containing fructose and dextrose - Google Patents

Liquid sweetener containing fructose and dextrose

Info

Publication number
DE69323414T2
DE69323414T2 DE69323414T DE69323414T DE69323414T2 DE 69323414 T2 DE69323414 T2 DE 69323414T2 DE 69323414 T DE69323414 T DE 69323414T DE 69323414 T DE69323414 T DE 69323414T DE 69323414 T2 DE69323414 T2 DE 69323414T2
Authority
DE
Germany
Prior art keywords
cooling
dextrose
containing fructose
liquid sweetener
sweetener containing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE69323414T
Other languages
German (de)
Other versions
DE69323414D1 (en
Inventor
Francis M Mallee
Lawrence R Schwab
Larry W Peckous
Donald W Lillard
Robert V Schanefelt
Daniel K Tang
Gary A Day
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Primary Products Ingredients Americas LLC
Original Assignee
Tate and Lyle Ingredients Americas LLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US07/747,764 external-priority patent/US5350456A/en
Priority claimed from US07/747,775 external-priority patent/US5234503A/en
Priority claimed from US07/747,773 external-priority patent/US5230742A/en
Application filed by Tate and Lyle Ingredients Americas LLC filed Critical Tate and Lyle Ingredients Americas LLC
Publication of DE69323414D1 publication Critical patent/DE69323414D1/en
Application granted granted Critical
Publication of DE69323414T2 publication Critical patent/DE69323414T2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
    • C13K1/00—Glucose; Glucose-containing syrups
    • C13K1/10—Crystallisation
    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
    • C13K11/00—Fructose
    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
    • C13K3/00—Invert sugar; Separation of glucose or fructose from invert sugar

Abstract

During fructose crystallization by cooling a fructose solution, the rate of cooling is first reduced and then increased again. The reduced cooling rate is preferably in the temperature band 46 +/- 3 DEG C and this controlled cooling results in an improved product. The process preferably uses the mother liquor remaining after crystallization for the preparation of a liquid phase sweetener.
DE69323414T 1991-08-20 1993-03-01 Liquid sweetener containing fructose and dextrose Expired - Fee Related DE69323414T2 (en)

Applications Claiming Priority (11)

Application Number Priority Date Filing Date Title
US07/747,764 US5350456A (en) 1987-02-02 1991-08-20 Integrated process for producing crystalline fructose and a high fructose, liquid-phase sweetener
US07/747,775 US5234503A (en) 1987-02-02 1991-08-20 Integrated process for producing crystalline fructose and a high-fructose, liquid-phase sweetener
US07/747,773 US5230742A (en) 1987-02-02 1991-08-20 Integrated process for producing crystalline fructose and high-fructose, liquid-phase sweetener
EP93301559A EP0613953B1 (en) 1991-08-20 1993-03-01 Fructose and dextrose containing liquid sweetener
EP93301560A EP0613954B1 (en) 1991-08-20 1993-03-01 Fructose crystallization
AU33991/93A AU662391B2 (en) 1991-08-20 1993-03-04 Fructose and dextrose containing liquid sweetener
ZA931871A ZA931871B (en) 1991-08-20 1993-03-16 Integrated process for producing crystalline fructose
CA002091706A CA2091706A1 (en) 1991-08-20 1993-03-16 Integrated process for producing crystalline fructose
JP07412893A JP3399576B2 (en) 1991-08-20 1993-03-31 Integrated process for producing crystalline fructose
HU9301156A HUT67470A (en) 1991-08-20 1993-04-19 Integrated process for producing crystalline fructose
BR9301098A BR9301098A (en) 1991-08-20 1993-05-17 Integrated process for the production of crystalline fructose

Publications (2)

Publication Number Publication Date
DE69323414D1 DE69323414D1 (en) 1999-03-18
DE69323414T2 true DE69323414T2 (en) 1999-06-10

Family

ID=27581357

Family Applications (2)

Application Number Title Priority Date Filing Date
DE69321456T Expired - Fee Related DE69321456T2 (en) 1991-08-20 1993-03-01 Crystallization of fructose
DE69323414T Expired - Fee Related DE69323414T2 (en) 1991-08-20 1993-03-01 Liquid sweetener containing fructose and dextrose

Family Applications Before (1)

Application Number Title Priority Date Filing Date
DE69321456T Expired - Fee Related DE69321456T2 (en) 1991-08-20 1993-03-01 Crystallization of fructose

Country Status (11)

Country Link
EP (2) EP0613954B1 (en)
JP (1) JP3399576B2 (en)
AT (2) ATE176503T1 (en)
AU (1) AU662391B2 (en)
BR (1) BR9301098A (en)
CA (1) CA2091706A1 (en)
DE (2) DE69321456T2 (en)
ES (2) ES2126627T3 (en)
GR (1) GR3029569T3 (en)
HU (1) HUT67470A (en)
ZA (1) ZA931871B (en)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BR0103406A (en) 2001-08-15 2004-05-04 Getec Guanabara Quimica Ind S Process of producing high purity crystalline fructose using low fructose syrup originating from sucrose and product obtained
FI115919B (en) * 2002-06-27 2005-08-15 Danisco Sweeteners Oy Procedure for removing crystallization inhibitors from a solution containing monosaccharide sugar
KR101217137B1 (en) * 2012-03-05 2012-12-31 한국생산기술연구원 Method for manufacturing 5-hydroxymethyl-2-furfural from corn syrup containing fructose
KR20150070097A (en) * 2012-08-20 2015-06-24 나뚜랄리아 잉그레졍츠 에세.에레.엘레. Method of producing a sugar product from fruit
CN103146849B (en) * 2013-03-25 2014-01-08 保龄宝生物股份有限公司 Method for co-producing crystalline fructose and fructose corn syrup by taking wheat as raw material, and preparation method of wheat starch
CN107567283B (en) * 2015-02-24 2021-05-28 泰特&莱尔组分美国公司 Allulose syrup
KR101695831B1 (en) 2015-05-15 2017-01-12 주식회사 삼양사 Saccharide mixture containing psicose with improved sweetness quality and crystallization
BR112018072410A2 (en) 2016-05-23 2019-02-12 Annikki Gmbh process for the enzymatic conversion of d-glucose to d-fructose by means of d-sorbitol
KR102065155B1 (en) * 2016-12-08 2020-02-11 주식회사 삼양사 Production of psciose
FR3061413B1 (en) 2017-01-05 2021-08-27 Roquette Freres PROCESS FOR MANUFACTURING D-ALLULOSE CRYSTALS
FR3061414B1 (en) 2017-01-05 2021-07-16 Roquette Freres D-ALLULOSE CRYSTALLIZABLE SYRUPS
KR102004940B1 (en) * 2017-06-30 2019-07-29 주식회사 삼양사 production of allulose as sweetener

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2007971A (en) * 1926-11-29 1935-07-16 Richard F Jackson Process of making sugar products
FR1534746A (en) * 1966-04-29 1968-08-02 Boehringer & Soehne Gmbh Process for obtaining fructose in the crystallized state
US3883365A (en) * 1972-01-04 1975-05-13 Suomen Sokeri Oy PH adjustment in fructose crystallization for increased yield
US3816175A (en) * 1972-07-03 1974-06-11 Suomen Sokeri Oy Process for formation of crystalline fructose-glucose blends
JPS5239901B2 (en) * 1973-02-12 1977-10-07
US4199373A (en) * 1979-04-13 1980-04-22 Chimicasa Gmbh Process for the manufacture of crystalline fructose
US4517021A (en) * 1983-10-28 1985-05-14 A. E. Staley Manufacturing Company Semi-crystalline fructose
US4634472A (en) * 1985-08-23 1987-01-06 A. E. Staley Manufacturing Company Enrichment of fructose syrups
US5047088A (en) * 1989-06-30 1991-09-10 A. E. Staley Manufacturing Company Method for crystallization of fructose

Also Published As

Publication number Publication date
GR3029569T3 (en) 1999-06-30
ZA931871B (en) 1993-10-06
HU9301156D0 (en) 1993-07-28
BR9301098A (en) 1994-11-29
ATE176503T1 (en) 1999-02-15
AU3399193A (en) 1994-09-15
AU662391B2 (en) 1995-08-31
JPH06277099A (en) 1994-10-04
DE69323414D1 (en) 1999-03-18
DE69321456T2 (en) 1999-06-17
HUT67470A (en) 1995-04-28
ES2126627T3 (en) 1999-04-01
ES2124283T3 (en) 1999-02-01
EP0613954A1 (en) 1994-09-07
EP0613953A1 (en) 1994-09-07
EP0613954B1 (en) 1998-10-07
EP0613953B1 (en) 1999-02-03
CA2091706A1 (en) 1994-09-17
ATE171982T1 (en) 1998-10-15
JP3399576B2 (en) 2003-04-21
DE69321456D1 (en) 1998-11-12

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Legal Events

Date Code Title Description
8364 No opposition during term of opposition
8339 Ceased/non-payment of the annual fee