YU18392A - Kontinualni postupak za dobijanje dinitrotoluena - Google Patents
Kontinualni postupak za dobijanje dinitrotoluenaInfo
- Publication number
- YU18392A YU18392A YU18392A YU18392A YU18392A YU 18392 A YU18392 A YU 18392A YU 18392 A YU18392 A YU 18392A YU 18392 A YU18392 A YU 18392A YU 18392 A YU18392 A YU 18392A
- Authority
- YU
- Yugoslavia
- Prior art keywords
- dinitrotoluene
- toluene
- nitric acid
- continuous process
- nitration
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
- C07C201/06—Preparation of nitro compounds
- C07C201/08—Preparation of nitro compounds by substitution of hydrogen atoms by nitro groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
KONTINUALNI POSTUPAK ZA DOBIJANJE DINITROTOLUENA, opisan je poboljšani kontinualni postupak za dobijanje dinitrotoluena reakcijom nitriranja toluena azotnom kiselinom u jednom reaktoru koji se izvodi tako što se toluen injektira u cirkulacioni reaktorski likvor sastavljen od azotne kiseline i vode, pri čemu reaktorski likvor obezbedjuje odvodjenje toplote iz reakcije nitriranja koja se izvodi na temperaturi od 0-90В°C pri molarnom odnosu azotne kiseline prema toluenu od 12:1 do 9:1, gde se toluen injektira u reaktorski likvor u zapreminskom odnosu od 1:100 do 1:50. U postupku se obrazuje izlazna mešavina dinitrotoluena, vode i neizreagovane azotne kiseline koja se meša sa nitratnom solju radi izazivanja razdvajanja faze dinitrotoluena od izlazne mešavine.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US07/666,330 US5099080A (en) | 1991-03-08 | 1991-03-08 | Process for preparing dinitrotoluene |
Publications (1)
Publication Number | Publication Date |
---|---|
YU18392A true YU18392A (sh) | 1994-06-24 |
Family
ID=24673751
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
YU18392A YU18392A (sh) | 1991-03-08 | 1993-02-21 | Kontinualni postupak za dobijanje dinitrotoluena |
Country Status (10)
Country | Link |
---|---|
US (1) | US5099080A (sh) |
EP (1) | EP0641307A1 (sh) |
CN (1) | CN1064860A (sh) |
AU (1) | AU654190B2 (sh) |
BR (1) | BR9205728A (sh) |
CA (1) | CA2105390C (sh) |
CS (1) | CS64592A3 (sh) |
MX (1) | MX9200841A (sh) |
WO (1) | WO1992015550A1 (sh) |
YU (1) | YU18392A (sh) |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5245092A (en) * | 1991-03-15 | 1993-09-14 | Olin Corporation | Process for preparing dinitrotoluene with low by-product content |
EP0649400A1 (en) * | 1992-06-17 | 1995-04-26 | Olin Corporation | Process for the production of dinitrotoluene |
US5302763A (en) * | 1993-03-01 | 1994-04-12 | Olin Corporation | Process for preparing dinitrotoluene |
DE4437047A1 (de) | 1994-10-17 | 1996-04-18 | Bayer Ag | Verfahren zur Dinitrierung von aromatischen Verbindungen |
US5948944A (en) * | 1998-11-18 | 1999-09-07 | Arco Chemical Technology, L.P. | Two-stage dinitrotoluene production process |
CN101245010B (zh) * | 2008-03-08 | 2011-06-29 | 西北师范大学 | 民用二硝基甲苯的制备工艺 |
US9079822B2 (en) | 2009-02-26 | 2015-07-14 | Basf Se | Process for the preparation of nitrated aromatics and mixtures thereof |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3178481A (en) * | 1963-01-07 | 1965-04-13 | Atlas Chem Ind | Dinitrotoluene manufacture |
US3928395A (en) * | 1972-10-05 | 1975-12-23 | Ciba Geigy Ag | Process for the nitration of aromatic compounds |
US3957889A (en) * | 1975-05-02 | 1976-05-18 | Air Products And Chemicals, Inc. | Selective nitration of aromatic and substituted aromatic compositions |
DE2521891B2 (de) * | 1975-05-16 | 1980-02-28 | Bayer Ag, 5090 Leverkusen | Verfahren zum Abstoppen von Nitrierungen durch Destillation |
US4804792A (en) * | 1988-01-28 | 1989-02-14 | Olin Corporation | Nitration of benzene or toluene in a molten nitrate salt |
US5001272A (en) * | 1988-06-22 | 1991-03-19 | Olin Corporation | Process for the production of dinitrotoluene |
US4918250A (en) * | 1989-04-21 | 1990-04-17 | Olin Corporation | Process for the production of dinitrotoluene using an inorganic salt as a phase separation agent |
-
1991
- 1991-03-08 US US07/666,330 patent/US5099080A/en not_active Expired - Fee Related
-
1992
- 1992-02-14 CA CA002105390A patent/CA2105390C/en not_active Expired - Fee Related
- 1992-02-14 EP EP92910136A patent/EP0641307A1/en not_active Withdrawn
- 1992-02-14 WO PCT/US1992/001065 patent/WO1992015550A1/en not_active Application Discontinuation
- 1992-02-14 AU AU17484/92A patent/AU654190B2/en not_active Ceased
- 1992-02-14 BR BR9205728A patent/BR9205728A/pt active Search and Examination
- 1992-02-27 MX MX9200841A patent/MX9200841A/es not_active IP Right Cessation
- 1992-03-04 CS CS92645A patent/CS64592A3/cs unknown
- 1992-03-08 CN CN92101484A patent/CN1064860A/zh active Pending
-
1993
- 1993-02-21 YU YU18392A patent/YU18392A/sh unknown
Also Published As
Publication number | Publication date |
---|---|
WO1992015550A1 (en) | 1992-09-17 |
AU654190B2 (en) | 1994-10-27 |
CA2105390A1 (en) | 1992-09-09 |
BR9205728A (pt) | 1994-12-27 |
CN1064860A (zh) | 1992-09-30 |
US5099080A (en) | 1992-03-24 |
CA2105390C (en) | 2002-05-21 |
CS64592A3 (en) | 1992-09-16 |
AU1748492A (en) | 1992-10-06 |
EP0641307A4 (en) | 1993-12-22 |
EP0641307A1 (en) | 1995-03-08 |
MX9200841A (es) | 1992-09-01 |
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