WO2023231246A1 - 一种六氟磷酸锂制备用具有夹套的四氟反应器 - Google Patents

一种六氟磷酸锂制备用具有夹套的四氟反应器 Download PDF

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Publication number
WO2023231246A1
WO2023231246A1 PCT/CN2022/121298 CN2022121298W WO2023231246A1 WO 2023231246 A1 WO2023231246 A1 WO 2023231246A1 CN 2022121298 W CN2022121298 W CN 2022121298W WO 2023231246 A1 WO2023231246 A1 WO 2023231246A1
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WO
WIPO (PCT)
Prior art keywords
plate
rod
groove
stabilizing
fixedly connected
Prior art date
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PCT/CN2022/121298
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English (en)
French (fr)
Inventor
刘庭
黄通生
刘滨
邱椿辉
吴华章
傅新文
Original Assignee
福建省龙德新能源有限公司
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Publication of WO2023231246A1 publication Critical patent/WO2023231246A1/zh

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00—Lithium compounds
    • C01D15/005—Lithium hexafluorophosphate
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00018—Construction aspects
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00245—Avoiding undesirable reactions or side-effects
    • B01J2219/00256—Leakage
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00718—Type of compounds synthesised
    • B01J2219/00745—Inorganic compounds
    • B01J2219/0075—Metal based compounds
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

Definitions

  • the invention relates to the technical field of preparing lithium hexafluorophosphate, specifically a jacketed tetrafluoro reactor for preparing lithium hexafluorophosphate.
  • Lithium hexafluorophosphate is a white crystal or powder with strong deliquescent properties; it is easily soluble in water and also soluble in low-concentration methanol, ethanol, acetone, carbonates and other organic solvents. When exposed to the air or heated, lithium hexafluorophosphate dissolves due to the action of water vapor in the air. It decomposes quickly and emits white smoke, so no leakage can occur during its production process. Lithium hexafluorophosphate is produced through PTFE reactors. The PTFE reactors are fixed by jackets, and the jackets are prone to leakage. If the clamping is not firm, loosens and falls, the PTFE reactor will fall over when the jacket cannot fix it.
  • lithium hexafluorophosphate When it falls, it will cause the leakage of lithium hexafluorophosphate, which will lead to production safety accidents.
  • the leaked lithium hexafluorophosphate comes into contact with the air After heating, it decomposes and emits a large amount of white smoke, which may have a certain impact on other production equipment in the factory.
  • the object of the present invention is to provide a jacketed tetrafluoro reactor for the preparation of lithium hexafluorophosphate, so as to solve the problems raised in the above background technology.
  • a jacketed PTFE reactor for preparing lithium hexafluorophosphate including a base, a support plate is fixedly installed on the base by bolts, and the lower end of the support plate is provided with a third A movable port, the upper surface of the base is provided with a movement groove for limiting movement, the inside of the movement groove is provided with a rolling groove for rolling, a movable plate is movable on the base, and the outside of the movable plate The movable plate is movably connected inside the first movable port.
  • the bottom of the movable plate is provided with rollers for stable movement through the mounting plate. The rollers are rollingly connected inside the rolling groove.
  • the movable plate is provided with a contact plate.
  • the connection point between the contact plate and the movable plate is provided with a stabilizing component for stabilizing the upper and lower parts of the contact plate.
  • the bottom of the movable plate and close to the inside of the movement groove are provided with a fixing component for limiting and fixing.
  • the base is fixedly installed with a supporting component.
  • the upper end of the support frame is provided with a detection component for detecting falling, the bottom of the detection component is fixedly connected with a downward pressure rod for pushing the contact plate, the bottom of the downward pressure rod is connected to the upper surface of the contact plate mutually abutting, the lower end of the detection component is fixedly connected with an abutting plate for lifting, the outer side of the abutting plate is movably connected to the outer wall of the support plate, and the abutting plate is penetrated with a movable rod for pressing down.
  • the second movable port, the middle part of the lower pressure rod is movably connected inside the second movable port, the top of the support plate is fixedly connected with a fixed top plate for fixed support through bolts, and a fixed top plate is fixedly installed on the fixed top plate.
  • Jacket, a PTFE reactor is fixedly connected to the inside of the fixed jacket, the bottom of the PTFE reactor and the upper surface of the abutment plate are in contact with each other, and the outer wall of the support frame is provided with a PTFE reactor for stably clamping the PTFE reactor.
  • Clamp assembly for fluorine reactor is provided.
  • the stabilizing component includes a first spring, a stabilizing telescopic rod, a stabilizing groove and a stabilizing plate.
  • the contact plate is fixedly connected to the top of the movable plate through the first spring, and the upper end of the stabilizing telescopic rod is rotatably connected to the contact plate.
  • the lower surface of the stabilizing telescopic rod is rotatably connected to the upper surface of the movable plate.
  • the movable plate is provided with a stabilizing slot for the movement of the stabilizing plate.
  • the stabilizing plate is fixedly connected to the lower surface of the contact plate.
  • the lower end of the stabilizing plate is movably connected inside the stabilizing groove.
  • the fixed assembly includes a lower pressure groove, a first lower pressure plate, a second lower pressure plate, a chute, a fixed frame and a guide groove
  • the movable plate is provided with a lower pressure groove for the movement of the first lower pressure plate, so
  • the lower end of the first lower pressure plate is movably connected inside the lower pressure groove
  • the second lower pressure plate is fixedly connected to the bottom of the first lower pressure plate
  • the outer wall of the second lower pressure plate has an inclined groove for pushing
  • the The fixed frame is fixedly connected to the bottom of the movable plate
  • the outer wall of the fixed frame is provided with a guide groove for guiding the movable plate.
  • the fixed component further includes a sliding rod, a stabilizing block, a clamping rod, a clamping groove and a second spring.
  • Both sides of the sliding rod are movably connected inside the chute, and both ends of the sliding rod are movable.
  • the two ends of the sliding rod are fixedly connected with stabilizing blocks for stabilizing the movement.
  • the inner side of the stabilizing block abuts against the outer wall of the fixed frame.
  • the clamping bar is fixedly connected to the middle part of the sliding rod.
  • a clamping slot for fixation is provided inside the movement slot, the outside of the clamping rod and the inside of the clamping slot are engaged with each other, the outer wall of the fixing frame is fixedly connected to one end of the second spring, and the second spring The other end is fixedly connected to the inner wall of the motion slot.
  • the detection component includes a lifting slot, a third spring, a lifting frame and a first stabilizing bar.
  • the upper end of the support frame is provided with a lifting slot for up and down movement, and the upper end of the third spring is fixedly connected to the support frame.
  • the lower surface of the lifting frame is fixedly connected to the lower end of the third spring.
  • the upper surface of the lifting frame and close to the interior of the third spring is connected to a first stabilizing bar.
  • the upper end of the first stabilizing bar is movably connected to the support.
  • the lower pressure rod is fixedly connected to the lower surface of the lifting frame.
  • the detection assembly further includes a lifting barrel column, an opening, a rotating shaft, a rotating hub, a movable groove, a fourth spring, a limit block, a limiting groove, a torsion spring and a connecting belt, and the lifting barrel column is fixedly connected to At both ends of the lifting frame, the lifting bucket column is movably connected to the inside of the lifting slot.
  • the outer wall of the lifting bucket column is provided with an opening for the connection belt to move.
  • the rotating hub is rotatably connected to the inside of the lifting bucket column through a rotating shaft.
  • the outer wall of the rotating hub is provided with a movable groove for movement
  • the fourth spring is fixedly connected inside the movable groove
  • the outside of the movable groove is fixedly connected with a limit block for fixed positioning
  • the lifting bucket The inner wall of the column is provided with a limit groove for fixed limit.
  • the inside of the rotating hub is fixedly connected to one end of the torsion spring.
  • the other end of the torsion spring is fixedly connected to the upper end of the connecting belt.
  • the lower end of the connecting belt is connected to the resistor.
  • the upper surface of the connecting plate is fixedly connected.
  • the clamping assembly includes a pull rod, a transmission rod, a connecting rod and a second stabilizer bar.
  • One end of the pull rod is rotatably mounted on the outside of the movable plate through a fixed seat, and the other end of the pull rod is fixedly connected to a transmission for transmission.
  • rod, the middle part of the outer wall connecting rod of the transmission rod is rotationally connected, the inner side of the connecting rod is rotationally connected to the outer wall of the support frame, one end of the second stabilizing rod is rotationally connected to the outside of the support frame through a fixed seat, and the clamp
  • the inner side of the stabilizer is rotationally connected to the outer side of the connecting rod.
  • the upper surface of the abutment plate is arranged in a tray shape, and the size of the tray at the top of the abutment plate matches the size of the bottom of the PTFE reactor.
  • the inner side of the clamping stabilizer is arranged in an arc shape, and the size of the arc on the inner side of the clamping stabilizer is adapted to the size of the PTFE reactor.
  • the beneficial effects of the present invention are: 1.
  • the fixed component drives the movable plate to move outward inside the first movable opening, and the movable plate moves through the fixed seat.
  • the pull rod drives the transmission rod to move, and the transmission rod drives the connecting rod to rotate inward.
  • the clamping stabilizer in conjunction with the inward movement of the second stabilizer rod, can stably clamp the PTFE reactor inward, thereby preventing the PTFE reactor from being The problem of dumping occurs after falling, thereby improving the safety of the PTFE reactor in the process of producing lithium hexafluorophosphate; 2.
  • the invention drives the connecting belt to rapidly extend downward through the abutting plate, and the connecting belt drives the torsion spring to rapidly extend, and the torsion spring
  • the rotating hub is driven to rotate rapidly on the rotating shaft.
  • the centrifugal force generated by the rotation of the rotating hub causes the limit block to move outward with a force greater than the elastic force of the fourth spring.
  • the limit block moves outward inside the movable groove and stretches the fourth spring.
  • the spring and the limit block move outward to the inside of the limit groove, so that the limit block and the limit groove are engaged with each other, which can make the rotating hub stop rotating.
  • the present invention uses the stabilizing blocks at both ends of the sliding rod to Under the action of sliding on the outer wall of the fixed frame, the sliding rod can be prevented from rotating during the movement, which in turn can stabilize the clamping rod during the movement, thereby enabling the clamping rod to effectively engage with the slot.
  • the PTFE reactor cannot be fixed through the fixed jacket of the present invention, and the PTFE reactor will move downward rapidly, and the PTFE reactor will pass through
  • the abutment plate contacts the contact plate and pushes the contact plate to move downward.
  • the contact plate will slow down the impact of the PTFE reactor on the equipment through the joint action of the first spring and the stable telescopic rod, and at the same time reduce the impact of the PTFE reactor and Damage to the equipment effectively avoids the problem of spilling or leaking lithium hexafluorophosphate inside the PTFE reactor caused by impact; 5.
  • the present invention drives the stabilizing groove to move downward inside the stabilizing plate through the downward movement of the contact plate, and then It can reduce the problem of the contact plate being skewed due to downward movement and unable to transmit. It also prevents the problem of the first spring being unable to buffer due to the skew, thereby improving the stability of the contact plate when it comes into contact with the PTFE reactor.
  • Figure 1 is a perspective view of the overall structure of the present invention.
  • Figure 2 is a perspective view of the overall cross-sectional structure of the present invention.
  • Figure 3 is an enlarged view of the structure at point A in Figure 2 of the present invention.
  • Figure 4 is a perspective view of the internal structure of the present invention.
  • Figure 5 is a perspective view of the structure of the fixing component of the present invention.
  • Figure 6 is a perspective view of the internal structure of the fixing component of the present invention.
  • Figure 7 is a perspective view of the internal structure of the lifting bucket column according to the present invention.
  • Figure 8 is an enlarged view of the structure at B in Figure 6 of the present invention.
  • Figure 9 is a perspective view of the cross-sectional structure of the lifting barrel column of the present invention.
  • Figure 10 is an enlarged view of the structure at C in Figure 8 of the present invention.
  • Figure 11 is a perspective view of the partial structure of the clamping assembly of the present invention.
  • Embodiment 1 Please refer to Figures 1 to 11, a jacketed tetrafluoro reactor for preparing lithium hexafluorophosphate, including a base 1, a base 1 A support plate 2 is fixedly mounted on the top by bolts. The lower end of the support plate 2 is provided with a first movable port 3. The upper surface of the base 1 is provided with a movement groove 4 for limiting movement. The interior of the movement groove 4 is provided with a rolling groove for rolling. The groove 5 and the base 1 are movable with a movable plate 6. The outside of the movable plate 6 is movably connected to the inside of the first movable port 3.
  • the bottom of the movable plate 6 is provided with a roller 7 for stable movement through the mounting plate.
  • the roller 7 is rollingly connected.
  • a contact plate 9 is provided on the movable plate 6.
  • a stabilizing component for stabilizing the up and down of the contact plate 9 is provided at the connection between the contact plate 9 and the movable plate 6.
  • the bottom of the movable plate 6 is close to the inside of the motion groove 4.
  • a fixed component for limiting and fixing is provided.
  • a support frame 24 is fixedly installed on the base 1 for support. The upper end of the support frame 24 is provided with a detection component for detecting falling.
  • the bottom of the detection component is fixedly connected with a push contact plate 9
  • the lower pressure rod 29, the bottom of the lower pressure rod 29 and the upper surface of the contact plate 9 are in contact with each other.
  • the lower end of the detection assembly is fixedly connected with an abutment plate 40 for lifting, and the outside of the abutment plate 40 is movably connected to the support plate.
  • the abutting plate 40 is provided with a second movable opening 41 for the movement of the pressing rod 29.
  • the middle part of the pressing rod 29 is movably connected inside the second movable opening 41, and the top of the supporting plate 2 is fixed by bolts.
  • a fixed top plate 42 is connected for fixed support.
  • a fixed jacket 43 is fixedly installed on the fixed top plate 42.
  • a PTFE reactor 44 is fixedly connected to the inside of the fixed jacket 43.
  • the bottom of the PTFE reactor 44 and the abutment plate 40 The upper surfaces abut each other, and the outer wall of the support frame 24 is provided with a clamping assembly for stably clamping the PTFE reactor 44 .
  • the PTFE reactor 44 When working, the PTFE reactor 44 is installed on the fixed top plate 42 through the fixed jacket 43, and then the lithium hexafluorophosphate is processed and produced.
  • the PTFE reactor 44 When the PTFE reactor 44 is in the process of producing and processing lithium hexafluorophosphate, if the PTFE reactor 44 is not fixed properly. When it is firm and falls, the PTFE reactor 44 will move downward quickly. At this time, the downward movement of the PTFE reactor 44 will drive the abutment plate 40 to move rapidly downward on the outer wall of the support plate 2.
  • the abutment plate 40 Rapid downward movement will drive the detection component to move downward.
  • the detection component drives the lower pressure rod 29 to move downward, causing the lower pressure rod 29 to push the contact plate 9 downward and make the fixed component contact the limit.
  • the fixed component drives the movable plate 6 to move on the base. 1 moves on, the movable plate 6 drives the clamping assembly so that the clamping stabilizer 49 clamps the PTFE
  • the PTFE reactor 44 If the PTFE reactor 44 becomes loose and falls, the PTFE reactor 44 will gradually move downward. When the PTFE reactor 44 moves downward to a position where the fixed jacket 43 cannot be fixed, the PTFE reaction will occur. The device 44 drives the contact plate 40 to move to the lowest position. If the PTFE reactor 44 falls, it will contact the contact plate 9. At this time, the stability component at the bottom of the contact plate 9 can slow down the fall of the PTFE reactor 44. falling, thereby protecting the PTFE reactor 44 from falling. At the same time, when the PTFE reactor 44 comes into contact with the contact plate 9 through the abutment plate 40, the contact plate 9 can be pushed downward to limit the contact of the fixed assembly, and the fixed assembly drives the The movable plate 6 moves on the base 1.
  • the movable plate 6 rolls inside the rolling groove 5 through the roller 7 so that the movable plate 6 moves outward inside the first movable opening 3.
  • the movable plate 6 drives the clamping assembly to make the clamping
  • the stable frame 49 clamps the PTFE reactor 44, thereby preventing the PTFE reactor 44 from tipping after falling.
  • Embodiment 2 Please refer to Figures 1 to 6.
  • the stabilizing assembly includes a first spring 8, a stabilizing telescopic rod 10, a stabilizing groove 11 and a stabilizing plate 12.
  • the contact plate 9 is fixedly connected to the movable plate 6 through the first spring 8.
  • the upper end of the stable telescopic rod 10 is rotationally connected to the lower surface of the contact plate 9, and the lower end of the stable telescopic rod 10 is rotationally connected to the upper surface of the movable plate 6.
  • the movable plate 6 is provided with a stabilizing slot 11 for the movement of the stable plate 12.
  • the stabilizing plate 12 is fixedly connected to the lower surface of the contact plate 9 , and the lower end of the stabilizing plate 12 is movably connected inside the stabilizing groove 11 .
  • the fixed assembly includes a lower pressure groove 13, a first lower pressure plate 14, a second lower pressure plate 15, a chute 16, a fixed frame 17 and a guide groove 18.
  • the movable plate 6 is provided with a lower pressure groove 13 for the movement of the first lower pressure plate 14.
  • the lower end of the first lower pressure plate 14 is movably connected inside the lower pressure groove 13
  • the second lower pressure plate 15 is fixedly connected to the bottom of the first lower pressure plate 14, and the outer wall of the second lower pressure plate 15 is provided with a chute 16 for pushing
  • the fixed frame 17 is fixedly connected to the bottom of the movable plate 6, and the outer wall of the fixed frame 17 is provided with a guide groove 18 for guiding the movable plate.
  • the fixed component also includes a sliding rod 19, a stabilizing block 20, a clamping rod 21, a slot 22 and a second spring 23. Both sides of the sliding rod 19 are movably connected inside the chute 16, and both ends of the sliding rod 19 are movably connected. Inside the guide groove 18, both ends of the sliding rod 19 are fixedly connected with stabilizing blocks 20 for stabilizing the movement. The inside of the stabilizing block 20 abuts against the outer wall of the fixed frame 17. The clamping rod 21 is fixedly connected to the middle part of the sliding rod 19.
  • the inside of the movement groove 4 is provided with a clamping slot 22 for fixation, the outside of the clamping rod 21 and the inside of the clamping slot 22 are engaged with each other, the outer wall of the fixed frame 17 is fixedly connected to one end of the second spring 23, and the second spring 23 The other end is fixedly connected to the inner wall of the motion slot 4.
  • the bottom of the lower pressure rod 29 pushes the contact plate 9 downward, the contact plate 9 drives the first lower pressure plate 14 to move downward inside the lower pressure groove 13, and the first lower pressure plate 14 drives the second lower pressure plate 15 to move downward.
  • the second lower pressure plate 15 moves the sliding rod 19 toward the middle inside the guide groove 18 through the inclined groove 16 opened in the outer wall, so that the clamping rod 21 moves inward from the inside of the clamping slot 22. At this time, the clamping rod 21 cannot interact with the clamping slot 22. snap, thereby releasing the fixed state of the fixed component.
  • the stabilizing blocks 20 at both ends of the sliding rod 19 slide on the outer wall of the fixed frame 17 to prevent the sliding rod 19 from rotating or deflecting during movement, so that the clamping rod 21 tends to be stable during the movement. This prevents the clamping rod 21 from being able to effectively engage with the clamping groove 22 during subsequent engagement, thereby improving the effectiveness of the fixing component in fixing the movable plate 6 .
  • the PTFE reactor 44 contacts the contact plate 9 through the abutment plate 40 and pushes the contact plate 9 to move downward.
  • the contact plate 9 slows down the PTFE reactor 44 under the joint action of the first spring 8 and the stable telescopic rod 10
  • the impact on the equipment simultaneously reduces the damage to the PTFE reactor 44 and the equipment, effectively avoiding the problem of spillage or leakage of lithium hexafluorophosphate inside the PTFE reactor 44 caused by the impact.
  • the The stabilizing groove 11 moves downward inside the stabilizing plate 12, which can reduce the problem of the contact plate 9 being skewed due to the downward movement of the contact plate 12 and unable to transmit. It also prevents the problem of the first spring 8 being unable to buffer due to the skewing, thereby improving the efficiency of the operation. This ensures the stability of the contact plate 9 when in contact with the PTFE reactor 44.
  • Embodiment 3 Please refer to Figures 7 to 11.
  • the detection assembly includes a lifting slot 25, a third spring 26, a lifting frame 27 and a first stabilizing bar 28.
  • the upper end of the support frame 24 is provided with a lifting slot 25 for up and down movement.
  • the upper end of the third spring 26 is fixedly connected to the lower surface of the support frame 24,
  • the lifting frame 27 is fixedly connected to the lower end of the third spring 26,
  • the upper surface of the lifting frame 27 and close to the interior of the third spring 26 is connected with a first stabilizer bar 28.
  • the upper end of the first stabilizer rod 28 is movably connected to the middle part of the support frame 24, and the lower pressure rod 29 is fixedly connected to the lower surface of the lifting frame 27.
  • the detection component also includes the lifting barrel column 30, the opening 31, the rotating shaft 32, the rotating hub 33, the movable groove 34, the fourth spring 35, the limiting block 36, the limiting groove 37, the torsion spring 38 and the connecting belt 39.
  • the lifting barrel column 30 is fixedly connected to both ends of the lifting frame 27, and the lifting barrel column 30 is movably connected inside the lifting slot 25.
  • the outer wall of the lifting barrel column 30 is provided with an opening 31 for the movement of the connecting belt 39, and the rotating hub 33 is rotationally connected through the rotating shaft 32.
  • the outer wall of the rotating hub 33 is provided with a movable groove 34 for movement.
  • the fourth spring 35 is fixedly connected inside the movable groove 34, and the outside of the movable groove 34 is fixedly connected with a limiter for fixed positioning.
  • Block 36 the inner wall of the lifting barrel column 30 is provided with a limit groove 37 for fixed limit, the inside of the rotating hub 33 is fixedly connected to one end of the torsion spring 38, the other end of the torsion spring 38 is fixedly connected to the upper end of the connecting belt 39, and the connection The lower end of the belt 39 is fixedly connected to the upper surface of the abutment plate 40 .
  • the clamping assembly includes a pull rod 45, a transmission rod 46, a connecting rod 47 and a second stabilizer rod 48.
  • One end of the pull rod 45 is rotatably installed on the outside of the movable plate 6 through a fixed seat, and the other end of the pull rod 45 is fixedly connected to a transmission rod 46 for transmission.
  • the middle part of the outer wall connecting rod 47 of the transmission rod 46 is rotationally connected
  • the inner side of the connecting rod 47 is rotationally connected to the outer wall of the support frame 24
  • one end of the second stabilizer rod 48 is rotationally connected to the outside of the support frame 24 through a fixed seat
  • the stabilizer frame is clamped
  • the inner side of 49 is rotationally connected with the outer side of connecting rod 47.
  • the PTFE reactor 44 drives the abutment plate 40 to move downward on the outer wall of the support plate 2 during its rapid downward movement.
  • the abutment plate 40 drives the connecting belt 39 to rapidly extend downward, and the connecting belt 39 drives the torsion spring 38 Rapidly extending, the torsion spring 38 drives the rotating hub 33 to rotate rapidly on the rotating shaft 32.
  • the centrifugal force generated by the rotation of the rotating hub 33 causes the outward movement force of the limiting block 36 to be greater than the elastic force of the fourth spring 35.
  • the limiting block 36 is The inside of the movable groove 34 moves outward and stretches the fourth spring 35, and the limiting block 36 moves outward to the inside of the limiting groove 37, so that the limiting block 36 and the limiting groove 37 engage with each other, allowing the wheel hub 33 to be rotated Stop rotating, and the connecting belt 39 cannot stretch at this time, thereby achieving the effect of detecting whether the PTFE reactor 44 has fallen, and can detect whether the PTFE reactor 44 has dropped abnormally, reducing the risk of the PTFE reaction
  • the slider 44 falls and cannot be warned in advance, the inward movement of the sliding rod 19 makes it impossible for the clamping rod 21 to engage with the clamping slot 22.
  • the fixed component drives the movable plate 6.
  • the inside of the first movable port 3 moves outward, and the movable plate 6 makes the pull rod 45 drive the transmission rod 46 to move through the fixed seat.
  • the transmission rod 46 drives the connecting rod 47 to rotate inward.
  • the clamp The stabilizing frame 49 stably clamps the PTFE reactor 44 inward, thereby preventing the PTFE reactor 44 from tipping after it falls, thereby improving the safety of the PTFE reactor 44 in the process of producing lithium hexafluorophosphate. .
  • the first spring 8 stretches to drive the contact plate 9 to the highest position, the contact plate 9 drives the second lower pressure plate 15 to the highest position through the first lower pressure plate 14, and the second lower pressure plate 15 drives the slider through the chute 16.
  • the rod 19 is located at the outermost side of the guide groove 18.
  • the sliding rod 19 drives the clamping rod 21 and the clamping slot 22 to engage with each other.
  • the second spring 23 is in a stretched state.
  • the connecting belt 39 drives the abutment plate. 40 and the bottom of the PTFE reactor 44 are in contact with each other, and the third spring 26 is stretched so that the lifting frame 27 drives the lifting barrel column 30 to be at the highest position of the lifting slot 25 .
  • the PTFE reactor 44 When in use, the PTFE reactor 44 is installed on the fixed top plate 42 through the fixed jacket 43, and then the lithium hexafluorophosphate is processed and produced. When the PTFE reactor 44 is in the process of producing and processing lithium hexafluorophosphate, in one case, the PTFE reactor 44 If the fixation is not firm and falls, the PTFE reactor 44 will quickly move downward in the fixed jacket 43 because the abutting plate 40 and the bottom of the PTFE reactor 44 are in contact with each other. During the rapid downward movement of the PTFE reactor 44, the abutment plate 40 is driven to move downward on the outer wall of the support plate 2.
  • the abutment plate 40 drives the connecting belt 39 to rapidly extend downward, and the connecting belt 39 drives the torsion spring 38 to rapidly extend.
  • the torsion spring 38 drives the rotating hub 33 to rotate rapidly on the rotating shaft 32.
  • the centrifugal force generated by the rotation of the rotating hub 33 causes the outward movement force of the limiting block 36 to be greater than the elastic force of the fourth spring 35.
  • the limiting block 36 moves in the movable groove 34
  • the inside of the movement moves outward and stretches the fourth spring 35, and the limiting block 36 moves outward to the inside of the limiting groove 37, so that the limiting block 36 and the limiting groove 37 engage with each other, which can cause the rotating hub 33 to stop rotating.
  • the connecting belt 39 cannot be stretched, thereby achieving the effect of detecting whether the PTFE reactor 44 has fallen, and can detect whether the PTFE reactor 44 has dropped abnormally, reducing the risk of the PTFE reactor 44 falling. Problems that cannot be warned in advance.
  • the PTFE reactor 44 causes the abutment plate 40 to continue to move downward.
  • the abutment plate 40 drives the lifting barrel column 30 to move in the lifting slot 25 through the connecting belt 39.
  • the interior moves downward, and the lifting barrel column 30 drives the lifting frame 27 to move downward and stretches the third spring 26.
  • the downward movement of the lifting frame 27 drives the downward pressure rod 29 to move downward inside the second movable port 41.
  • the bottom of the rod 29 pushes the contact plate 9 downward.
  • the contact plate 9 drives the first lower pressure plate 14 to move downward inside the lower pressure groove 13.
  • the first lower pressure plate 14 drives the second lower pressure plate 15 to move downward.
  • the second lower pressure plate 15 Through the inclined groove 16 opened on the outer wall, the sliding rod 19 moves toward the middle inside the guide groove 18, causing the clamping rod 21 to move inward from the inside of the clamping slot 22. At this time, the clamping rod 21 cannot engage with the clamping slot 22, and then the clamping rod 21 cannot engage with the clamping slot 22, and the clamping rod 21 can be released. In the fixed state of the fixed component, the sliding rod 19 can be prevented from rotating during the movement by the stabilizing blocks 20 at both ends of the sliding rod 19 sliding on the outer wall of the fixed frame 17, thereby causing the clamping rod 21 to tend to rotate during the movement.
  • the clamping rod 21 can be effectively clamped during the clamping process with the clamping groove 22, thereby improving the effectiveness of the fixing component in fixing the movable plate 6; when the sliding rod 19 moves inward, the clamping lever 21 can be effectively clamped.
  • the rod 21 cannot engage with the slot 22.
  • the fixed component drives the movable plate 6 to move outward inside the first movable opening 3.
  • the movable plate 6 passes through the fixed seat to make the pull rod 45
  • the transmission rod 46 is driven to move, and the transmission rod 46 drives the connecting rod 47 to rotate inward.
  • the clamping stabilizer 49 can stably clamp the PTFE reactor 44 inward, thereby enabling This prevents the PTFE reactor 44 from tipping after being dropped, thereby improving the safety of the PTFE reactor 44 in the process of producing lithium hexafluorophosphate.
  • the PTFE reactor 44 contacts the contact plate 9 through the abutment plate 40 and pushes the contact plate 9 to move downward.
  • the contact plate 9 will slow down the PTFE reactor under the joint action of the first spring 8 and the stable telescopic rod 10 44's impact on the equipment simultaneously reduces the damage to the PTFE reactor 44 and the equipment, effectively avoiding the problem of spillage or leakage of lithium hexafluorophosphate inside the PTFE reactor 44 caused by the impact.
  • the stabilizing groove 11 is driven to move downward inside the stabilizing plate 12, thereby reducing the problem of the contact plate 9 being skewed and unable to transmit due to the downward movement of the contact plate 9, and at the same time preventing the first spring 8 from being unable to buffer due to the skewing.
  • the stability of the contact plate 9 when in contact with the PTFE reactor 44 is improved.
  • the fixed assembly When the contact plate 9 moves downward, the fixed assembly is triggered to contact and fix.
  • the fixed assembly drives the movable plate 6 to move on the base 1.
  • the movable plate 6 rolls inside the rolling groove 5 through the roller 7 so that the movable plate 6 moves in the first movement.
  • the inside of the port 3 moves outward, and the movable plate 6 drives the clamping assembly so that the clamping stabilizer 49 clamps the PTFE reactor 44, thereby preventing the PTFE reactor 44 from tipping after it falls.

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Abstract

一种六氟磷酸锂制备用具有夹套的四氟反应器，包括底座（1），底座（1）上通过螺栓固定安装有支撑板（2），支撑板（2）的下端开设有第一活动口（3），底座（1）的上表面开设有用于限位活动的运动槽（4），运动槽（4）的内部开设有用于滚动的滚动槽（5），底座（1）上活动设置有活动板（6），通过第二弹簧（23）的收缩作用下使得固定组件带动活动板（6）在第一活动口（3）的内部向外活动，活动板（6）通过固定座使得拉杆（45）带动传动杆（46）运动，传动杆（46）带动连杆（47）向内侧转动，同时配合第二稳定杆（48）向内侧运动能够使得夹持稳定架（49）稳定的向内侧对四氟反应器进行夹持。

Description

一种六氟磷酸锂制备用具有夹套的四氟反应器 技术领域
本发明涉及六氟磷酸锂制备技术领域，具体为一种六氟磷酸锂制备用具有夹套的四氟反应器。
 背景技术
六氟磷酸锂为白色结晶或粉末，潮解性强；易溶于水、还溶于低浓度甲醇、乙醇、丙酮、碳酸酯类等有机溶剂，暴露空气中或加热时六氟磷酸锂在空气中由于水蒸气的作用而迅速分解，放出白色烟雾，进而在其生产过程中不能够出现泄漏的情况，六氟磷酸锂在都是通过四氟反应器进行生产，其中四氟反应器都是通过夹套进行固定，其夹套容易出现夹持不牢固松动掉落的情况，当夹套无法固定四氟反应器后就会出现倾倒，其倾倒后就会造成六氟磷酸锂的泄漏，进而导致生产安全事故的发生，当泄漏的六氟磷酸锂与空气接触后加热分解，进而散发出大量的白色烟雾，对工厂的其他生产设备可能会造成一定的影响。
为此，提出一种六氟磷酸锂制备用具有夹套的四氟反应器。
 技术问题
本发明的目的在于提供一种六氟磷酸锂制备用具有夹套的四氟反应器，以解决上述背景技术中提出的问题。
 技术解决方案
为实现上述目的，本发明提供如下技术方案：一种六氟磷酸锂制备用具有夹套的四氟反应器，包括底座，所述底座上通过螺栓固定安装有支撑板，所述支撑板的下端开设有第一活动口，所述底座的上表面开设有用于限位活动的运动槽，所述运动槽的内部开设有用于滚动的滚动槽，所述底座上活动设置有活动板，所述活动板的外侧活动连接在第一活动口的内部，所述活动板的底部通过安装板设置有用于稳定活动的滚轮，所述滚轮滚动连接在滚动槽的内部，所述活动板上设置有接触板，所述接触板与活动板连接处设置有用于稳定接触板上下的稳定组件，所述活动板的底部且靠近运动槽的内部设置有用于限位固定的固定组件，所述底座上固定安装有用于支撑的支撑架，所述支撑架的上端设置有用于检测掉落的检测组件，所述检测组件的底部固定连接有用于推动接触板的下压杆，所述下压杆的底部与接触板的上表面相互抵接，所述检测组件的下端固定连接有用于托举的抵接板，所述抵接板的外侧活动连接在支撑板的外壁，所述抵接板上贯穿开设有用于下压杆活动的第二活动口，所述下压杆的中部活动连接在第二活动口的内部，所述支撑板的顶部通过螺栓固定连接有用于固定支撑的固定顶板，所述固定顶板上固定安装有固定夹套，所述固定夹套的内部固定连接有四氟反应器，所述四氟反应器的底部与抵接板的上表面相互抵接，所述支撑架的外壁设置有用于稳定夹持四氟反应器的夹持组件。
优选的，所述稳定组件包括第一弹簧、稳定伸缩杆、稳定槽和稳定板，所述接触板通过第一弹簧固定连接在活动板的顶部，所述稳定伸缩杆的上端转动连接在接触板的下表面，所述稳定伸缩杆的下端转动连接在活动板的上表面，所述活动板上开设有用于稳定板活动的稳定槽，所述稳定板固定连接在接触板的下表面，所述稳定板的下端活动连接在稳定槽的内部。
优选的，所述固定组件包括下压槽、第一下压板、第二下压板、斜槽、固定框和导向槽，所述活动板上开设有用于第一下压板活动的下压槽，所述第一下压板的下端活动连接在下压槽的内部，所述第二下压板固定连接在第一下压板的底部，所述第二下压板的外壁贯穿开设有用于推动的斜槽，所述固定框固定连接在活动板的底部，所述固定框的外壁开设有用于导向活动导向槽。
优选的，所述固定组件还包括滑杆、稳定块、卡杆、卡槽和第二弹簧，所述滑杆的两侧均活动连接在斜槽的内部，所述滑杆的两端均活动连接在导向槽的内部，所述滑杆的两端固定连接有用于稳定活动的稳定块，所述稳定块的内侧与固定框的外壁相互抵接，所述卡杆固定连接在滑杆的中部，所述运动槽的内部开设有用于固定的卡槽，所述卡杆的外侧与卡槽的内部相互卡接，所述固定框的外壁与第二弹簧的一端固定连接，所述第二弹簧的另一端与运动槽的内壁固定连接。
优选的，所述检测组件包括升降槽、第三弹簧、升降架和第一稳定杆，所述支撑架的上端开设有用于上下活动的升降槽，所述第三弹簧的上端固定连接在支撑架的下表面，所述升降架固定连接在第三弹簧的下端，所述升降架的上表面且靠近第三弹簧的内部连接有第一稳定杆，所述第一稳定杆的上端活动连接在支撑架的中部，所述下压杆固定连接在升降架的下表面。
优选的，所述检测组件还包括升降桶柱、开口、转动轴、转动轮毂、活动槽、第四弹簧、限位块、限位槽、扭簧和连接带，所述升降桶柱固定连接在升降架的两端，所述升降桶柱活动连接在升降槽的内部，所述升降桶柱的外壁开设有用于连接带活动的开口，所述转动轮毂通过转动轴转动连接在升降桶柱的内部，所述转动轮毂的外壁开设有用于活动的活动槽，所述第四弹簧固定连接在活动槽的内部，所述活动槽的外侧固定连接有用于固定限位的限位块，所述升降桶柱的内壁开设有用于固定限位的限位槽，所述转动轮毂内部与扭簧的一端固定连接，所述扭簧的另一端与连接带的上端固定连接，所述连接带的下端与抵接板的上表面固定连接。
优选的，所述夹持组件包括拉杆、传动杆、连杆和第二稳定杆，所述拉杆一端通过固定座转动安装在活动板的外侧，所述拉杆的另一端固定连接有用于传动的传动杆，所述传动杆的外壁连杆的中部转动连接，所述连杆的内侧与支撑架的外壁转动连接，所述第二稳定杆一端通过固定座转动连接在支撑架的外侧，所述夹持稳定架的内侧与连杆的外侧转动连接。
优选的，所述抵接板的上表面设置为托盘状，所述抵接板顶部的托盘尺寸与四氟反应器底部的尺寸相互适配。
优选的，所述夹持稳定架的内侧设置为圆弧状，所述夹持稳定架内侧的圆弧尺寸与四氟反应器的尺寸相互适配。
 有益效果
与现有技术相比，本发明的有益效果是：1、本发明通过在第二弹簧的收缩作用下使得固定组件带动活动板在第一活动口的内部向外活动，活动板通过固定座使得拉杆带动传动杆运动，传动杆带动连杆向内侧转动，同时配合第二稳定杆向内侧运动能够使得夹持稳定架稳定的向内侧对四氟反应器进行夹持，进而能够防止四氟反应器掉落后出现倾倒的问题，进而提高了四氟反应器在生产六氟磷酸锂过程中的安全性；2、本发明通过抵接板带动连接带迅速向下伸展，连接带带动扭簧迅速伸展，扭簧带动转动轮毂在转动轴上快速转动，此时转动轮毂转动产生的离心力使得限位块向外运动的力大于第四弹簧的弹力，限位块在活动槽的内部向外侧运动并拉伸第四弹簧，限位块向外运动到限位槽的内部，使得限位块与限位槽相互卡接，能够使得转动轮毂停止转动，此时连接带无法伸展，进而实现了对四氟反应器是否掉落的进行检测的效果，能够检测四氟反应器是否出现异常掉落的情况，减少了因为四氟反应器掉落而无法提前预警的问题；3、本发明通过滑杆两端的稳定块在固定框外壁滑动的作用下，能够防止滑杆在运动的过程中出现转动，进而能够使得卡杆在运动的过程中趋于稳定，进而能够使得卡杆在与卡槽卡接的过程中能够有效地进行卡接，提高了固定组件对活动板进行固定的有效性；4、本发明通过固定夹套无法固定四氟反应器，进而会出现四氟反应器迅速向下运动，四氟反应器通过抵接板与接触板接触并推动接触板向下运动，接触板会通过在第一弹簧与稳定伸缩杆的共同作用下会减缓四氟反应器对设备的冲击，同时降低了四氟反应器与设备的损伤，有效地避免了撞击造成四氟反应器内部的六氟磷酸锂洒落或是泄漏的问题；5、本发明通过接触板向下运动的过程中带动稳定槽在稳定板的内部向下运动，进而能够减少接触板向下运动使得出现歪斜而无法传动的问题，同时也防止歪斜而导致的第一弹簧无法进行缓冲的问题，进而提高了接触板与四氟反应器接触时的稳定性。
 附图说明
图1为本发明整体结构立体图。
图2为本发明整体剖视结构立体图。
图3为本发明图2中A处结构放大图。
图4为本发明内部结构立体图。
图5为本发明固定组件结构立体图。
图6为本发明固定组件内部结构立体图。
图7为本发明升降桶柱内部结构立体图。
图8为本发明图6中B处结构放大图。
图9为本发明升降桶柱剖视结构立体图。
图10为本发明图8中C处结构放大图。
图11为本发明夹持组件局部结构立体图。
图中：1、底座；2、支撑板；3、第一活动口；4、运动槽；5、滚动槽；6、活动板；7、滚轮；8、第一弹簧；9、接触板；10、稳定伸缩杆；11、稳定槽；12、稳定板；13、下压槽；14、第一下压板；15、第二下压板；16、斜槽；17、固定框；18、导向槽；19、滑杆；20、稳定块；21、卡杆；22、卡槽；23、第二弹簧；24、支撑架；25、升降槽；26、第三弹簧；27、升降架；28、第一稳定杆；29、下压杆；30、升降桶柱；31、开口；32、转动轴；33、转动轮毂；34、活动槽；35、第四弹簧；36、限位块；37、限位槽；38、扭簧；39、连接带；40、抵接板；41、第二活动口；42、固定顶板；43、固定夹套；44、四氟反应器；45、拉杆；46、传动杆；47、连杆；48、第二稳定杆；49、夹持稳定架。
 本发明的实施方式
下面将结合本发明实施例中的附图，对本发明实施例中的技术方案进行清楚、完整地描述，显然，所描述的实施例仅仅是本发明一部分实施例，而不是全部的实施例。基于本发明中的实施例，本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例，都属于本发明的保护的范围。
请参阅图1至图11，本发明提供一种技术方案：实施例一:请参照图1至图11所示，一种六氟磷酸锂制备用具有夹套的四氟反应器，包括底座1，底座1上通过螺栓固定安装有支撑板2，支撑板2的下端开设有第一活动口3，底座1的上表面开设有用于限位活动的运动槽4，运动槽4的内部开设有用于滚动的滚动槽5，底座1上活动设置有活动板6，活动板6的外侧活动连接在第一活动口3的内部，活动板6的底部通过安装板设置有用于稳定活动的滚轮7，滚轮7滚动连接在滚动槽5的内部，活动板6上设置有接触板9，接触板9与活动板6连接处设置有用于稳定接触板9上下的稳定组件，活动板6的底部且靠近运动槽4的内部设置有用于限位固定的固定组件，底座1上固定安装有用于支撑的支撑架24，支撑架24的上端设置有用于检测掉落的检测组件，检测组件的底部固定连接有用于推动接触板9的下压杆29，下压杆29的底部与接触板9的上表面相互抵接，检测组件的下端固定连接有用于托举的抵接板40，抵接板40的外侧活动连接在支撑板2的外壁，抵接板40上贯穿开设有用于下压杆29活动的第二活动口41，下压杆29的中部活动连接在第二活动口41的内部，支撑板2的顶部通过螺栓固定连接有用于固定支撑的固定顶板42，固定顶板42上固定安装有固定夹套43，固定夹套43的内部固定连接有四氟反应器44，四氟反应器44的底部与抵接板40的上表面相互抵接，支撑架24的外壁设置有用于稳定夹持四氟反应器44的夹持组件。
工作时，将四氟反应器44通过固定夹套43安装在固定顶板42上，进而对六氟磷酸锂进行加工生产，当四氟反应器44在生产加工六氟磷酸锂过程中，四氟反应器44若出现固定不牢固而掉落的情况时，四氟反应器44会迅速地向下运动，此时四氟反应器44向下运动会带动抵接板40在支撑板2的外壁迅速向下运动，抵接板40迅速向下运动时会带动检测组件向下运动，检测组件带动下压杆29向下运动，使得下压杆29向下推动接触板9并使得固定组件接触限制，固定组件带动活动板6在底座1上进行运动，活动板6带动夹持组件使得夹持稳定架49对四氟反应器44进行夹持。
四氟反应器44若出现松动掉落的情况时，四氟反应器44会逐渐向下运动，当四氟反应器44向下运动到固定夹套43无法固定的位置后，此时四氟反应器44带动抵接板40已运动到最低位置，四氟反应器44掉落会与接触板9抵接，此时通过接触板9底部的稳定组件的作用下能够减缓四氟反应器44的掉落，进而对四氟反应器44的掉落进行保护，同时四氟反应器44通过抵接板40与接触板9接触时，进而能够推动接触板9向下使得固定组件接触限制，固定组件带动活动板6在底座1上进行运动，同时活动板6通过滚轮7在滚动槽5的内部滚动使得活动板6在第一活动口3的内部向外侧运动，活动板6带动夹持组件使得夹持稳定架49对四氟反应器44进行夹持，进而能够防止四氟反应器44掉落后出现倾倒的问题。
实施例二:请参照图1至图6所示，稳定组件包括第一弹簧8、稳定伸缩杆10、稳定槽11和稳定板12，接触板9通过第一弹簧8固定连接在活动板6的顶部，稳定伸缩杆10的上端转动连接在接触板9的下表面，稳定伸缩杆10的下端转动连接在活动板6的上表面，活动板6上开设有用于稳定板12活动的稳定槽11，稳定板12固定连接在接触板9的下表面，稳定板12的下端活动连接在稳定槽11的内部。
固定组件包括下压槽13、第一下压板14、第二下压板15、斜槽16、固定框17和导向槽18，活动板6上开设有用于第一下压板14活动的下压槽13，第一下压板14的下端活动连接在下压槽13的内部，第二下压板15固定连接在第一下压板14的底部，第二下压板15的外壁贯穿开设有用于推动的斜槽16，固定框17固定连接在活动板6的底部，固定框17的外壁开设有用于导向活动导向槽18。
固定组件还包括滑杆19、稳定块20、卡杆21、卡槽22和第二弹簧23，滑杆19的两侧均活动连接在斜槽16的内部，滑杆19的两端均活动连接在导向槽18的内部，滑杆19的两端固定连接有用于稳定活动的稳定块20，稳定块20的内侧与固定框17的外壁相互抵接，卡杆21固定连接在滑杆19的中部，运动槽4的内部开设有用于固定的卡槽22，卡杆21的外侧与卡槽22的内部相互卡接，固定框17的外壁与第二弹簧23的一端固定连接，第二弹簧23的另一端与运动槽4的内壁固定连接。
工作时，下压杆29的底部向下推动接触板9，接触板9带动第一下压板14在下压槽13的内部向下运动，第一下压板14带动第二下压板15向下运动，第二下压板15通过外壁开设的斜槽16使得滑杆19在导向槽18的内部向中部运动，使得卡杆21从卡槽22内部向内侧运动，此时卡杆21无法与卡槽22相互卡接，进而解除固定组件的固定状态。
通过滑杆19两端的稳定块20在固定框17外壁滑动的作用下，能够防止滑杆19在运动的过程中出现转动或偏转的问题，使得卡杆21在运动的过程中趋于稳定，能够防止卡杆21在与卡槽22后续卡接的过程中能够有效地进行卡接，进而提高了固定组件对活动板6进行固定的有效性。
四氟反应器44通过抵接板40与接触板9接触并推动接触板9向下运动，接触板9会通过在第一弹簧8与稳定伸缩杆10的共同作用下会减缓四氟反应器44对设备的冲击，同时降低了四氟反应器44与设备的损伤，有效地避免了撞击造成四氟反应器44内部的六氟磷酸锂洒落或是泄漏的问题，在接触板9向下运动的过程中带动稳定槽11在稳定板12的内部向下运动，进而能够减少接触板9向下运动使得出现歪斜而无法传动的问题，同时也防止歪斜而导致的第一弹簧8无法进行缓冲的问题，进而提高了接触板9与四氟反应器44接触时的稳定性。
实施例三:请参照图7至图11所示，检测组件包括升降槽25、第三弹簧26、升降架27和第一稳定杆28，支撑架24的上端开设有用于上下活动的升降槽25，第三弹簧26的上端固定连接在支撑架24的下表面，升降架27固定连接在第三弹簧26的下端，升降架27的上表面且靠近第三弹簧26的内部连接有第一稳定杆28，第一稳定杆28的上端活动连接在支撑架24的中部，下压杆29固定连接在升降架27的下表面。
检测组件还包括升降桶柱30、开口31、转动轴32、转动轮毂33、活动槽34、第四弹簧35、限位块36、限位槽37、扭簧38和连接带39，升降桶柱30固定连接在升降架27的两端，升降桶柱30活动连接在升降槽25的内部，升降桶柱30的外壁开设有用于连接带39活动的开口31，转动轮毂33通过转动轴32转动连接在升降桶柱30的内部，转动轮毂33的外壁开设有用于活动的活动槽34，第四弹簧35固定连接在活动槽34的内部，活动槽34的外侧固定连接有用于固定限位的限位块36，升降桶柱30的内壁开设有用于固定限位的限位槽37，转动轮毂33内部与扭簧38的一端固定连接，扭簧38的另一端与连接带39的上端固定连接，连接带39的下端与抵接板40的上表面固定连接。
夹持组件包括拉杆45、传动杆46、连杆47和第二稳定杆48，拉杆45一端通过固定座转动安装在活动板6的外侧，拉杆45的另一端固定连接有用于传动的传动杆46，传动杆46的外壁连杆47的中部转动连接，连杆47的内侧与支撑架24的外壁转动连接，第二稳定杆48一端通过固定座转动连接在支撑架24的外侧，夹持稳定架49的内侧与连杆47的外侧转动连接。
工作时，四氟反应器44迅速向下运动的过程中带动抵接板40在支撑板2的外壁向下运动，抵接板40带动连接带39迅速向下伸展，连接带39带动扭簧38迅速伸展，扭簧38带动转动轮毂33在转动轴32快速转动，此时转动轮毂33的转动产生的离心力使得限位块36向外运动的力大于第四弹簧35的弹力，限位块36在活动槽34的内部向外侧运动并拉伸第四弹簧35，限位块36向外运动到限位槽37的内部，使得限位块36与限位槽37相互卡接，能够使得转动轮毂33停止转动，此时连接带39无法伸展，进而实现了对四氟反应器44是否掉落的进行检测的效果，能够检测四氟反应器44是否出现异常掉落的情况，减少了因为四氟反应器44掉落而无法提前预警的问题，滑杆19向内运动时使得卡杆21无法与卡槽22相互卡接，此时在第二弹簧23的收缩作用下使得固定组件带动活动板6在第一活动口3的内部向外活动，活动板6通过固定座使得拉杆45带动传动杆46运动，传动杆46带动连杆47向内侧转动，同时配合第二稳定杆48向内侧运动能够使得夹持稳定架49稳定的向内侧对四氟反应器44进行夹持，进而能够防止四氟反应器44掉落后出现倾倒的问题，进而提高了四氟反应器44在生产六氟磷酸锂过程中的安全性。
工作原理：初始状态下：第一弹簧8伸展带动接触板9处于最高位置，接触板9通过第一下压板14带动第二下压板15处于最高位置，第二下压板15通过斜槽16带动滑杆19处于导向槽18的最外侧，滑杆19带动卡杆21与卡槽22相互卡接，第二弹簧23处于拉伸状态，同时在扭簧38收缩作用下使得连接带39带动抵接板40与四氟反应器44的底部相互抵接，第三弹簧26拉伸使得升降架27带动升降桶柱30处于升降槽25的最高位置。
使用时，将四氟反应器44通过固定夹套43安装在固定顶板42上，进而对六氟磷酸锂进行加工生产，当四氟反应器44在生产加工六氟磷酸锂过程中，其中一种情况，四氟反应器44若出现固定不牢固而掉落的情况时，此时四氟反应器44会在固定夹套43内迅速向下运动，因为抵接板40与四氟反应器44的底部相互抵接，在四氟反应器44迅速向下运动的过程中带动抵接板40在支撑板2的外壁向下运动，抵接板40带动连接带39迅速向下伸展，连接带39带动扭簧38迅速伸展，扭簧38带动转动轮毂33在转动轴32快速转动，此时转动轮毂33的转动产生的离心力使得限位块36向外运动的力大于第四弹簧35的弹力，限位块36在活动槽34的内部向外侧运动并拉伸第四弹簧35，限位块36向外运动到限位槽37的内部，使得限位块36与限位槽37相互卡接，能够使得转动轮毂33停止转动，此时连接带39无法伸展，进而实现了对四氟反应器44是否掉落的进行检测的效果，能够检测四氟反应器44是否出现异常掉落的情况，减少了因为四氟反应器44掉落而无法提前预警的问题。
与此同时在四氟反应器44向下运动的推力作用下，四氟反应器44使得抵接板40继续向下运动，抵接板40通过连接带39带动升降桶柱30在升降槽25的内部向下运动，升降桶柱30带动升降架27向下运动并拉伸第三弹簧26，升降架27向下运动带动下压杆29在第二活动口41的内部向下运动，此时下压杆29的底部向下推动接触板9，接触板9带动第一下压板14在下压槽13的内部向下运动，第一下压板14带动第二下压板15向下运动，第二下压板15通过外壁开设的斜槽16使得滑杆19在导向槽18的内部向中部运动，使得卡杆21从卡槽22内部向内侧运动，此时卡杆21无法与卡槽22相互卡接，进而解除固定组件的固定状态，通过滑杆19两端的稳定块20在固定框17外壁滑动的作用下，能够防止滑杆19在运动的过程中出现转动，进而能够使得卡杆21在运动的过程中趋于稳定，进而能够使得卡杆21在与卡槽22卡接的过程中能够有效地进行卡接，提高了固定组件对活动板6进行固定的有效性；在滑杆19向内运动时使得卡杆21无法与卡槽22相互卡接，此时在第二弹簧23的收缩作用下使得固定组件带动活动板6在第一活动口3的内部向外活动，活动板6通过固定座使得拉杆45带动传动杆46运动，传动杆46带动连杆47向内侧转动，同时配合第二稳定杆48向内侧运动能够使得夹持稳定架49稳定的向内侧对四氟反应器44进行夹持，进而能够防止四氟反应器44掉落后出现倾倒的问题，进而提高了四氟反应器44在生产六氟磷酸锂过程中的安全性。
另一种情况，若四氟反应器44出现松动而掉落时，四氟反应器44会在固定夹套43的内部缓慢地向下运动，四氟反应器44缓慢地向下掉落，四氟反应器44会带动抵接板40缓慢地向下运动，抵接板40带动连接带39缓慢地在升降桶柱30的内部缓慢向下伸展，连接带39通过扭簧38缓慢地带动转动轮毂33转动，此时无法触发检测组件进行检测，但是当四氟反应器44掉落到最低位置时，固定夹套43无法固定四氟反应器44，进而会出现四氟反应器44迅速向下运动，四氟反应器44通过抵接板40与接触板9接触并推动接触板9向下运动，接触板9会通过在第一弹簧8与稳定伸缩杆10的共同作用下会减缓四氟反应器44对设备的冲击，同时降低了四氟反应器44与设备的损伤，有效地避免了撞击造成四氟反应器44内部的六氟磷酸锂洒落或是泄漏的问题，在接触板9向下运动的过程中带动稳定槽11在稳定板12的内部向下运动，进而能够减少接触板9向下运动使得出现歪斜而无法传动的问题，同时也防止歪斜而导致的第一弹簧8无法进行缓冲的问题，进而提高了接触板9与四氟反应器44接触时的稳定性。
当接触板9向下运动后会触发固定组件接触固定，固定组件带动活动板6在底座1上进行运动，同时活动板6通过滚轮7在滚动槽5的内部滚动使得活动板6在第一活动口3的内部向外侧运动，活动板6带动夹持组件使得夹持稳定架49对四氟反应器44进行夹持，进而能够防止四氟反应器44掉落后出现倾倒的问题。
需要说明的是，在本文中，诸如第一和第二等之类的关系术语仅仅用来将一个实体或者操作与另一个实体或操作区分开来，而不一定要求或者暗示这些实体或操作之间存在任何这种实际的关系或者顺序。而且，术语“包括”、“包含”或者其任何其他变体意在涵盖非排他性地包含，从而使得包括一系列要素的过程、方法、物品或者设备不仅包括那些要素，而且还包括没有明确列出的其他要素，或者是还包括为这种过程、方法、物品或者设备所固有的要素。在没有更多限制的情况下，由语句“包括一个……”限定的要素，并不排除在包括所述要素的过程、方法、物品或者设备中还存在另外的相同要素。
尽管已经示出和描述了本发明的实施例，对于本领域的普通技术人员而言，可以理解在不脱离本发明的原理和精神的情况下可以对这些实施例进行多种变化、修改、替换和变型，本发明的范围由所附权利要求及其等同物限定。

Claims (9)

  1. 一种六氟磷酸锂制备用具有夹套的四氟反应器，包括底座（1），其特征在于：所述底座（1）上通过螺栓固定安装有支撑板（2），所述支撑板（2）的下端开设有第一活动口（3），所述底座（1）的上表面开设有用于限位活动的运动槽（4），所述运动槽（4）的内部开设有用于滚动的滚动槽（5），所述底座（1）上活动设置有活动板（6），所述活动板（6）的外侧活动连接在第一活动口（3）的内部，所述活动板（6）的底部通过安装板设置有用于稳定活动的滚轮（7），所述滚轮（7）滚动连接在滚动槽（5）的内部，所述活动板（6）上设置有接触板（9），所述接触板（9）与活动板（6）连接处设置有用于稳定接触板（9）上下的稳定组件，所述活动板（6）的底部且靠近运动槽（4）的内部设置有用于限位固定的固定组件，所述底座（1）上固定安装有用于支撑的支撑架（24），所述支撑架（24）的上端设置有用于检测掉落的检测组件，所述检测组件的底部固定连接有用于推动接触板（9）的下压杆（29），所述下压杆（29）的底部与接触板（9）的上表面相互抵接，所述检测组件的下端固定连接有用于托举的抵接板（40），所述抵接板（40）的外侧活动连接在支撑板（2）的外壁，所述抵接板（40）上贯穿开设有用于下压杆（29）活动的第二活动口（41），所述下压杆（29）的中部活动连接在第二活动口（41）的内部，所述支撑板（2）的顶部通过螺栓固定连接有用于固定支撑的固定顶板（42），所述固定顶板（42）上固定安装有固定夹套（43），所述固定夹套（43）的内部固定连接有四氟反应器（44），所述四氟反应器（44）的底部与抵接板（40）的上表面相互抵接，所述支撑架（24）的外壁设置有用于稳定夹持四氟反应器（44）的夹持组件。
  2. 根据权利要求1所述的一种六氟磷酸锂制备用具有夹套的四氟反应器，其特征在于：所述稳定组件包括第一弹簧（8）、稳定伸缩杆（10）、稳定槽（11）和稳定板（12），所述接触板（9）通过第一弹簧（8）固定连接在活动板（6）的顶部，所述稳定伸缩杆（10）的上端转动连接在接触板（9）的下表面，所述稳定伸缩杆（10）的下端转动连接在活动板（6）的上表面，所述活动板（6）上开设有用于稳定板（12）活动的稳定槽（11），所述稳定板（12）固定连接在接触板（9）的下表面，所述稳定板（12）的下端活动连接在稳定槽（11）的内部。
  3. 根据权利要求1所述的一种六氟磷酸锂制备用具有夹套的四氟反应器，其特征在于：所述固定组件包括下压槽（13）、第一下压板（14）、第二下压板（15）、斜槽（16）、固定框（17）和导向槽（18），所述活动板（6）上开设有用于第一下压板（14）活动的下压槽（13），所述第一下压板（14）的下端活动连接在下压槽（13）的内部，所述第二下压板（15）固定连接在第一下压板（14）的底部，所述第二下压板（15）的外壁贯穿开设有用于推动的斜槽（16），所述固定框（17）固定连接在活动板（6）的底部，所述固定框（17）的外壁开设有用于导向活动导向槽（18）。
  4. 根据权利要求3所述的一种六氟磷酸锂制备用具有夹套的四氟反应器，其特征在于：所述固定组件还包括滑杆（19）、稳定块（20）、卡杆（21）、卡槽（22）和第二弹簧（23），所述滑杆（19）的两侧均活动连接在斜槽（16）的内部，所述滑杆（19）的两端均活动连接在导向槽（18）的内部，所述滑杆（19）的两端固定连接有用于稳定活动的稳定块（20），所述稳定块（20）的内侧与固定框（17）的外壁相互抵接，所述卡杆（21）固定连接在滑杆（19）的中部，所述运动槽（4）的内部开设有用于固定的卡槽（22），所述卡杆（21）的外侧与卡槽（22）的内部相互卡接，所述固定框（17）的外壁与第二弹簧（23）的一端固定连接，所述第二弹簧（23）的另一端与运动槽（4）的内壁固定连接。
  5. 根据权利要求1所述的一种六氟磷酸锂制备用具有夹套的四氟反应器，其特征在于：所述检测组件包括升降槽（25）、第三弹簧（26）、升降架（27）和第一稳定杆（28），所述支撑架（24）的上端开设有用于上下活动的升降槽（25），所述第三弹簧（26）的上端固定连接在支撑架（24）的下表面，所述升降架（27）固定连接在第三弹簧（26）的下端，所述升降架（27）的上表面且靠近第三弹簧（26）的内部连接有第一稳定杆（28），所述第一稳定杆（28）的上端活动连接在支撑架（24）的中部，所述下压杆（29）固定连接在升降架（27）的下表面。
  6. 根据权利要求5所述的一种六氟磷酸锂制备用具有夹套的四氟反应器，其特征在于：所述检测组件还包括升降桶柱（30）、开口（31）、转动轴（32）、转动轮毂（33）、活动槽（34）、第四弹簧（35）、限位块（36）、限位槽（37）、扭簧（38）和连接带（39），所述升降桶柱（30）固定连接在升降架（27）的两端，所述升降桶柱（30）活动连接在升降槽（25）的内部，所述升降桶柱（30）的外壁开设有用于连接带（39）活动的开口（31），所述转动轮毂（33）通过转动轴（32）转动连接在升降桶柱（30）的内部，所述转动轮毂（33）的外壁开设有用于活动的活动槽（34），所述第四弹簧（35）固定连接在活动槽（34）的内部，所述活动槽（34）的外侧固定连接有用于固定限位的限位块（36），所述升降桶柱（30）的内壁开设有用于固定限位的限位槽（37），所述转动轮毂（33）内部与扭簧（38）的一端固定连接，所述扭簧（38）的另一端与连接带（39）的上端固定连接，所述连接带（39）的下端与抵接板（40）的上表面固定连接。
  7. 根据权利要求1所述的一种六氟磷酸锂制备用具有夹套的四氟反应器，其特征在于：所述夹持组件包括拉杆（45）、传动杆（46）、连杆（47）和第二稳定杆（48），所述拉杆（45）一端通过固定座转动安装在活动板（6）的外侧，所述拉杆（45）的另一端固定连接有用于传动的传动杆（46），所述传动杆（46）的外壁连杆（47）的中部转动连接，所述连杆（47）的内侧与支撑架（24）的外壁转动连接，所述第二稳定杆（48）一端通过固定座转动连接在支撑架（24）的外侧，所述夹持稳定架（49）的内侧与连杆（47）的外侧转动连接。
  8. 根据权利要求1所述的一种六氟磷酸锂制备用具有夹套的四氟反应器，其特征在于：所述抵接板（40）的上表面设置为托盘状，所述抵接板（40）顶部的托盘尺寸与四氟反应器（44）底部的尺寸相互适配。
  9. 根据权利要求7所述的一种六氟磷酸锂制备用具有夹套的四氟反应器，其特征在于：所述夹持稳定架（49）的内侧设置为圆弧状，所述夹持稳定架（49）内侧的圆弧尺寸与四氟反应器（44）的尺寸相互适配。
PCT/CN2022/121298 2022-05-30 2022-09-26 一种六氟磷酸锂制备用具有夹套的四氟反应器 WO2023231246A1 (zh)

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