WO2023029708A1 - Heater and single crystal furnace thermal field - Google Patents

Heater and single crystal furnace thermal field Download PDF

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Publication number
WO2023029708A1
WO2023029708A1 PCT/CN2022/102105 CN2022102105W WO2023029708A1 WO 2023029708 A1 WO2023029708 A1 WO 2023029708A1 CN 2022102105 W CN2022102105 W CN 2022102105W WO 2023029708 A1 WO2023029708 A1 WO 2023029708A1
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WIPO (PCT)
Prior art keywords
heating
heater
area
connection
areas
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PCT/CN2022/102105
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French (fr)
Chinese (zh)
Inventor
周永波
王玉龙
赵鹏
杨东
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银川隆基硅材料有限公司
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Publication of WO2023029708A1 publication Critical patent/WO2023029708A1/en

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    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B15/00Single-crystal growth by pulling from a melt, e.g. Czochralski method
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B15/00Single-crystal growth by pulling from a melt, e.g. Czochralski method
    • C30B15/14Heating of the melt or the crystallised materials
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/02Elements
    • C30B29/06Silicon

Definitions

  • the invention relates to the technical field of single crystal manufacturing, in particular to a heater and a single crystal furnace thermal field.
  • the main source of oxygen content is that the quartz crucible reacts with the molten silicon contained in the quartz crucible to form SiO, and most of the oxygen evaporates in the form of SiO gas.
  • the circulatory system discharges, and the remaining part of the oxygen is not discharged in time, and will enter the molten silicon again, and the solid-liquid crystallization surface gathered in the crucible will enter the single crystal silicon as the crystal grows.
  • the heating area of the heater is shortened to reduce the reaction area between the heater and the molten silicon, thereby reducing the generation of oxygen content. But this will lead to the concentration of the heating area, thereby reducing the life of the heater and increasing the cost of the heater.
  • the object of the present invention is to provide a heater and a single crystal furnace thermal field, so as to reduce the heating area of the heater without shortening the heating area of the heater, thereby reducing the oxygen content of the single crystal silicon.
  • the present invention provides a heater, which is applied in the thermal field of a single crystal furnace.
  • the heater is arranged on the outer periphery of the crucible in the thermal field of the single crystal furnace, and is used to heat at least the liquid surface of molten silicon in the crucible.
  • the heater includes: multiple heating areas and multiple slotted areas, each slotted area is connected between two adjacent heating areas; the openings of the multiple slotted areas have the same opening direction, and the openings of the slotted areas
  • the width is greater than or equal to the width of the heating zone.
  • the heater provided by the present invention includes multiple heating zones and multiple slit zones, and each slit zone is connected between two adjacent heating zones, that is to say, the heating zone and the The slit areas are arranged alternately, and the heating area of the entire heater is more concentrated, reducing the radiation area of the heater to the crucible, weakening the heat convection in the molten silicon, reducing the generation of oxygen content, and thus reducing the defects of single crystal silicon .
  • the present invention reduces the effective heating area of the heater by arranging the heating area and the slit area at intervals. Compared with the prior art, shortening the heating area of the heater will not cause the heating area to be too concentrated, so the heating area of the heater will not be reduced. life, increasing heater cost.
  • the multiple slit areas have the same opening direction, and the width of the slit area is larger than the width of the heating area. Based on this, since the heating zones and the slit zones are arranged alternately and the multiple slit zones have the same opening direction, and the width of the slit zones is greater than the width of the heating zone, the heating zone of one of the two identical heaters It can be nested into the slit area of another heater, and when making the heater, a complete embryo can be processed into two identical heaters, thereby increasing the output ratio of the heater and reducing the use cost of the heater .
  • multiple heating zones have the same size parameter
  • multiple slit zones have the same size parameter
  • the heating zone includes at least one heating element, and the opening depth of the slit area matches the height of at least one heating element in the heating zone; In the direction perpendicular to the arrangement direction of each heating zone and the plurality of slit zones, the size of the heating element.
  • the heating area when the opening depth of the slit area matches the height of at least one heating element in the heating area, when the heater is manufactured, the heating area can be fitly nested into the slit area , thereby saving fabrication space and embryo body material.
  • the heating zone includes a plurality of heating elements
  • the plurality of heating elements are arranged in parallel, and the plurality of heating elements are connected end-to-end through the first connecting element.
  • at least one end of the heating element is provided with a chamfer.
  • the area of the heating element can be reduced, thereby increasing the resistance of the heating element, and then when the heating element is energized, the unit area of the heating element can be increased on the heating efficiency.
  • the slotted area includes a second connecting piece, and the second connecting piece is located on a side of the slotted area away from the opening of the slotted area, and is used for connecting two adjacent heating areas.
  • the second connecting member is used to connect two adjacent heating zones, so that the multiple heating zones and the multiple slit zones form a stable integral structure.
  • the multiple heating zones and the multiple slit zones are connected alternately, they are surrounded to form a shape matching the crucible in the thermal field of the single crystal furnace.
  • the multiple heating zones and the multiple slit zones are connected alternately, they are enclosed to form a shape that matches the crucible in the thermal field of the single crystal furnace, so as to adapt to the thermal field of the single crystal furnace
  • the shape of the middle crucible so as to heat the silicon material in the crucible.
  • the heater further includes at least two supports and at least two support connection structures; each support is connected to the corresponding support connection structure through a detachable connection.
  • Each of the support connection structures is disposed between a target heating area of the heater and a slit area adjacent to the target heating area, wherein the target heating area is one of the plurality of heating areas one.
  • the two support connection structures are located at symmetrical positions of the heater.
  • the heater when the heater includes more than two support connection structures, multiple support connection structures are evenly arranged at corresponding positions of the heater along the circumferential direction of the heater.
  • the supporting member since the supporting member is connected to the connecting structure of the supporting member through the detachable connecting member, it is used to support the heater. Moreover, for thermal fields of different heights, it can be achieved by disassembling and replacing the support members, while other thermal field components are not affected, thereby further saving costs.
  • the above arrangement of the connecting structure of the supporting member can make the heater more stably arranged in the thermal field of the single crystal furnace.
  • each of the supporting member connection heating area structures includes a connected connection area and a connection opening area; the width of the connection opening area is greater than or equal to the width of the connection area.
  • connection opening areas of at least two support member connection structures have the same opening direction.
  • connection opening area and the connection area are arranged along the arrangement direction of the multiple heating areas and the multiple slit areas; the opening depth of the connection opening area is greater than or equal to the height of the connection area.
  • connection opening area and the connection area are arranged on the surface of the heater along a direction perpendicular to the arrangement direction of the plurality of heating areas and the plurality of slit areas, and the minimum opening depth of the connection opening area is greater than or equal to the height of the connection area.
  • connection structure of the support in the present invention can be adapted to the structure of the heater of the present invention, so that the heating area of one heater in two identical heaters can be nested into the slit area of the other heater , and then when making the heater, a complete embryo body can be processed into two identical heaters, thereby increasing the output ratio of the heater and reducing the use cost of the heater.
  • the present invention also discloses a thermal field of a single crystal furnace, including the above-mentioned heater.
  • Fig. 1 shows a structural diagram of a heater provided by an embodiment of the present invention
  • Fig. 2 shows a structural diagram of one embryonic body with two heaters provided by the embodiment of the present invention
  • FIG. 3 shows a structural diagram of another heater provided by an embodiment of the present invention
  • Fig. 4 shows another structural diagram of one embryonic body with two heaters provided by the embodiment of the present invention
  • Fig. 5 shows a schematic structural diagram of a connection structure of a heater support provided by an embodiment of the present invention
  • Fig. 6 shows a schematic structural diagram of a connection structure of a heater support provided by an embodiment of the present invention.
  • first and second are used for descriptive purposes only, and cannot be interpreted as indicating or implying relative importance or implicitly specifying the quantity of indicated technical features. Thus, a feature defined as “first” and “second” may explicitly or implicitly include one or more of these features.
  • plurality means two or more, unless otherwise specifically defined. "Several” means one or more than one, unless otherwise clearly and specifically defined.
  • the main source of oxygen content is that the quartz crucible reacts with the molten silicon contained in the quartz crucible to form SiO, and most of the oxygen evaporates in the form of SiO gas.
  • the circulatory system discharges, and the remaining part of the oxygen is not discharged in time, and will enter the molten silicon again, and the solid-liquid crystallization surface gathered in the crucible will enter the single crystal silicon as the crystal grows.
  • the heating area of the heater is shortened to reduce the reaction area between the heater and the molten silicon, thereby reducing the generation of oxygen content. But this will lead to the concentration of the heating area, thereby reducing the life of the heater and increasing the cost of the heater.
  • an embodiment of the present invention discloses a heater to provide a technical solution to reduce the heating area of the heater without shortening the heating area of the heater, thereby reducing the oxygen content of single crystal silicon, thereby solving the problem of above technical issues.
  • the heater provided by the embodiment of the present invention is arranged on the outer periphery of the crucible in the thermal field of the single crystal furnace, and is used for heating at least the molten silicon liquid level in the crucible, so as to ensure continuous pulling of single crystal silicon.
  • the heater includes: multiple heating zones 10 and multiple slotted zones 20 , each slotted zone 20 is connected between two adjacent heating zones 10 . That is to say, the heating zone 10 is alternately connected with the slit zone 20. Based on this, the heat generation of the heating zone 10 of the entire heater is more concentrated, the radiation area of the heater to the crucible is reduced, the heat convection in the molten silicon is weakened, and the The generation of oxygen content is reduced, thereby reducing the defects of single crystal silicon. In practice, the oxygen content dropped by 1.2 ppma due to the structure of the heater in the embodiment of the present invention.
  • the embodiment of the present invention reduces the effective heating area of the heater by arranging the heating area 10 and the slit area 20 at intervals. Compared with the prior art, shortening the heating area of the heater will not cause the heating area to be too concentrated, so it is not necessary to It will reduce the life of the heater and increase the cost of the heater.
  • the plurality of slotted areas 20 have the same opening direction, and the width of the slotted areas 20 is greater than or equal to the width of the heating area 10 .
  • the heating area of the first heater 1 can be nested into the slit area of the second heater 2 .
  • the heating area of the third heater 3 among the two identical heaters can be nested into the slit area of the fourth heater 4 . Therefore, when making the heater, a complete embryo body can be processed into two identical heaters, thereby increasing the output ratio of the heater and reducing the use cost of the heater.
  • two identical heaters can be processed from one complete blank body. Therefore, the cost can be reduced by 50%.
  • the plurality of heating zones 10 of the heater in the embodiment of the present invention have the same size parameters.
  • Each slit area 20 also has the same size parameters.
  • the dimensional parameters of the plurality of heating zones 10 may include the height and width of the plurality of heating zones 10 .
  • the size parameters of the plurality of slotted areas 20 may include the opening depth and opening width of the plurality of slotted areas 20 .
  • the size of the heating zone 10 is the width of the heating zone 10
  • the size of the slit zone 20 is the opening width of the slit zone 20, perpendicular to the heating zone
  • the dimension in the width direction of 10 is the height of the heating zone 10
  • the dimension perpendicular to the width direction of the opening of the slotted area 20 is the opening depth of the slotted area 20 .
  • the heating zone includes at least one heating element, and the opening depth of the slotted area matches the height of the at least one heating element in the heating zone.
  • the height of the heating element is: the size of the heating element along the direction perpendicular to the arrangement direction of the multiple heating zones and the multiple slit zones. Based on this, when manufacturing the heater, the heating area can be fitly nested into the slit area, thereby saving manufacturing space and blank body material.
  • direction A is the arrangement direction of the plurality of heating zones 10 and the plurality of slit zones 20 .
  • the direction B is the height direction of the heating element (101, 102) or the heating area 10 or the slit area 20, and the direction B is perpendicular to the direction A.
  • the direction C is the width direction of the slit area 20 or the heating area 10 , and the direction C is perpendicular to the direction B.
  • the multiple heating elements are arranged in parallel, and the multiple heating elements are connected end-to-end through the first connecting element.
  • a heating zone 10 includes two heating elements 101 and 102 arranged parallel to each other. At the same end of the two heating elements 101 and 102, the two heating elements 101 and 102 pass through a first connecting piece 103 are connected, and the other ends of the two heating elements form a narrow opening 104. At this time, the opening width of the slit area 20 is greater than the sum of the widths of the two heating elements 101 and 102 and the width of the narrow opening 104 .
  • the opening width of the slit area 20 is the opening size of the slit area 20 along the arrangement direction of the plurality of heating areas 10 and the plurality of slit areas 20 .
  • the width of the heating zone 10 is the size of the heating zone 10 along the arrangement direction of the multiple heating zones 10 and the multiple slit zones 20 .
  • the width of the heating element (101, 102) is the size of the heating element along the arrangement direction of the plurality of heating regions 10 and the plurality of slit regions 20.
  • the width of the narrow opening 104 is the size of the narrow opening 104 along the arrangement direction of the plurality of heating regions 10 and the plurality of slit regions 20 .
  • Fig. 3 is a schematic diagram of another kind of heater provided by the embodiment of the present invention, which is formed by alternately processing the heating zone 1 and the slotted area in sequence, which is different from the two heating elements nested in the slotted area in the figure.
  • Four heating elements are nested in the wide slit area of the heater; it can be understood that as long as nesting processing or other deformation nesting is satisfied, all equal changes and improvements made to the number of heating elements within the scope of the embodiments of the present invention are acceptable. should still belong to the scope covered by this patent.
  • one heating zone 10 in FIG. 1011 connected end to end. Since a narrow opening is formed between every two heating elements, three narrow openings are formed between the four heating elements. At this time, the opening width of the slit area is greater than the sum of the widths of the four heating elements and the widths of the three narrow openings, so that the slit area can be nested into the heating area.
  • the heating element and the first connecting element in the heating zone included in the heater are made of carbon-carbon composite material or graphite.
  • the slit area 20 is formed by two heating elements 11 and 12 close to the slit area in two adjacent heating areas.
  • the slotted area 20 also includes a second connecting piece 202, which is located on the side of the slotted area 20 away from the opening 201 of the slotted area, and is used to connect two adjacent heating areas, so that multiple heating area and multiple slotted areas form a solid overall structure.
  • chamfers 13 are provided at both ends of each heating element.
  • each heating element In the case where at least one end of each heating element is provided with a chamfer, the area of the heating element can be reduced, thereby increasing the resistance of the heating element, and furthermore, when the heating element is energized, the heating efficiency per unit area of the heating element can be increased.
  • chamfers can be provided at both ends of each heating element, so as to further reduce the area of the heating element and increase the unit heating efficiency of the heating element to a greater extent.
  • the heater provided in the embodiment of the present invention needs to have a shape matching the crucible, that is to say, in the embodiment of the present invention, multiple heating zones and multiple slit zones After alternate connections, the enclosure forms a shape that matches the crucible in the thermal field of the single crystal furnace.
  • the heater provided by the embodiment of the present invention further includes at least two supports (not shown in the figure), and at least two support connection structures 30 .
  • Each support is connected to the corresponding support connection structure 30 through a detachable connection.
  • the above-mentioned supporting member is used to support the heater, so that the heater can be stably placed in the thermal field of the single crystal furnace.
  • Each support is connected to the corresponding support connection structure through a detachable connection. Based on this, for different heights of the heat field, it can be realized by disassembling and replacing the support, while other heat field components are not affected , resulting in further cost savings.
  • each support connecting structure is arranged between the target heating area of the heater and the slit area adjacent to the target heating area, wherein the target heating area is any one of the plurality of heating areas.
  • the embodiment of the present invention does not specifically limit the specific position of the support member connection structure in the heater.
  • the two support member connection structures are located at symmetrical positions of the heater, so as to realize stable support for the heater. It can be understood that when the heater includes a plurality of support member connection structures, the plurality of support member connection structures are evenly arranged at corresponding positions of the heater along the circumferential direction of the heater.
  • each support member connection structure 30 includes a connected connection area 301 and a connection opening area 302 .
  • the width d of the connection opening region 302 is greater than or equal to the width b of the connection region 301 .
  • the width of the connecting opening area is: the size of the connecting opening area in the same direction as the arrangement direction of the plurality of heating areas and the plurality of slit areas.
  • the width direction of the connection opening area 302 is the same as the arrangement direction of the plurality of heating areas and the plurality of slit areas
  • the width direction of the connection opening area 302 is E
  • the width of the connection opening area is the connection opening The size of the zone along the direction E.
  • the width of the connection area is: the size of the connection area in the same direction as the arrangement direction of the plurality of heating areas and the plurality of slit areas.
  • the width direction of the connection zone 301 is the same as the arrangement direction of the multiple heating zones and the plurality of slit zones
  • the width direction of the connection zone 301 is E
  • the width of the connection zone is E along the direction E of the connection zone. on the size.
  • connection opening regions 302 of at least two support member connection structures 30 included in each heater have the same opening direction.
  • connection opening area 302 and the connection area 301 are arranged along the arrangement direction of the plurality of heating areas and the plurality of slit areas; the opening depth c1 of the connection opening area 302 is greater than or It is equal to the height a of the connection area 301 .
  • connection opening area 302 and the connection area 301 are arranged on the surface of the heater along a direction perpendicular to the arrangement direction of the plurality of heating areas and the plurality of slit areas. It can be seen that the minimum depth of the connection opening area in FIG. 6 is c2. And the minimum opening depth c2 of the connecting opening area 302 is greater than or equal to the height a of the connecting area 301 .
  • the opening depth of the connection opening area 302 is: the size of the connection opening area in a direction D perpendicular to the width direction E of the connection opening area 302 .
  • the height of the connection region 301 is: the size of the connection region in a direction D perpendicular to the width direction E of the connection region 301 .
  • connection structure of the support in the embodiment of the present invention can be adapted to the structure of the heater of the present invention, so that the heating area of one of the two identical heaters can be nested into the slit area of the other heater, and then When making a heater, a complete embryo body can be processed into two identical heaters, thereby increasing the output ratio of the heater and reducing the cost of using the heater.
  • the processing method of the connection structure of the above-mentioned support member can be as follows: since the heating area of the heater is annularly symmetrical, no slits are made for any reserved heating area, and no slits are made at the symmetrical positions;
  • the support connection structure is set at half of the height of the device.
  • the support connection structure and the support are connected by carbon-carbon bolts.
  • the height of the support can be processed with other blanks according to different thermal field sizes, and other thermal field components Unaffected, therefore, further cost savings can be achieved.
  • the width of the heating zone is preferably 35mm-50mm, and the total height of the heater is preferably 240mm-280mm.
  • An embodiment of the present invention also provides a thermal field of a single crystal furnace, including the above-mentioned heater.
  • the beneficial effect of the thermal field of the single crystal furnace provided by the embodiment of the present invention is the same as that of the above-mentioned heater, and will not be repeated here.

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  • Engineering & Computer Science (AREA)
  • Crystallography & Structural Chemistry (AREA)
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  • Metallurgy (AREA)
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Abstract

A heater and a single crystal furnace thermal field, relating to the technical field of single crystal manufacturing. The heater is applied to a single crystal furnace thermal field, is provided on the outer periphery of a crucible in the single crystal furnace thermal field, and is used for at least heating a molten silicon liquid level in the crucible. The heater comprises: a plurality of heating areas and a plurality of slotted areas, each slotted area is connected between two adjacent heating areas; and openings of the plurality of slotted areas have a same opening directions, and the width of the slotted areas is greater than or equal to the width of the heating areas. According to the heater, under the condition that the heating areas of the heater are not shortened, the heating areas are reduced, thereby reducing the oxygen content of a single crystal silicon.

Description

一种加热器及单晶炉热场A heater and a single crystal furnace thermal field
本申请要求在2021年8月31日提交中国专利局、申请号为202111016078.9、发明名称为“一种加热器及单晶炉热场”的中国专利申请的优先权,其全部内容通过引用均结合在本申请中。This application claims the priority of a Chinese patent application filed with the China Patent Office on August 31, 2021, with application number 202111016078.9, and the title of the invention is "A Heater and Thermal Field of a Single Crystal Furnace", the entire contents of which are hereby incorporated by reference in this application.
技术领域technical field
本发明涉及单晶制造技术领域,尤其涉及一种加热器及单晶炉热场。The invention relates to the technical field of single crystal manufacturing, in particular to a heater and a single crystal furnace thermal field.
背景技术Background technique
在直拉单晶的过程中,氧含量的来源主要是石英坩埚与盛放在石英坩埚中的熔硅发生反应生成SiO,其中大部分的氧以SiO气体形式蒸发,随单晶炉内的气体循环系统排出,剩余一部分未及时排出氧,会再次进入熔硅中,聚集在坩埚的固液结晶面随着晶体生长进入单晶硅中。In the process of Czochralski single crystal, the main source of oxygen content is that the quartz crucible reacts with the molten silicon contained in the quartz crucible to form SiO, and most of the oxygen evaporates in the form of SiO gas. The circulatory system discharges, and the remaining part of the oxygen is not discharged in time, and will enter the molten silicon again, and the solid-liquid crystallization surface gathered in the crucible will enter the single crystal silicon as the crystal grows.
当氧随着晶体生长进入单晶硅中时,拉制的单晶硅会存在各种缺陷,因此,降低单晶硅氧含量是目前亟待解决的难题。When oxygen enters the single crystal silicon as the crystal grows, there will be various defects in the drawn single crystal silicon. Therefore, reducing the oxygen content of the single crystal silicon is an urgent problem to be solved at present.
目前,采用将加热器的加热区缩短,以减少加热器与熔硅的反应面积,从而减少氧含量的产生。但是这样会导致加热区集中,从而使加热器寿命降低,增加加热器的使用成本。At present, the heating area of the heater is shortened to reduce the reaction area between the heater and the molten silicon, thereby reducing the generation of oxygen content. But this will lead to the concentration of the heating area, thereby reducing the life of the heater and increasing the cost of the heater.
发明内容Contents of the invention
基于此,本发明的目的在于提供一种加热器及单晶炉热场,以提供一种在不缩短加热器加热区的情况下,减少加热器的加热区,从而降低单晶硅的氧含量的技术方案。Based on this, the object of the present invention is to provide a heater and a single crystal furnace thermal field, so as to reduce the heating area of the heater without shortening the heating area of the heater, thereby reducing the oxygen content of the single crystal silicon. technical solutions.
第一方面,本发明提供一种加热器,应用于单晶炉热场中,加热器设置在单晶炉热场中坩埚的外周,用于至少对坩埚中的熔硅液面进行加热。In a first aspect, the present invention provides a heater, which is applied in the thermal field of a single crystal furnace. The heater is arranged on the outer periphery of the crucible in the thermal field of the single crystal furnace, and is used to heat at least the liquid surface of molten silicon in the crucible.
加热器包括:多个加热区以及多个开缝区,每个开缝区均连接于相邻两个加热区之间;多个开缝区的开口具有相同的开口方向,且开缝区的宽度大于或等于加热区的宽度。The heater includes: multiple heating areas and multiple slotted areas, each slotted area is connected between two adjacent heating areas; the openings of the multiple slotted areas have the same opening direction, and the openings of the slotted areas The width is greater than or equal to the width of the heating zone.
在采用上述方案的情况下,本发明提供的加热器包括多个加热区以及多个开缝区,且每个开缝区连接于相邻两个加热区之间,也就是说,加热区与开缝区交替排列,整个加热器的加热区发热量更集中,减少加热器对坩埚的辐射面积,减弱熔硅中的热对流,减少了氧含量的产生,进而减小了单晶硅的缺陷。且本发明通过加热区与开缝区的间隔排列来减小加热器的有效加热区,相比现有技术中缩短加热器的加热区,不会导致加热区过于集中,故不会降低加热器寿命,增加加热器成本。In the case of adopting the above scheme, the heater provided by the present invention includes multiple heating zones and multiple slit zones, and each slit zone is connected between two adjacent heating zones, that is to say, the heating zone and the The slit areas are arranged alternately, and the heating area of the entire heater is more concentrated, reducing the radiation area of the heater to the crucible, weakening the heat convection in the molten silicon, reducing the generation of oxygen content, and thus reducing the defects of single crystal silicon . And the present invention reduces the effective heating area of the heater by arranging the heating area and the slit area at intervals. Compared with the prior art, shortening the heating area of the heater will not cause the heating area to be too concentrated, so the heating area of the heater will not be reduced. life, increasing heater cost.
再者,本发明中多个开缝区具有相同的开口方向,且开缝区的宽度大于加热区的宽度。基于此,由于加热区和开缝区交替排列以及多个开缝区具有相同的开口方向,且开缝区的宽度大于加热区的宽度,故两个相同的加热器中一个加热器的加热区可以嵌套进另一个加热器的开缝区中,进而在制作加热器时,一个完整胚体可以加工成两个相同的加热器,从而提升加热器产出比,同时降低加热器的使用成本。Furthermore, in the present invention, the multiple slit areas have the same opening direction, and the width of the slit area is larger than the width of the heating area. Based on this, since the heating zones and the slit zones are arranged alternately and the multiple slit zones have the same opening direction, and the width of the slit zones is greater than the width of the heating zone, the heating zone of one of the two identical heaters It can be nested into the slit area of another heater, and when making the heater, a complete embryo can be processed into two identical heaters, thereby increasing the output ratio of the heater and reducing the use cost of the heater .
在一种可能的实现方式中,多个加热区具有相同的尺寸参数,多个开缝区具有相同的尺寸参数。In a possible implementation manner, multiple heating zones have the same size parameter, and multiple slit zones have the same size parameter.
在采用上述技术方案的情况下,由于多个加热区具有相同的尺寸参数,多个开缝区具有相同的尺寸参数,基于此,在制作加热器时,可以简化坯体的复杂度。In the case of adopting the above technical solution, since the multiple heating zones have the same size parameters and the multiple slit zones have the same size parameters, based on this, the complexity of the green body can be simplified when making the heater.
在一种可能的实现方式中,加热区包括至少一个加热件,开缝区的开口深度与加热区中至少一个加热件的高度相匹配;其中,所述加热件的高度为沿与所述多个加热区及所述多个开缝区的排列方向垂直的方向上,所述加热件的尺寸。In a possible implementation manner, the heating zone includes at least one heating element, and the opening depth of the slit area matches the height of at least one heating element in the heating zone; In the direction perpendicular to the arrangement direction of each heating zone and the plurality of slit zones, the size of the heating element.
在采用上述技术方案的情况下,在开缝区的开口深度与加热区中至少一个加热件的高度相匹配的情况下,在制作加热器时,加热区可以契合的嵌套进开缝区中,从而节省制作空间和胚体材料。In the case of adopting the above technical solution, when the opening depth of the slit area matches the height of at least one heating element in the heating area, when the heater is manufactured, the heating area can be fitly nested into the slit area , thereby saving fabrication space and embryo body material.
进一步的,当加热区包括多个加热件时,多个加热件平行设置,且多个加热件通过第一连接件首尾相连接。沿至少一个加热件的排列方向,加热件的至少一端设置有倒角。Further, when the heating zone includes a plurality of heating elements, the plurality of heating elements are arranged in parallel, and the plurality of heating elements are connected end-to-end through the first connecting element. Along the arrangement direction of at least one heating element, at least one end of the heating element is provided with a chamfer.
在采用上述技术方案的情况下,当加热件的至少一端设置有倒角时,可以减小加热件的面积,从而增加加热件的电阻,进而当加热件通电后,可以增大加热件单位面积上的加热效率。In the case of adopting the above technical solution, when at least one end of the heating element is provided with a chamfer, the area of the heating element can be reduced, thereby increasing the resistance of the heating element, and then when the heating element is energized, the unit area of the heating element can be increased on the heating efficiency.
在一种可能的实现方式中,开缝区包括第二连接件,第二连接件位于开缝区背离所述开缝区的开口一侧,用于连接相邻两个加热区。In a possible implementation manner, the slotted area includes a second connecting piece, and the second connecting piece is located on a side of the slotted area away from the opening of the slotted area, and is used for connecting two adjacent heating areas.
在采用上述技术方案的情况下,第二连接件用于连接相邻两个加热区,从而使多个加热区和多个开缝区形成一个稳固的整体结构。In the case of adopting the above technical solution, the second connecting member is used to connect two adjacent heating zones, so that the multiple heating zones and the multiple slit zones form a stable integral structure.
在一种可能的实现方式中,多个所述加热区和多个所述开缝区交替连接后,围合形成与所述单晶炉热场中坩埚相匹配的形状。In a possible implementation manner, after the multiple heating zones and the multiple slit zones are connected alternately, they are surrounded to form a shape matching the crucible in the thermal field of the single crystal furnace.
在采用上述技术方案的情况下,多个所述加热区和多个所述开缝区交替连接后,围合形成与单晶炉热场中坩埚相匹配的形状,以适应单晶炉热场中坩埚的形状,从而对坩埚中的硅料进行加热。In the case of adopting the above technical solution, after the multiple heating zones and the multiple slit zones are connected alternately, they are enclosed to form a shape that matches the crucible in the thermal field of the single crystal furnace, so as to adapt to the thermal field of the single crystal furnace The shape of the middle crucible, so as to heat the silicon material in the crucible.
在一种可能的实现方式中,加热器还包括至少两个支撑件和至少两个支撑件连接结构;每个所述支撑件通过可拆卸连接件与相应所述支撑件连接结构相连接。每个所述支撑件连接结构设置于所述加热器的目标加热区和与所述目标加热区相邻的开缝区之间, 其中,所述目标加热区为所述多个加热区中的一个。In a possible implementation manner, the heater further includes at least two supports and at least two support connection structures; each support is connected to the corresponding support connection structure through a detachable connection. Each of the support connection structures is disposed between a target heating area of the heater and a slit area adjacent to the target heating area, wherein the target heating area is one of the plurality of heating areas one.
当所述加热器包括两个支撑件连接结构时,所述两个支撑件连接结构位于所述加热器的对称位置处。When the heater includes two support connection structures, the two support connection structures are located at symmetrical positions of the heater.
或,当所述加热器包括的支撑件连接结构数量大于两个时,多个所述支撑件连接结构,沿所述加热器的周向,均匀的设置在所述加热器的相应位置处。Or, when the heater includes more than two support connection structures, multiple support connection structures are evenly arranged at corresponding positions of the heater along the circumferential direction of the heater.
在采用上述技术方案的情况下,由于支撑件通过可拆卸连接件与支撑件连接结构相连接,用以实现对加热器的支撑。且对于不同高度的热场,可通过对支撑件的拆卸和更换来实现,而其他热场部件不受影响,从而进一步节省成本。In the case of adopting the above technical solution, since the supporting member is connected to the connecting structure of the supporting member through the detachable connecting member, it is used to support the heater. Moreover, for thermal fields of different heights, it can be achieved by disassembling and replacing the support members, while other thermal field components are not affected, thereby further saving costs.
再者,上述支撑件连接结构的设置方式,可以使加热器更加稳固的设置在单晶炉热场中。Furthermore, the above arrangement of the connecting structure of the supporting member can make the heater more stably arranged in the thermal field of the single crystal furnace.
在一种可能的实现方式中,每个所述支撑件连接加热区结构均包括相连接的连接区以及连接开口区;所述连接开口区的宽度大于或等于所述连接区的宽度。In a possible implementation manner, each of the supporting member connection heating area structures includes a connected connection area and a connection opening area; the width of the connection opening area is greater than or equal to the width of the connection area.
进一步的,至少两个支撑件连接结构的连接开口区具有相同的开口方向。Further, the connection opening areas of at least two support member connection structures have the same opening direction.
连接开口区与连接区沿多个加热区及多个开缝区的排列方向排布;连接开口区的开口深度大于或等于连接区的高度。The connection opening area and the connection area are arranged along the arrangement direction of the multiple heating areas and the multiple slit areas; the opening depth of the connection opening area is greater than or equal to the height of the connection area.
或,连接开口区与连接区在加热器表面上沿垂直于多个加热区及多个开缝区的排列方向排布,连接开口区的最小开口深度大于或等于连接区的高度。Or, the connection opening area and the connection area are arranged on the surface of the heater along a direction perpendicular to the arrangement direction of the plurality of heating areas and the plurality of slit areas, and the minimum opening depth of the connection opening area is greater than or equal to the height of the connection area.
在采用上述技术方案的情况下,由于至少两个支撑件连接结构的连接开口区具有相同的开口方向,且连接开口区的宽度大于或等于连接区的宽度,连接开口区的开口深度大于或等于连接区的高度,故本发明中支撑件连接结构可以适应本发明加热器的结构,以使两个相同的加热器中一个加热器的加热区可以嵌套进另一个加热器的开缝区中,进而在制作加热器时,一个完整胚体可以加工成两个相同的加热器,从而提升加热器产出比,同时降低加热器的使用成本。In the case of adopting the above technical solution, since the connection opening areas of at least two supporting member connection structures have the same opening direction, and the width of the connection opening area is greater than or equal to the width of the connection area, the opening depth of the connection opening area is greater than or equal to The height of the connection area, so the connection structure of the support in the present invention can be adapted to the structure of the heater of the present invention, so that the heating area of one heater in two identical heaters can be nested into the slit area of the other heater , and then when making the heater, a complete embryo body can be processed into two identical heaters, thereby increasing the output ratio of the heater and reducing the use cost of the heater.
第二方面,本发明还公开了一种单晶炉热场,包括上述加热器。In the second aspect, the present invention also discloses a thermal field of a single crystal furnace, including the above-mentioned heater.
本发明中第二方面及其各种实现方式的有益效果与第一方面或第一方面任一可能的实现方式的有益效果相同,此处不再赘述。The beneficial effects of the second aspect and various implementations thereof in the present invention are the same as those of the first aspect or any possible implementation of the first aspect, and will not be repeated here.
上述说明仅是本公开技术方案的概述,为了能够更清楚了解本公开的技术手段,而可依照说明书的内容予以实施,并且为了让本公开的上述和其它目的、特征和优点能够更明显易懂,以下特举本公开的具体实施方式。The above description is only an overview of the technical solution of the present disclosure. In order to better understand the technical means of the present disclosure, it can be implemented according to the contents of the description, and in order to make the above and other purposes, features and advantages of the present disclosure more obvious and understandable , the specific embodiments of the present disclosure are enumerated below.
附图说明Description of drawings
为了更清楚地说明本申请实施例或现有技术中的技术方案,下面将对实施例或现有 技术描述中所需要使用的附图作一简单地介绍,显而易见地,下面描述中的附图是本申请的一些实施例,对于本领域普通技术人员来讲,在不付出创造性劳动的前提下,还可以根据这些附图获得其他的附图。In order to more clearly illustrate the technical solutions in the embodiments of the present application or the prior art, the following will briefly introduce the drawings that need to be used in the description of the embodiments or the prior art. Obviously, the accompanying drawings in the following description These are some embodiments of the present application. Those skilled in the art can also obtain other drawings based on these drawings without creative work.
附图用于更好地理解本申请,不构成对本申请的不当限定。其中:The accompanying drawings are used for better understanding of the present application, and do not constitute an improper limitation of the present application. in:
图1示出了本发明实施例提供的一种加热器的结构图;Fig. 1 shows a structural diagram of a heater provided by an embodiment of the present invention;
图2示出了本发明实施例提供的一种一胚体出两个加热器的结构图;Fig. 2 shows a structural diagram of one embryonic body with two heaters provided by the embodiment of the present invention;
图3示出了本发明实施例提供的另一种加热器的结构图;FIG. 3 shows a structural diagram of another heater provided by an embodiment of the present invention;
图4示出了本发明实施例提供的另一种一胚体出两个加热器的结构图;Fig. 4 shows another structural diagram of one embryonic body with two heaters provided by the embodiment of the present invention;
图5示出了本发明实施例提供的一种加热器支撑件连接结构的结构示意图;Fig. 5 shows a schematic structural diagram of a connection structure of a heater support provided by an embodiment of the present invention;
图6示出了本发明实施例提供的一种加热器支撑件连接结构的结构示意图。Fig. 6 shows a schematic structural diagram of a connection structure of a heater support provided by an embodiment of the present invention.
附图编号说明:Explanation of attached drawing numbers:
1-第一加热器,2-第二加热器,3-第三加热器,4-第四加热器,10-加热区,11-加热件,12-加热件,13-倒角,20-开缝区,30-支撑件连接结构,101-加热件,102-加热件,103-第一连接件,104-窄开口,105-加热件,106加热件,107-加热件,108-加热件,109-第一连接件,1010-第一连接件,1011-第一连接件,201-开缝区的开口,202-第二连接件,301-连接区,302-连接开口区。1-first heater, 2-second heater, 3-third heater, 4-fourth heater, 10-heating zone, 11-heating element, 12-heating element, 13-chamfering, 20- Slit area, 30-support connecting structure, 101-heating part, 102-heating part, 103-first connecting part, 104-narrow opening, 105-heating part, 106 heating part, 107-heating part, 108-heating 109-the first connector, 1010-the first connector, 1011-the first connector, 201-the opening of the slit area, 202-the second connector, 301-the connection area, 302-the connection opening area.
具体实施例specific embodiment
以下,将参照附图来描述本公开的实施例。但是应该理解,这些描述只是示例性的,而并非要限制本公开的范围。此外,在以下说明中,省略了对公知结构和技术的描述,以避免不必要地混淆本公开的概念。Hereinafter, embodiments of the present disclosure will be described with reference to the drawings. It should be understood, however, that these descriptions are exemplary only, and are not intended to limit the scope of the present disclosure. Also, in the following description, descriptions of well-known structures and techniques are omitted to avoid unnecessarily obscuring the concept of the present disclosure.
此外,术语“第一”、“第二”仅用于描述目的,而不能理解为指示或暗示相对重要性或者隐含指明所指示的技术特征的数量。由此,限定有“第一”、“第二”的特征可以明示或者隐含地包括一个或者更多个该特征。在本发明的描述中,“多个”的含义是两个或两个以上,除非另有明确具体的限定。“若干”的含义是一个或一个以上,除非另有明确具体的限定。In addition, the terms "first" and "second" are used for descriptive purposes only, and cannot be interpreted as indicating or implying relative importance or implicitly specifying the quantity of indicated technical features. Thus, a feature defined as "first" and "second" may explicitly or implicitly include one or more of these features. In the description of the present invention, "plurality" means two or more, unless otherwise specifically defined. "Several" means one or more than one, unless otherwise clearly and specifically defined.
在直拉单晶的过程中,氧含量的来源主要是石英坩埚与盛放在石英坩埚中的熔硅发生反应生成SiO,其中大部分的氧以SiO气体形式蒸发,随单晶炉内的气体循环系统排出,剩余一部分未及时排出氧,会再次进入熔硅中,聚集在坩埚的固液结晶面随着晶体生长进入单晶硅中。In the process of Czochralski single crystal, the main source of oxygen content is that the quartz crucible reacts with the molten silicon contained in the quartz crucible to form SiO, and most of the oxygen evaporates in the form of SiO gas. The circulatory system discharges, and the remaining part of the oxygen is not discharged in time, and will enter the molten silicon again, and the solid-liquid crystallization surface gathered in the crucible will enter the single crystal silicon as the crystal grows.
当氧随着晶体生长进入单晶硅中时,拉制的单晶硅会存在各种缺陷,因此,降低单晶硅氧含量是目前亟待解决的难题。When oxygen enters the single crystal silicon as the crystal grows, there will be various defects in the drawn single crystal silicon. Therefore, reducing the oxygen content of the single crystal silicon is an urgent problem to be solved at present.
目前,采用将加热器的加热区缩短,以减少加热器与熔硅的反应面积,从而减少氧 含量的产生。但是这样会导致加热区集中,从而使加热器寿命降低,增加加热器的使用成本。At present, the heating area of the heater is shortened to reduce the reaction area between the heater and the molten silicon, thereby reducing the generation of oxygen content. But this will lead to the concentration of the heating area, thereby reducing the life of the heater and increasing the cost of the heater.
基于此,本发明实施例公开了一种加热器,以提供一种在不缩短加热器加热区的情况下,减少加热器的加热区,从而降低单晶硅的氧含量的技术方案,从而解决上述技术问题。Based on this, an embodiment of the present invention discloses a heater to provide a technical solution to reduce the heating area of the heater without shortening the heating area of the heater, thereby reducing the oxygen content of single crystal silicon, thereby solving the problem of above technical issues.
本发明实施例提供的加热器设置在单晶炉热场中坩埚的外周,用于至少对坩埚中的熔硅液面进行加热,以保证连续拉制单晶硅。The heater provided by the embodiment of the present invention is arranged on the outer periphery of the crucible in the thermal field of the single crystal furnace, and is used for heating at least the molten silicon liquid level in the crucible, so as to ensure continuous pulling of single crystal silicon.
参照图1和图3,上述加热器包括:多个加热区10以及多个开缝区20,每个开缝区20均连接于相邻两个加热区10之间。也就是说,加热区10与开缝区20交替连接,基于此,使整个加热器的加热区10的发热量更集中,减少加热器对坩埚的辐射面积,减弱熔硅中的热对流,减少了氧含量的产生,进而减小了单晶硅的缺陷。在实际中,由于本发明实施例中加热器的结构,氧含量下降了1.2ppma。Referring to FIG. 1 and FIG. 3 , the heater includes: multiple heating zones 10 and multiple slotted zones 20 , each slotted zone 20 is connected between two adjacent heating zones 10 . That is to say, the heating zone 10 is alternately connected with the slit zone 20. Based on this, the heat generation of the heating zone 10 of the entire heater is more concentrated, the radiation area of the heater to the crucible is reduced, the heat convection in the molten silicon is weakened, and the The generation of oxygen content is reduced, thereby reducing the defects of single crystal silicon. In practice, the oxygen content dropped by 1.2 ppma due to the structure of the heater in the embodiment of the present invention.
且本发明实施例通过加热区10与开缝区20的间隔排列来减小加热器的有效加热区,相比现有技术中缩短加热器的加热区,不会导致加热区过于集中,故不会降低加热器寿命,增加加热器成本。Moreover, the embodiment of the present invention reduces the effective heating area of the heater by arranging the heating area 10 and the slit area 20 at intervals. Compared with the prior art, shortening the heating area of the heater will not cause the heating area to be too concentrated, so it is not necessary to It will reduce the life of the heater and increase the cost of the heater.
再者,参照图1和图3,多个开缝区20具有相同的开口方向,且开缝区20的宽度大于或等于加热区10的宽度。基于此,参照图2,两个相同的加热器中第一加热器1的加热区可以嵌套进第二加热器2的开缝区中。或,参照图4,两个相同的加热器中第三加热器3的加热区可以嵌套进第四加热器4的开缝区中。故在制作加热器时,一个完整胚体可以加工成两个相同的加热器,从而提升加热器产出比,同时降低加热器的使用成本。在实际应用中,在制作本发明实施例提供的加热器时,由于一个完整胚体可以加工成两个相同的加热器。故可以降低50%的成本。Furthermore, referring to FIG. 1 and FIG. 3 , the plurality of slotted areas 20 have the same opening direction, and the width of the slotted areas 20 is greater than or equal to the width of the heating area 10 . Based on this, referring to FIG. 2 , among two identical heaters, the heating area of the first heater 1 can be nested into the slit area of the second heater 2 . Or, referring to FIG. 4 , the heating area of the third heater 3 among the two identical heaters can be nested into the slit area of the fourth heater 4 . Therefore, when making the heater, a complete embryo body can be processed into two identical heaters, thereby increasing the output ratio of the heater and reducing the use cost of the heater. In practical application, when manufacturing the heater provided by the embodiment of the present invention, two identical heaters can be processed from one complete blank body. Therefore, the cost can be reduced by 50%.
可以理解,为了减小加热器的制作难度,以及简化制作加热器的胚体难度,参照图1或图3,本发明实施例中的加热器的多个加热区10具有相同的尺寸参数,多个开缝区20也具有相同的尺寸参数。It can be understood that, in order to reduce the difficulty of making the heater and simplify the difficulty of making the body of the heater, referring to FIG. 1 or FIG. 3 , the plurality of heating zones 10 of the heater in the embodiment of the present invention have the same size parameters. Each slit area 20 also has the same size parameters.
参照图1或图3,上述多个加热区10的尺寸参数可以包括多个加热区10的高度和宽度。上述多个开缝区20的尺寸参数可以包括多个开缝区20的开口深度和开口宽度。其中,沿多个加热区10和多个开缝区20的排列方向,加热区10的尺寸为加热区10的宽度,开缝区20的尺寸为开缝区20的开口宽度,垂直于加热区10宽度方向的尺寸为加热区10的高度,垂直于开缝区20开口宽度方向的尺寸为开缝区20的开口深度。Referring to FIG. 1 or FIG. 3 , the dimensional parameters of the plurality of heating zones 10 may include the height and width of the plurality of heating zones 10 . The size parameters of the plurality of slotted areas 20 may include the opening depth and opening width of the plurality of slotted areas 20 . Wherein, along the arrangement direction of multiple heating zones 10 and multiple slit zones 20, the size of the heating zone 10 is the width of the heating zone 10, and the size of the slit zone 20 is the opening width of the slit zone 20, perpendicular to the heating zone The dimension in the width direction of 10 is the height of the heating zone 10 , and the dimension perpendicular to the width direction of the opening of the slotted area 20 is the opening depth of the slotted area 20 .
在本发明实施例中,上述加热区包括至少一个加热件,开缝区的开口深度与加热区中至少一个加热件的高度相匹配。其中,加热件的高度为:沿与多个加热区及多个开缝 区的排列方向垂直的方向上,加热件的尺寸。基于此,在制作加热器时,加热区可以契合的嵌套进开缝区中,从而节省制作空间和胚体材料。In an embodiment of the present invention, the heating zone includes at least one heating element, and the opening depth of the slotted area matches the height of the at least one heating element in the heating zone. Wherein, the height of the heating element is: the size of the heating element along the direction perpendicular to the arrangement direction of the multiple heating zones and the multiple slit zones. Based on this, when manufacturing the heater, the heating area can be fitly nested into the slit area, thereby saving manufacturing space and blank body material.
参照图1,方向A为多个加热区10及多个开缝区20的排列方向。方向B为加热件(101、102)或加热区10或开缝区20的高度方向,方向B与方向A相垂直。方向C为为开缝区20或加热区10的宽度方向,方向C与方向B相垂直。Referring to FIG. 1 , direction A is the arrangement direction of the plurality of heating zones 10 and the plurality of slit zones 20 . The direction B is the height direction of the heating element (101, 102) or the heating area 10 or the slit area 20, and the direction B is perpendicular to the direction A. The direction C is the width direction of the slit area 20 or the heating area 10 , and the direction C is perpendicular to the direction B.
当加热区包括多个加热件时,多个加热件平行设置,且多个加热件通过第一连接件首尾相连接。When the heating zone includes multiple heating elements, the multiple heating elements are arranged in parallel, and the multiple heating elements are connected end-to-end through the first connecting element.
示例性的,参照图1,一个加热区10包括两个相互平行设置的加热件101和102,在两个加热件101和102的同一端,两个加热件101和102通过一个第一连接件103相连接,两个加热件的另一端形成一个窄开口104。此时,开缝区20的开口宽度大于两个加热件101和102的宽度与上述窄开口104的宽度之和。其中,开缝区20的开口宽度为沿多个加热区10及多个开缝区20的排列方向,开缝区20的开口尺寸。加热区10的宽度为沿多个加热区10及多个开缝区20的排列方向,所述加热区10的尺寸。Exemplarily, referring to FIG. 1 , a heating zone 10 includes two heating elements 101 and 102 arranged parallel to each other. At the same end of the two heating elements 101 and 102, the two heating elements 101 and 102 pass through a first connecting piece 103 are connected, and the other ends of the two heating elements form a narrow opening 104. At this time, the opening width of the slit area 20 is greater than the sum of the widths of the two heating elements 101 and 102 and the width of the narrow opening 104 . Wherein, the opening width of the slit area 20 is the opening size of the slit area 20 along the arrangement direction of the plurality of heating areas 10 and the plurality of slit areas 20 . The width of the heating zone 10 is the size of the heating zone 10 along the arrangement direction of the multiple heating zones 10 and the multiple slit zones 20 .
加热件(101、102)的宽度为沿多个加热区10及多个开缝区20的排列方向,加热件的尺寸。窄开口104的宽度,为沿多个加热区10及多个开缝区20的排列方向,窄开口104的尺寸。The width of the heating element (101, 102) is the size of the heating element along the arrangement direction of the plurality of heating regions 10 and the plurality of slit regions 20. The width of the narrow opening 104 is the size of the narrow opening 104 along the arrangement direction of the plurality of heating regions 10 and the plurality of slit regions 20 .
示例性的,图3为本发明实施例提供的另一种加热器示意图,采用加热区1和开缝区按顺序交替加工而成,不同于图开缝区中嵌套2个加热件,此加热器宽开缝区嵌套4个加热件;可以理解,只要满足嵌套加工,或者其他变形嵌套,凡依本发明实施例范围,对加热件的数量所作的均等变化与改进等,均应仍归属于本专利涵盖范围之内。具体的,图3中一个加热区10包括四个加热件105、106、107和108,该四个加热件105、106、107和108平行设置,且通过三个第一连接件109、1010和1011首尾相连。由于每两个加热件之间形成一个窄开口,故四个加热件之间形成三个窄开口。此时,开缝区的开口宽度大于四个加热件的宽度与上述三个窄开口的宽度之和,以实现开缝区可以嵌套进加热区。Exemplarily, Fig. 3 is a schematic diagram of another kind of heater provided by the embodiment of the present invention, which is formed by alternately processing the heating zone 1 and the slotted area in sequence, which is different from the two heating elements nested in the slotted area in the figure. Four heating elements are nested in the wide slit area of the heater; it can be understood that as long as nesting processing or other deformation nesting is satisfied, all equal changes and improvements made to the number of heating elements within the scope of the embodiments of the present invention are acceptable. should still belong to the scope covered by this patent. Specifically, one heating zone 10 in FIG. 1011 connected end to end. Since a narrow opening is formed between every two heating elements, three narrow openings are formed between the four heating elements. At this time, the opening width of the slit area is greater than the sum of the widths of the four heating elements and the widths of the three narrow openings, so that the slit area can be nested into the heating area.
其中,上述加热器所包括的加热区中的加热件以及第一连接件均由碳碳复合材料或石墨制成。Wherein, the heating element and the first connecting element in the heating zone included in the heater are made of carbon-carbon composite material or graphite.
在实际中,参照图1,开缝区20由两个相邻加热区中靠近开缝区的两个加热件11和12形成。开缝区20还包括第二连接件202,该第二连接件202位于开缝区20背离所述开缝区的开口201一侧,用于连接相邻两个加热区,从而使多个加热区和多个开缝区形成一个稳固的整体结构。In practice, referring to FIG. 1 , the slit area 20 is formed by two heating elements 11 and 12 close to the slit area in two adjacent heating areas. The slotted area 20 also includes a second connecting piece 202, which is located on the side of the slotted area 20 away from the opening 201 of the slotted area, and is used to connect two adjacent heating areas, so that multiple heating area and multiple slotted areas form a solid overall structure.
在一种可能的实现方式中,参照图1,沿加热区10中多个加热件的排列方向,每个 加热件的两端均设置有倒角13。In a possible implementation, referring to FIG. 1 , along the arrangement direction of the plurality of heating elements in the heating zone 10, chamfers 13 are provided at both ends of each heating element.
在每个加热件的至少一端设置有倒角的情况下,可以减小加热件的面积,从而增加加热件的电阻,进而当加热件通电后,可以增大加热件单位面积上的加热效率。In the case where at least one end of each heating element is provided with a chamfer, the area of the heating element can be reduced, thereby increasing the resistance of the heating element, and furthermore, when the heating element is energized, the heating efficiency per unit area of the heating element can be increased.
更进一步的,可以在每个加热件的两端均设置有倒角,从而进一步地减小加热件的面积,更大程度的增加加热件的单位加热效率。Furthermore, chamfers can be provided at both ends of each heating element, so as to further reduce the area of the heating element and increase the unit heating efficiency of the heating element to a greater extent.
可以理解,为了适应单晶炉热场中坩埚的形状,本发明实施例提供的加热器需要具有与坩埚匹配的形状,也就是说,本发明实施例中多个加热区和多个开缝区交替连接后,围合形成与单晶炉热场中坩埚相匹配的形状。It can be understood that, in order to adapt to the shape of the crucible in the thermal field of the single crystal furnace, the heater provided in the embodiment of the present invention needs to have a shape matching the crucible, that is to say, in the embodiment of the present invention, multiple heating zones and multiple slit zones After alternate connections, the enclosure forms a shape that matches the crucible in the thermal field of the single crystal furnace.
参照图1或图3,为了能够适应单晶炉热场,本发明实施例提供的加热器还包括至少两个支撑件(图中未示出),以及至少两个支撑件连接结构30。每个支撑件通过可拆卸连接件与相应所述支撑件连接结构30相连接。Referring to FIG. 1 or FIG. 3 , in order to adapt to the thermal field of the single crystal furnace, the heater provided by the embodiment of the present invention further includes at least two supports (not shown in the figure), and at least two support connection structures 30 . Each support is connected to the corresponding support connection structure 30 through a detachable connection.
可以理解,上述支撑件用于支撑加热器,以使加热器能够稳固的放置在单晶炉热场中。每个支撑件通过可拆卸连接件与相应所述支撑件连接结构相连接,基于此,对于不同高度的热场,可通过对支撑件的拆卸和更换来实现,而其他热场部件不受影响,从而进一步节省成本。It can be understood that the above-mentioned supporting member is used to support the heater, so that the heater can be stably placed in the thermal field of the single crystal furnace. Each support is connected to the corresponding support connection structure through a detachable connection. Based on this, for different heights of the heat field, it can be realized by disassembling and replacing the support, while other heat field components are not affected , resulting in further cost savings.
其中,上述每个支撑件连接结构设置于加热器的目标加热区和与目标加热区相邻的开缝区之间,其中,目标加热区为所述多个加热区中的任意一个。对于支撑件连接结构在加热器中的具体位置,本发明实施例不作具体的限定。Wherein, each support connecting structure is arranged between the target heating area of the heater and the slit area adjacent to the target heating area, wherein the target heating area is any one of the plurality of heating areas. The embodiment of the present invention does not specifically limit the specific position of the support member connection structure in the heater.
具体的,当所述加热器包括两个支撑件连接结构时,所述两个支撑件连接结构位于所述加热器的对称位置处,以实现对加热器的稳固支撑。可以理解,当加热器包括多个支撑件连接结构时,该多个支撑件连接结构,沿所述加热器的周向,均匀的设置在所述加热器的相应位置处。Specifically, when the heater includes two support member connection structures, the two support member connection structures are located at symmetrical positions of the heater, so as to realize stable support for the heater. It can be understood that when the heater includes a plurality of support member connection structures, the plurality of support member connection structures are evenly arranged at corresponding positions of the heater along the circumferential direction of the heater.
进一步的,参照图5和图6,每个支撑件连接结构30均包括相连接的连接区301以及连接开口区302。Further, referring to FIG. 5 and FIG. 6 , each support member connection structure 30 includes a connected connection area 301 and a connection opening area 302 .
参照图5或图6,连接开口区302的宽度d大于或等于连接区301的宽度b。Referring to FIG. 5 or FIG. 6 , the width d of the connection opening region 302 is greater than or equal to the width b of the connection region 301 .
其中,连接开口区的宽度为:与多个加热区及所述多个开缝区的排列方向相同的方向上,连接开口区的尺寸。具体的,参照图1,连接开口区302的宽度方向与多个加热区及所述多个开缝区的排列方向相同,连接开口区302的宽度方向为E,连接开口区的宽度为连接开口区沿方向E上的尺寸。Wherein, the width of the connecting opening area is: the size of the connecting opening area in the same direction as the arrangement direction of the plurality of heating areas and the plurality of slit areas. Specifically, referring to Fig. 1, the width direction of the connection opening area 302 is the same as the arrangement direction of the plurality of heating areas and the plurality of slit areas, the width direction of the connection opening area 302 is E, and the width of the connection opening area is the connection opening The size of the zone along the direction E.
所述连接区的宽度为:与多个加热区及多个开缝区的排列方向相同的方向上,连接区的尺寸。具体的,参照图1,连接区301的宽度方向与多个加热区及所述多个开缝区的排列方向相同,连接区301的宽度方向为E,连接区的宽度为连接区沿方向E上的尺寸。The width of the connection area is: the size of the connection area in the same direction as the arrangement direction of the plurality of heating areas and the plurality of slit areas. Specifically, referring to Fig. 1, the width direction of the connection zone 301 is the same as the arrangement direction of the multiple heating zones and the plurality of slit zones, the width direction of the connection zone 301 is E, and the width of the connection zone is E along the direction E of the connection zone. on the size.
每个加热器所包括的至少两个支撑件连接结构30的连接开口区302具有相同的开口方向。The connection opening regions 302 of at least two support member connection structures 30 included in each heater have the same opening direction.
在一种可能的实现方式中,参照图5,连接开口区302与连接区301沿多个加热区及所述多个开缝区的排列方向排布;连接开口区302的开口深度c1大于或等于连接区301的高度a。In a possible implementation, referring to FIG. 5 , the connection opening area 302 and the connection area 301 are arranged along the arrangement direction of the plurality of heating areas and the plurality of slit areas; the opening depth c1 of the connection opening area 302 is greater than or It is equal to the height a of the connection area 301 .
在另一种可能的实现方式中,参照图6,连接开口区302与连接区301在加热器表面上沿垂直于多个加热区及多个开缝区的排列方向排布。可以看出,图6中连接开口区的最小深度为c2。且连接开口区302的最小开口深度c2大于或等于连接区301的高度a。In another possible implementation, referring to FIG. 6 , the connection opening area 302 and the connection area 301 are arranged on the surface of the heater along a direction perpendicular to the arrangement direction of the plurality of heating areas and the plurality of slit areas. It can be seen that the minimum depth of the connection opening area in FIG. 6 is c2. And the minimum opening depth c2 of the connecting opening area 302 is greater than or equal to the height a of the connecting area 301 .
其中,参照图1,连接开口区302的开口深度为:与连接开口区302的宽度方向E相垂直的方向D上所述连接开口区的尺寸。Wherein, referring to FIG. 1 , the opening depth of the connection opening area 302 is: the size of the connection opening area in a direction D perpendicular to the width direction E of the connection opening area 302 .
连接区301的高度为:与连接区301的宽度方向E相垂直的方向D上连接区的尺寸。The height of the connection region 301 is: the size of the connection region in a direction D perpendicular to the width direction E of the connection region 301 .
基于以上描述,由于至少两个支撑件连接结构的连接开口区具有相同的开口方向,且连接开口区的宽度大于或等于连接区的宽度,连接开口区的开口深度大于或等于与连接区的高度,故本发明实施例中支撑件连接结构可以适应本发明加热器的结构,以使两个相同的加热器中一个加热器的加热区可以嵌套进另一个加热器的开缝区中,进而在制作加热器时,一个完整胚体可以加工成两个相同的加热器,从而提升加热器产出比,同时降低加热器的使用成本。Based on the above description, since the connection opening areas of at least two supporting member connection structures have the same opening direction, and the width of the connection opening area is greater than or equal to the width of the connection area, the opening depth of the connection opening area is greater than or equal to the height of the connection area , so the connection structure of the support in the embodiment of the present invention can be adapted to the structure of the heater of the present invention, so that the heating area of one of the two identical heaters can be nested into the slit area of the other heater, and then When making a heater, a complete embryo body can be processed into two identical heaters, thereby increasing the output ratio of the heater and reducing the cost of using the heater.
在一种具体的示例中,上述支撑件连接结构的加工方法可以为:由于加热器的加热区环状对称,对任意预留加热区不做开缝,且对称位置也不开缝;在加热器高度的二分之一处设置支撑件连接结构,支撑件连接结构与支撑件通过碳碳螺栓连接而成,支撑件的高度可以根据不同热场尺寸用其他胚体加工,且其他热场部件不受影响,因此,可以进一步节省成本。In a specific example, the processing method of the connection structure of the above-mentioned support member can be as follows: since the heating area of the heater is annularly symmetrical, no slits are made for any reserved heating area, and no slits are made at the symmetrical positions; The support connection structure is set at half of the height of the device. The support connection structure and the support are connected by carbon-carbon bolts. The height of the support can be processed with other blanks according to different thermal field sizes, and other thermal field components Unaffected, therefore, further cost savings can be achieved.
在实际的应用中,为了满足电阻要求和加热器寿命,加热区的宽度优选35mm-50mm,加热器总高度优选240mm-280mm。In practical applications, in order to meet the resistance requirements and the life of the heater, the width of the heating zone is preferably 35mm-50mm, and the total height of the heater is preferably 240mm-280mm.
本发明实施例还提供了一种单晶炉热场,包括上述加热器。An embodiment of the present invention also provides a thermal field of a single crystal furnace, including the above-mentioned heater.
本发明实施例还提供的单晶炉热场的有益效果与上述加热器的有益效果相同,此处不再赘述。The beneficial effect of the thermal field of the single crystal furnace provided by the embodiment of the present invention is the same as that of the above-mentioned heater, and will not be repeated here.
尽管在此结合各实施例对本发明进行了描述,然而,在实施所要求保护的本发明过程中,本领域技术人员通过查看附图、公开内容、以及所附权利要求书,可理解并实现公开实施例的其他变化。在权利要求中,“包括”(comprising)一词不排除其他组成部分或步骤,“一”或“一个”不排除多个的情况。单个处理器或其他单元可以实现权利要求中列举的若干项功能。相互不同的从属权利要求中记载了某些措施,但这并不表示 这些措施不能组合起来产生良好的效果。Although the present invention has been described in conjunction with various embodiments herein, in implementing the claimed invention, those skilled in the art can understand and realize the disclosure by referring to the drawings, the disclosure, and the appended claims. Other Variations of Embodiments. In the claims, the word "comprising" does not exclude other components or steps, and "a" or "an" does not exclude a plurality. A single processor or other unit may fulfill the functions of several items recited in the claims. The mere fact that certain measures are recited in mutually different dependent claims does not indicate that these measures cannot be combined to advantage.
尽管结合具体特征及其实施例对本发明进行了描述,显而易见的,在不脱离本发明的精神和范围的情况下,可对其进行各种修改和组合。相应地,本说明书和附图仅仅是所附权利要求所界定的本发明的示例性说明,且视为已覆盖本发明范围内的任意和所有修改、变化、组合或等同物。显然,本领域的技术人员可以对本发明进行各种改动和变型而不脱离本发明的精神和范围。这样,倘若本发明的这些修改和变型属于本发明权利要求及其等同技术的范围之内,则本发明也意图包括这些改动和变型在内。Although the invention has been described in conjunction with specific features and embodiments thereof, it will be apparent that various modifications and combinations can be made therein without departing from the spirit and scope of the invention. Accordingly, the specification and drawings are merely illustrative of the invention as defined by the appended claims and are deemed to cover any and all modifications, variations, combinations or equivalents within the scope of the invention. Obviously, those skilled in the art can make various changes and modifications to the present invention without departing from the spirit and scope of the present invention. Thus, if these modifications and variations of the present invention fall within the scope of the claims of the present invention and equivalent technologies thereof, the present invention also intends to include these modifications and variations.

Claims (13)

  1. 一种加热器,其特征在于,应用于单晶炉热场中,所述加热器设置在所述单晶炉热场中坩埚的外周,用于至少对所述坩埚中的熔硅液面进行加热;A heater, characterized in that it is applied in the thermal field of a single crystal furnace, the heater is arranged on the outer periphery of a crucible in the thermal field of a single crystal furnace, and is used to at least control the molten silicon liquid level in the crucible heating;
    所述加热器包括:多个加热区以及多个开缝区,每个所述开缝区均连接于相邻两个所述加热区之间;所述多个开缝区的开口具有相同的开口方向,且所述开缝区的宽度大于或等于所述加热区的宽度。The heater includes: a plurality of heating areas and a plurality of slit areas, and each of the slit areas is connected between two adjacent heating areas; the openings of the plurality of slit areas have the same The opening direction, and the width of the slit area is greater than or equal to the width of the heating area.
  2. 根据权利要求1所述的加热器,其特征在于,所述多个加热区具有相同的尺寸参数,所述多个开缝区具有相同的尺寸参数。The heater according to claim 1, wherein the plurality of heating regions have the same size parameter, and the plurality of slotted regions have the same size parameter.
  3. 根据权利要求1所述的加热器,其特征在于,每个所述加热区包括至少一个加热件,所述开缝区的开口深度,与所述加热区中所述至少一个加热件的高度相匹配;其中,所述加热件的高度为:沿与所述多个加热区及所述多个开缝区的排列方向垂直的方向上,所述加热件的尺寸。The heater according to claim 1, wherein each of the heating zones includes at least one heating element, and the opening depth of the slotted zone is the same as the height of the at least one heating element in the heating zone. matching; wherein, the height of the heating element is: the size of the heating element along a direction perpendicular to the arrangement direction of the plurality of heating regions and the plurality of slit regions.
  4. 根据权利要求3所述的加热器,其特征在于,当所述加热区包括多个加热件时,所述多个加热件平行设置,且所述多个加热件通过相应第一连接件首尾相连接。The heater according to claim 3, wherein when the heating zone includes a plurality of heating elements, the plurality of heating elements are arranged in parallel, and the plurality of heating elements are arranged end to end through corresponding first connecting elements connect.
  5. 根据权利3所述的加热器,其特征在于,每个所述加热件的至少一端设置有倒角。The heater according to claim 3, wherein at least one end of each heating element is provided with a chamfer.
  6. 根据权利要求1所述的加热器,其特征在于,所述开缝区包括第二连接件,所述第二连接件位于所述开缝区背离所述开缝区的开口一侧,用于连接相邻两个所述加热区。The heater according to claim 1, wherein the slotted area includes a second connecting piece, the second connecting piece is located on the side of the slotted area away from the opening of the slotted area, for Two adjacent heating zones are connected.
  7. 根据权利要求1-6任一项所述的加热器,其特征在于,多个所述加热区和多个所述开缝区交替连接后,围合形成与所述单晶炉热场中坩埚相匹配的形状。The heater according to any one of claims 1-6, characterized in that, after a plurality of said heating zones and a plurality of said slit zones are alternately connected, they are surrounded to form a crucible in the thermal field of the single crystal furnace. Match the shape.
  8. 根据权利要求1-6任一项所述的加热器,其特征在于,所述加热器还包括至少两个支撑件和至少两个支撑件连接结构;每个所述支撑件通过可拆卸连接件与相应所述支撑件连接结构相连接;The heater according to any one of claims 1-6, characterized in that, the heater further comprises at least two supports and at least two support connection structures; each of the supports is connected through a detachable connection be connected with the corresponding support connecting structure;
    每个所述支撑件连接结构设置于所述加热器的目标加热区和与所述目标加热区相邻的开缝区之间,其中,所述目标加热区为所述多个加热区中的一个。Each support connecting structure is disposed between a target heating area of the heater and a slit area adjacent to the target heating area, wherein the target heating area is one of the plurality of heating areas one.
  9. 根据权利要求8所述的加热器,其特征在于,当所述加热器包括两个支撑件连接结构时,所述两个支撑件连接结构位于所述加热器的对称位置处;The heater according to claim 8, wherein when the heater includes two support connection structures, the two support connection structures are located at symmetrical positions of the heater;
    或,当所述加热器包括的支撑件连接结构数量大于两个时,多个所述支撑件连接结构均匀的设置在所述加热器的相应位置处。Or, when the heater includes more than two support connection structures, multiple support connection structures are evenly arranged at corresponding positions of the heater.
  10. 根据权利要求8所述的加热器,其特征在于,每个所述支撑件连接结构均包括相连接的连接区以及连接开口区;The heater according to claim 8, characterized in that, each of the supporting member connection structures includes a connected connection area and a connection opening area;
    所述连接开口区的宽度大于或等于所述连接区的宽度。The width of the connection opening area is greater than or equal to the width of the connection area.
  11. 根据权利要求10所述的加热器,其特征在于,所述至少两个支撑件连接结构的 连接开口区具有相同的开口方向。The heater according to claim 10, characterized in that the connecting opening areas of the at least two supporting member connecting structures have the same opening direction.
  12. 根据权利要求10所述的加热器,其特征在于,所述连接开口区与所述连接区沿所述多个加热区及所述多个开缝区的排列方向排布;所述连接开口区的开口深度大于或等于所述连接区的高度;The heater according to claim 10, wherein the connection opening area and the connection area are arranged along the arrangement direction of the plurality of heating areas and the plurality of slit areas; the connection opening area The depth of the opening is greater than or equal to the height of the connection area;
    或,所述连接开口区与所述连接区在所述加热器表面上沿垂直于所述多个加热区及所述多个开缝区的排列方向排布,所述连接开口区的最小开口深度大于或等于所述连接区的高度。Or, the connection opening area and the connection area are arranged on the surface of the heater along a direction perpendicular to the arrangement direction of the plurality of heating areas and the plurality of slit areas, and the smallest opening of the connection opening area The depth is greater than or equal to the height of the connection zone.
  13. 一种单晶炉热场,其特征在于,包括权利要求1-12任一项所述的加热器。A thermal field of a single crystal furnace, characterized by comprising the heater described in any one of claims 1-12.
PCT/CN2022/102105 2021-08-31 2022-06-29 Heater and single crystal furnace thermal field WO2023029708A1 (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116397316B (en) * 2023-06-07 2023-08-08 苏州晨晖智能设备有限公司 Oxygen-reducing single crystal furnace and oxygen-reducing single crystal growth method

Citations (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102758245A (en) * 2012-06-20 2012-10-31 合肥景坤新能源有限公司 Deoxidizing type single crystal furnace
CN102828236A (en) * 2012-06-20 2012-12-19 合肥景坤新能源有限公司 Self-controlled heating system for monocrystal furnace
JP2013134880A (en) * 2011-12-26 2013-07-08 Valeo Japan Co Ltd Ceramic heater and electric heating type hot water heating device using the same
CN106521624A (en) * 2016-12-13 2017-03-22 晶澳太阳能有限公司 Silicon solar low-oxygen low-light-attenuation single crystal thermal field
CN206188922U (en) * 2016-10-17 2017-05-24 宁夏协鑫晶体科技发展有限公司 Heater for pulling of crystals
CN107460539A (en) * 2017-06-30 2017-12-12 内蒙古中环光伏材料有限公司 A kind of monocrystalline silicon production method of heater and the application heater
CN207130360U (en) * 2017-06-30 2018-03-23 内蒙古中环光伏材料有限公司 A kind of heater
CN208667897U (en) * 2018-06-11 2019-03-29 杞县东磁新能源有限公司 A kind of single crystal growing furnace for the monocrystalline silicon continuous production crystallization promoting pulling rate
CN110521279A (en) * 2017-04-26 2019-11-29 京瓷株式会社 Heater
CN111733447A (en) * 2020-05-27 2020-10-02 西安奕斯伟硅片技术有限公司 Single crystal furnace heating device, single crystal furnace and heating method of single crystal furnace
CN211689295U (en) * 2019-12-17 2020-10-16 内蒙古中环光伏材料有限公司 Main heater for reducing silicon oxygen content of czochralski single crystal and improving crystallization rate
CN212955439U (en) * 2020-07-22 2021-04-13 杞县东磁新能源有限公司 Special-shaped combined type heating device for solar monocrystalline silicon production
CN113174627A (en) * 2021-05-13 2021-07-27 路景刚 Asymmetric double-loop side heater

Patent Citations (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2013134880A (en) * 2011-12-26 2013-07-08 Valeo Japan Co Ltd Ceramic heater and electric heating type hot water heating device using the same
CN102758245A (en) * 2012-06-20 2012-10-31 合肥景坤新能源有限公司 Deoxidizing type single crystal furnace
CN102828236A (en) * 2012-06-20 2012-12-19 合肥景坤新能源有限公司 Self-controlled heating system for monocrystal furnace
CN206188922U (en) * 2016-10-17 2017-05-24 宁夏协鑫晶体科技发展有限公司 Heater for pulling of crystals
CN106521624A (en) * 2016-12-13 2017-03-22 晶澳太阳能有限公司 Silicon solar low-oxygen low-light-attenuation single crystal thermal field
CN110521279A (en) * 2017-04-26 2019-11-29 京瓷株式会社 Heater
CN207130360U (en) * 2017-06-30 2018-03-23 内蒙古中环光伏材料有限公司 A kind of heater
CN107460539A (en) * 2017-06-30 2017-12-12 内蒙古中环光伏材料有限公司 A kind of monocrystalline silicon production method of heater and the application heater
CN208667897U (en) * 2018-06-11 2019-03-29 杞县东磁新能源有限公司 A kind of single crystal growing furnace for the monocrystalline silicon continuous production crystallization promoting pulling rate
CN211689295U (en) * 2019-12-17 2020-10-16 内蒙古中环光伏材料有限公司 Main heater for reducing silicon oxygen content of czochralski single crystal and improving crystallization rate
CN111733447A (en) * 2020-05-27 2020-10-02 西安奕斯伟硅片技术有限公司 Single crystal furnace heating device, single crystal furnace and heating method of single crystal furnace
CN212955439U (en) * 2020-07-22 2021-04-13 杞县东磁新能源有限公司 Special-shaped combined type heating device for solar monocrystalline silicon production
CN113174627A (en) * 2021-05-13 2021-07-27 路景刚 Asymmetric double-loop side heater

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