TWI827250B - Water cooling jacket device and single crystal furnace - Google Patents
Water cooling jacket device and single crystal furnace Download PDFInfo
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- TWI827250B TWI827250B TW111134427A TW111134427A TWI827250B TW I827250 B TWI827250 B TW I827250B TW 111134427 A TW111134427 A TW 111134427A TW 111134427 A TW111134427 A TW 111134427A TW I827250 B TWI827250 B TW I827250B
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- 238000001816 cooling Methods 0.000 title claims abstract description 107
- 239000013078 crystal Substances 0.000 title claims abstract description 59
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims description 34
- 230000005540 biological transmission Effects 0.000 claims abstract description 26
- 239000010410 layer Substances 0.000 description 26
- 239000011248 coating agent Substances 0.000 description 23
- 238000000576 coating method Methods 0.000 description 23
- 230000000694 effects Effects 0.000 description 19
- 230000007547 defect Effects 0.000 description 12
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- 238000009413 insulation Methods 0.000 description 6
- 238000006243 chemical reaction Methods 0.000 description 5
- 238000010521 absorption reaction Methods 0.000 description 4
- 239000002131 composite material Substances 0.000 description 4
- 230000017525 heat dissipation Effects 0.000 description 4
- 230000007704 transition Effects 0.000 description 4
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 3
- 238000009826 distribution Methods 0.000 description 3
- 230000005855 radiation Effects 0.000 description 3
- 229910052710 silicon Inorganic materials 0.000 description 3
- 239000010703 silicon Substances 0.000 description 3
- 235000012431 wafers Nutrition 0.000 description 3
- 229920000049 Carbon (fiber) Polymers 0.000 description 2
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 2
- 238000009825 accumulation Methods 0.000 description 2
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- 239000007770 graphite material Substances 0.000 description 2
- 239000011261 inert gas Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 230000006911 nucleation Effects 0.000 description 2
- 238000010899 nucleation Methods 0.000 description 2
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 239000012790 adhesive layer Substances 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
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- 230000007246 mechanism Effects 0.000 description 1
- 229910021421 monocrystalline silicon Inorganic materials 0.000 description 1
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Classifications
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- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B27/00—Single-crystal growth under a protective fluid
- C30B27/02—Single-crystal growth under a protective fluid by pulling from a melt
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- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
- C30B29/02—Elements
- C30B29/06—Silicon
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E30/00—Energy generation of nuclear origin
- Y02E30/30—Nuclear fission reactors
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Crystallography & Structural Chemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
Abstract
本發明屬於一種水冷套裝置和單晶爐,水冷套裝置包括水冷套本體和用於控制水冷套本體升降的升降結構;水冷套本體包括內筒和位於內筒外部的外筒;升降結構包括相對設置於水冷套本體的兩側的兩個升降部,每個升降部包括驅動件和傳動件,傳動件通過連接結構與外筒連接,使得兩個升降部能夠非同步運動以帶動水冷套本體傾斜預設角度。The invention belongs to a water-cooling jacket device and a single crystal furnace. The water-cooling jacket device includes a water-cooling jacket body and a lifting structure for controlling the lifting and lowering of the water-cooling jacket body; the water-cooling jacket body includes an inner cylinder and an outer cylinder located outside the inner cylinder; the lifting structure includes a relative Two lifting parts are provided on both sides of the water-cooling jacket body. Each lifting part includes a driving part and a transmission part. The transmission part is connected to the outer cylinder through a connecting structure, so that the two lifting parts can move asynchronously to drive the water-cooling jacket body to tilt. Default angle.
Description
本發明屬於單晶矽產品製作技術領域,尤其關於一種水冷套裝置和單晶爐。The invention belongs to the technical field of manufacturing single crystal silicon products, and in particular relates to a water cooling jacket device and a single crystal furnace.
隨著半導體先進製程地不斷提高,對半導體晶圓的品質要求越來越高,而對於晶圓的品質,拉晶步驟對晶圓核心品質的影響非常大,如氧含量、體積微缺陷(Bulk Micro Defects,BMD)、層錯、晶體原生顆粒缺陷(Crystal Originated Particles,COPs)、流動圖形缺陷(Flow Pattern Defects,FPD)、雷射散射缺陷(Laser Scattering Tomography Defects,LSTDs)等品質都與拉晶步驟有密切關係。With the continuous improvement of advanced semiconductor processes, the quality requirements for semiconductor wafers are getting higher and higher. As for the quality of the wafers, the crystal pulling step has a great impact on the core quality of the wafers, such as oxygen content, volume micro-defects (Bulk Micro Defects (BMD), stacking faults, Crystal Originated Particles (COPs), Flow Pattern Defects (FPD), Laser Scattering Tomography Defects (LSTDs) and other qualities are closely related to crystal pulling. The steps are closely related.
晶棒生長過程中所經歷的熱歷史很大程度上影響著晶棒的整體品質,而熱歷史主要受晶棒的縱向和軸向溫度梯度影響,拉晶爐的結構部件對溫梯的影響很大,這其中非常重要的一個部件就是水冷套,其很大程度上改變了晶棒的縱向和橫向溫度梯度,提高了晶棒的冷卻速率,進而影響晶棒的拉制速率。The thermal history experienced during the growth process of the crystal rod greatly affects the overall quality of the crystal rod, and the thermal history is mainly affected by the longitudinal and axial temperature gradient of the crystal rod. The structural components of the crystal pulling furnace have a great influence on the temperature gradient. Large, a very important component of this is the water-cooling jacket, which greatly changes the longitudinal and transverse temperature gradients of the crystal rod, increases the cooling rate of the crystal rod, and thereby affects the drawing rate of the crystal rod.
為了解決上述技術問題,本發明提供一種水冷套裝置和單晶爐,解決晶棒軸向和縱向的溫度調節受限的問題。In order to solve the above technical problems, the present invention provides a water cooling jacket device and a single crystal furnace to solve the problem of limited temperature adjustment in the axial and longitudinal directions of the crystal ingot.
為了達到上述目的,本發明實施例採用的技術方案是:一種水冷套裝置,包括水冷套本體和用於控制該水冷套本體升降的升降結構; 該水冷套本體包括內筒和位於該內筒外部的外筒; 該升降結構包括相對設置於該水冷套本體的兩側的兩個升降部,每個該升降部包括驅動件和傳動件,該傳動件通過連接結構與該外筒連接,使得兩個該升降部能夠非同步運動以帶動該水冷套本體傾斜預設角度。 In order to achieve the above object, the technical solution adopted in the embodiment of the present invention is: a water-cooling jacket device, including a water-cooling jacket body and a lifting structure for controlling the lifting and lowering of the water-cooling jacket body; The water cooling jacket body includes an inner cylinder and an outer cylinder located outside the inner cylinder; The lifting structure includes two lifting parts disposed oppositely on both sides of the water-cooling jacket body. Each lifting part includes a driving part and a transmission part. The transmission part is connected to the outer cylinder through a connecting structure, so that the two lifting parts It can move asynchronously to drive the water-cooling jacket body to tilt at a preset angle.
可選地,該傳動件包括: 升降桿,沿該外筒的軸向方向延伸,且該升降桿外表面上設置有齒條結構; 傳動齒輪,該傳動齒輪通過與該齒條結構嚙合以與該升降桿傳動連接。 Optionally, the transmission component includes: A lifting rod extends along the axial direction of the outer cylinder, and a rack structure is provided on the outer surface of the lifting rod; A transmission gear, which is in transmission connection with the lifting rod by meshing with the rack structure.
可選地,兩個該升降桿中的一個該升降桿的外表面具有遠離該另一個該升降桿設置的第一區域,該第一區域內凹形成一連接面,該連接面上設置該齒條結構。Optionally, the outer surface of one of the two lifting rods has a first area disposed away from the other lifting rod, and the first area is concave to form a connecting surface, and the tooth is disposed on the connecting surface. bar structure.
可選地,該齒條結構包括凸設於該連接面上的多個相平行設置的齒條,多個該齒條沿該外筒的軸向方向並排設置,相鄰兩個該齒條之間形成齒槽。Optionally, the rack structure includes a plurality of parallel racks protruding from the connecting surface, and a plurality of the racks are arranged side by side along the axial direction of the outer cylinder, and between two adjacent racks Alveoli are formed between them.
可選地,該升降桿遠離該外筒的一端設置有限位台。Optionally, a limiting platform is provided at one end of the lifting rod away from the outer cylinder.
可選地,在該外筒的軸向方向上,該第一區域的長度小於該升降桿的長度,且該第一區域位於該升降桿遠離該外筒的一端。Optionally, in the axial direction of the outer cylinder, the length of the first region is less than the length of the lifting rod, and the first region is located at an end of the lifting rod away from the outer cylinder.
可選地,在該外筒的軸向方向上,該第一區域的長度大於該升降桿的長度的一半。Optionally, the length of the first region is greater than half the length of the lifting rod in the axial direction of the outer cylinder.
可選地,該連接部包括套設於該外筒外部的卡環,該卡環的相對的兩側凸設形成兩個凸起,每個該凸起上設置有用於與相應的該升降桿連接的連接通孔。Optionally, the connection part includes a snap ring that is sleeved on the outside of the outer cylinder. Two protrusions are formed on opposite sides of the snap ring, and each protrusion is provided with a corresponding lifting rod. Connection vias for connections.
可選地,該外筒的頂部設置有第一凸緣,該卡環設置於該第一凸緣靠近該外筒的底部的一側。Optionally, a first flange is provided on the top of the outer cylinder, and the snap ring is disposed on a side of the first flange close to the bottom of the outer cylinder.
本發明實施例還提供一種單晶爐,包括上述的水冷套裝置。An embodiment of the present invention also provides a single crystal furnace, including the above water-cooling jacket device.
本發明的有益效果是:通過該升降結構的設置,控制該水冷套本體的升降,且兩個升降部採用獨立驅動的方式,以使得兩個該升降部可非同步運動,使得水冷套本體可在預設角度範圍內傾斜,從而形成不對稱的水冷效果,以此達到徑向和軸向的梯度溫梯變化,大大提高晶棒軸向和徑向的散熱,減少內部熱量累積,改變晶棒的熱歷史,減少錯排及其他晶體缺陷的產生,提高晶棒品質。The beneficial effects of the present invention are: through the setting of the lifting structure, the lifting of the water-cooling jacket body is controlled, and the two lifting parts are independently driven, so that the two lifting parts can move asynchronously, so that the water-cooling jacket body can Tilt within the preset angle range to form an asymmetric water cooling effect, thereby achieving radial and axial gradient temperature gradient changes, greatly improving the axial and radial heat dissipation of the crystal ingot, reducing internal heat accumulation, and changing the crystal ingot Thermal history can reduce the occurrence of misalignment and other crystal defects and improve the quality of ingots.
為利 貴審查委員了解本發明之技術特徵、內容與優點及其所能達到之功效,茲將本發明配合附圖及附件,並以實施例之表達形式詳細說明如下,而其中所使用之圖式,其主旨僅為示意及輔助說明書之用,未必為本發明實施後之真實比例與精準配置,故不應就所附之圖式的比例與配置關係解讀、侷限本發明於實際實施上的申請範圍,合先敘明。In order to help the review committee understand the technical features, content and advantages of the present invention and the effects it can achieve, the present invention is described in detail below in the form of embodiments with the accompanying drawings and attachments, and the drawings used therein are , its purpose is only for illustration and auxiliary description, and may not represent the actual proportions and precise configurations after implementation of the present invention. Therefore, the proportions and configuration relationships of the attached drawings should not be interpreted or limited to the actual implementation of the present invention. The scope shall be stated first.
在本發明實施例的描述中,需要理解的是,術語“長度”、“寬度”、“上”、“下”、“前”、“後”、“左”、“右”、“垂直”、“水平”、“頂”、“底”“內”、“外”等指示的方位或位置關係為基於附圖所示的方位或位置關係,僅是為了便於描述本發明實施例和簡化描述,而不是指示或暗示所指的裝置或元件必須具有特定的方位、以特定的方位構造和操作,因此不能理解為對本發明的限制。In the description of the embodiments of the present invention, it should be understood that the terms "length", "width", "upper", "lower", "front", "back", "left", "right", "vertical" The orientations or positional relationships indicated by "horizontal", "top", "bottom", "inner", "outer", etc. are based on the orientations or positional relationships shown in the drawings, and are only for the convenience of describing the embodiments of the present invention and simplifying the description. , rather than indicating or implying that the device or element referred to must have a specific orientation, be constructed and operate in a specific orientation, and therefore cannot be construed as a limitation of the present invention.
此外,術語“第一”、“第二”僅用於描述目的,而不能理解為指示或暗示相對重要性或者隱含指明所指示的技術特徵的數量。由此,限定有“第一”、“第二”的特徵可以明示或者隱含地包括一個或者更多個所述特徵。在本發明實施例的描述中,“多個”的含義是兩個或兩個以上,除非另有明確具體的限定。In addition, the terms “first” and “second” are used for descriptive purposes only and cannot be understood as indicating or implying relative importance or implicitly indicating the quantity of indicated technical features. Thus, features defined as “first” and “second” may explicitly or implicitly include one or more of the described features. In the description of the embodiments of the present invention, "plurality" means two or more than two, unless otherwise explicitly and specifically limited.
在本發明實施例中,除非另有明確的規定和限定,術語“安裝”、“相連”、“連接”、“固定”等術語應做廣義理解,例如,可以是固定連接,也可以是可拆卸連接,或成一體;可以是機械連接,也可以是電連接;可以是直接相連,也可以通過中間媒介間接相連,可以是兩個元件內部的連通或兩個元件的相互作用關係。對於本領域的具通常知識者而言,可以根據具體情況理解上述術語在本發明實施例中的具體含義。In the embodiments of the present invention, unless otherwise expressly stipulated and limited, the terms "installation", "connection", "connection", "fixing" and other terms should be understood in a broad sense. For example, it can be a fixed connection or a removable connection. Disassembly and connection, or integration; it can be a mechanical connection or an electrical connection; it can be a direct connection or an indirect connection through an intermediate medium; it can be an internal connection between two elements or an interaction between two elements. For those with ordinary knowledge in the art, the specific meanings of the above terms in the embodiments of the present invention can be understood according to specific circumstances.
參考圖1至圖4,本實施例中提供一種水冷套裝置,包括水冷套本體和用於控制該水冷套本體升降的升降結構; 該水冷套本體包括內筒2和位於該內筒2外部的外筒1; 該升降結構包括相對設置於該水冷套本體的兩側的兩個升降部4,每個該升降部4包括驅動件和傳動件,該傳動件通過連接結構與該外筒1連接,使得兩個該升降部4能夠非同步運動以帶動該水冷套本體傾斜預設角度。 Referring to Figures 1 to 4, this embodiment provides a water-cooling jacket device, including a water-cooling jacket body and a lifting structure for controlling the lifting and lowering of the water-cooling jacket body; The water cooling jacket body includes an inner cylinder 2 and an outer cylinder 1 located outside the inner cylinder 2; The lifting structure includes two lifting parts 4 arranged oppositely on both sides of the water-cooling jacket body. Each lifting part 4 includes a driving part and a transmission part. The transmission part is connected to the outer cylinder 1 through a connecting structure, so that the two lifting parts 4 The lifting part 4 can move asynchronously to drive the water cooling jacket body to tilt at a preset angle.
通過該升降結構的設置,控制該水冷套本體的升降,且兩個升降部4採用獨立驅動的方式,以使得兩個該升降部4可非同步運動,使得水冷套本體可在預設角度範圍內傾斜從而形成不對稱的水冷效果,大的梯度變化可加快晶棒熱量向水冷套進行傳輸,提高傳熱效率,加快晶棒軸向和徑向的散熱。且可根據拉晶步驟需要,很大限度地調節晶棒的縱向溫度梯度和徑向溫度梯度,控制晶棒中缺陷的反應速率,調節缺陷分佈,具有很好的冷卻速率,可拉制不同缺陷類型的晶棒(如無層錯晶棒,BMD晶棒)。Through the setting of the lifting structure, the lifting of the water-cooling jacket body is controlled, and the two lifting parts 4 are driven independently, so that the two lifting parts 4 can move asynchronously, so that the water-cooling jacket body can move within a preset angle range The inner tilt forms an asymmetric water cooling effect. The large gradient change can accelerate the heat transfer of the crystal ingot to the water cooling jacket, improve the heat transfer efficiency, and accelerate the axial and radial heat dissipation of the crystal ingot. And according to the needs of the crystal pulling step, the longitudinal and radial temperature gradients of the crystal rod can be adjusted to a large extent, the reaction rate of defects in the crystal rod can be controlled, and the defect distribution can be adjusted. It has a good cooling rate and can pull different defects. Types of crystal rods (such as fault-free crystal rods, BMD crystal rods).
不同步驟參數要求的晶棒需要匹配不同的水冷效果,非同步移動的水冷套裝置可以根據需求進行相應調整得到合適的冷卻效果。Crystal ingots with different step parameter requirements need to match different water cooling effects. The asynchronously moving water cooling jacket device can be adjusted accordingly to obtain appropriate cooling effects according to needs.
非同步移動的目的是造成徑向不對稱效果,提高水冷效果,升降機構的作用:當拉制外延晶棒時,需要大的拉速拉制,通過水冷套向液面移動,增加冷卻效果,以此來提高拉速;當拉制無缺陷拋光晶棒時,可將水冷套向上移動,抑制COP的形成;當拉制BMD晶棒時,會促進BMD的形核及長大,可通過水冷套的移動調節,BMD在650℃-700℃的低溫形核,同時對於高溫區域,通過非同步移動調節,擴大在750℃-1100℃溫度範圍內的晶棒區間。以此來促進BMD的高溫形核。The purpose of asynchronous movement is to create a radial asymmetry effect and improve the water cooling effect. The role of the lifting mechanism: when drawing epitaxial crystal ingots, a large drawing speed is required, and the water cooling jacket moves toward the liquid surface to increase the cooling effect. This can be used to increase the pulling speed; when drawing defect-free polished crystal ingots, the water-cooling jacket can be moved upward to inhibit the formation of COP; when drawing BMD crystal ingots, it will promote the nucleation and growth of BMD and can be passed through the water-cooling jacket. Through movement adjustment, BMD nucleates at a low temperature of 650℃-700℃. At the same time, for high temperature areas, through asynchronous movement adjustment, the ingot range is expanded within the temperature range of 750℃-1100℃. This is used to promote the high-temperature nucleation of BMD.
需要說明的是,在該升降結構的作用下,兩個相對設置的該升降部4相配合可使得該水冷套本體傾斜升降,即通過兩個該升降部4非同步運動傾斜預設角度後,再控制兩個該升降部4同步運動以控制該水冷套本體以傾斜的狀態進行升降運動。It should be noted that under the action of the lifting structure, the cooperation of the two opposite lifting parts 4 can make the water-cooling jacket body tilt and lift, that is, after the two lifting parts 4 are tilted at a preset angle through asynchronous movement, Then, the two lifting parts 4 are controlled to move synchronously to control the water cooling jacket body to perform lifting movement in an inclined state.
需要說明的是,升降結構所包括的該升降部4的數量並不做限定,該水冷套本體的相對的兩側設置兩個該升降部4,兩個相對設置的升降部4為一組,該升降結構可以包括多組該升降部4,每一組該升降部4可以實現該水冷套本體在一個方向上的傾斜,從而可以根據實際需要,設置多組該升降部4,從而靈活控制該水冷套本體的傾斜方向,從而可以更好的控制水冷效果。It should be noted that the number of the lifting parts 4 included in the lifting structure is not limited. Two lifting parts 4 are provided on opposite sides of the water cooling jacket body, and the two opposite lifting parts 4 form a group. The lifting structure may include multiple groups of the lifting parts 4. Each group of the lifting parts 4 can tilt the water-cooling jacket body in one direction, so that multiple groups of the lifting parts 4 can be provided according to actual needs, thereby flexibly controlling the water-cooling jacket body. The tilt direction of the water cooling jacket body can better control the water cooling effect.
需要說明的是,兩個相對設置的該升降部4相配合可使得該水冷套本體傾斜升降,傾斜的角度可以根據實際需要設定,例如可以為0-17度,但並不以此為限。It should be noted that the cooperation of the two opposite lifting parts 4 can make the water-cooling jacket body tilt and lift. The tilt angle can be set according to actual needs, for example, it can be 0-17 degrees, but it is not limited to this.
示例性的,該傳動件包括: 升降桿41,沿該外筒1的軸向方向延伸,且該升降桿41外表面上設置有齒條411結構; 傳動齒輪42,該傳動齒輪42通過與該齒條411結構嚙合以與該升降桿41傳動連接。 By way of example, the transmission parts include: The lifting rod 41 extends along the axial direction of the outer cylinder 1, and a rack 411 structure is provided on the outer surface of the lifting rod 41; The transmission gear 42 is transmission connected to the lifting rod 41 by meshing with the rack 411 structure.
本實施例中採用傳動齒輪42和升降桿41相配合的方式,傳動齒輪42旋轉,在該升降桿41的傳動作用下,實現該水冷套本體的升降。In this embodiment, the transmission gear 42 and the lifting rod 41 are matched. The transmission gear 42 rotates, and under the driving action of the lifting rod 41, the water cooling jacket body is raised and lowered.
示例性的,每個該升降部4的該驅動件可以為驅動電機。For example, the driving member of each lifting part 4 may be a driving motor.
示例性的,一個該升降桿41的外表面具有遠離該另一個該升降桿41設置的第一區域,該第一區域內凹形成一連接面,該連接面上設置該齒條411結構。For example, the outer surface of one lifting rod 41 has a first area located away from the other lifting rod 41. The first area is concave to form a connecting surface, and the rack 411 structure is disposed on the connecting surface.
該連接面為與該外筒1的軸向方向相平行的平面,在該連接面上設置該齒條411結構,利於該齒條411結構與該傳動齒輪42的配合。The connecting surface is a plane parallel to the axial direction of the outer cylinder 1. The rack 411 structure is provided on the connecting surface, which facilitates the cooperation between the rack 411 structure and the transmission gear 42.
示例性的,該齒條411結構包括凸設於該連接面上的多個相平行設置的齒條411,多個該齒條411沿該外筒1的軸向方向並排設置,相鄰兩個該齒條411之間形成齒槽。Exemplarily, the rack 411 structure includes a plurality of parallel racks 411 protruding from the connection surface. The plurality of racks 411 are arranged side by side along the axial direction of the outer cylinder 1. Two adjacent racks 411 are arranged side by side. A tooth gap is formed between the racks 411 .
該齒條411的延伸方向與該外筒1的軸向方向相垂直,該傳動齒輪42的軸向方向與該齒條411的延伸方向相平行,該傳動齒輪42的齒對應於該齒槽,從而該傳動齒輪42旋轉,帶動該升降桿41進行升降運動,從而帶動該水冷套本體進行升降運動。The extension direction of the rack 411 is perpendicular to the axial direction of the outer cylinder 1, the axial direction of the transmission gear 42 is parallel to the extension direction of the rack 411, and the teeth of the transmission gear 42 correspond to the tooth groove, Thereby, the transmission gear 42 rotates, driving the lifting rod 41 to perform lifting movement, thereby driving the water cooling jacket body to perform lifting movement.
示例性的,該齒條411為螺紋齒條,螺紋齒條具有高精度和大負載的特點。For example, the rack 411 is a threaded rack, and the threaded rack has the characteristics of high precision and large load.
示例性的,該升降桿41遠離該外筒1的一端設置有限位台43。Exemplarily, a limiting platform 43 is provided at one end of the lifting rod 41 away from the outer cylinder 1 .
該限位台43的設置,防止該傳動齒輪42與該升降桿41脫離,該限位台43可以為圓形結構,且該限位台43在該升降桿41的徑向方向上的面積大於該升降桿41的端面的截面面積。The setting of the limiting platform 43 prevents the transmission gear 42 from being separated from the lifting rod 41. The limiting platform 43 can be a circular structure, and the area of the limiting platform 43 in the radial direction of the lifting rod 41 is larger than The cross-sectional area of the end surface of the lift rod 41.
該限位台43可以是與該升降桿41為一體結構,可以是經過焊接等步驟連接的,也可以是在該連接面形成時同步形成的,該第一區域可以位於該升降桿41的中部,該第一區域內凹形成凹槽,該凹槽的底面為該連接面,從而在該升降桿41的軸向方向上,該凹槽的遠離該外筒1的一端的第一側壁形成該限位台43,該凹槽的與該第一側壁相對的第二側壁形成用於限制該傳動齒輪42的運動行程的限位擋牆。The limiting platform 43 can be an integral structure with the lifting rod 41 , can be connected through welding and other steps, or can be formed simultaneously when the connection surface is formed. The first area can be located in the middle of the lifting rod 41 , a groove is formed in the first area, and the bottom surface of the groove is the connecting surface, so that in the axial direction of the lifting rod 41, the first side wall of the end of the groove away from the outer cylinder 1 forms the The limiting platform 43 and the second side wall of the groove that is opposite to the first side wall form a limiting retaining wall for limiting the movement stroke of the transmission gear 42 .
示例性的,在該外筒1的軸向方向上,該第一區域的長度小於該升降桿41的長度,且該第一區域位於該升降桿41遠離該外筒1的一端。For example, in the axial direction of the outer cylinder 1 , the length of the first region is less than the length of the lifting rod 41 , and the first region is located at an end of the lifting rod 41 away from the outer cylinder 1 .
示例性的,在該外筒1的軸向方向上,該第一區域的長度大於該升降桿41的長度的一半。For example, in the axial direction of the outer cylinder 1 , the length of the first region is greater than half of the length of the lifting rod 41 .
示例性的,該連接部5包括套設於該外筒1外部的卡環51,該卡環51的相對的兩側凸設形成兩個凸起52,每個該凸起52上設置有用於與相應的該升降桿41連接的連接通孔521。Exemplarily, the connection part 5 includes a snap ring 51 that is sleeved on the outside of the outer cylinder 1. Two protrusions 52 are formed on opposite sides of the snap ring 51, and each protrusion 52 is provided with a The connecting through hole 521 is connected to the corresponding lifting rod 41 .
示例性的,該升降桿41靠近該外筒1的一端設置有連接環44,該連接環44與該升降桿41通過螺紋連接,該升降桿41與該凸起52以間隙寬鬆配合,這樣便於在兩個該升降桿41非同步運動的時候,實現水冷套的傾斜。Exemplarily, the lifting rod 41 is provided with a connecting ring 44 at one end close to the outer cylinder 1. The connecting ring 44 is threadedly connected to the lifting rod 41. The lifting rod 41 and the protrusion 52 are loosely matched with a gap, which facilitates When the two lifting rods 41 move asynchronously, the water cooling jacket is tilted.
示例性的,該外筒1的頂部設置有第一凸緣11,該卡環51設置於該第一凸緣11靠近該外筒1的底部的一側。For example, the top of the outer cylinder 1 is provided with a first flange 11 , and the snap ring 51 is provided on a side of the first flange 11 close to the bottom of the outer cylinder 1 .
該卡環51可通過黏結層與該第一凸緣11黏接,以增強該連接部5與該外筒1之間的連接強度。The snap ring 51 can be bonded to the first flange 11 through an adhesive layer to enhance the connection strength between the connecting portion 5 and the outer cylinder 1 .
參考圖1、圖5和圖6,示例性的,該內筒2呈倒錐形結構。Referring to Figures 1, 5 and 6, as an example, the inner cylinder 2 has an inverted conical structure.
相比於單一的直筒式結構,本實施例中採用套設的內筒和外筒的雙層結構,該外筒採用直筒式結構,該外筒起到阻隔熱的作用,該內筒採用倒錐形結構,可以形成縱向梯度水冷的效果,因晶棒縱向(即晶棒的軸向方向)的溫度呈梯度變化(下端熱上端冷,靠近矽熔液的一端為下端,遠離矽熔液的一端為上端),晶棒的熱量主要是以輻射的方式傳輸給周圍溫度低的物體,輻射傳熱的強度與距離的三次方呈反比,即距離越近輻射傳熱越強,相應的水冷效果越好,該內筒呈倒錐形,沿縱向方向,該內筒的內壁與晶棒在該晶棒的徑向方向上的距離呈梯度變化,可以實現梯度水冷地效果,即縱向不對稱效果,以此達到徑向和軸向的梯度溫梯變化,大大提高晶棒軸向和徑向的散熱,減少內部熱量累積,改變晶棒的熱歷史,減少錯排及其他晶體缺陷的產生,提高晶棒品質。可根據拉晶步驟需要,調節該內筒的內壁的傾斜角度,可以很大限度地調節晶棒的縱向(即為軸向)和徑向溫度梯度,控制晶棒中缺陷的反應速率,調節缺陷分佈。Compared with a single straight cylinder structure, this embodiment adopts a double-layer structure of an inner cylinder and an outer cylinder. The outer cylinder adopts a straight cylinder structure. The outer cylinder plays a role in blocking heat. The inner cylinder adopts an inverted cylinder. The tapered structure can form a longitudinal gradient water cooling effect, because the temperature in the longitudinal direction of the crystal rod (that is, the axial direction of the crystal rod) changes in a gradient (the lower end is hot and the upper end is cold, the end close to the silicon melt is the lower end, and the end far away from the silicon melt is One end is the upper end), the heat of the crystal rod is mainly transmitted to the surrounding low-temperature objects by radiation. The intensity of radiation heat transfer is inversely proportional to the cube of the distance, that is, the closer the distance, the stronger the radiation heat transfer, and the corresponding water cooling effect The better, the inner cylinder has an inverted conical shape, and along the longitudinal direction, the distance between the inner wall of the inner cylinder and the crystal rod in the radial direction of the crystal rod changes in a gradient, which can achieve the effect of gradient water cooling, that is, longitudinal asymmetry. The effect is to achieve radial and axial gradient temperature gradient changes, greatly improve the axial and radial heat dissipation of the crystal rod, reduce internal heat accumulation, change the thermal history of the crystal rod, and reduce the occurrence of misalignment and other crystal defects. Improve the quality of crystal ingots. According to the needs of the crystal pulling step, the inclination angle of the inner wall of the inner cylinder can be adjusted to greatly adjust the longitudinal (ie axial) and radial temperature gradient of the crystal rod, control the reaction rate of defects in the crystal rod, and adjust Defect distribution.
本實施例中,兩個升降部4採用獨立驅動的方式,以使得兩個該升降部4可非同步運動,使得水冷套本體可在預設角度範圍內傾斜從而形成徑向方向上的不對稱的水冷效果,該內筒採用倒錐形結構形成的縱向(即軸向)不對稱效果,從而兩者想配合達到晶棒徑向和軸向的雙不對稱,進而提高晶棒軸向和徑向的散熱效率。In this embodiment, the two lifting parts 4 are driven independently, so that the two lifting parts 4 can move asynchronously, so that the water cooling jacket body can tilt within a preset angle range to form asymmetry in the radial direction. The inner cylinder adopts the longitudinal (i.e. axial) asymmetry effect formed by the inverted cone structure, so that the two work together to achieve double asymmetry in the radial and axial directions of the crystal rod, thereby improving the axial and radial dimensions of the crystal rod. Directional heat dissipation efficiency.
示例性的,該內筒的頂部的內直徑為450mm,該內筒的底部的內直徑為390mm,但並不以此為限。For example, the inner diameter of the top of the inner cylinder is 450 mm, and the inner diameter of the bottom of the inner cylinder is 390 mm, but this is not a limitation.
該內筒的頂部設置有第二凸緣22,該外筒的頂部設置有第一凸緣11,該第一凸緣11靠近該內筒的一側設置有臺階形凹槽13,該第二凸緣22搭接於該臺階形凹槽13內。The top of the inner cylinder is provided with a second flange 22. The top of the outer cylinder is provided with a first flange 11. The first flange 11 is provided with a step-shaped groove 13 on one side close to the inner cylinder. The second flange 22 is provided on the top of the inner cylinder. The flange 22 overlaps in the stepped groove 13 .
該第二凸緣22遠離該內筒底部的第一面與該第一凸緣11遠離該內筒底部的第二面位於同一平面。The first surface of the second flange 22 away from the bottom of the inner cylinder and the second surface of the first flange 11 away from the bottom of the inner cylinder are located on the same plane.
該內筒的底部具有第一通孔,該外筒的底部具有第二通孔12,該第一通孔的圓心在該外筒1的底部上的正投影與該第二通孔12的圓心重合。The bottom of the inner cylinder has a first through hole, and the bottom of the outer cylinder has a second through hole 12. The orthogonal projection of the center of the first through hole on the bottom of the outer cylinder 1 is equal to the center of the second through hole 12. coincide.
示例性的,該第二通孔12的邊緣朝向該外筒1的頂部凸設有環形凸起14,該環形凸起14起到擋牆的作用,用於對該內筒2進行限位。For example, an annular protrusion 14 protrudes from the edge of the second through hole 12 toward the top of the outer cylinder 1 . The annular protrusion 14 functions as a retaining wall for limiting the position of the inner cylinder 2 .
示例性的,沿該內筒2的軸向方向,該內筒2的內側壁上設置有齒狀波紋結構21。For example, along the axial direction of the inner cylinder 2, a toothed corrugated structure 21 is provided on the inner wall of the inner cylinder 2.
齒狀波紋結構21的設置可以增加該內筒的內壁的表面積,即增加水冷套的吸熱面積,相較於平滑表面,這樣的表面吸熱效果更好,具有很好的冷卻晶棒效果。The arrangement of the toothed corrugated structure 21 can increase the surface area of the inner wall of the inner cylinder, that is, increase the heat absorption area of the water cooling jacket. Compared with a smooth surface, such a surface has a better heat absorption effect and has a good cooling effect of the ingot.
該齒狀波紋結構21包括多個沿該內筒2的周向延伸的環形齒,多個該環形齒沿該內筒2的軸向排列形成,單個環形齒的截面形狀可以為三角形、梯形、弧形等。The toothed corrugated structure 21 includes a plurality of ring-shaped teeth extending along the circumferential direction of the inner cylinder 2. The plurality of ring-shaped teeth are arranged along the axial direction of the inner cylinder 2. The cross-sectional shape of a single ring-shaped tooth can be triangular, trapezoidal, or Arc etc.
示例性的,從該內筒2的頂端到該內筒2的底部的方向上,該齒狀波紋結構21在該內筒2的徑向方向上的厚度逐漸增大。For example, in the direction from the top of the inner cylinder 2 to the bottom of the inner cylinder 2 , the thickness of the toothed corrugated structure 21 in the radial direction of the inner cylinder 2 gradually increases.
示例性的,該內筒2的內側壁設置有吸熱塗層。For example, the inner side wall of the inner cylinder 2 is provided with a heat-absorbing coating.
該吸熱塗層設置於該齒狀波紋結構21遠離該外筒1的一側,該吸熱塗層的形狀與該齒狀波紋結構21的形狀相符,即該吸熱塗層與該內筒2的連接面和與該連接面相對設置的內表面均為齒狀波紋結構21。The heat-absorbing coating is disposed on the side of the toothed corrugated structure 21 away from the outer cylinder 1 . The shape of the heat-absorbing coating is consistent with the shape of the toothed corrugated structure 21 , that is, the connection between the heat-absorbing coating and the inner cylinder 2 Both the surface and the inner surface opposite to the connecting surface are toothed corrugated structures 21 .
該吸熱塗層具有吸熱作用,該吸熱塗層與該內筒2的結合強度高,可有效緩解吸熱塗層介面(該吸熱塗層與該內筒2的連接面)的熱應力,熱力學性能穩定,該內筒2可以很好地即時帶走晶棒傳輸的熱量,大大提高晶棒的冷卻速率,提高拉速,增加拉晶效率。The heat-absorbing coating has a heat-absorbing effect. The bonding strength between the heat-absorbing coating and the inner cylinder 2 is high, which can effectively alleviate the thermal stress at the interface of the heat-absorbing coating (the connection surface between the heat-absorbing coating and the inner cylinder 2), and has stable thermodynamic properties. , the inner cylinder 2 can take away the heat transmitted by the crystal rod very well and instantly, greatly improving the cooling rate of the crystal rod, increasing the pulling speed, and increasing the crystal pulling efficiency.
示例性的,該內筒2的外側壁設置有隔熱塗層,從該內筒2的頂端到該內筒2的底部的方向上,該吸熱塗層在該內筒2的徑向方向上的厚度逐漸增大。Exemplarily, the outer wall of the inner cylinder 2 is provided with a heat-insulating coating, and the heat-absorbing coating is in the radial direction of the inner cylinder 2 from the top of the inner cylinder 2 to the bottom of the inner cylinder 2 The thickness gradually increases.
示例性的,該吸熱塗層採用陶瓷製成,但並不以此為限。Illustratively, the heat-absorbing coating is made of ceramic, but is not limited to this.
示例性的,該吸熱塗層的厚度為200±50微米。For example, the thickness of the heat-absorbing coating is 200±50 microns.
示例性的,該內筒2的外側壁和/或該外筒1的內側壁設置有隔熱塗層。For example, the outer side wall of the inner cylinder 2 and/or the inner side wall of the outer cylinder 1 is provided with a heat-insulating coating.
該隔熱塗層具有反射及遮罩熱的作用,防止外面的熱量從該外筒1向水冷套(即該內筒2的內部)內部傳輸,維持水冷套內部的溫度恆定。The heat-insulating coating has the function of reflecting and shielding heat, preventing external heat from being transmitted from the outer cylinder 1 to the inside of the water-cooling jacket (ie, the inside of the inner cylinder 2), and maintaining a constant temperature inside the water-cooling jacket.
示例性的,從該內筒2的頂端到該內筒2的底部的方向上,該隔熱塗層在該內筒2的徑向方向上的厚度逐漸增大。For example, the thickness of the heat-insulating coating in the radial direction of the inner cylinder 2 gradually increases from the top of the inner cylinder 2 to the bottom of the inner cylinder 2 .
示例性的,該隔熱塗層採用耐高溫隔熱氧化鋯陶瓷製成。For example, the heat-insulating coating is made of high-temperature-resistant and heat-insulating zirconia ceramics.
示例性的,該隔熱塗層的厚度為100±25微米,但並不以此為限。For example, the thickness of the thermal insulation coating is 100±25 microns, but is not limited to this.
示例性的,沿著該內筒2的軸向方向,該水冷管道3螺旋式環繞分佈於該內筒2的外側壁上。For example, along the axial direction of the inner cylinder 2 , the water-cooling pipes 3 are spirally distributed around the outer wall of the inner cylinder 2 .
該水冷管道3可以設置在該內筒2的外側壁上,也可以設置在該外筒1的內側壁上。The water-cooling pipe 3 can be provided on the outer side wall of the inner cylinder 2 or on the inner side wall of the outer cylinder 1 .
該水冷管道3的具體結構形式並不以此為限,例如該水冷管道3可呈蛇形,分佈於該內筒2的外側壁,該水冷管道3呈蛇形,包括沿該內筒2的軸向延伸的多個直線形管道和設置於相鄰兩個直線形管道之間的彎折形管道。The specific structural form of the water-cooling pipe 3 is not limited to this. For example, the water-cooling pipe 3 can be in a serpentine shape and is distributed on the outer wall of the inner cylinder 2. The water-cooling pipe 3 is in a serpentine shape, including along the inner cylinder 2. A plurality of axially extending linear pipes and a bent pipe arranged between two adjacent linear pipes.
示例性的,從該內筒2的頂端到該內筒2的底部的方向上,該水冷管道3的直徑逐漸增大。For example, the diameter of the water-cooling pipe 3 gradually increases in the direction from the top of the inner cylinder 2 to the bottom of the inner cylinder 2 .
採用上述方案,水冷管道3的水冷效果沿著該內筒2的軸向方向呈梯度變化,有利於徑向向和軸向的梯度溫度的調節。Using the above solution, the water cooling effect of the water cooling pipe 3 changes in a gradient along the axial direction of the inner cylinder 2, which is conducive to the adjustment of the gradient temperature in the radial direction and the axial direction.
示例性的,該水冷管道的直徑為5mm-10mm,但並不以此為限。For example, the diameter of the water-cooling pipe is 5mm-10mm, but it is not limited to this.
示例性的,從該內筒2的頂端到該內筒2的底部的方向上,水冷管道的環繞間距為48mm。For example, the circumferential spacing of the water-cooling pipes in the direction from the top of the inner cylinder 2 to the bottom of the inner cylinder 2 is 48 mm.
參考圖1和圖7,示例性的,該水冷套本體的底部設置與該水冷套本體內部連通的調節套筒6,該調節套筒6包括與該水冷套本體連接的第一端,和與該第一端相對的第二端,從該第一端到該第二端,該調節套筒6在該水冷套本體的徑向方向上截面的面積逐漸減小。Referring to Figures 1 and 7, for example, the bottom of the water-cooling jacket body is provided with an adjustment sleeve 6 that communicates with the inside of the water-cooling jacket body. The adjustment sleeve 6 includes a first end connected to the water-cooling jacket body, and At the second end opposite to the first end, from the first end to the second end, the cross-sectional area of the adjusting sleeve 6 in the radial direction of the water-cooling jacket body gradually decreases.
通過該調節套筒6的設置,阻擋該水冷套本體下方熱量傳輸到水冷套內部空間,有效阻擋熱量的自下而上的散失。且該調節套筒6在該水冷套本體的徑向方向上截面的面積逐漸減小,當惰性氣體流從拉晶爐上方吹撒流經該調節套筒時,流速變大,保證了惰性氣體流與晶棒的充分接觸,提高了晶棒的冷卻速率,很好地調節晶棒的縱向和徑向溫梯,控制晶棒中缺陷的反應速率,調節缺陷分佈,拉制不同類型的晶棒。Through the arrangement of the adjusting sleeve 6, the heat below the water-cooling jacket body is blocked from being transmitted to the internal space of the water-cooling jacket, effectively blocking the bottom-up dissipation of heat. And the cross-sectional area of the adjusting sleeve 6 gradually decreases in the radial direction of the water-cooling jacket body. When the inert gas flow blows through the adjusting sleeve from above the crystal pulling furnace, the flow rate becomes larger, ensuring that the inert gas The full contact between the flow and the crystal rod increases the cooling rate of the crystal rod, well adjusts the longitudinal and radial temperature gradients of the crystal rod, controls the reaction rate of defects in the crystal rod, adjusts the defect distribution, and draws different types of crystal rods .
示例性的,該調節套筒6的內表面為曲面。For example, the inner surface of the adjustment sleeve 6 is a curved surface.
示例性的,該調節套筒6在該水冷套本體的軸向方向上的截面的形狀呈抛物線形狀。For example, the cross-section shape of the adjustment sleeve 6 in the axial direction of the water-cooling jacket body is a parabolic shape.
示例性的,在該水冷套本體的軸向方向上,該調節套筒6包括靠近該水冷套本體的第一部分和與該第一部分相鄰的第二部分,該第二部分的外表面內凹形成凹部61。For example, in the axial direction of the water-cooling jacket body, the adjustment sleeve 6 includes a first part close to the water-cooling jacket body and a second part adjacent to the first part, and the outer surface of the second part is concave. The recess 61 is formed.
水冷套位於坩堝的上方,該凹部61的設置可將下方的熱量定向反射至水冷套下方石墨部件或矽熔液液面,維持下方溫度場的穩定。The water-cooling jacket is located above the crucible, and the concave portion 61 is provided to directionally reflect the heat below to the graphite component or the silicon melt liquid surface below the water-cooling jacket, thereby maintaining the stability of the temperature field below.
示例性的,該調節套筒6的內表面設置有吸熱層。For example, the inner surface of the adjustment sleeve 6 is provided with a heat absorption layer.
該吸熱層具有吸熱作用,該吸熱層與該調節套筒6的結合強度高,可有效緩解吸熱層介面(該吸熱層與該調節套筒6的連接面)的熱應力,熱力學性能穩定,該調節套筒6可以很好地即時帶走晶棒傳輸的熱量,大大提高晶棒的冷卻速率,提高拉速,增加拉晶效率。The heat-absorbing layer has a heat-absorbing effect. The bonding strength between the heat-absorbing layer and the adjusting sleeve 6 is high, which can effectively alleviate the thermal stress at the interface of the heat-absorbing layer (the connection surface between the heat-absorbing layer and the adjusting sleeve 6). The thermodynamic properties are stable. The adjusting sleeve 6 can effectively and immediately take away the heat transmitted by the crystal rod, greatly improve the cooling rate of the crystal rod, increase the pulling speed, and increase the crystal pulling efficiency.
示例性的,該吸熱層包括靠近該調節套筒6的第一層和遠離該調節套筒的第二層,該第一層為石墨材質與該調節套筒6的內壁發生化學反應形成的過渡層。For example, the heat-absorbing layer includes a first layer close to the adjustment sleeve 6 and a second layer far away from the adjustment sleeve. The first layer is formed by a chemical reaction between graphite material and the inner wall of the adjustment sleeve 6 . Transition layer.
該調節套筒的材質為碳纖維複合材料,該第一層為_C+SiC複合過渡塗層(厚度為80±10微米),該第二層為_SiC塗層(厚度為50±5微米)。這樣的塗層結構(上述該吸熱層與該調節套筒的結合方式)具有高結合強度、高緻密度等特點。可以很好的保護基體,延長其使用壽命。The adjusting sleeve is made of carbon fiber composite material, the first layer is _C+SiC composite transition coating (thickness is 80±10 microns), and the second layer is _SiC coating (thickness is 50±5 microns) . Such a coating structure (the above-mentioned combination of the heat-absorbing layer and the adjusting sleeve) has the characteristics of high bonding strength and high density. It can protect the substrate very well and extend its service life.
示例性的,該吸熱層的厚度為130±15微米。For example, the thickness of the heat absorption layer is 130±15 microns.
示例性的,該調節套筒6的外表面設置有隔熱層。For example, the outer surface of the adjustment sleeve 6 is provided with a heat insulation layer.
該隔熱層具有反射及遮罩熱的作用,防止外面的熱量從該調節套筒6向水冷套內部傳輸,維持水冷套內部的溫度恆定。The heat insulation layer has the function of reflecting and shielding heat, preventing external heat from being transmitted from the adjusting sleeve 6 to the inside of the water-cooling jacket, and maintaining a constant temperature inside the water-cooling jacket.
示例性的,該隔熱層包括靠近該調節套筒6的第三層和遠離該調節套筒的第四層,該第三層為石墨材質與該調節套筒的外壁發生化學反應形成的過渡層。For example, the heat insulation layer includes a third layer close to the adjustment sleeve 6 and a fourth layer far away from the adjustment sleeve. The third layer is a transition formed by a chemical reaction between the graphite material and the outer wall of the adjustment sleeve. layer.
該調節套筒的材質為碳纖維複合材料,該第三層為_C+SiC複合過渡塗層(厚度為80±10微米),該第四層為_SiC塗層(厚度為50±5微米)。這樣的塗層結構(上述該隔熱層與該調節套筒的結合方式)具有高結合強度、高緻密度等特點。可以很好的保護基體,延長其使用壽命。The adjustment sleeve is made of carbon fiber composite material, the third layer is _C+SiC composite transition coating (thickness is 80±10 microns), and the fourth layer is _SiC coating (thickness is 50±5 microns) . Such a coating structure (the above-mentioned combination of the heat insulation layer and the adjustment sleeve) has the characteristics of high bonding strength and high density. It can protect the substrate very well and extend its service life.
示例性的,該隔熱層的厚度為160±15微米。For example, the thickness of the thermal insulation layer is 160±15 microns.
示例性的,該水冷套本體包括內筒2和位於該內筒2的外部的外筒1,該外筒1的底部包括用於承載該內筒的第一區和與該第一區相鄰的第二區,該第一區靠近該外筒1的側壁設置,該調節套筒6的頂部設置有凸緣(第三凸緣62),該凸緣與該第二區連接。Exemplarily, the water-cooling jacket body includes an inner cylinder 2 and an outer cylinder 1 located outside the inner cylinder 2. The bottom of the outer cylinder 1 includes a first area for carrying the inner cylinder and is adjacent to the first area. The second area is located close to the side wall of the outer cylinder 1. A flange (third flange 62) is provided on the top of the adjusting sleeve 6, and the flange is connected to the second area.
本發明實施例還提供一種單晶爐,包括爐體,位於該爐體內的坩堝,在該升降結構的升降作用的,將該水冷套本體固定於該坩堝上方。An embodiment of the present invention also provides a single crystal furnace, which includes a furnace body, a crucible located in the furnace body, and the water-cooling jacket body is fixed above the crucible due to the lifting function of the lifting structure.
以上僅為本發明之較佳實施例,並非用來限定本發明之實施範圍,如果不脫離本發明之精神和範圍,對本發明進行修改或者等同替換,均應涵蓋在本發明申請專利範圍的保護範圍當中。The above are only preferred embodiments of the present invention and are not intended to limit the implementation scope of the present invention. If the present invention is modified or equivalently substituted without departing from the spirit and scope of the present invention, the protection shall be covered by the patent scope of the present invention. within the range.
1:外筒 2:內筒 3:水冷管道 4:升降部 5:連接部 6:調節套筒 11:第一凸緣 12:第二通孔 13:臺階形凹槽 14:環形凸起 21:齒狀波紋結構 22:第二凸緣 41:升降桿 42:傳動齒輪 43:限位台 44:連接環 411:齒條 51:卡環 52:凸起 521:通孔 61:凹部 62:第三凸緣 1:Outer barrel 2: Inner cylinder 3:Water cooling pipe 4:Lifting part 5:Connection part 6:Adjustment sleeve 11:First flange 12:Second through hole 13: Step-shaped groove 14: Annular bulge 21:Toothed corrugated structure 22:Second flange 41:Lifting rod 42:Transmission gear 43:Limiting table 44:Connecting ring 411:Rack 51: snap ring 52:bulge 521:Through hole 61: concave part 62:Third flange
圖1表示本發明實施例中水冷套裝置結構示意圖; 圖2表示本發明實施例中升降桿的結構示意圖一; 圖3表示本發明實施例中升降桿的結構示意圖二; 圖4表示本發明實施例中的連接部的結構示意圖; 圖5表示本發明實施例中的內筒的結構示意圖; 圖6表示本發明實施例中的外筒的結構示意圖; 圖7表示本發明實施例中的調節套筒的結構示意圖。 Figure 1 shows a schematic structural diagram of the water cooling jacket device in the embodiment of the present invention; Figure 2 shows a schematic structural diagram of the lifting rod in the embodiment of the present invention; Figure 3 shows the second structural schematic diagram of the lifting rod in the embodiment of the present invention; Figure 4 shows a schematic structural diagram of the connection part in the embodiment of the present invention; Figure 5 shows a schematic structural diagram of the inner cylinder in an embodiment of the present invention; Figure 6 shows a schematic structural diagram of the outer cylinder in the embodiment of the present invention; Figure 7 shows a schematic structural diagram of the adjusting sleeve in the embodiment of the present invention.
1:外筒 1:Outer barrel
2:內筒 2: Inner cylinder
3:水冷管道 3:Water cooling pipe
4:升降部 4:Lifting part
5:連接部 5:Connection part
6:調節套筒 6:Adjustment sleeve
11:第一凸緣 11:First flange
22:第二凸緣 22:Second flange
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CN114790575A (en) * | 2022-05-18 | 2022-07-26 | 西安奕斯伟材料科技有限公司 | Water cooling jacket and single crystal furnace |
CN114892268A (en) * | 2022-05-18 | 2022-08-12 | 西安奕斯伟材料科技有限公司 | Water-cooling jacket device and single crystal furnace |
CN117026364A (en) * | 2023-06-01 | 2023-11-10 | 清电光伏科技有限公司 | Crystal bar production method and device, auxiliary furnace chamber, electronic equipment and storage medium |
CN117646273B (en) * | 2024-01-29 | 2024-04-02 | 中国科学院沈阳科学仪器股份有限公司 | Integrated water cooling jacket applied to ultra-high vacuum environment |
CN118621423A (en) * | 2024-08-08 | 2024-09-10 | 浙江晶阳机电股份有限公司 | Cooling device for cooling crystal bars of multiple crystal growth furnaces |
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