WO2022233533A1 - Maintien de la structure capillaire par rapport aux influences de l'environnement à l'aide d'un phénol et d'une alpha-hydroxycétone - Google Patents

Maintien de la structure capillaire par rapport aux influences de l'environnement à l'aide d'un phénol et d'une alpha-hydroxycétone Download PDF

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Publication number
WO2022233533A1
WO2022233533A1 PCT/EP2022/059379 EP2022059379W WO2022233533A1 WO 2022233533 A1 WO2022233533 A1 WO 2022233533A1 EP 2022059379 W EP2022059379 W EP 2022059379W WO 2022233533 A1 WO2022233533 A1 WO 2022233533A1
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WO
WIPO (PCT)
Prior art keywords
weight
cosmetic agent
cosmetic
alpha
surfactant
Prior art date
Application number
PCT/EP2022/059379
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German (de)
English (en)
Inventor
Katharina Madita BODE
Volker Scheunemann
Camille Grosjacques
Original Assignee
Henkel Ag & Co. Kgaa
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Henkel Ag & Co. Kgaa filed Critical Henkel Ag & Co. Kgaa
Publication of WO2022233533A1 publication Critical patent/WO2022233533A1/fr

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Classifications

    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34—Alcohols
    • A61K8/347—Phenols
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/35—Ketones, e.g. benzophenone
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00—Preparations for care of the hair
    • A61Q5/002—Preparations for repairing the hair, e.g. hair cure
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00—Preparations for care of the hair
    • A61Q5/02—Preparations for cleaning the hair
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00—Preparations for care of the hair
    • A61Q5/12—Preparations containing hair conditioners

Definitions

  • the invention relates to cosmetic agents, in particular shampoos and conditioners, with a combination of active ingredients for gentle and effective cleaning or care of the hair.
  • the structure of human hair is influenced by external and internal factors.
  • External factors include, in particular, the use of care products, especially the frequency and intensity of hair washing, chemical and environmental influences (tinting, coloring, hair bleaching, permanent or temporary hair shaping, chlorinated water in swimming pools, various types of environmental toxins, etc.), mechanical influences (strong drafts e.g. by shaping the hair) and thermal influences (hot blow-drying, permanent waves or the influence of ultraviolet light e.g. by exposure to the sun).
  • the internal factors include a balanced diet rich in vitamins, drinking enough fluids or taking medication if necessary.
  • the hair is usually treated with special active substances, for example antioxidants.
  • active substances for example antioxidants.
  • the treatment improves the combability, hold and fullness of the hair and reduces damage, the rate of split ends and brittleness.
  • Multifunctional cosmetic products containing care products are known in the prior art. These multifunctional cosmetic products include, in particular, the so-called "2 in 1" shampoos, which not only clean the hair, but also condition it. Such products are highly valued by consumers because their product performance means that they have at least one process step, for example conditioning with a classic hair conditioner, are superfluous. These cosmetic products are often provided primarily as cleaning agents, but they also have a care effect and reduce structural damage.
  • the object on which the invention is based is to provide a cosmetic agent which prevents or reduces a damaging effect on keratinic fibers. Furthermore, the object on which the invention is based is to provide a cosmetic agent which has a repairing effect on keratinic fibers.
  • a first subject matter of the invention is therefore a cosmetic agent for the treatment of a keratinic material, in particular for the treatment of human hair, comprising 0.001 to 20% by weight of an alpha-hydroxyketone, based on the total weight of the cosmetic agent, and 0.001 to 10% by weight of hydroxytyrosol, based on the total weight of the cosmetic agent, the pH of the cosmetic agent being between pH 1 and pH 7.
  • the combination of an alpha-hydroxyketone and hydroxytyrosol protects the hair from damage and has a repairing effect.
  • the combination of the antioxidant and the alpha-hydroxyketone protects against structural damage caused by chemical treatment and environmental stress such as UV light exposure.
  • a synergistic repair effect is achieved.
  • With the alpha-hydroxyketone in combination with the antioxidant it is possible to strengthen the hair structure. There is an assumption, without being able to commit to a mechanism of action, that the effect is achieved because the alpha-hydroxyketone supports the reduction in keratin loss. A loss of keratin leads to a reduced strength of the hair fibers.
  • a synergistic effect is achieved in which the hair is protected from damage and even a restoration (repair effect) can be observed.
  • keratinic material should be understood to mean, in particular, human hair.
  • an alpha-hydroxy ketone is a ketone that has a hydroxy group in the alpha position to the ketone.
  • the cosmetic agent contains an alpha-hydroxyketone which is from 5 to 12, more preferably 6 to 10, even more preferably ? has up to 9 carbon atoms.
  • the alpha-hydroxyketone is 1-hydroxyoctan-2-one.
  • Hydroxytyrosol is a phenolic acid also known as 2-(3,4-dihydroxyphenyl)ethanol.
  • the cosmetic agent comprises the alpha-hydroxyketone in an amount of 0.01 to 10% by weight, more preferably 0.05 to 5% by weight.
  • Amounts and weights in the present application always relate to the total weight of the cosmetic agent, unless stated otherwise.
  • the cosmetic agent comprises 0.01 to 8% by weight, more preferably 0.02 to 7% by weight, even more preferably 0.04 to 6% by weight, of hydroxytyrosol.
  • the preferably used amounts of alpha-hydroxyketone and hydroxytyrosol can be combined.
  • the pH value of the cosmetic product supports the beneficial effects of the active ingredient combination of alpha-hydroxyketone and hydroxytyrosol.
  • the pH is from pH 2 to less than pH 7, preferably pH 3 to pH 6.
  • the preferred embodiments accordingly include cosmetic agents that are acidified.
  • the proportion by weight of alpha-hydroxyketone in the cosmetic agent is preferably greater than the proportion by weight of hydroxytyrosol.
  • the ratio of alpha-hydroxyketone to hydroxytyrosol is between 500:1 and 1:1, more preferably between 100:1 and 5:4, even more preferably between 10:1 and 2:1.
  • the care effect can be supported by the use of cationic surfactants or cationic polymers.
  • the cosmetic agent comprises a cationic surfactant.
  • the cationic surfactant is selected from the group consisting of one
  • Alkylammonium salt of the formula RiFkRsF N X- where one or two of Ri, R2, R3, and R4 is a branched or unbranched C4 to C26, preferably a branched or unbranched C5 to C20, more preferably a branched or unbranched C14 to cis-alkyl group and the rest of R 1 , R 2 , R 3 , and R 4 are hydrogen, methyl or ethyl, and X - is a cosmetically acceptable anion, preferably chloride, bromide or methosulfate, with preference being given to the alkylammonium salt of the formula RiF ⁇ RsF N X- is selected from the group consisting of cetrimonium chloride and behentrimonium chloride;
  • Alkylenamidopropyltrimonium salt more preferably undecylenamidopropyltrimonium methosulfate;
  • Quaternium-87 and mixtures thereof wherein the cationic surfactant is contained in the cosmetic in an amount of 0 to 10% by weight, preferably 0.01 to 8% by weight, more preferably 0.2 to 5% by weight, based on the total weight of the cosmetic is.
  • the cationic surfactant is an alkylammonium salt of the formula RIR2R3R4N + X _
  • Ri , R2, R3, and R4 represent a branched or unbranched C4 to C26, preferably a branched or unbranched Cs to C20, more preferably represents a branched or unbranched C14 to C18 alkyl group, the others from R1, R2, R3 and R4 representing hydrogen, methyl or ethyl, and X represents a cosmetically acceptable anion.
  • the cosmetically acceptable anion is preferably chloride, bromide or methosulfate.
  • the alkyl ammonium salt of the formula RIR 2 R 3 R 4 N + X _ is selected from the group consisting of cetrimonium chloride and behentrimonium chloride.
  • the cationic surfactant is an alkylamidoamine.
  • the alkylamidoamine can exist in aqueous solution as a quaternized salt.
  • Alkylamidoamines are usually prepared by amidating natural or synthetic Cs-C24 fatty acids and fatty acid cuts with di-(Ci-C3)alkylaminoamines.
  • particularly suitable compounds from this class of substances are, for example, the compounds known under the INCI names stearamidopropyl dimethylamine, behenamidopropyl dimethylamine or brassicamidopropyl dimethylamine.
  • an alkylamidopropyltrimonium salt is used as a quaternized alkylamidoamine.
  • Another preferred cationic surfactant is the alkylenamidopropyltrimonium salt, especially undecylenamidopropyltrimonium methosulfate.
  • cationic surfactants the imidazolium compounds known under the INCI names Quaternium-27, Quaternium-83, Quaternium-87 and Quaternium-91. Quaternium-87 is very particularly preferred among these.
  • cationic surfactants can also be used in the cosmetic agents.
  • the cationic surfactant is present in the cosmetic in amounts of 0 to 10% by weight, preferably 0.01 to 8% by weight, more preferably 0.2 to 5% by weight, based on the total weight of the cosmetic .
  • the cosmetic agent contains a cationic polymer, which is preferably selected from the group consisting of
  • a cationic cellulose polymer preferably polyquaternium-10 and/or polyquaternium-24 and/or polyquaternium-67 and/or polyquaternium-72;
  • the cosmetic agent comprises a further cosmetic active ingredient for care.
  • the cosmetic agent contains one or more cosmetic active ingredients selected from the group consisting of a linear or branched fatty alcohol, preferably a C10 to C24 fatty alcohol, more preferably a C12 to C20 fatty alcohol, most preferably a C1 to C18 fatty alcohol - fatty alcohol; a fatty acid ester, preferably one of a linear or branched C10 to C22, more preferably C12 to Cis fatty acid and a Cs to Cis, preferably C10 to Ci6 monoalcohol; an organic carbonate, preferably one comprising identical or different, branched or linear Cs to C14, more preferably Cs to Ci2, alkyl groups; an alkylenyl diester, preferably one consisting of identical or dissimilar fatty acid residues comprising 6 to 18, more preferably e to 14, most preferably 9 to 12 carbon atoms and a branched or linear alkyleny
  • the fatty alcohol is preferably a C10 to C24 fatty alcohol, more preferably a C12 to C20 fatty alcohol, most preferably a cis to cis fatty alcohol.
  • the fatty alcohols are particularly preferably linear fatty alcohols.
  • fatty acid esters are selected from those made from a linear or branched C10 to C22, more preferably C12 to Cis fatty acid and a Cs to Cis, more preferably C10 to Ci6 monoalcohol.
  • An organic carbonate is preferably used as a further cosmetic active ingredient.
  • the organic carbonate preferably comprises an identical or different, branched or linear C6 to Cu, more preferably Cs to Ci2, alkyl group.
  • alkylenyl diester is preferably made from identical or dissimilar fatty acid residues comprising 6 to 18, more preferably 8 to 14, most preferably 9 to 12 carbon atoms and a branched or linear alkylenyl residue comprising 2 to 10, more preferably 4 to 8, most preferably 5 to 6 carbon atoms.
  • the cosmetic agent preferably comprises a mineral oil or a vegetable oil.
  • the mineral oil can be selected from alkanes, in particular from an alkane mixture that has two or more alkanes that differ from one another in the number of carbon atoms.
  • the preferred vegetable oil used is either modified or unmodified.
  • Preferred vegetable oils are apricot kernel oil, argan oil, jojoba oil, marula oil, almond oil, olive oil, coconut oil and/or sunflower oil.
  • the cosmetic agent contains shea butter (INCI name Butyrospermaum Parkii (Shea) Butter) or argan oil as very particularly preferred cosmetic active ingredients.
  • the cosmetic agent contains shea butter (INCI name Butyrospermaum Parkii (Shea) butter) and argan oil as very particularly preferred cosmetic active ingredients.
  • the cosmetic active ingredients mentioned above are present in the cosmetic agent in amounts of 0.1 to 25% by weight, preferably 0.5 to 15% by weight, more preferably 1 to 9% by weight.
  • the fatty alcohol in particular is present in amounts of from 0.1 to 25% by weight, more preferably from 0.5 to 15% by weight, even more preferably from 1 to 9% by weight, most preferably in amounts of 2 to 5 wt .-% contained in the cosmetic agent.
  • the cleaning compositions or the care compositions contain surfactant.
  • the cosmetic agent comprises a nonionic surfactant, an amphoteric surfactant and/or an anionic surfactant, preferably a cationic surfactant together with a further surfactant selected from the group consisting of a nonionic surfactant and an amphoteric surfactant.
  • the cosmetic agent comprises a nonionic surfactant and an amphoteric surfactant, or a nonionic surfactant and an anionic surfactant, or an amphoteric surfactant and an anionic surfactant.
  • the cosmetic agent contains cationic surfactant with another surfactant. It is thus preferred if the cosmetic agent contains a cationic surfactant and a nonionic surfactant, or a cationic surfactant and an amphoteric surfactant.
  • the cosmetic agent comprises the nonionic surfactant selected from the group consisting of C6 to Cie, preferably Cs to Cie, more preferably C10 to Ci 4 -alkylpolyglucosides, preferably cocoglucoside or decylglucoside; polyglyceryl alkylates, preferably PEG 7 glyceryl cocoate; cocamide MEA; and alkyl glycol ethers composed of Cs to C24, preferably C12 to C18, alkyl groups and 1 to 8, preferably 2 to 5, ethylene oxide units.
  • the nonionic surfactant selected from the group consisting of C6 to Cie, preferably Cs to Cie, more preferably C10 to Ci 4 -alkylpolyglucosides, preferably cocoglucoside or decylglucoside; polyglyceryl alkylates, preferably PEG 7 glyceryl cocoate; cocamide MEA; and alkyl glycol ethers composed of Cs to C24, preferably C12
  • the nonionic surfactant is an alkyl polyglucoside
  • this is preferably selected from C6 to C18, more preferably Cs to Cie, most preferably C10 to Ci4 alkyl polyglucosides. It is particularly preferred when the alkyl polyglucoside is coco glucoside or decyl glucoside.
  • polyglyceryl alkylates are polyglycerol adducts with fatty acid esters, fatty acid alkanolamides or fatty acid glucamides, or ethylene oxide and polyglycerol adducts with fatty acid esters, fatty acid alkanolamides or fatty acid glucamides.
  • Particularly preferred is the PEG 7 glyceryl cocoate.
  • the nonionic surfactants are alkyl glycol ethers consisting of a Cs to C24, preferably C12 to Cis, alkyl group and 1 to 8, preferably 2 to 5, ethylene oxide units.
  • the cosmetic agents contain 0.3 to 10% by weight, more preferably 0.5 to 8% by weight, even more preferably 0.75 to 6% by weight and in particular 1 to 5% by weight of nonionic surfactant .
  • the cosmetic agents can contain an amphoteric surfactant.
  • Amphoteric surfactants or zwitterionic surfactants are surfactants that have both a negatively and a positively charged functional group.
  • the cosmetic composition contains an amphoteric surfactant, which is preferably a Cs-is-, preferably Cio-i6-alkylamido-(Ci-4-alkyl) betaine, a Cs-is-, preferably C10-16-alkylamido-(Ci - 4 -alkyl)sultaine, a Cio-is-alkylamphoacetate or a Cio-is-alkylamphodiacetate.
  • the amphoteric surfactant is selected from the group consisting of cocamidopropylbetaine, amophoacetate, preferably disodium amphodiacetate, cocobetaine and mixtures thereof.
  • cocamidopropyl betaine is a particularly preferred fatty acid amide derivative, which is particularly suitable as an amphoteric surfactant.
  • Suitable zwitterionic surfactants are also the so-called betaines, such as the N-alkyl-N,N-dimethylammonium glycinates, for example coconut alkyldimethylammonium glycinate, N-acylaminopropyl-N,N-dimethylammonium glycinates, for example cocoacylaminopropyldimethylammonium glycinate, and 2-alkyl-3-carboxymethyl -S-hydroxyethylimidazolines each having 8 to 18 carbon atoms in the alkyl or acyl group, and cocoacylaminoethyl-hydroxyethylcarboxymethylglycinate.
  • betaines such as the N-alkyl-N,N-dimethylammonium glycinates, for example coconut alkyldimethylammonium glycinate, N-acylaminopropyl-N,N-dimethylammonium glycinates,
  • ampholytic surfactants are N-alkylglycines, N-alkylaminopropionic acids, N-alkylaminobutyric acids, N-alkyliminodipropionic acids, N-hydroxyethyl-N-alkylamidopropylglycines, N-alkyltaurines, N-alkylsarcosines, 2-alkylaminopropionic acids and alkylaminoacetic acids, each with about 8 to 24 C atoms in the alkyl group.
  • Particularly preferred amphoteric surfactants are N-cocoalkylaminopropionate, cocoacylaminoethylaminopropionate and Ci2-Ci8-acylsarcosine.
  • the cosmetic agents contain 0.3 to 20% by weight, preferably 0.5 to 8% by weight, more preferably 0.75 to 6% by weight and in particular 1 to 5% by weight amphoteric surfactant .
  • surfactants i.e. also several cationic or several nonionic or several amphoteric or several nonionic and amphoteric surfactants or several cationic and nonionic surfactants or several cationic and amphoteric surfactants are contained in the cosmetic agent, the amounts in % by weight always relate to the sum the surfactants.
  • Anionic surfactants are preferably included in cleaning compositions.
  • the cosmetic is a cleansing composition
  • anionic surfactants and no cationic surfactants are contained in the cosmetic.
  • Preferred anionic surfactants are acyl glutamates, acyl isethionates, acyl sarcosinates and acyl taurates, each with a linear or branched acyl radical having 6 to 22 carbon atoms and 0, 1, 2 or 3 double bonds, which in particularly preferred embodiments consists of an octanoyl, decanoyl, lauroy
  • More preferred anionic surfactants are alkyl sulfates, alkyl polyglycol ether sulfates and ether carboxylic acid salts with 10 to 18 carbon atoms in the alkyl group and up to 12 glycol ether groups in the molecule and sulfosuccinic acid mono- and dialkyl esters with 8 to 18 carbon atoms in the alkyl group and sulfosuccinic acid mono-alkylpolyoxyethyl ester 8 to 18 carbon atoms in the alkyl group and 1 to 6 oxyethyl groups.
  • Particularly preferred anionic surfactants are the alkali metal or ammonium salts of lauryl ether sulfate with a degree of ethoxylation of 2 to 4 EO.
  • a second subject matter of the present invention is therefore a method for treating a keratinic material, in particular for treating human hair, in which a cosmetic agent according to the invention is applied to the keratinic material , in particular on human hair, is applied, preferably immediately after cleaning the keratinic material, in particular after cleaning human hair, and is left to act there for a period of 2 minutes or more until the next cleaning or less, preferably from 5 Minutes or more up to 12 hours or less.
  • the cosmetic agent according to the invention is used as a leave-on composition.
  • the cosmetic agent is left in the hair.
  • the human hair is preferably treated with the cosmetic agent after cleaning.
  • the cosmetic agent is applied and left to act there.
  • the exposure time may vary.
  • the cosmetic agent is preferably left in the hair until the next cleansing, particularly preferably left there for up to 12 hours.
  • the cosmetic agent is preferably rinsed out with water.
  • a third subject matter of the present invention is therefore a method for treating a keratinic material, in particular for treating human hair, in which the cosmetic agent according to the invention is applied to the keratinic material, in particular applied to human hair and then rinsed out with water.
  • the cosmetic product in this case is a cleaning product or a "2 in 1" cosmetic product.
  • the exposure time ie the time between application and rinsing, is significantly shorter than in the method in which the cosmetic agent is a leave-on cosmetic agent.
  • the exposure time is therefore preferably less than 5 minutes.
  • a fourth subject matter of the present invention is therefore the use of the cosmetic agent according to the invention to reduce or prevent harmful effects from chemical treatments of the keratin material, from air and water pollution free radicals or by UV radiation; or as a means of exerting a repair effect.
  • the cosmetic agent according to the invention is preferably used as a conditioner, hair treatment, shampoo, as a “2 in 1” cosmetic agent or in the form of a spray.

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Dermatology (AREA)
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Abstract

L'invention concerne des agents cosmétiques pour le traitement d'une matière kératinique, comprenant a) 0,001 à 20 % en poids d'une alpha-hydroxycétone et b) 0,001 à 10 %. d'hydroxytyrosol, le pH de l'agent cosmétique étant compris entre 1 et 7. L'invention concerne en outre un procédé selon lequel l'agent cosmétique selon l'invention est utilisé, ainsi que l'utilisation de l'agent cosmétique selon l'invention.
PCT/EP2022/059379 2021-05-05 2022-04-08 Maintien de la structure capillaire par rapport aux influences de l'environnement à l'aide d'un phénol et d'une alpha-hydroxycétone WO2022233533A1 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102021111722.4 2021-05-05
DE102021111722.4A DE102021111722A1 (de) 2021-05-05 2021-05-05 Erhalt der Haarstruktur gegenüber Umwelteinflüssen umfassend ein Phenol und ein alpha-Hydroxyketon

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WO2022233533A1 true WO2022233533A1 (fr) 2022-11-10

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PCT/EP2022/059379 WO2022233533A1 (fr) 2021-05-05 2022-04-08 Maintien de la structure capillaire par rapport aux influences de l'environnement à l'aide d'un phénol et d'une alpha-hydroxycétone

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DE (1) DE102021111722A1 (fr)
WO (1) WO2022233533A1 (fr)

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2006134160A2 (fr) * 2005-06-17 2006-12-21 Symrise Gmbh & Co. Kg Melanges synergiques d'alcools aromatiques et de derives de ces derniers et de tropolone (derives)
CN112641693A (zh) * 2020-12-31 2021-04-13 广州植境生物科技有限公司 一种护发组合物、制备方法及其应用

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2006134160A2 (fr) * 2005-06-17 2006-12-21 Symrise Gmbh & Co. Kg Melanges synergiques d'alcools aromatiques et de derives de ces derniers et de tropolone (derives)
CN112641693A (zh) * 2020-12-31 2021-04-13 广州植境生物科技有限公司 一种护发组合物、制备方法及其应用

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
DATABASE GNPD [online] MINTEL; 16 June 2016 (2016-06-16), ANONYMOUS: "Gentle Shampoo", XP055951198, retrieved from https://www.gnpd.com/sinatra/recordpage/4077025/ Database accession no. 4077025 *
DATABASE GNPD [online] MINTEL; 24 June 2020 (2020-06-24), ANONYMOUS: "Shampoo", XP055951137, retrieved from https://www.gnpd.com/sinatra/recordpage/7895625/ Database accession no. 7895625 *

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