WO2021152334A1 - Aerosol-generating material - Google Patents

Aerosol-generating material Download PDF

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Publication number
WO2021152334A1
WO2021152334A1 PCT/GB2021/050222 GB2021050222W WO2021152334A1 WO 2021152334 A1 WO2021152334 A1 WO 2021152334A1 GB 2021050222 W GB2021050222 W GB 2021050222W WO 2021152334 A1 WO2021152334 A1 WO 2021152334A1
Authority
WO
WIPO (PCT)
Prior art keywords
aerosol
amorphous solid
strips
tobacco
generating material
Prior art date
Application number
PCT/GB2021/050222
Other languages
English (en)
French (fr)
Inventor
Richard Hepworth
Walid Abi Aoun
Benjamin Jenkins
Original Assignee
Nicoventures Trading Limited
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to AU2021213960A priority Critical patent/AU2021213960B2/en
Priority to JP2022544808A priority patent/JP2023511955A/ja
Priority to IL294813A priority patent/IL294813A/en
Priority to BR112022015248A priority patent/BR112022015248A2/pt
Priority to KR1020227029503A priority patent/KR20220130785A/ko
Priority to EP21703544.3A priority patent/EP4096443A1/en
Application filed by Nicoventures Trading Limited filed Critical Nicoventures Trading Limited
Priority to US17/759,847 priority patent/US20230143930A1/en
Priority to CA3164907A priority patent/CA3164907A1/en
Priority to CN202180024436.2A priority patent/CN115666277A/zh
Priority to MX2022009211A priority patent/MX2022009211A/es
Publication of WO2021152334A1 publication Critical patent/WO2021152334A1/en
Priority to JP2024079917A priority patent/JP2024105585A/ja

Links

Classifications

    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00—Preparing tobacco in the factory
    • A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10—Chemical features of tobacco products or tobacco substitutes
    • A24B15/12—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10—Chemical features of tobacco products or tobacco substitutes
    • A24B15/12—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
    • A24B15/14—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco made of tobacco and a binding agent not derived from tobacco
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10—Chemical features of tobacco products or tobacco substitutes
    • A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A24B15/32—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by acyclic compounds
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A24B15/34—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances containing a carbocyclic ring other than a six-membered aromatic ring
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B5/00—Stripping tobacco; Treatment of stems or ribs
    • A24B5/10—Stripping tobacco; Treatment of stems or ribs by crushing the leaves with subsequent separating
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B7/00—Cutting tobacco
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24C—MACHINES FOR MAKING CIGARS OR CIGARETTES
    • A24C5/00—Making cigarettes; Making tipping materials for, or attaching filters or mouthpieces to, cigars or cigarettes
    • A24C5/01—Making cigarettes for simulated smoking devices
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D1/00—Cigars; Cigarettes
    • A24D1/20—Cigarettes specially adapted for simulated smoking devices
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00—Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/20—Devices using solid inhalable precursors

Definitions

  • the present invention relates to an aerosol-generating material, an article comprising an aerosol generating material, a pack of articles, a consumable for use in an aerosol provision system, a non-combustible aerosol provision system, and a method for producing an aerosol-generating material.
  • tobacco industry products produce an aerosol during use, which is inhaled by a user.
  • tobacco heating devices heat an aerosol generating substrate such as tobacco to form an aerosol by heating, but not burning, the substrate.
  • tobacco industry products can include mouthpieces through which the aerosol passes to reach the user’s mouth.
  • an aerosol-generating material comprising a plurality of strands and/or strips of a tobacco material and a plurality of strips of amorphous solid material, wherein the plurality of strands and/ or strips of tobacco material and the plurality of strips of amorphous solid material each have a length of at least about 5 mm.
  • an article comprising an aerosol-generating material according to the first aspect.
  • a pack comprising a plurality of articles, each article according to the second aspect above, wherein the number of the plurality of strips of amorphous solid material varies by less than 40% between the articles in the pack, or less than 30% between the articles in the pack, or less than 20% between the articles in the pack.
  • a pack comprising a plurality of articles, each article according to the second aspect above, wherein the plurality of strips of amorphous solid material comprise a flavourant, optionally menthol, and wherein the delivery of the flavourant from each of the plurality of articles, in use, varies by less than 50% between the articles in the pack, or varies by less than 20% between the articles in the pack.
  • pack comprising a plurality of articles, each article according to the second aspect above, wherein the plurality of strips of amorphous solid material comprise a flavourant, optionally menthol, and wherein the total content of said flavourant in each of the plurality of articles, in use, has a standard deviation of less than 30% of the mean content of said flavourant in said articles, or has a standard deviation of less than 20% of the mean content of said flavourant in said articles, and wherein at least 20% of the mean flavourant is provided in said strips of amorphous solid material.
  • pack comprising a plurality of articles, each article according to the second aspect above, wherein the plurality of strips of amorphous solid material comprise a flavourant, optionally menthol, and the total amount of flavourant is between 5 mg per article and 30 mg per article, or between 16 mg per article and 22 mg per article, or between 5 mg per article and 10 mg per article, or between 17 mg per article and 30 mg per article.
  • a seventh aspect there is provided pack comprising a plurality of articles, each article according to the second aspect above, wherein the plurality of strips of amorphous solid material comprise a flavourant, optionally menthol, and the standard deviation in the total amount of flavourant between the articles in the pack is less than 30% or 20% of the mean total amount of flavourant by wt%, and wherein the amorphous solid comprises at least 50% of the mean total amount of flavourant in each article.
  • an eighth aspect there is provided pack comprising a plurality of articles, each article according to the second aspect above, wherein the article is provided with ventilation, and wherein the standard deviation in the ventilation level between articles in the pack is less than 15%, or less than 10%, or less than 9%.
  • pack comprising a plurality of articles, each article according to the second aspect above, wherein the plurality of strips of amorphous solid material comprise an aerosol-former, optionally glycerol, and wherein the total content of said aerosol- former in each of the plurality of articles, in use, has a standard deviation of less than 30% of the mean content of said aerosol-former in said articles, or has a standard deviation of less than 25% of the mean content of said aerosol-former in said articles, and wherein at least 20% of the mean aerosol-former is provided in said strips of amorphous solid material.
  • a consumable for use in an aerosol provision system wherein the consumable comprises an article according to the second aspect.
  • a non-combustible aerosol provision system comprising a non-combustible aerosol provision device and a consumable according to the fifth aspect, wherein the device is arranged to heat the aerosol-generating material of the consumable.
  • a method for producing an aerosol-generating material according the first aspect comprising cutting a sheet of amorphous solid material to form a plurality of strips of amorphous solid material having a cut length of at least about 5 mm.
  • a method for producing an aerosol-generating material comprising feeding a single thickness sheet of an amorphous solid material to a cutting apparatus and cutting the single thickness sheet.
  • a fourteenth aspect there is provided a method for producing an aerosol-generating material, the method comprising cutting a first portion of amorphous solid material to form a first component comprising a plurality of strips of amorphous solid material having a first length and cutting a second portion of amorphous solid material to form a second component comprising a plurality of strips of amorphous solid material having a second length different to the first length.
  • a fifteenth aspect there is provided method for producing an aerosol-generating material, comprising cutting a sheet of amorphous solid material to form a plurality of strips of the amorphous solid material, and mixing the plurality of strips of amorphous solid material with a tobacco material, wherein the cutting step and the mixing step are performed within 12 hours of each other, or within 6 hours of each other, or within 2 hours of each other, or within 30 minutes of each other.
  • Figure 1 is a side-on cross sectional view of an article for use with a non-combustible aerosol provision device, the article including a mouthpiece;
  • Figure 2a is a side-on cross sectional view of a further article for use with a non- combustible aerosol provision device, in this example the article including a capsule- containing mouthpiece;
  • Figure 2b is a cross sectional view of the capsule-containing mouthpiece shown in Figure 2a;
  • Figure 3 is a perspective illustration of a non-combustible aerosol provision device for generating aerosol from the aerosol-generating material of the articles of Figures 1, 2a and 2b;
  • Figure 4 illustrates the device of Figure 3 with the outer cover removed and without an article present
  • Figure 5 is a side view of the device of Figure 3 in partial cross-section;
  • Figure 6 is an exploded view of the device of Figure 3, with the outer cover omitted;
  • Figure 7A is a cross sectional view of a portion of the device of Figure 3;
  • Figure 7B is a close-up illustration of a region of the device of Figure 7A;
  • Figure 8 is a flow diagram illustrating a first method of manufacturing an aerosol-generating material
  • Figure 9 is a flow diagram illustrating a second method of manufacturing an aerosol-generating material.
  • the term “delivery system” is intended to encompass systems that deliver at least one substance to a user, and includes: combustible aerosol provision systems, such as cigarettes, cigarillos, cigars, and tobacco for pipes or for roll-your-own or for make-your-own cigarettes (whether based on tobacco, tobacco derivatives, expanded tobacco, reconstituted tobacco, tobacco substitutes or other smokable material); non-combustible aerosol provision systems that release compounds from an aerosol-generating material without combusting the aerosol-generating material, such as electronic cigarettes, tobacco heating products, and hybrid systems to generate aerosol using a combination of aerosol-generating materials; and aerosol-free delivery systems that deliver the at least one substance to a user orally, nasally, transdermally or in another way without forming an aerosol, including but not limited to, lozenges, gums, patches, articles comprising inhalable powders, and oral products such as oral tobacco which includes snus or moist snuff, wherein the at least one substance may or may not
  • a “combustible” aerosol provision system is one where a constituent aerosol-generating material of the aerosol provision system (or component thereof) is combusted or burned during use in order to facilitate delivery of at least one substance to a user.
  • the delivery system is a combustible aerosol provision system, such as a system selected from the group consisting of a cigarette, a cigarillo and a cigar.
  • the disclosure relates to a component for use in a combustible aerosol provision system, such as a filter, a filter rod, a filter segment, a tobacco rod, a spill, an aerosol-modifying agent release component such as a capsule, a thread, or a bead, or a paper such as a plug wrap, a tipping paper or a cigarette paper.
  • a component for use in a combustible aerosol provision system such as a filter, a filter rod, a filter segment, a tobacco rod, a spill, an aerosol-modifying agent release component such as a capsule, a thread, or a bead, or a paper such as a plug wrap, a tipping paper or a cigarette paper.
  • a “non-combustible” aerosol provision system is one where a constituent aerosol-generating material of the aerosol provision system (or component thereof) is not combusted or burned in order to facilitate delivery of at least one substance to a user.
  • the delivery system is a non-combustible aerosol provision system, such as a powered non-combustible aerosol provision system.
  • the non-combustible aerosol provision system is an electronic cigarette, also known as a vaping device or electronic nicotine delivery system (END), although it is noted that the presence of nicotine in the aerosol-generating material is not a requirement.
  • END electronic nicotine delivery system
  • the non-combustible aerosol provision system is an aerosol generating material heating system, also known as a heat-not-burn system.
  • An example of such a system is a tobacco heating system.
  • the non-combustible aerosol provision system is a hybrid system to generate aerosol using a combination of aerosol-generating materials, one or a plurality of which may be heated.
  • Each of the aerosol-generating materials may be, for example, in the form of a solid, liquid or gel and may or may not contain nicotine.
  • the hybrid system comprises a liquid or gel aerosol-generating material and a solid aerosol-generating material.
  • the solid aerosol-generating material may comprise, for example, tobacco or a non-tobacco product.
  • the non-combustible aerosol provision system may comprise a non combustible aerosol provision device and a consumable for use with the non- combustible aerosol provision device.
  • the disclosure relates to consumables comprising aerosol generating material and configured to be used with non-combustible aerosol provision devices. These consumables are sometimes referred to as articles throughout the disclosure.
  • the non-combustible aerosol provision system such as a non combustible aerosol provision device thereof, may comprise a power source and a controller.
  • the power source may, for example, be an electric power source or an exothermic power source.
  • the exothermic power source comprises a carbon substrate which may be energised so as to distribute power in the form of heat to an aerosol-generating material or to a heat transfer material in proximity to the exothermic power source.
  • the non-combustible aerosol provision system may comprise an area for receiving the consumable, an aerosol generator, an aerosol generation area, a housing, a mouthpiece, a filter and/ or an aerosol-modifying agent.
  • the consumable for use with the non-combustible aerosol provision device may comprise aerosol-generating material, an aerosol-generating material storage area, an aerosol-generating material transfer component, an aerosol generator, an aerosol generation area, a housing, a wrapper, a filter, a mouthpiece, and/ or an aerosol-modifying agent.
  • the substance to be delivered may be an aerosol-generating material or a material that is not intended to be aerosolised.
  • either material may comprise one or more active constituents, one or more flavours, one or more aerosol-former materials, and/or one or more other functional materials.
  • the substance to be delivered comprises an active substance.
  • the active substance comprises nicotine.
  • the active substance comprises caffeine, melatonin or vitamin B12.
  • the active substance may comprise or be derived from one or more botanicals or constituents, derivatives or extracts thereof.
  • the term "botanical” includes any material derived from plants including, but not limited to, extracts, leaves, bark, fibres, stems, roots, seeds, flowers, fruits, pollen, husk, shells or the like.
  • the material may comprise an active compound naturally existing in a botanical, obtained synthetically. The material may be in the form of liquid, gas, solid, powder, dust, crushed particles, granules, pellets, shreds, strips, sheets, or the like.
  • Example botanicals are tobacco, eucalyptus, star anise, hemp, cocoa, cannabis, fennel, lemongrass, peppermint, spearmint, rooibos, chamomile, flax, ginger, ginkgo biloba, hazel, hibiscus, laurel, licorice (liquorice), matcha, mate, orange skin, papaya, rose, sage, tea such as green tea or black tea, thyme, clove, cinnamon, coffee, aniseed (anise), basil, bay leaves, cardamom, coriander, cumin, nutmeg, oregano, paprika, rosemary, saffron, lavender, lemon peel, mint, juniper, elderflower, vanilla, wintergreen, beefsteak plant, curcuma, turmeric, sandalwood, cilantro, bergamot, orange blossom, myrtle, cassis, valerian, pimento, mace, damien, marjoram, olive, lemon
  • the mint maybe chosen from the following mint varieties: Mentha Arventis, Mentha c.v., Mentha niliaca, Mentha piperita, Mentha piperita citrata c.v., Mentha piperita c.v, Mentha spicata crispa, Mentha cardifolia, Memtha longifolia, Mentha suaveolens variegata, Mentha pulegium, Mentha spicata c.v. and Mentha suaveolens
  • the active substance comprises or is derived from one or more botanicals or constituents, derivatives or extracts thereof and the botanical is tobacco. In some embodiments, the active substance comprises or derived from one or more botanicals or constituents, derivatives or extracts thereof and the botanical is selected from eucalyptus, star anise, cocoa and hemp.
  • the active substance comprises or derived from one or more botanicals or constituents, derivatives or extracts thereof and the botanical is selected from rooibos and fennel.
  • the substance to be delivered comprises a flavour.
  • flavour and “flavourant” refer to materials which, where local regulations permit, maybe used to create a desired taste, aroma or other somatosensorial sensation in a product for adult consumers.
  • a suitable heat effect agent may be, but is not limited to, vanillyl ethyl ether and a suitable cooling agent may be, but not limited to eucolyptol, WS-3.
  • Aerosol-generating material is a material that is capable of generating aerosol, for example when heated, irradiated or energized in any other way. Aerosol-generating material may, for example, be in the form of a solid, liquid or gel which may or may not contain an active substance and/or flavourants.
  • the aerosol generating material may comprise an “amorphous solid”, which may alternatively be referred to as a “monolithic solid” (i.e. non-fibrous).
  • the amorphous solid may be a dried gel.
  • the amorphous solid is a solid material that may retain some fluid, such as liquid, within it.
  • the amorphous solid comprises:
  • the amorphous solid comprises:
  • the amorphous solid material may be provided in sheet form.
  • the amorphous solid comprises: aerosol-former material in an amount of from about 40 to 8owt% of the amorphous solid; gelling agent and optional filler (i.e. in some examples filler is present in the amorphous solid, in other examples filler is not present in the amorphous solid), wherein the amount of gelling agent and filler taken together is from about 10 to 6owt% of the amorphous solid (i.e. the gelling agent and filler taken together account for about 10 to 6owt% of the amorphous solid); and optionally, active substance and/or flavourant in an amount of up to about 20wt% of the amorphous solid (i.e.
  • the amorphous solid comprises ⁇ 20wt% active substance).
  • the amorphous solid material can be formed from a dried gel. The inventors have found that using these component proportions means as the gel sets, flavour compounds are stabilised within the gel matrix allowing a higher flavour loading to be achieved than in non-gel compositions.
  • the flavouring e.g. menthol
  • the flavouring is stabilised at high concentrations and the products have a good shelf life.
  • the amorphous solid may comprise from about iwt%, 5wt%, iowt%, I5wt%, 20wt%, 25wt%, 30wt% or 35wt% to about 6owt%, 55wt%, 50wt%, 45wt%, 40wt% or 35wt% of a gelling agent (all calculated on a dry weight basis).
  • the amorphous solid may comprise i-6owt%, 5-6owt%, 20-6owt%, 25-55wt%, 30-50wt%, 35-45wt%, i-50wt%, 5 45wt%, io-40wt% or 20-35wt% of a gelling agent.
  • the gelling agent comprises a hydrocolloid.
  • the gelling agent comprises one or more compounds selected from the group comprising alginates, pectins, starches (and derivatives), celluloses (and derivatives), gums, silica or silicones compounds, clays, polyvinyl alcohol and combinations thereof.
  • the gelling agent comprises one or more of alginates, pectins, hydroxyethyl cellulose, hydroxypropyl cellulose, carboxymethylcellulose, pullulan, xanthan gum guar gum, carrageenan, agarose, acacia gum, fumed silica, PDMS, sodium silicate, kaolin and polyvinyl alcohol.
  • the gelling agent comprises alginate and/ or pectin, and may be combined with a setting agent (such as a calcium source) during formation of the amorphous solid.
  • the amorphous solid may comprise a calcium-crosslinked alginate and/ or a calcium- crosslinked pectin.
  • the gelling agent comprises alginate, and the alginate is present in the amorphous solid in an amount of from 5-40wt%, for example io-30wt% of the amorphous solid (calculated on a dry weight basis).
  • alginate is the only gelling agent present in the amorphous solid.
  • the gelling agent comprises alginate and at least one further gelling agent, such as pectin.
  • alginate is comprised in the gelling agent in an amount of from about 5 to 40wt% of the amorphous solid, or 15 to 40wt%. That is, the amorphous solid comprises alginate in an amount of about 5 to 40wt% by dry weight of the amorphous solid, or 15 to 40wt%. In some examples, the amorphous solid comprises alginate in an amount of from about 20 to 40wt%, or about I5wt% to 35wt% of the amorphous solid. In some examples, pectin is comprised in the gelling agent in an amount of from about 3 to I5wt% of the amorphous solid.
  • the amorphous solid comprises pectin in an amount of from about 3 to I5wt% by dry weight of the amorphous solid. In some examples, the amorphous solid comprises pectin in an amount of from about 5 to iowt% of the amorphous solid.
  • guar gum is comprised in the gelling agent in an amount of from about 3 to 40wt% of the amorphous solid. That is, the amorphous solid comprises guar gum in an amount of from about 3 to 40wt% by dry weight of the amorphous solid. In some examples, the amorphous solid comprises guar gum in an amount of from about 5 to iowt% of the amorphous solid. In some examples, the amorphous solid comprises guar gum in an amount of from about 15 to 40wt% of the amorphous solid, or from about 20 to 40wt%, or from about 15 to 35wt%. In some examples, the alginate is present in an amount of at least about 50wt% of the gelling agent.
  • the amorphous solid comprises alginate and pectin, and the ratio of the alginate to the pectin is from 1:1 to 10:1.
  • the ratio of the alginate to the pectin is typically >1:1, i.e. the alginate is present in an amount greater than the amount of pectin.
  • the ratio of alginate to pectin is from about 2:1 to 8:1, or about 3:1 to 6:1, or is approximately 4:1.
  • the amorphous solid may include gelling agent comprising carrageenan.
  • the gelling agent may comprise one or more compounds selected from cellulosic gelling agents, non-cellulosic gelling agents, guar gum, acacia gum and mixtures thereof.
  • the cellulosic gelling agent is selected from the group consisting of: hydroxymethyl cellulose, hydroxyethyl cellulose, hydroxypropyl cellulose, carboxymethylcellulose (CMC), hydroxypropyl methylcellulose (HPMC), methyl cellulose, ethyl cellulose, cellulose acetate (CA), cellulose acetate butyrate (CAB), cellulose acetate propionate (CAP) and combinations thereof.
  • the amorphous solid may comprise from about o.iwt%, o.5wt%, iwt%, 3wt%, 5wt%, 7wt% or 10% to about 8owt%, 50wt%, 45wt%, 40wt%, 35wt%, 30wt% or 25wt of an aerosol-former material (all calculated on a dry weight basis).
  • the amorphous solid may comprise about 40-8owt%, 40-75wt%, 50-70wt%, or 55-65wt aerosol-former material.
  • the aerosol-former material may act as a plasticiser.
  • the amorphous solid may comprise 0.5-40wt%, 3-35wt% or io-25wt% of an aerosol-former material.
  • the aerosol-former material comprises one or more compound selected from erythritol, propylene glycol, glycerol, triacetin, sorbitol and xylitol.
  • the aerosol-former material comprises, consists essentially of or consists of glycerol.
  • the aerosol-former comprises one or more polyhydric alcohols, such as propylene glycol, triethylene glycol, l ,3-butanediol and glycerin; esters of polyhydric alcohols, such as glycerol mono-, di- or triacetate; and/or aliphatic esters of mono-, di- or polycarboxylic acids, such as dimethyl dodecanedioate and dimethyl tetradecanedioate.
  • polyhydric alcohols such as propylene glycol, triethylene glycol, l ,3-butanediol and glycerin
  • esters of polyhydric alcohols such as glycerol mono-, di- or triacetate
  • aliphatic esters of mono-, di- or polycarboxylic acids such as dimethyl dodecanedioate and dimethyl tetradecanedioate.
  • the amorphous solid may comprise a flavour.
  • the amorphous solid may comprise up to about 8owt%, 70wt%, 6owt%, 55wt%, 50wt% or 45wt of a flavour.
  • the amorphous solid may comprise at least about o.iwt%, iwt%, iowt%, 20wt%, 30wt%, 35wt% or 40wt% of a flavour (all calculated on a dry weight basis).
  • the amorphous solid may comprise i-8owt%, io-8owt%, 20-70wt%, 30- 6owt%, 35 55wt% or 30-45wt of a flavour.
  • the flavour comprises, consists essentially of or consists of menthol.
  • the amorphous solid may additionally comprise an emulsifying agent, which emulsified molten flavour during manufacture.
  • the amorphous solid may comprise from about 5wt% to about I5wt of an emulsifying agent (calculated on a dry weight basis), suitably about iowt%.
  • the emulsifying agent may comprise acacia gum.
  • the amorphous solid may comprise 5- 6owt% (calculated on a dry weight basis) of a tobacco material and/or nicotine. In some cases, the amorphous solid may comprise from about iwt%, 5wt%, iowt%, I5wt%, 20wt% or 25wt% to about 70wt%, 6owt%, 50wt%, 45wt%, 40wt%, 35wt%, 30wt%,
  • the amorphous solid may comprise from about iwt%, 5wt%, iowt%, I5wt%, 20wt% or 25wt% to about 70wt%, 6owt%, 50wt%, 45wt%, 40wt%, 35wt%, or 30wt% (calculated on a dry weight basis) of a tobacco material.
  • the amorphous solid may comprise io-50wt%, i5-40wt% or 20-35wt% of a tobacco material.
  • the amorphous solid may comprise from about iwt%, 2wt%, 3wt% or 4wt% to about 20wt%, i8wt%, i5wt% or i2wt% (calculated on a dry weight basis) of nicotine.
  • the amorphous solid may comprise i-20wt%, 2-i8wt% or 3-i2wt% of nicotine.
  • the amorphous solid comprises an active substance such as tobacco extract.
  • the amorphous solid may comprise 5-6owt% (calculated on a dry weight basis) of tobacco extract.
  • the amorphous solid may comprise from about 5wt%, iowt%, I5wt%, 20wt% or 25wt% to about 6owt%, 50wt%, 45wt%, 40wt%, 35wt%, or 30wt% (calculated on a dry weight basis) tobacco extract.
  • the amorphous solid may comprise io-50wt%, i5-40wt% or 20-35wt% of tobacco extract.
  • the tobacco extract may contain nicotine at a concentration such that the amorphous solid comprises iwt% i.5wt%, 2wt% or 2.5wt% to about 6wt%, 5wt%, 4-5wt% or 4wt% (calculated on a dry weight basis) of nicotine. In some cases, there may be no nicotine in the amorphous solid other than that which results from the tobacco extract.
  • the amorphous solid comprises no tobacco material but does comprise nicotine.
  • the amorphous solid may comprise from about iwt%, 2wt%, 3wt% or 4wt% to about 20wt%, i8wt%, i5wt% or i2wt% (calculated on a dry weight basis) of nicotine.
  • the amorphous solid may comprise l- 20wt%, 2-i8wt% or 3-i2wt% of nicotine.
  • the total content of active substance and/ or flavour may be at least about o.iwt%, iwt%, 5wt%, iowt%, 20wt%, 25wt% or 30wt%.
  • the total content of active substance and/or flavour maybe less than about 90wt%, 8owt%, 70wt%, 6owt%, 50wt% or 40wt% (all calculated on a dry weight basis).
  • the total content of tobacco material, nicotine and flavour may be at least about o.iwt%, iwt%, 5wt%, iowt%, 20wt%, 25wt% or 30wt%.
  • the total content of active substance and/or flavour maybe less than about 90wt%, 8owt%, 70wt%, 6owt%, 50wt% or 40wt% (all calculated on a dry weight basis).
  • the amorphous solid may be made from a gel, and this gel may additionally comprise a solvent, included at o.i-50wt%.
  • a solvent included at o.i-50wt%.
  • the inventors have established that the inclusion of a solvent in which the flavour is soluble may reduce the gel stability and the flavour may crystallise out of the gel. As such, in some cases, the gel does not include a solvent in which the flavour is soluble.
  • the amorphous solid may comprise filler.
  • the amorphous solid typically comprises gelling agent and filler (if present) in an amount of from about 10 to 6owt% of the amorphous solid.
  • the amorphous solid comprises filler in an amount of from 1 to I5wt% of the amorphous solid, such as 5wt% to I5wt%, or 8 to I2wt%.
  • the amorphous solid comprises filler in an amount greater than iwt%, 5wt%, or 8wt% of the amorphous solid.
  • the amorphous solid comprises less than 6owt% of a filler, such as from iwt% to 6owt%, or 5wt% to 50wt%, or 5wt% to 30wt%, or iowt% to 20wt%. In other embodiments, the amorphous solid comprises less than 40wt% 20wt%, suitably less than iowt% or less than 5wt% of a filler. In some cases, the amorphous solid comprises less than iwt% of a filler, and in some cases, comprises no filler.
  • the filler may comprise one or more inorganic filler materials, such as calcium carbonate, perlite, vermiculite, diatomaceous earth, colloidal silica, magnesium oxide, magnesium sulphate, magnesium carbonate, and suitable inorganic sorbents, such as molecular sieves.
  • the filler may comprise one or more organic filler materials such as wood pulp, cellulose and cellulose derivatives.
  • the amorphous solid comprises no calcium carbonate such as chalk.
  • the filler is fibrous.
  • the filler may be a fibrous organic filler material such as wood pulp, hemp fibre, cellulose or cellulose derivatives.
  • fibrous filler in an amorphous solid may increase the tensile strength of the material.
  • the amorphous solid comprises one or more cannabinoid compounds selected from the group consisting of: cannabidiol (CBD), tetrahydrocannabinol (THC), tetrahydrocannabinolic acid (THCA), cannabidiolic acid (CBDA), cannabinol (CBN), cannabigerol (CBG), cannabichromene (CBC), cannabicyclol (CBL), cannabivarin (CBV), tetrahydrocannabivarin (THCV), cannabidivarin (CBDV), cannabichromevarin (CBCV), cannabigerovarin (CBGV), cannabigerol monomethyl ether (CBGM) and cannabielsoin (CBE), cannabicitran (CBT).
  • CBD cannabidiol
  • THC tetrahydrocannabinol
  • THCA tetrahydrocannabinolic acid
  • the amorphous solid may comprise one or more cannabinoid compounds selected from the group consisting of cannabidiol (CBD) and THC (tetrahydrocannabinol).
  • CBD cannabidiol
  • THC tetrahydrocannabinol
  • CBD cannabidiol
  • the amorphous solid may comprise nicotine and cannabidiol (CBD).
  • CBD cannabidiol
  • the amorphous solid may comprise nicotine, cannabidiol (CBD), and THC (tetrahydrocannabinol). In some embodiments, the amorphous solid does not comprise tobacco fibres.
  • the amorphous solid may have a tensile strength of from 150 N/m to 3000 N/m, for example 500 N/m to 1200 N/m, or from 600 N/m to 900 N/m, or from 700 N/m to 900 N/m, or around 800 N/m or greater. In some examples, the amorphous solid may have a tensile strength of greater than 500 N/m, greater than 1000 N/m or greater than 1500 N/m. Such tensile strengths may be particularly suitable for embodiments wherein the amorphous solid material is included in an aerosol-generating article as a rolled sheet, suitably in the form of a tube.
  • the amorphous solid comprises a gelling agent comprising a cellulosic gelling agent and/or a non-cellulosic gelling agent, an active substance and an acid.
  • the amorphous solid may consist essentially of, or consist of a gelling agent, water, an aerosol-former material, a flavour, and optionally an active substance.
  • the amorphous solid may consist essentially of, or consist of a gelling agent, water, an aerosol-former material, a flavour, and optionally a tobacco material and/ or a nicotine source.
  • the amorphous solid may comprise one or more active substances and/or flavours, one or more aerosol-former materials, and optionally one or more other functional material.
  • the aerosol-former material may comprise one or more constituents capable of forming an aerosol.
  • the aerosol-former material may comprise one or more of glycerine, glycerol, propylene glycol, diethylene glycol, triethylene glycol, tetraethylene glycol, 1,3-butylene glycol, erythritol, meso-Erythritol, ethyl vanillate, ethyl laurate, a diethyl suberate, triethyl citrate, triacetin, a diacetin mixture, benzyl benzoate, benzyl phenyl acetate, tributyrin, lauryl acetate, lauric acid, myristic acid, and propylene carbonate.
  • the amorphous solid may comprise an acid.
  • the acid may be an organic acid.
  • the acid may be at least one of a monop rotic acid, a diprotic acid and a triprotic acid.
  • the acid may contain at least one carboxyl functional group.
  • the acid maybe at least one of an alpha-hydroxy acid, carboxylic acid, di carboxylic acid, tricarboxylic acid and keto acid.
  • the acid maybe an alpha-keto acid.
  • the acid may be at least one of succinic acid, lactic acid, benzoic acid, citric acid, tartaric acid, fumaric acid, levulinic acid, acetic acid, malic acid, formic acid, sorbic acid, benzoic acid, propanoic and pyruvic acid.
  • the acid is lactic acid.
  • the acid is benzoic acid.
  • the acid may be an inorganic acid.
  • the acid may be a mineral acid.
  • the acid may be at least one of sulphuric acid, hydrochloric acid, boric acid and phosphoric acid.
  • the acid is levulinic acid.
  • an acid is particularly preferred in embodiments in which amorphous solid comprises nicotine.
  • the presence of an acid may stabilise dissolved species in the slurry from which the aerosol-generating material is formed.
  • the presence of the acid may reduce or substantially prevent evaporation of nicotine during drying of the slurry, thereby reducing loss of nicotine during manufacturing.
  • the amorphous solid may comprise a colourant.
  • the addition of a colourant may alter the visual appearance of the amorphous solid.
  • the presence of colourant in the amorphous solid may enhance the visual appearance of the amorphous solid and the aerosol-generating material.
  • the amorphous solid may be colour-matched to other components of the aerosol- generating material or to other components of an article comprising the amorphous solid.
  • colourants may be used depending on the desired colour of the amorphous solid.
  • the colour of amorphous solid may be, for example, white, green, red, purple, blue, brown or black. Other colours are also envisaged.
  • Natural or synthetic colourants such as natural or synthetic dyes, food-grade colourants and pharmaceutical-grade colourants may be used.
  • the colourant is caramel, which may confer the amorphous solid with a brown appearance.
  • the colour of the amorphous solid may be similar to the colour of other components (such as tobacco material) in an aerosol-generating material comprising the amorphous solid.
  • the addition of a colourant to the amorphous solid renders it visually indistinguishable from other components in the aerosol-generating material.
  • the colourant maybe incorporated during the formation of the amorphous solid (e.g. when forming a slurry comprising the materials that form the amorphous solid) or it maybe applied to the amorphous solid after its formation (e.g. by spraying it onto the amorphous solid).
  • the one or more other functional materials may comprise one or more of pH regulators, colouring agents, preservatives, binders, fillers, stabilizers, and/or antioxidants.
  • a consumable is an article comprising or consisting of aerosol-generating material, part or all of which is intended to be consumed during use by a user.
  • a consumable may comprise one or more other components, such as an aerosol-generating material storage area, an aerosol-generating material transfer component, an aerosol generation area, a housing, a wrapper, a mouthpiece, a filter and/ or an aerosol-modifying agent.
  • a consumable may also comprise an aerosol generator, such as a heater, that emits heat to cause the aerosol-generating material to generate aerosol in use.
  • the heater may, for example, comprise combustible material, a material heatable by electrical conduction, or a susceptor.
  • a susceptor is a material that is heatable by penetration with a varying magnetic field, such as an alternating magnetic field.
  • the susceptor may be an electrically-conductive material, so that penetration thereof with a varying magnetic field causes induction heating of the heating material.
  • the heating material may be magnetic material, so that penetration thereof with a varying magnetic field causes magnetic hysteresis heating of the heating material.
  • the susceptor maybe both electrically-conductive and magnetic, so that the susceptor is heatable by both heating mechanisms.
  • the device that is configured to generate the varying magnetic field is referred to as a magnetic field generator, herein.
  • An aerosol-modifying agent is a substance, typically located downstream of the aerosol generation area, that is configured to modify the aerosol generated, for example by changing the taste, flavour, acidity or another characteristic of the aerosol.
  • the aerosol modifying agent may be provided in an aerosol-modifying agent release component, that is operable to selectively release the aerosol-modifying agent.
  • the aerosol-modifying agent may, for example, be an additive or a sorbent.
  • the aerosol-modifying agent may, for example, comprise one or more of a flavourant, a colourant, water, and a carbon adsorbent.
  • the aerosol-modifying agent may, for example, be a solid, a liquid, or a gel.
  • the aerosol-modifying agent maybe in powder, thread or granule form.
  • the aerosol-modifying agent may be free from filtration material.
  • An aerosol generator is an apparatus configured to cause aerosol to be generated from the aerosol-generating material.
  • the aerosol generator is a heater configured to subject the aerosol-generating material to heat energy, so as to release one or more volatiles from the aerosol-generating material to form an aerosol.
  • the aerosol generator is configured to cause an aerosol to be generated from the aerosol-generating material without heating.
  • the aerosol generator maybe configured to subject the aerosol-generating material to one or more of vibration, increased pressure, or electrostatic energy.
  • Articles, for instance those in the shape of rods, are often named according to the product length: “regular” (typically in the range 68 - 75 mm, e.g. from about 68 mm to about 72 mm), “short” or “mini” (68 mm or less), “king-size” (typically in the range 75 - 91 mm, e.g. from about 79 mm to about 88 mm), “long” or “super-king” (typically in the range 91 - 105 mm, e.g. from about 94 mm to about 101 mm) and “ultra-long” (typically in the range from about no mm to about 121 mm).
  • an article in a king-size, super-slim format will, for example, have a length of about 83 mm and a circumference of about 17 mm.
  • Each format may be produced with mouthpieces of different lengths.
  • the mouthpiece length will be from about 30 mm to 50 mm.
  • a tipping paper connects the mouthpiece to the aerosol-generating material and will usually have a greater length than the mouthpiece, for example from 3 to 10 mm longer, such that the tipping paper covers the mouthpiece and overlaps the aerosol-generating material, for instance in the form of a rod of substrate material, to connect the mouthpiece to the rod.
  • Articles and their aerosol-generating materials and mouthpieces described herein can be made in, but are not limited to, any of the above formats.
  • the terms ‘upstream’ and ‘downstream’ used herein are relative terms defined in relation to the direction of mainstream aerosol drawn though an article or device in use.
  • the filamentary tow material described herein can comprise cellulose acetate fibre tow.
  • the filamentary tow can also be formed using other materials used to form fibres, such as polyvinyl alcohol (PVOH), polylactic acid (PLA), polycaprolactone (PCL), poly(i-4 butanediol succinate) (PBS), poly(butylene adipate-co-terephthalate)(PBAT), starch based materials, cotton, aliphatic polyester materials and polysaccharide polymers or a combination thereof.
  • the filamentary tow may be plasticised with a suitable plasticiser for the tow, such as triacetin where the material is cellulose acetate tow, or the tow may be non-plasticised.
  • the tow can have any suitable specification, such as fibres having a ⁇ ’ shaped or other cross section such as ‘X’ shaped, filamentary denier values between 2.5 and 15 denier per filament, for example between 8.0 and 11.0 denier per filament and total denier values of 5,000 to 50,000, for example between 10,000 and 40,000.
  • tobacco material refers to any material comprising tobacco or derivatives or substitutes thereof.
  • tobacco material may include one or more of tobacco, tobacco derivatives, expanded tobacco, reconstituted tobacco or tobacco substitutes.
  • the tobacco material may comprise one or more of ground tobacco, tobacco fibre, cut tobacco, extruded tobacco, tobacco stem, tobacco lamina, reconstituted tobacco and/or tobacco extract.
  • the tobacco material may contain a filler component.
  • the filler component is generally a non-tobacco component, that is, a component that does not include ingredients originating from tobacco.
  • the filler component may be a non-tobacco fibre such as wood fibre or pulp or wheat fibre.
  • the filler component may also be an inorganic material such as chalk, perlite, vermiculite, diatomaceous earth, colloidal silica, magnesium oxide, magnesium sulphate, magnesium carbonate.
  • the filler component may also be a non-tobacco cast material or a non-tobacco extruded material.
  • the filler component may be present in an amount of o to 20% by weight of the tobacco material, or in an amount of from l to io% by weight of an overall composition, for instance the aerosol-generating material described herein. In some embodiments, the filler component is absent. In the tobacco material described herein, the tobacco material contains an aerosol- former material.
  • the aerosol-former material of the tobacco material may be glycerol, propylene glycol, or a mixture of glycerol and propylene glycol.
  • Glycerol may be present in an amount of from to to 20 % by weight of the tobacco material, for example 13 to 16 % by weight of the composition, i.e. the overall aerosol-generating material described herein, or about 14% or 15% by weight of the composition.
  • Propylene glycol if present, may be present in an amount of from 0.1 to 0.3% by weight of the composition.
  • the aerosol-former material may be included in any component, for example any tobacco component, of the tobacco material, and/ or in the filler component, if present. Alternatively or additionally the aerosol-former material may be added to the tobacco material separately. In either case, the total amount of the aerosol-former material in the tobacco material can be as defined herein.
  • the tobacco material can contain between 10% and 90% by weight tobacco leaf, for instance tobacco lamina.
  • An aerosol-former material can be provided in the tobacco material, in addition to any aerosol-former material provided via the amorphous solid material. For instance, aerosol-former material as described herein can be provided in the tobacco material in an amount of between 2% and 20%, for instance between about 5% and about 15% by weight of the tobacco material.
  • the aerosol-former can comprise up to about 10% by weight of the leaf tobacco. To achieve an overall level of aerosol-former material between 10% and 20% by weight of the tobacco material, it has been advantageously found that this can be added in higher weight percentages to the another component of the tobacco material, such as reconstituted tobacco material.
  • the tobacco material consists essentially of leaf tobacco, for instance lamina tobacco.
  • the tobacco material described herein contains nicotine.
  • the nicotine content is from 0.5 to 1.75% by weight of the tobacco material, and may be, for example, from 0.8 to
  • the tobacco material contains between 10% and 90% by weight tobacco leaf having a nicotine content of greater than 1.5% by weight of the tobacco leaf. It has been advantageously found that using a tobacco leaf with nicotine content higher than 1.5% in combination with a lower nicotine base material, such as paper reconstituted tobacco, provides a tobacco material with an appropriate nicotine level but better sensory performance than the use of paper reconstituted tobacco alone.
  • the tobacco leaf for instance cut rag tobacco, can, for instance, have a nicotine content of between 1.5% and 5% by weight of the tobacco leaf.
  • the tobacco material described herein can contain an aerosol modifying agent, such as any of the flavours described herein.
  • the tobacco material contains menthol, forming a mentholated article.
  • the tobacco material can comprise from 3mg to 2omg of menthol, preferably between 5mg and i8mg and more preferably between 8mg and i6mg of menthol.
  • the tobacco material comprises i6mg of menthol.
  • the tobacco material can contain between 2% and 8% by weight of menthol, preferably between 3% and 7% by weight of menthol and more preferably between 4% and 5.5% by weight of menthol.
  • the tobacco material includes 4.7% by weight of menthol.
  • Such high levels of menthol loading can be achieved using a high percentage of reconstituted tobacco material, for instance greater than 50% of the tobacco material by weight.
  • a high volume of aerosol-generating material for instance tobacco material
  • any water that may be present in the tobacco material, or in any component thereof, is entirely disregarded for the purposes of the determination of the weight %.
  • the water content of the tobacco material described herein may vary and may be, for example, from 5 to 15% by weight.
  • the water content of the tobacco material described herein may vary according to, for example, the temperature, pressure and humidity conditions at which the compositions are maintained. The water content can be determined by Karl-Fisher analysis, as known to those skilled in the art.
  • any component other than water is included in the weight of the tobacco material.
  • the aerosol-former material is not included in the weight of the tobacco component or filler component, but is included in the weight of the "aerosol-former material" in the weight % as defined herein. All other ingredients present in the tobacco component are included in the weight of the tobacco component, even if of non-tobacco origin (for example non-tobacco fibres in the case of paper reconstituted tobacco).
  • the tobacco material comprises the tobacco component as defined herein and the aerosol-former material as defined herein. In an embodiment, the tobacco material consists essentially of the tobacco component as defined herein and the aerosol-former material as defined herein. In an embodiment, the tobacco material consists of the tobacco component as defined herein and the aerosol-former material as defined herein.
  • Paper reconstituted tobacco maybe present in the tobacco component of the tobacco material described herein in an amount of from 10% to 100% by weight of the tobacco component.
  • the paper reconstituted tobacco is present in an amount of from 10% to 80% by weight, or 20% to 70% by weight, of the tobacco component.
  • the tobacco component consists essentially of, or consists of, paper reconstituted tobacco.
  • leaf or lamina tobacco is present in the tobacco component of the tobacco material in an amount of from at least 10% by weight of the tobacco component.
  • leaf tobacco can be present in an amount of at least 10% by weight of the tobacco component, while the remainder of the tobacco component comprises paper reconstituted tobacco, bandcast reconstituted tobacco, or a combination of bandcast reconstituted tobacco and another form of tobacco such as tobacco granules.
  • leaf tobacco can be present in an amount up to 40 % or 60% of the tobacco material, while the remainder of the tobacco component comprises paper reconstituted tobacco, bandcast reconstituted tobacco, or a combination of bandcast reconstituted tobacco and another form of tobacco such as tobacco granules.
  • Paper reconstituted tobacco refers to tobacco material formed by a process in which tobacco feedstock is extracted with a solvent to afford an extract of solubles and a residue comprising fibrous material, and then the extract (usually after concentration, and optionally after further processing) is recombined with fibrous material from the residue (usually after refining of the fibrous material, and optionally with the addition of a portion of non-tobacco fibres) by deposition of the extract onto the fibrous material.
  • the process of recombination resembles the process for making paper.
  • the paper reconstituted tobacco may be any type of paper reconstituted tobacco that is known in the art.
  • the paper reconstituted tobacco is made from a feedstock comprising one or more of tobacco strips, tobacco stems, and whole leaf tobacco.
  • the paper reconstituted tobacco is made from a feedstock consisting of tobacco strips and/or whole leaf tobacco, and tobacco stems.
  • scraps, fines and winnowings can alternatively or additionally be employed in the feedstock.
  • FIG. 1 is a side-on cross sectional view of an article 1 for use in an aerosol delivery system.
  • the article 1 comprises a mouthpiece 2, and a cylindrical rod of aerosol-generating material 3, connected to the mouthpiece 2.
  • the aerosol-generating material comprises a blend of at least two distinct components.
  • the aerosol-generating material comprises a plurality of strands and/ or strips of a tobacco material and a plurality of strips of amorphous solid material, wherein the plurality of strands and/ or strips of tobacco material and the plurality of strips of amorphous solid material each have a length of at least about 5 mm.
  • the material properties and/or dimensions of the at least two components may be suitably selected in other ways, to ensure a relatively uniform mix of the components is possible, and to reduce separation or un-mixing of the components during or after manufacture of the rod of aerosol-generating material.
  • the aerosol-generating material can be provided in other forms, for instance a plug, pouch, or packet of material within an article.
  • the article can comprise a consumable for an aerosol delivery or provision system such as a non-combustible aerosol delivery or provision system as described herein.
  • a first component is a tobacco material
  • a second component is an amorphous solid material.
  • the tobacco material comprises a paper reconstituted tobacco material.
  • the tobacco material can alternatively or additionally comprise any of the forms described herein.
  • the tobacco material contains between 10% and 90% by weight tobacco leaf, wherein aerosol-former material is provided in an amount of up to about 10% by weight of the leaf tobacco.
  • aerosol-former can be provided in addition to aerosol-former provided in the amorphous solid material. For instance, between 3% and 8% aerosol-former by weight of the tobacco material can be used, or between 4% and 7%, or between 5% and 7%.
  • the remainder of the tobacco material can comprise paper reconstituted tobacco.
  • the tobacco material comprises up to 100% tobacco leaf, for instance up to 100% tobacco lamina, which can be in the form of cut rag tobacco. It can be advantageous to adjust the aerosol former and/ or water content of the tobacco lamina material to avoid a material which is too dry and may become too fragile.
  • the tobacco lamina can include between 5% and 8% aerosol-former such as glycerol and/or between 9% and 12% water.
  • the amorphous solid material is a dried gel comprising menthol.
  • the amorphous solid may have any composition as described herein.
  • an improved article may be produced comprising aerosol-generating material comprising a first component comprising tobacco material and a second component comprising amorphous solid, wherein the material properties (e.g. density) and specification (e.g. thickness, length, and cut width) fall within the ranges set out herein.
  • material properties e.g. density
  • specification e.g. thickness, length, and cut width
  • the amorphous solid may have a thickness of about 0.015 mm to about 1.5 mm.
  • the thickness maybe in the range of about 0.05 mm, 0.1 mm or 0.15 mm to about 0.5 mm, 0.3 mm, or 1 mm.
  • the inventors have found that a material having a thickness of about 0.2 mm can be used.
  • the amorphous solid may comprise more than one layer, and the thickness described herein refers to the aggregate thickness of those layers.
  • the thickness of the amorphous solid material may be measured using a calliper or a microscope such as a scanning electron microscope (SEM), as known to those skilled in the art, or any other suitable technique known to those skilled in the art.
  • SEM scanning electron microscope
  • the inventors have established that if the amorphous solid is too thick, then heating efficiency can be compromised. This can adversely affect power consumption in use, for instance the power consumption for release of flavour from the amorphous solid. Conversely, if the aerosol-forming amorphous solid is too thin, it can be difficult to manufacture and handle; a very thin material can be harder to cast and may be fragile, compromising aerosol formation in use.
  • the inventors have established that the amorphous solid thicknesses stipulated herein optimise the material properties in view of these competing considerations.
  • an individual strip or piece of the amorphous solid has a minimum thickness over its area of about 0.015 mm. In some cases, an individual strip or piece of the amorphous solid has a minimum thickness over its area of about 0.05 mm or about 0.1 mm. In some cases, an individual strip or piece of the amorphous solid has a maximum thickness over its area of about l.omm. In some cases, an individual strip or piece of the amorphous solid has a maximum thickness over its area of about 0.5 mm or about 0.3 mm. The inventors have found that providing amorphous solid material and tobacco material having area density values that differ from each other by less than a given percentage results in less separation in a mixture of these materials.
  • the area density of the amorphous solid material may be between 50% and 150% of the area density of the tobacco material.
  • the area density of the amorphous solid material may be between 60% and 140% of the density of the tobacco material, or between 70% and 110% of the area density of the tobacco material, or between 80% and 120% of the area density of the tobacco material.
  • area density this refers to an average area density calculated for a given strip, piece or sheet of amorphous solid material, the area density calculated by measuring the surface area and weight of the given strip, piece or sheet of amorphous solid material.
  • the amorphous solid thickness may vary by no more than 25%, 20%, 15%, 10%, 5% or 1% across its area.
  • the amorphous solid material may be incorporated into the article in sheet form.
  • the amorphous solid material in sheet form may be shredded and then incorporated into the article, suitably mixed into an aerosolisable material such as a tobacco material (as described further hereinbelow).
  • the amorphous solid sheet may additionally be incorporated as a planar sheet, as a gathered or bunched sheet, as a crimped sheet, or as a rolled sheet (i.e. in the form of a tube).
  • the amorphous solid of these embodiments may be included in an aerosol-generating article as a sheet, such as a sheet circumscribing a rod of aerosolisable material (e.g. tobacco).
  • the amorphous solid sheet maybe formed on a wrapping paper which circumscribes an aerosolisable material such as tobacco.
  • the amorphous solid in sheet form may have any suitable area density, such as from about 30 g/m 2 to about 150 g/m 2 .
  • the sheet may have a mass per unit area of about 55 g/m 2 to about 135 g/m 2 , or about 80 to about 120 g/m 2 , or from about 70 to about 110 g/ m 2 , or from about 100 g/m 2 to about 125 g/ m 2 , or particularly from about 90 to about 110 g/m 2 , or suitably about 100 g/m 2 , 120 g/m 2 or 110 g/m 2 .
  • These ranges can provide a density which is similar to the density of cut rag tobacco and as a result a mixture of these substances can be provided which will not readily separate.
  • the amorphous solid material is included in an aerosol-generating article as a shredded sheet (described further hereinbelow).
  • the sheet may have a mass per unit area of about 30 to 70 g/m 2 , 40 to 60 g/m 2 , or 25 to 60 g/m 2 and maybe used to wrap an aerosolisable material such as tobacco.
  • the density of the tobacco material has an impact on the speed at which heat conducts through the material, with lower densities, for instance those below 700 mg/ cc, conducting heat more slowly through the material, and therefore enabling a more sustained release of aerosol.
  • the tobacco material can comprise reconstituted tobacco material having a density of less than about 700 mg/cc, for instance paper reconstituted tobacco material.
  • the aerosol-generating material 3 comprises reconstituted tobacco material having a density of less than about 600 mg/cc.
  • the aerosol generating material 3 can comprise reconstituted tobacco material having a density of at least 350 mg/ cc.
  • the tobacco material maybe provided in the form of cut rag tobacco.
  • the cut rag tobacco can have a cut width of at least 15 cuts per inch (about 5.9 cuts per cm, equivalent to a cut width of about 1.7mm).
  • the cut rag tobacco has a cut width of at least 18 cuts per inch (about 7.1 cuts per cm, equivalent to a cut width of about 1.4mm), more preferably at least 20 cuts per inch (about 7.9 cuts per cm, equivalent to a cut width of about 1.27mm).
  • the cut rag tobacco has a cut width of 22 cuts per inch (about 8.7 cuts per cm, equivalent to a cut width of about 1.15mm).
  • the cut rag tobacco has a cut width at or below 40 cuts per inch (about 15.7 cuts per cm, equivalent to a cut width of about 0.64mm). Cut widths between 0.5 mm and 2.0 mm, for instance between 0.6 and 1.7mm or between 0.6 mm and 1.5 mm, have been found to result in tobacco material which is preferably in terms of surface area to volume ratio, particularly when heated, and the overall density and pressure drop of the rod of aerosol-generating material 3.
  • the cut rag tobacco can be formed from a mixture of forms of tobacco material, for instance a mixture of one or more of paper reconstituted tobacco, leaf tobacco, extruded tobacco and bandcast tobacco.
  • the tobacco material comprises paper reconstituted tobacco or a mixture of paper reconstituted tobacco and leaf tobacco.
  • the tobacco material may have any suitable thickness.
  • the tobacco material may have a thickness of at least about 0.145 mm, for instance at least about 0.15 mm, or at least about 0.16 mm.
  • the tobacco material may have a maximum thickness of about 0.25 mm, for instance the thickness of the tobacco material maybe less than about 0.22 mm, or less than about 0.2 mm.
  • the tobacco material may have an average thickness in the range 0.175 mm to 0.195 mm. Such thicknesses maybe particularly suitable where the tobacco material is a reconstituted tobacco material.
  • an aerosol-generating material comprising a blend of at least two components, such as a first component comprising tobacco material and a second component comprising amorphous solid material as described herein.
  • Such aerosol-generating material can provide an aerosol, in use, with a desirable flavour profile, since additional flavour may be introduced to the aerosol-generating material by inclusion in the amorphous solid material component.
  • Flavour provided in the amorphous solid material may be more stably retained within the amorphous solid material compared to flavour added directly to the tobacco material, resulting in a more consistent flavour profile between articles produced according to this invention.
  • tobacco material having a density of at least 350 mg/cc and less than about 700 mg/ cc has been advantageously found to result in a more sustained release of aerosol.
  • the amorphous solid material component of the aerosol-generating material should be evenly distributed throughout the rod. The inventors have advantageously found that this can be achieved by casting the amorphous solid material to have a thickness as described herein, to provide an amorphous solid material having an area density which is similar to the area density of the tobacco material, and processing the amorphous solid material as described hereinbelow to ensure an even distribution throughout the aerosol-generating material.
  • the inventors have advantageously found that sufficiently even mixing of the tobacco material component and the amorphous solid material component can be achieved when the amorphous solid material in sheet form is shredded.
  • the cut width of the shredded amorphous solid material is between 0.75 mm and 2 mm, for instance between 1 mm and 1.5 mm.
  • the strands of amorphous solid material formed by shredding maybe cut width-wise, for example in a cross-cut type shredding process, to define a cut length for the shredded amorphous solid material, in addition to a cut width.
  • the cut length of the shredded amorphous solid material is preferably at least 5 mm, for instance at least 10 mm, or at least 20 mm.
  • the cut length of the shredded amorphous solid material can be less than 60 mm, less than 50 mm, or less than 40 mm.
  • the inventors have advantageously found that to achieve even mixing of the shredded amorphous solid material with cut rag tobacco, the cut length of the shredded amorphous solid material is preferably non-uniform.
  • the distribution of cut lengths may be a multi-modal distribution, such as a bimodal distribution.
  • a first portion of amorphous solid material may be cut to a first length
  • a second portion of amorphous solid material may be cut to a second length, and the cut material mixed together to form a plurality of strands or strips of amorphous solid material having a bimodal distribution of lengths.
  • the first cut length may be from 30 mm to 50 mm, or 35 mm for 45 mm, or about 40 mm
  • the second cut length may be from 10 mm to 30 mm, or from 15 mm to 25 mm, or about 20 mm.
  • the number of cut lengths may be selected to match the number of modes in the distribution of lengths of a shredded tobacco material.
  • the strands of amorphous material having different cut lengths may be mixed together in a ratio selected to match the distribution of lengths of the shredded tobacco material. The inventors have found that matching the distribution of lengths of the strands and/or strips of amorphous solid material to the distribution of lengths of the strands of tobacco material can result in a more even mixing of the amorphous solid with the tobacco material.
  • the length of the shreds or strips of amorphous solid material can alternatively or additionally be dictated by a dimension of the material determined during its manufacture, for instance the width of a sheet of the material as manufactured.
  • a plurality of strips of amorphous solid is provided and at least one of the plurality of strips of amorphous solid material has a length greater than about 10 mm. At least one of the plurality of strips of amorphous solid material can alternatively or in addition have a length between about 10 mm and about 60 mm, or between about 20 mm and about 50 mm. Each of the plurality of strips of amorphous solid material can have a length between about 10 mm and about 60 mm, or between about 20 mm and about 50 mm.
  • the rod of aerosol generating material comprises a first component comprising a tobacco material in an amount from 50 % to 98 %, for instance from 80% to 95%, wherein the tobacco material is for instance provided as a cut rag tobacco, and a second component comprising shredded amorphous solid material in an amount from 2 % to 50 %, for instance from 5% to 20%.
  • the inventors have found that it can be advantageous for manufacturing to form the rod of aerosol generating material from a relatively low amount, within the ranges set out herein, of shredded amorphous solid material comprising a relatively high level of aerosol-former, within the ranges set out herein, such that for a given aerosol-former content in the aerosol generating material, a lower number of the plurality of strips of amorphous solid material are required.
  • This can be beneficial for manufacture because relatively more tobacco material comes into contact with components of the manufacturing machinery compared to the amorphous solid material, which can reduce the likelihood of material clumping on the machinery and/or blockages forming during manufacture.
  • the amount of aerosol-former, such as glycerol, in the amorphous solid material can comprise between 20% and 70%, for instance between 25% and 55%, between 30% and 40% or between 45% and 55% by weight of the amorphous solid material.
  • aerosol-generating material according to the present disclosure can have a more uniform distribution of the shredded amorphous solid material throughout the aerosol-generating material.
  • the standard deviation (expressed as a percentage of the mean) in the percentage weight inclusion level of the strips of amorphous solid material in the aerosol-generating material between consumables made using the aerosol generating material as described herein can be less than 35%, or less than 30% by weight of the aerosol-generating material, based on a measurement of 10 consumables in the present case each containing about 650mg of the aerosol-generating material.
  • Table la shows the % inclusion achieved for three aerosol-generating materials, namely material A with a mean of 4.6307% amorphous solid content, material B with a mean of 10.625% amorphous solid content and material C with a mean of 19.722% amorphous solid content. It has been found, for instance, that for a mean amorphous solid inclusion rate of greater than 10%, a standard deviation of less than 30% as a percentage of the mean can be achieved. The measurement is performed by carefully opening the aerosol-generating material rod of the consumables and manually separating the amorphous solid material from tobacco material.
  • Table la Total amorphous solid content by percentage weight in aerosol-generating material according to the present disclosure.
  • Exemplary aerosol-generating materials were produced according to the present disclosure, and chemical analysis, as known to those skilled in the art, was carried out on samples of each exemplary aerosol-generating material to determine the total nicotine, glycerol and water content of the material. Ten samples of 10 g were taken from a batch of aerosol-generating material for chemical analysis, and the process repeated ten times to obtain the mean nicotine, glycerol and water content and standard deviations thereof within a batch of aerosol-generating material manufactured according to the methods described herein.
  • Each of the exemplary aerosol-generating materials 1-3 comprised 100% leaf tobacco as the tobacco material component, and each was produced to a different specification in terms of the inclusion level of the amorphous solid material component, and the composition of the amorphous solid material.
  • the tobacco material included 4.5% glycerol by weight of the tobacco material.
  • Table lb shows that in aerosol-generating materials produced according to the present disclosure, the standard deviation in the total glycerol content within a given batch of material was less than 35% of the mean in all cases, or less than 30% or less than 25%.
  • Table lb Total nicotine, glycerol and water content by percentage weight in aerosol generating material according to the present disclosure.
  • the total flavourant in the article may comprise the flavourant provided in the amorphous solid material, and optionally further flavourant applied to the tobacco material or present in a component of the article other than the aerosol-generating material 3.
  • the total flavourant content of the article maybe determined by deconstructing the article into its component parts and performing chemical analysis as known to those skilled in the art to determine the flavourant content of each component, and thereby the total flavourant content.
  • the total flavourant content of the article maybe between 5 mg and 30 mg per article, for instance between 16 mg and 22 mg per article, or between 5 mg and 10 mg per article or between 17 mg and 30 mg per article.
  • the amorphous solid may comprise at least 20% of the total flavourant content.
  • Articles comprising aerosol-generating material according to the present disclosure were produced, where the aerosol-generating material included 5wt%, i2wt% or 20wt% amorphous solid comprising 35wt% menthol as a flavourant.
  • Table 2 shows the menthol content in mg per article of articles comprising the aerosol-generating material. Standard deviations in the menthol content were determined by analysing ten articles produced from each batch of aerosol-generating material. As shown, the total menthol inclusion in each article can vary between articles by a standard deviation of less than 20% of the mean menthol inclusion in mg.
  • Table 2 Total menthol content per article for articles including aerosol-generating material comprising amorphous solid material comprising 35% menthol by percentage weight of the amorphous solid, in varying weight percentages of the aerosol-generating material.
  • the aerosol-generating material can be provided in the form of a rod having a first end and a second end. The portion of the rod between the first end of the rod and a longitudinal position half-way between the first and second ends can include from 20% to 80% of the amorphous solid material in the rod.
  • the mouthpiece 2, in the present example, includes a body of material 6 upstream of the hollow tubular element 4, in this example adjacent to and in an abutting relationship with the hollow tubular element 4.
  • the body of material 6 and hollow tubular element 4 each define a substantially cylindrical overall outer shape and share a common longitudinal axis.
  • the body of material 6 is wrapped in a first plug wrap 7.
  • the first plug wrap 7 has a basis weight of less than 50 gsm, more preferably between about 20 gsm and 40 gsm.
  • the first plug wrap 7 has a thickness of between 30 pm and 60 pm, more preferably between 35 pm and 45 pm.
  • the first plug wrap 7 is a non-porous plug wrap, for instance having a permeability of less than 100 Coresta units, for instance less than 50 Coresta units.
  • the first plug wrap 7 can be a porous plug wrap, for instance having a permeability of greater than 200 Coresta Units.
  • the length of the body of material 6 is less than about 15 mm. More preferably, the length of the body of material 6 is less than about 10 mm. In addition, or as an alternative, the length of the body of material 6 is at least about 5 mm. Preferably, the length of the body of material 6 is at least about 6 mm. In some preferred embodiments, the length of the body of material 6 is from about 5 mm to about 15 mm, more preferably from about 6 mm to about 12 mm, even more preferably from about 6 mm to about 12 mm, most preferably about 6 mm, 7 mm, 8 mm, 9 mm or 10 mm. In the present example, the length of the body of material 6 is 10 mm.
  • the body of material 6 is formed from filamentary tow.
  • the tow used in the body of material 6 has a denier per filament (d.p.f.) of 8.4 and a total denier of 21,000.
  • the tow can, for instance, have a denier per filament (d.p.f.) of 9.5 and a total denier of 12,000.
  • the tow comprises plasticised cellulose acetate tow.
  • the plasticiser used in the tow comprises about 7% by weight of the tow.
  • the plasticiser is triacetin.
  • different materials can be used to form the body of material 6.
  • the body 6 can be formed from paper, for instance in a similar way to paper filters known for use in cigarettes.
  • the body 6 can be formed from tows other than cellulose acetate, for instance polylactic acid (PLA), other materials described herein for filamentary tow or similar materials.
  • the tow is preferably formed from cellulose acetate.
  • the tow, whether formed from cellulose acetate or other materials, preferably has a d.p.f. of at least 5, more preferably at least 6 and still more preferably at least 7. These values of denier per filament provide a tow which has relatively coarse, thick fibres with a lower surface area which result in a lower pressure drop across the mouthpiece 2 than tows having lower d.p.f. values.
  • the tow has a denier per filament of no more than 12 d.p.f., preferably no more than 11 d.p.f. and still more preferably no more than 10 d.p.f.
  • the total denier of the tow forming the body of material 6 is preferably at most 30,000, more preferably at most 28,000 and still more preferably at most 25,000. These values of total denier provide a tow which takes up a reduced proportion of the cross sectional area of the mouthpiece 2 which results in a lower pressure drop across the mouthpiece 2 than tows having higher total denier values.
  • the tow preferably has a total denier of at least 8,000 and more preferably at least 10,000.
  • the denier per filament is between 5 and 12 while the total denier is between 10,000 and 25,000. More preferably, the denier per filament is between 6 and 10 while the total denier is between 11,000 and 22,000.
  • the cross-sectional shape of the filaments of tow are ⁇ shaped, although in other embodiments other shapes such as ‘X’ shaped filaments can be used, with the same d.p.f. and total denier values as provided herein.
  • the mouthpiece 2 of the article 1 comprises an upstream end 2a adjacent to the rod of aerosol-generating material 3 and a downstream end 2b distal from the rod of aerosol-generating material 3.
  • the mouthpiece 2 has a hollow tubular element 4 formed from filamentary tow. This has advantageously been found to significantly reduce the temperature of the outer surface of the mouthpiece 2 at the downstream end 2b of the mouthpiece which comes into contact with a consumer’s mouth when the article 1 is in use.
  • the use of the tubular element 4 has also been found to significantly reduce the temperature of the outer surface of the mouthpiece 2 even upstream of the tubular element 4. Without wishing to be bound by theory, it is hypothesised that this is due to the tubular element 4 channelling aerosol closer to the centre of the mouthpiece 2, and therefore reducing the transfer of heat from the aerosol to the outer surface of the mouthpiece 2.
  • the article 1 has an outer circumference of about 21 mm (i.e. the article is in the demi-slim format).
  • the article can be provided in any of the formats described herein, for instance having an outer circumference of between 15mm and 25mm. Since the article is to be heated to release an aerosol, improved heating efficiency can be achieved using articles having lower outer circumferences within this range, for instance circumferences of less than 23mm. To achieve improved aerosol via heating, while maintaining a suitable product length, article circumferences of greater than 19mm have also been found to be particularly effective. Articles having circumferences of between 19mm and 23mm, and more preferably between 20mm and 22mm, have been found to provide a good balance between providing effective aerosol delivery while allowing for efficient heating.
  • the outer circumference of the mouthpiece 2 is substantially the same as the outer circumference of the rod of aerosol-generating material 3, such that there is a smooth transition between these components.
  • the outer circumference of the mouthpiece 2 is about 20.8mm.
  • a tipping paper 5 is wrapped around the full length of the mouthpiece 2 and over part of the rod of aerosol-generating material 3 and has an adhesive on its inner surface to connect the mouthpiece 2 and rod 3.
  • the tipping paper 5 extends 5 mm over the rod of aerosol-generating material 3 but it can alternatively extend between 3 mm and 10 mm over the rod 3, or more preferably between 4 mm and 6 mm, to provide a secure attachment between the mouthpiece 2 and rod 3.
  • the tipping paper 5 can have a basis weight which is higher than the basis weight of plug wraps used in the article 1, for instance a basis weight of 40 gsm to 80 gsm, more preferably between 50 gsm and 70 gsm, and in the present example 58 gsm. These ranges of basis weights have been found to result in tipping papers having acceptable tensile strength while being flexible enough to wrap around the article 1 and adhere to itself along a longitudinal lap seam on the paper.
  • the outer circumference of the tipping paper 5, once wrapped around the mouthpiece 2 is about 21 mm.
  • the "wall thickness" of the hollow tubular element 4 corresponds to the thickness of the wall of the tube 4 in a radial direction. This may be measured, for example, using a calliper.
  • the wall thickness is advantageously greater than 0.9 mm, and more preferably 1.0mm or greater.
  • the wall thickness is substantially constant around the entire wall of the hollow tubular element 4.
  • the wall thickness is preferably greater than 0.9 mm at any point around the hollow tubular element 4, more preferably 1.0mm or greater.
  • the length of the hollow tubular element 4 is less than about 20 mm. More preferably, the length of the hollow tubular element 4 is less than about 15 mm. Still more preferably, the length of the hollow tubular element 4 is less than about 10 mm.
  • the length of the hollow tubular element 4 is at least about 5 mm.
  • the length of the hollow tubular element 4 is at least about 6 mm.
  • the length of the hollow tubular element 4 is from about 5 mm to about 20 mm, more preferably from about 6 mm to about 10 mm, even more preferably from about 6 mm to about 8 mm, most preferably about 6 mm, 7 mm or about 8 mm.
  • the length of the hollow tubular element 4 is 6 mm.
  • the density of the hollow tubular element 4 is at least about 0.25 grams per cubic centimetre (g/cc), more preferably at least about 0.3 g/cc.
  • the density of the hollow tubular element 4 is less than about 0.75 grams per cubic centimetre (g/cc), more preferably less than 0.6 g/cc.
  • the density of the hollow tubular element 4 is between 0.25 and 0.75 g/ cc, more preferably between 0.3 and 0.6 g/cc, and more preferably between 0.4 g/cc and 0.6 g/cc or about 0.5 g/cc.
  • the filamentary tow forming the hollow tubular element 4 preferably has a total denier of less than 45,000, more preferably less than 42,000. This total denier has been found to allow the formation of a tubular element 4 which is not too dense.
  • the total denier is at least 20,000, more preferably at least 25,000.
  • the filamentary tow forming the hollow tubular element 4 has a total denier between 25,000 and 45,000, more preferably between 35,000 and 45,000.
  • the cross-sectional shape of the filaments of tow are ⁇ ’ shaped, although in other embodiments other shapes such as ‘X’ shaped filaments can be used.
  • the filamentary tow forming the hollow tubular element 4 preferably has a denier per filament of greater than 3.
  • the denier per filament has been found to allow the formation of a tubular element 4 which is not too dense.
  • the denier per filament is at least 4, more preferably at least 5.
  • the filamentary tow forming the hollow tubular element 4 has a denier per filament between 4 and 10, more preferably between 4 and 9.
  • the filamentary tow forming the hollow tubular element 4 has an 8Y40,ooo tow formed from cellulose acetate and comprising 18% plasticiser, for instance triacetin.
  • the hollow tubular element 4 preferably has an internal diameter of greater than 3.0mm. Smaller diameters than this can result in increasing the velocity of aerosol passing though the mouthpiece 2 to the consumers mouth more than is desirable, such that the aerosol becomes too warm, for instance reaching temperatures greater than 40°C or greater than 45°C. More preferably, the hollow tubular element 4 has an internal diameter of greater than 3.1mm, and still more preferably greater than 3.5mm or 3.6mm. In one embodiment, the internal diameter of the hollow tubular element 4 is about 3.9mm.
  • the hollow tubular element 4 preferably comprises from 15% to 22% by weight of plasticiser.
  • the plasticiser is preferably triacetin, although other plasticisers such as polyethelyne glycol (PEG) can be used. More preferably, the tubular element 4 comprises from 16% to 20% by weight of plasticiser, for instance about 17%, about 18% or about 19% plasticiser.
  • the hollow tubular element 4 is a first hollow tubular element 4 and the mouthpiece includes a second hollow tubular element 8, also referred to as a cooling element, upstream of the first hollow tubular element 4.
  • the second hollow tubular element 8 is upstream of, adjacent to and in an abutting relationship with the body of material 6.
  • the body of material 6 and second hollow tubular element 8 each define a substantially cylindrical overall outer shape and share a common longitudinal axis.
  • the second hollow tubular element 8 is formed from a plurality of layers of paper which are parallel wound, with butted seams, to form the tubular element 8.
  • first and second paper layers are provided in a two-ply tube, although in other examples 3, 4 or more paper layers can be used forming 3, 4 or more ply tubes.
  • Other constructions can be used, such as spirally wound layers of paper, cardboard tubes, tubes formed using a papier-mache type process, moulded or extruded plastic tubes or similar.
  • the second hollow tubular element 8 can also be formed using a stiff plug wrap and/ or tipping paper as the second plug wrap 9 and/or tipping paper 5 described herein, meaning that a separate tubular element is not required.
  • the stiff plug wrap and/or tipping paper is manufactured to have a rigidity that is sufficient to withstand the axial compressive forces and bending moments that might arise during manufacture and whilst the article 1 is in use.
  • the stiff plug wrap and/ or tipping paper can have a basis weight between 70 gsm and 120 gsm, more preferably between 80 gsm and 110 gsm. Additionally or alternatively, the stiff plug wrap and/or tipping paper can have a thickness between 80 pm and 200 pm, more preferably between too pm and 160 pm, or from 120 pm to 150 pm. It can be desirable for both the second plug wrap 9 and tipping paper 5 to have values in these ranges, to achieve an acceptable overall level of rigidity for the second hollow tubular element 8.
  • the second hollow tubular element 8 preferably has a wall thickness, which can be measured in the same way as that of the first hollow tubular element 4, of at least about too pm and up to about 1.5mm, preferably between 100 pm and 1 mm and more preferably between 150 pm and 500 pm, or about 300 pm. In the present example, the second hollow tubular element 8 has a wall thickness of about 290 pm.
  • the length of the second hollow tubular element 8 is less than about 50 mm. More preferably, the length of the second hollow tubular element 8 is less than about
  • the length of the second hollow tubular element 8 is less than about 30 mm. In addition, or as an alternative, the length of the second hollow tubular element 8 is preferably at least about 10 mm. Preferably, the length of the second hollow tubular element 8 is at least about 15 mm. In some preferred embodiments, the length of the second hollow tubular element 8 is from about 20 mm to about 30 mm, more preferably from about 22 mm to about 28 mm, even more preferably from about 24 to about 26 mm, most preferably about 25 mm. In the present example, the length of the second hollow tubular element 8 is 25 mm.
  • the second hollow tubular element 8 is located around and defines an air gap within the mouthpiece 2 which acts as a cooling segment.
  • the air gap provides a chamber through which heated volatilised components generated by the aerosol-generating material 3 flow.
  • the second hollow tubular element 8 is hollow to provide a chamber for aerosol accumulation yet rigid enough to withstand axial compressive forces and bending moments that might arise during manufacture and whilst the article 1 is in use.
  • the second hollow tubular element 8 provides a physical displacement between the aerosol-generating material 3 and the body of material 6. The physical displacement provided by the second hollow tubular element 8 will provide a thermal gradient across the length of the second hollow tubular element 8.
  • the mouthpiece 2 comprises a cavity having an internal volume greater than 450 mm3. Providing a cavity of at least this volume has been found to enable the formation of an improved aerosol.
  • a cavity size provides sufficient space within the mouthpiece 2 to allow heated volatilised components to cool, therefore allowing the exposure of the aerosol-generating material 3 to higher temperatures than would otherwise be possible, since they may result in an aerosol which is too warm.
  • the cavity is formed by the second hollow tubular element 8, but in alternative arrangements it could be formed within a different part of the mouthpiece 2.
  • the second hollow tubular element 8 can be configured to provide a temperature differential of at least 40 degrees Celsius between a heated volatilised component entering a first, upstream end of the second hollow tubular element 8 and a heated volatilised component exiting a second, downstream end of the second hollow tubular element 8.
  • the second hollow tubular element 8 is preferably configured to provide a temperature differential of at least 60 degrees Celsius, preferably at least 80 degrees Celsius and more preferably at least too degrees Celsius between a heated volatilised component entering a first, upstream end of the second hollow tubular element 8 and a heated volatilised component exiting a second, downstream end of the second hollow tubular element 8. This temperature differential across the length of the second hollow tubular element 8 protects the temperature sensitive body of material 6 from the high temperatures of the aerosol-generating material 3 when it is heated.
  • the second hollow tubular element 8 can be replaced with an alternative cooling element, for instance an element formed from a body of material which allows aerosol to pass through it longitudinally, and which also performs the function of cooling the aerosol.
  • an alternative cooling element for instance an element formed from a body of material which allows aerosol to pass through it longitudinally, and which also performs the function of cooling the aerosol.
  • the first hollow tubular element 4, body of material 6 and second hollow tubular element 8 are combined using a second plug wrap 9 which is wrapped around all three sections.
  • the second plug wrap 9 has a basis weight of less than 50 gsm, more preferably between about 20 gsm and 45 gsm.
  • the second plug wrap 9 has a thickness of between 30 pm and 60 pm, more preferably between 35 pm and 45 pm.
  • the second plug wrap 9 is preferably a non- porous plug wrap having a permeability of less than too Coresta Units, for instance less than 50 Coresta Units.
  • the second plug wrap 9 can be a porous plug wrap, for instance having a permeability of greater than 200
  • the aerosol-generating material 3 is wrapped in a wrapper 10.
  • the wrapper 10 can, for instance, be a paper or paper-backed foil wrapper.
  • the wrapper 10 is substantially impermeable to air.
  • the wrapper 10 preferably has a permeability of less than too Coresta Units, more preferably less than 60 Coresta Units. It has been found that low permeability wrappers, for instance having a permeability of less than 100 Coresta Units, more preferably less than 60 Coresta Units, result in an improvement in the aerosol formation in the aerosol-generating material 3. Without wishing to be bound by theory, it is hypothesised that this is due to reduced loss of aerosol compounds through the wrapper 10.
  • the permeability of the wrapper 10 can be measured in accordance with ISO 2965:2009 concerning the determination of air permeability for materials used as cigarette papers, filter plug wrap and filter joining paper.
  • the wrapper 10 comprises aluminium foil. Aluminium foil has been found to be particularly effective at enhancing the formation of aerosol within the aerosol-generating material 3.
  • the aluminium foil has a metal layer having a thickness of about 6 pm.
  • the aluminium foil has a paper backing.
  • the aluminium foil can be other thicknesses, for instance between 4 pm and 16 pm in thickness.
  • the aluminium foil also need not have a paper backing, but could have a backing formed from other materials, for instance to help provide an appropriate tensile strength to the foil, or it could have no backing material.
  • Metallic layers or foils other than aluminium can also be used.
  • the total thickness of the wrapper is preferably between 20 pm and 60 pm, more preferably between 30 pm and 50 pm, which can provide a wrapper having appropriate structural integrity and heat transfer characteristics.
  • the tensile force which can be applied to the wrapper before it breaks can be greater than 3,000 grams force, for instance between 3,000 and 10,000 grams force or between 3,000 and 4,500 grams force.
  • the article has a ventilation level of about 75% of the aerosol drawn through the article.
  • the article can have a ventilation level of between 50% and 80% of aerosol drawn through the article, for instance between 65% and 75%.
  • the standard deviation in the level of ventilation in a batch of articles produced according to the present disclosure is less than 5%, or less than 4% or less than 3%.
  • a batch refers to at least 10 articles produced to the same specification.
  • those articles provided in a pack of articles can be used as basis for the measurements.
  • Such standard deviations can be achieved due to the improved blending of the tobacco material and amorphous solid material in aerosol-generating material produced according to the present invention, since the improved blend can result in a more consistent packing of the aerosol-generating material in the articles.
  • Ventilation at these levels helps to slow down the flow of aerosol drawn through the mouthpiece 2 and thereby enable the aerosol to cool sufficiently before it reaches the downstream end 2b of the mouthpiece 2.
  • the ventilation is provided directly into the mouthpiece 2 of the article 1.
  • the ventilation is provided into the second hollow tubular element 8, which has been found to be particularly beneficial in assisting with the aerosol generation process.
  • the ventilation is provided via first and second parallel rows of perforations 12, in the present case formed as laser perforations, at positions 17.925 mm and 18.625 mm respectively from the downstream, mouth-end 2b of the mouthpiece 2. These perforations pass though the tipping paper 5, second plug wrap 9 and second hollow tubular element 8.
  • the ventilation can be provided into the mouthpiece at other locations, for instance into the body of material 6 or first tubular element 4.
  • the volume of aerosol-generating material 3 provided can vary from about 200 mm3 to about 4300 mm3, preferably from about 500 mm3 to 1500 mm3, more preferably from about 1000 mm3 to about 1300 mm3.
  • the provision of these volumes of aerosol generating material, for instance from about 1000 mm3 to about 1300 mm3, has been advantageously shown to achieve a superior aerosol, having a greater visibility and sensory performance compared to that achieved with volumes selected from the lower end of the range.
  • the mass of aerosol-generating material 3 provided can be greater than 200 mg, for instance from about 200 mg to 400 mg, preferably from about 230 mg to 360 mg, more preferably from about 250 mg to 360 mg. It has been advantageously found that providing a higher mass of aerosol-generating material results in improved sensory performance compared to aerosol generated from a lower mass of tobacco material.
  • Figure 2a is a side-on cross sectional view of a further article i’ including a capsule- containing mouthpiece 2’.
  • Figure 2b is a cross sectional view of the capsule-containing mouthpiece shown in Figure 2a through the line A- A’ thereof.
  • Article 1’ and capsule- containing mouthpiece 2’ are the same as the article 1 and mouthpiece 2 illustrated in Figure 1, except that an aerosol modifying agent is provided within the body of material 6, in the present example in the form of a capsule 11, and that an oil-resistant first plug wrap 7’ surrounds the body of material 6.
  • the aerosol modifying agent can be provided in other forms, such as material injected into the body of material 6 or provided on a thread, for instance the thread carrying a flavourant or other aerosol modifying agent, which may also be disposed within the body of material
  • the capsule 11 can comprise a breakable capsule, for instance a capsule which has a solid, frangible shell surrounding a liquid payload. In the present example, a single capsule 11 is used. The capsule 11 is entirely embedded within the body of material 6.
  • the capsule 11 is completely surrounded by the material forming the body 6.
  • a plurality of breakable capsules maybe disposed within the body of material 6, for instance 2, 3 or more breakable capsules.
  • the length of the body of material 6 can be increased to accommodate the number of capsules required.
  • the individual capsules may be the same as each other, or may differ from one another in terms of size and/or capsule payload.
  • multiple bodies of material 6 may be provided, with each body containing one or more capsules.
  • the capsule 11 has a core-shell structure.
  • the capsule 11 comprises a shell encapsulating a liquid agent, for instance a flavourant or other agent, which can be any one of the flavourants or aerosol modifying agents described herein.
  • the shell of the capsule can be ruptured by a user to release the flavourant or other agent into the body of material 6.
  • the first plug wrap 7’ can comprise a barrier coating to make the material of the plug wrap substantially impermeable to the liquid payload of the capsule 11.
  • the second plug wrap 9 and/or tipping paper 5 can comprise a barrier coating to make the material of that plug wrap and/or tipping paper substantially impermeable to the liquid payload of the capsule 11.
  • the capsule 11 is spherical and has a diameter of about 3 mm.
  • the total weight of the capsule 11 may be in the range about 10 mg to about 50 mg.
  • the capsule 11 is located at a longitudinally central position within the body of material 6. That is, the capsule 11 is positioned so that its centre is 4 mm from each end of the body of material 6.
  • the capsule 11 can be located at a position other than a longitudinally central position in the body of material 6, i.e. closer to the downstream end of the body of material 6 than the upstream end, or closer to the upstream end of the body of material 6 than the downstream end.
  • the mouthpiece 2’ is configured so that the capsule 11 and the ventilation holes 12 are longitudinally offset from each other in the mouthpiece 2’.
  • FIG. 2b A cross section of the mouthpiece 2’ is shown in Figure 2b, this being taken through line A- A’ of Figure 2a.
  • Figure 2b shows the capsule 11, the body of material 6, the first and second plug wraps 7’, 9 and the tipping paper 5.
  • the capsule 11 is centred on the longitudinal axis (not shown) of the mouthpiece 2’.
  • the first and second plug wraps 7’, 9 and tipping 5 are arranged concentrically around the body of material 6.
  • the breakable capsule 11 has a core-shell structure. That is, the encapsulating material or barrier material creates a shell around a core that comprises the aerosol modifying agent.
  • the shell structure hinders migration of the aerosol modifying agent during storage of the article 1’ but allows controlled release of the aerosol modifying agent, also referred to as an aerosol modifier, during use.
  • the barrier material (also referred to herein as the encapsulating material) is frangible.
  • the capsule is crushed or otherwise fractured or broken by the user to release the encapsulated aerosol modifier. Typically, the capsule is broken immediately prior to heating being initiated but the user can select when to release the aerosol modifier.
  • breakable capsule refers to a capsule, wherein the shell can be broken by means of a pressure to release the core; more specifically the shell can be ruptured under the pressure imposed by the user's fingers when the user wants to release the core of the capsule.
  • the barrier material is heat resistant. That is to say, in some cases, the barrier will not rupture, melt or otherwise fail at the temperature reached at the capsule site during operation of the aerosol provision device.
  • a capsule located in a mouthpiece maybe exposed to temperatures in the range of 30°C to ioo°C for example, and the barrier material may continue to retain the liquid core up to at least about 50°C to 120°C.
  • the capsule releases the core composition on heating, for example by melting of the barrier material or by capsule swelling leading to rupture of the barrier material.
  • the total weight of a capsule may be in the range of about 1 mg to about too mg, suitably about 5 mg to about 60 mg, about 8 mg to about 50 mg, about 10 mg to about 20 mg, or about 12 mg to about 18 mg.
  • the total weight of the core formulation may be in the range of about 2 mg to about 90 mg, suitably about 3 mg to about 70 mg, about 5 mg to about 25 mg, about 8 mg to about 20 mg, or about 10 mg to about 15 mg.
  • the capsule according to the invention comprises a core as described above, and a shell.
  • the capsules may present a crush strength from about 4.5 N to about 40 N, more preferably from about 5 N to about 30 N or to about 28 N (for instance about 9.8 N to about 24.5 N).
  • the capsule burst strength can be measured when the capsule is removed from the body of material 6 and using a force gauge to measure the force at which the capsule bursts when pressed between two flat metal plates.
  • a suitable measurement device is the Sauter FK 50 force gauge with a flat headed attachment, which can be used to crush the capsule against a flat, hard surface having a surface similar to the attachment.
  • the capsules may be substantially spherical and have a diameter of at least about 0.4 mm, 0.6 mm, 0.8 mm, 1.0 mm, 2.0 mm, 2.5 mm, 2.8 mm or 3.0 mm.
  • the diameter of the capsules maybe less than about 10.0 mm, 8.0 mm, 7.0 mm, 6.0 mm, 5.5 mm, 5.0 mm, 4.5 mm, 4.0 mm, 3.5 mm or 3.2 mm.
  • the capsule diameter maybe in the range of about 0.4 mm to about 10.0 mm, about 0.8 mm to about 6.0 mm, about 2.5 mm to about 5.5 mm or about 2.8 mm to about 3.2 mm. In some cases, the capsule may have a diameter of about 3.0 mm. These sizes are particularly suitable for incorporation of the capsule into an article as described herein.
  • the cross-sectional area of the capsule 11 at its largest cross sectional area is in some embodiments less than 28% of the cross sectional area of the portion of the mouthpiece
  • the capsule 11 in which the capsule 11 is provided, more preferably less than 27% and still more preferably less than 25%.
  • the largest cross sectional area of the capsule is 7.07 mm 2 .
  • the body of material 6 has an outer circumference of 20.8 mm, and the radius of this component will be 3.31 mm, corresponding to a cross sectional area of 34.43 mm 2 .
  • the capsule cross sectional area is, in this example, 20.5% of the cross-sectional area of the mouthpiece 2’.
  • the capsule had a diameter of 3.2mm its largest cross sectional area would be 8.04 mm 2 .
  • the cross sectional area of the capsule would be 23.4% of the cross sectional area of the body of material 6.
  • a capsule with a largest cross sectional area less than 28% of the cross sectional area of the portion of the mouthpiece 2’ in which the capsule 11 is provided has the advantage that the pressure drop across the mouthpiece 2’ is reduced as compared to capsules with larger cross sectional areas and adequate space remains around the capsule for aerosol to pass without the body of material 6 removing significant amounts of the aerosol mass as it passes through the mouthpiece 2’.
  • the pressure drop or difference (also referred to a resistance to draw) across the article reduces by less than 8 mmH 2 0 when the capsule is broken. More preferably, the open pressure drop reduces by less than 6 mmH 2 0 and more preferably less than 5 mmH 2 0. These values are measured as the average achieved by at least 80 articles made to the same design. Such small changes in pressure drop mean that other aspects of the product design, such as setting the correct ventilation level for a given product pressure drop, can be achieved irrespective of whether or not the consumer chooses to break the capsule.
  • the barrier material may comprise one or more of a gelling agent, a bulking agent, a buffer, a colouring agent and a plasticiser.
  • the gelling agent of the capsule may be, for example, a polysaccharide or cellulosic gelling agent, a gelatin, a gum, a gel, a wax or a mixture thereof.
  • Suitable polysaccharides include alginates, dextrans, maltodextrins, cyclodextrins and pectins.
  • Suitable alginates include, for instance, a salt of alginic acid, an esterified alginate or glyceryl alginate.
  • Salts of alginic acid include ammonium alginate, triethanolamine alginate, and group I or II metal ion alginates like sodium, potassium, calcium and magnesium alginate.
  • Esterified alginates include propylene glycol alginate and glyceryl alginate.
  • the barrier material is sodium alginate and/ or calcium alginate.
  • Suitable cellulosic materials include methyl cellulose, ethyl cellulose, hydroxyethyl cellulose, hydroxypropyl cellulose, carboxymethyl cellulose, cellulose acetate and cellulose ethers.
  • the gelling agent may comprise one or more modified starches.
  • the gelling agent may comprise carrageenans.
  • Suitable gums include agar, gellan gum, gum Arabic, pullulan gum, mannan gum, gum ghatti, gum tragacanth, Karaya, locust bean, acacia gum, guar, quince seed and xanthan gums.
  • Suitable gels include agar, agarose, carrageenans, furoidan and furcellaran.
  • Suitable waxes include carnauba wax.
  • the gelling agent may comprise carrageenans and/ or gellan gum; these gelling agents are particularly suitable for inclusion as the gelling agent as the pressure required to break the resulting capsules is particularly suitable.
  • the barrier material may comprise one or more bulking agents, such as starches, modified starches (such as oxidised starches) and sugar alcohols such as maltitol.
  • the barrier material may comprise a colouring agent which renders easier the location of the capsule within the aerosol generating device during the manufacturing process of the aerosol generating device.
  • the colouring agent is preferably chosen among colorants and pigments.
  • the barrier material may further comprise at least one buffer, such as a citrate or phosphate compound.
  • the barrier material may further comprise at least one plasticiser, which may be glycerol, sorbitol, maltitol, triacetin, polyethylene glycol, propylene glycol or another polyalcohol with plasticising properties, and optionally one acid of the monoacid, diacid or triacid type, especially citric acid, fumaric acid, malic acid, and the like.
  • the amount of plasticiser ranges from 1% to 30% by weight, preferably from 2% to 15% by weight, and even more preferably from 3 to 10% by weight of the total dry weight of the shell.
  • the barrier material may also comprise one or more filler materials.
  • Suitable filler materials include comprising starch derivatives such as dextrin, maltodextrin, cyclodextrin (alpha, beta or gamma), or cellulose derivatives such as hydroxypropyl- methylcellulose (HPMC), hydroxypropylcellulose (HPC), methylcellulose (MC), carboxy-methylcellulose (CMC), polyvinyl alcohol, polyols or mixture thereof.
  • Dextrin is a preferred filler.
  • the amount of filler in the shell is at most 98.5%, preferably from 25 to 95% more preferably from 40 to 80% and even more preferably from 50 to 60 % by weight on the total dry weight of the shell.
  • the capsule shell may additionally comprise a hydrophobic outer layer which reduces the susceptibility of the capsule to moisture-induced degradation.
  • the hydrophobic outer layer is suitably selected from the group comprising waxes, especially carnauba wax, candelilla wax or beeswax, carbowax, shellac (in alcoholic or aqueous solution), ethyl cellulose, hydroxypropyl methyl cellulose, hydroxyl- propylcellulose, latex composition, polyvinyl alcohol, or a combination thereof. More preferably, the at least one moisture barrier agent is ethyl cellulose or a mixture of ethyl cellulose and shellac.
  • the capsule core comprises the aerosol modifier.
  • This aerosol modifier may be any volatile substance which modifies at least one property of the aerosol.
  • the aerosol substance may modify the pH, the sensorial properties, the water content, the delivery characteristics or the flavour.
  • the aerosol modifier may be selected from an acid, a base, water or a flavourant.
  • the aerosol modifier comprises one or more flavourants.
  • the flavourant may suitably be licorice, rose oil, vanilla, lemon oil, orange oil, a mint- flavour, suitably menthol and/or a mint oil from any species of the genus Mentha such as peppermint oil and/or spearmint oil, or lavender, fennel or anise.
  • the flavourant comprises menthol.
  • the capsule may comprise at least about 25% w/w flavourant (based on the total weight of the capsule), suitably at least about 30% w/w flavourant, 35% w/w flavourant, 40% w/w flavourant, 45% w/w flavourant or 50% w/w flavourant.
  • the core may comprise at least about 25% w/w flavourant (based on the total weight of the core), suitably at least about 30% w/w flavourant, 35% w/w flavourant, 40% w/w flavourant, 45% w/w flavourant or 50% w/w flavourant.
  • the core may comprise less than or equal to about 75% w/w flavourant (based on the total weight of the core), suitably less than or equal to about 65% w/w flavourant, 55% w/w flavourant, or 50% w/w flavourant.
  • the capsule may include an amount of flavourant in the range of 25-75% w/w (based on the total weight of the core), about 35-60% w/w or about 40-55% w/w.
  • the capsules may include at least about 2 mg, 3 mg or 4 mg of the aerosol modifier, suitably at least about 4.5 mg of the aerosol modifier, 5 mg of the aerosol modifier, 5.5 mg of the aerosol modifier or 6 mg of the aerosol modifier.
  • the consumable comprises at least about 7 mg of the aerosol modifier, suitably at least about 8 mg of the aerosol modifier, 10 mg of the aerosol modifier, 12 mg of the aerosol modifier or 15 mg of the aerosol modifier.
  • the core may also comprise a solvent which dissolves the aerosol modifier.
  • Any suitable solvent may be used.
  • the solvent may suitably comprise short or medium chain fats and oils.
  • the solvent may comprise tri-esters of glycerol such as C2-C12 triglycerides, suitably C6-C10 triglycerides or Cs- C12 triglycerides.
  • the solvent may comprise medium chain triglycerides (MCT - C8-C12), which may be derived from palm oil and/ or coconut oil.
  • the esters maybe formed with caprylic acid and/or capric acid.
  • the solvent may comprise medium chain triglycerides which are caprylic triglycerides and/or capric tryglycerides.
  • the solvent may comprise compounds identified in the CAS registry by numbers 73398-61-5, 65381-09-1, 85409-09-2. Such medium chain triglycerides are odourless and tasteless.
  • the hydrophilic-lipophilic balance (HLB) of the solvent may be in the range of 9 to 13, suitably 10 to 12.
  • Methods of making the capsules include co-extrusion, optionally followed by centrifugation and curing and/ or drying.
  • the contents of WO 2007/ 010407 A2 is incorporated by reference, in its entirety.
  • the mouthpieces 2, 2’ each comprise a single body of material 6.
  • either the mouthpiece of Figure 1 or of Figures 2a and 2b may include multiple bodies of material.
  • the mouthpieces 2, 2’ may comprise a cavity between the bodies of material.
  • Transfer of the aerosol modifying agent or other sensate material to the consumer’s lips during use of the article may modify the organoleptic properties (e.g. taste) of the aerosol generated by the aerosol generating substrate 3 or otherwise provide the consumer with an alternative sensory experience.
  • the aerosol modifying agent or other sensate material may impart flavour to the aerosol generated by the aerosol generating substrate 3.
  • the aerosol modifying agent or other sensate material maybe at least partially soluble in water such that it is transferred to the user via the consumer’s saliva.
  • the aerosol modifying agent or other sensate material may be one that volatilises by the heat generated by the aerosol provision system. This may facilitate transfer of the aerosol modifying agent to the aerosol generated by the aerosol generating substrate 3.
  • a suitable sensate material may be a flavour as described herein, sucralose or a cooling agent such as menthol or similar.
  • a pack can be provided comprising a plurality of articles as described herein.
  • the number of the plurality of strips of amorphous solid material in each article can vary by less than 40% between the articles in the pack, or less than 30% between the articles in the pack, or less than 20% between the articles in the pack.
  • the plurality of strips of amorphous solid material in each article in a pack can comprise a flavourant, and the delivery of the flavourant from each of the plurality of articles, in use, varies by less than 50% between the articles in the pack, or varies by less than 20% between the articles in the pack.
  • the standard deviation in the inclusion level of the flavourant by percentage weight between articles in the pack maybe less than 50%, or less than 30%, or less than 20%, for instance between 5% and 50%, or between 5% and 30%, or between 10% and 25% of the mean.
  • the flavourant level may be determined by chemical analysis as known to those skilled in the art, and the standard deviation may be determined for a batch of at least 10 articles, for instance a pack of articles.
  • Figure 3 shows an example of a non-combustible aerosol provision device 100 for generating aerosol from an aerosol generating medium/material such as the aerosol generating material 3 of the articles 1, T described herein.
  • the device too maybe used to heat a replaceable article 110 comprising the aerosol generating medium, for instance the articles 1, 1’ described herein, to generate an aerosol or other inhalable medium which is inhaled by a user of the device too.
  • the device too and replaceable article 110 together form a system.
  • the device too comprises a housing 102 (in the form of an outer cover) which surrounds and houses various components of the device too.
  • the device too has an opening 104 in one end, through which the article 110 maybe inserted for heating by a heating assembly. In use, the article 110 may be fully or partially inserted into the heating assembly where it may be heated by one or more components of the heater assembly.
  • the device too of this example comprises a first end member 106 which comprises a lid 108 which is moveable relative to the first end member 106 to close the opening 104 when no article 110 is in place.
  • the lid 108 is shown in an open configuration, however the lid 108 may move into a closed configuration.
  • a user may cause the lid 108 to slide in the direction of arrow “B”.
  • the device too may also include a user-operable control element 112, such as a button or switch, which operates the device too when pressed. For example, a user may turn on the device too by operating the switch 112.
  • the device too may also comprise an electrical component, such as a socket/port 114, which can receive a cable to charge a battery of the device too.
  • the socket 114 may be a charging port, such as a USB charging port.
  • Figure 4 depicts the device 100 of Figure 3 with the outer cover 102 removed and without an article 110 present.
  • the device 100 defines a longitudinal axis 134.
  • the first end member 106 is arranged at one end of the device 100 and a second end member 116 is arranged at an opposite end of the device 100.
  • the first and second end members 106, 116 together at least partially define end surfaces of the device 100.
  • the bottom surface of the second end member 116 at least partially defines a bottom surface of the device 100.
  • Edges of the outer cover 102 may also define a portion of the end surfaces.
  • the lid 108 also defines a portion of a top surface of the device 100.
  • the end of the device closest to the opening 104 may be known as the proximal end (or mouth end) of the device 100 because, in use, it is closest to the mouth of the user.
  • a user inserts an article 110 into the opening 104, operates the user control 112 to begin heating the aerosol generating material and draws on the aerosol generated in the device. This causes the aerosol to flow through the device too along a flow path towards the proximal end of the device too.
  • the other end of the device furthest away from the opening 104 may be known as the distal end of the device too because, in use, it is the end furthest away from the mouth of the user. As a user draws on the aerosol generated in the device, the aerosol flows away from the distal end of the device too.
  • the power source 118 maybe, for example, a battery, such as a rechargeable battery or a non-rechargeable battery.
  • suitable batteries include, for example, a lithium battery (such as a lithium-ion battery), a nickel battery (such as a nickel-cadmium battery), and an alkaline battery.
  • the battery is electrically coupled to the heating assembly to supply electrical power when required and under control of a controller (not shown) to heat the aerosol generating material.
  • the battery is connected to a central support 120 which holds the battery 118 in place.
  • the device further comprises at least one electronics module 122.
  • the electronics module 122 may comprise, for example, a printed circuit board (PCB).
  • the PCB 122 may support at least one controller, such as a processor, and memory.
  • the PCB 122 may also comprise one or more electrical tracks to electrically connect together various electronic components of the device 100.
  • the battery terminals maybe electrically connected to the PCB 122 so that power can be distributed throughout the device 100.
  • the socket 114 may also be electrically coupled to the battery via the electrical tracks.
  • the heating assembly is an inductive heating assembly and comprises various components to heat the aerosol generating material of the article 110 via an inductive heating process.
  • Induction heating is a process of heating an electrically conducting object (such as a susceptor) by electromagnetic induction.
  • An induction heating assembly may comprise an inductive element, for example, one or more inductor coils, and a device for passing a varying electric current, such as an alternating electric current, through the inductive element.
  • the varying electric current in the inductive element produces a varying magnetic field.
  • the varying magnetic field penetrates a susceptor suitably positioned with respect to the inductive element, and generates eddy currents inside the susceptor.
  • the susceptor has electrical resistance to the eddy currents, and hence the flow of the eddy currents against this resistance causes the susceptor to be heated by Joule heating.
  • the susceptor comprises ferromagnetic material such as iron, nickel or cobalt
  • heat may also be generated by magnetic hysteresis losses in the susceptor, i.e. by the varying orientation of magnetic dipoles in the magnetic material as a result of their alignment with the varying magnetic field.
  • inductive heating as compared to heating by conduction for example, heat is generated inside the susceptor, allowing for rapid heating. Further, there need not be any physical contact between the inductive heater and the susceptor, allowing for enhanced freedom in construction and application.
  • the induction heating assembly of the example device too comprises a susceptor arrangement 132 (herein referred to as “a susceptor”), a first inductor coil 124 and a second inductor coil 126.
  • the first and second inductor coils 124, 126 are made from an electrically conducting material.
  • the first and second inductor coils 124, 126 are made from Litz wire/cable which is wound in a helical fashion to provide helical inductor coils 124, 126.
  • Litz wire comprises a plurality of individual wires which are individually insulated and are twisted together to form a single wire. Litz wires are designed to reduce the skin effect losses in a conductor.
  • the first and second inductor coils 124, 126 are made from copper Litz wire which has a rectangular cross section. In other examples the Litz wire can have other shape cross sections, such as circular.
  • the first inductor coil 124 is configured to generate a first varying magnetic field for heating a first section of the susceptor 132 and the second inductor coil 126 is configured to generate a second varying magnetic field for heating a second section of the susceptor 132.
  • the first inductor coil 124 is adjacent to the second inductor coil 126 in a direction along the longitudinal axis 134 of the device 100 (that is, the first and second inductor coils 124, 126 to not overlap).
  • the susceptor arrangement 132 may comprise a single susceptor, or two or more separate susceptors. Ends 130 of the first and second inductor coils 124, 126 can be connected to the PCB 122.
  • first and second inductor coils 124, 126 may have at least one characteristic different from each other.
  • the first inductor coil 124 may have at least one characteristic different from the second inductor coil 126.
  • the first inductor coil 124 may have a different value of inductance than the second inductor coil 126.
  • the first and second inductor coils 124, 126 are of different lengths such that the first inductor coil 124 is wound over a smaller section of the susceptor 132 than the second inductor coil 126.
  • the first inductor coil 124 may comprise a different number of turns than the second inductor coil 126 (assuming that the spacing between individual turns is substantially the same).
  • the first inductor coil 124 may be made from a different material to the second inductor coil 126.
  • the first and second inductor coils 124, 126 may be substantially identical.
  • the first inductor coil 124 and the second inductor coil 126 are wound in opposite directions. This can be useful when the inductor coils are active at different times. For example, initially, the first inductor coil 124 may be operating to heat a first section/portion of the article 110, and at a later time, the second inductor coil 126 may be operating to heat a second section/portion of the article 110. Winding the coils in opposite directions helps reduce the current induced in the inactive coil when used in conjunction with a particular type of control circuit. In Figure 4, the first inductor coil 124 is a right-hand helix and the second inductor coil 126 is a left-hand helix.
  • the inductor coils 124, 126 may be wound in the same direction, or the first inductor coil 124 may be a left-hand helix and the second inductor coil 126 may be a right-hand helix.
  • the susceptor 132 of this example is hollow and therefore defines a receptacle within which aerosol generating material is received.
  • the article 110 can be inserted into the susceptor 132.
  • the susceptor 120 is tubular, with a circular cross section.
  • the first and second materials maybe adjacent along an axis defined by the susceptor 132, or may form different layers within the susceptor 132.
  • the second section may comprise third and fourth materials, where the third and fourth materials can be heated differently based upon operation of the second inductor coil 126.
  • the third and fourth materials maybe adjacent along an axis defined by the susceptor 132, or may form different layers within the susceptor 132.
  • Third material may the same as the first material, and the fourth material may be the same as the second material, for example. Alternatively, each of the materials may be different.
  • the susceptor may comprise carbon steel or aluminium for example.
  • the device too of Figure 4 further comprises an insulating member 128 which may be generally tubular and at least partially surround the susceptor 132.
  • the insulating member 128 may be constructed from any insulating material, such as plastic for example.
  • the insulating member is constructed from polyether ether ketone (PEEK).
  • PEEK polyether ether ketone
  • the insulating member 128 can also fully or partially support the first and second inductor coils 124, 126.
  • the first and second inductor coils 124, 126 are positioned around the insulating member 128 and are in contact with a radially outward surface of the insulating member 128.
  • the insulating member 128 does not abut the first and second inductor coils 124, 126.
  • a small gap may be present between the outer surface of the insulating member 128 and the inner surface of the first and second inductor coils 124, 126.
  • the susceptor 132, the insulating member 128, and the first and second inductor coils 124, 126 are coaxial around a central longitudinal axis of the susceptor 132.
  • Figure 5 shows a side view of device 100 in partial cross-section.
  • the outer cover 102 is present in this example.
  • the rectangular cross-sectional shape of the first and second inductor coils 124, 126 is more clearly visible.
  • the device too further comprises a support 136 which engages one end of the susceptor 132 to hold the susceptor 132 in place.
  • the support 136 is connected to the second end member 116.
  • the device may also comprise a second printed circuit board 138 associated within the control element 112.
  • the device too further comprises a second lid/cap 140 and a spring 142, arranged towards the distal end of the device too.
  • the spring 142 allows the second lid 140 to be opened, to provide access to the susceptor 132.
  • a user may open the second lid 140 to clean the susceptor 132 and/ or the support 136.
  • the device too further comprises an expansion chamber 144 which extends away from a proximal end of the susceptor 132 towards the opening 104 of the device. Located at least partially within the expansion chamber 144 is a retention clip 146 to abut and hold the article 110 when received within the device too.
  • the expansion chamber 144 is connected to the end member 106.
  • Figure 6 is an exploded view of the device too of Figure 5, with the outer cover 102 omitted.
  • Figure 7A depicts a cross section of a portion of the device 100 of Figure 5.
  • Figure 7B depicts a close-up of a region of Figure 7A.
  • Figures 7A and 7B show the article 110 received within the susceptor 132, where the article 110 is dimensioned so that the outer surface of the article 110 abuts the inner surface of the susceptor 132. This ensures that the heating is most efficient.
  • the article 110 of this example comprises aerosol generating material 110a.
  • the aerosol generating material 110a is positioned within the susceptor 132.
  • the article 110 may also comprise other components such as a filter, wrapping materials and/ or a cooling structure.
  • Figure 7B shows that the outer surface of the susceptor 132 is spaced apart from the inner surface of the inductor coils 124, 126 by a distance 150, measured in a direction perpendicular to a longitudinal axis 158 of the susceptor 132.
  • the distance 150 is about 3mm to 4mm, about 3-3-5mm, or about 3.25mm.
  • Figure 7B further shows that the outer surface of the insulating member 128 is spaced apart from the inner surface of the inductor coils 124, 126 by a distance 152, measured in a direction perpendicular to a longitudinal axis 158 of the susceptor 132.
  • the distance 152 is about 0.05mm.
  • the distance 152 is substantially omm, such that the inductor coils 124, 126 abut and touch the insulating member 128.
  • the susceptor 132 has a wall thickness 154 of about 0.025mm to imm, or about 0.05mm. In one example, the susceptor 132 has a length of about 40mm to 60mm, about 40mm to 45mm, or about 44.5mm.
  • the insulating member 128 has a wall thickness 156 of about 0.25mm to 2mm, 0.25mm to imm, or about 0.5mm.
  • the articles 1, 1’ described herein can be inserted into a non-combustible aerosol provision device such as the device too described with reference to Figures 3 to 7. At least a portion of the mouthpiece 2, 2’ of the article 1, 1’ protrudes from the non combustible aerosol provision device too and can be placed into a user’s mouth.
  • An aerosol is produced by heating the aerosol generating material 3 using the device too. The aerosol produced by the aerosol-generating material 3 passes through the mouthpiece 2 to the user’s mouth.
  • Figure 8 illustrates a first method of manufacturing an aerosol-generating material, for instance and aerosol-generating material for use in an article for use in a non combustible aerosol provision system.
  • a single thickness of amorphous solid material in sheet form is fed into a shredding apparatus.
  • This can be achieved, for example, by providing a bobbin of amorphous solid sheet material which can be continuously fed into a shredding apparatus.
  • a discrete portion of amorphous solid material in sheet form such as a sheet known to those skilled in the art as a flag, can be fed into a shredding apparatus.
  • the inventors have surprisingly found that, in contrast to the conventional tobacco cutting process where several sheets of lamina material are fed to a cutting apparatus simultaneously, there are benefits for amorphous solid material in sheet form when shredded in single sheet thicknesses.
  • Feeding multiple thicknesses of amorphous solid sheet material into a shredding apparatus in a single pass tends to result in uneven distribution of the material in the final aerosol-generating material, as multiple thicknesses of the sheet material potentially adhere together, resulting in the formation of clumps.
  • multiple thicknesses of amorphous solid sheet material can be fed into a shredding apparatus in a single pass, for instance where the ‘tackiness’ of the amorphous solid sheet is relatively low, avoiding the formation of clumps.
  • said single thickness of amorphous solid material is shredded to obtain strips of amorphous solid material having a defined cut width.
  • the amorphous solid material maybe subject to a second cutting step, such as in a cross-cut type shredding process, to obtain a defined cut length.
  • a second cutting step such as in a cross-cut type shredding process
  • the strips of amorphous solid material obtained in step S102 are mixed with a tobacco material.
  • the inventors have advantageously found that mixing of the shredded amorphous solid material with a tobacco material should preferably be carried out as soon after step S102 as possible.
  • the inventors have found that prolonged storage of shredded amorphous solid material can result in clumps of amorphous solid shreds forming in the shredded material, such that when the shredded amorphous solid material is mixed with a tobacco material, and used to form articles as described herein, the clumps of amorphous solid material result in an uneven distribution of amorphous solid material between articles, and within individual rods of aerosol-generating material.
  • the shredded amorphous solid material is incorporated into the tobacco material fewer than 12 hours after the cutting step, for instance fewer than 6 hours, or fewer than 4 hours, or fewer than 2 hours, or fewer than 1 hour.
  • the shredded amorphous solid material may be fed into tobacco material in an online process, such that the time between shredding of the amorphous solid material and incorporation of the shredded material into a tobacco material to form the final aerosol-generating material may be less than 30 seconds, for instance less than 20 seconds, or less than 10 seconds.
  • a method of producing an aerosol-generating material comprises cutting a sheet of amorphous solid material to form a plurality of strips of amorphous solid material having a cut length of at least about 5 mm, or at least about 10 mm, or at least about 20 mm. In some embodiments, the method comprises cutting a sheet of amorphous solid material to form a plurality of strips of amorphous solid material each having a cut length of between about 5 mm and about 60 mm, or between about 10 mm and about 55 mm, or between about 20 mm and about 50 mm.
  • the mixing step can be performed using a rotary drum blender, for instance rotating at an RPM of 5 to 30 RPM, for instance 10 - 15RPM.
  • the drum diameter can be between 0.8m and 1.2m with 5 sets of 10 to 20 pins (optional) projecting from the inner walls of the drum towards the centre of the drum, the pins having a length of between 5% and 15% of the drum diameter, for instance about 10%, with the pins of each set spaced longitudinally along the length of the drum and each set spaced around the inner circumference.
  • the drum angle of its central axis during the mixing operation can be approximately 10 to 30 degrees from horizontal (open side up). Batches of 5 - 20 kg total solids, typically 8 - 10kg, can be mixed in such a drum, with a mixing time of 30 seconds to 10 minutes, for instance 30 seconds to 2 minutes.
  • the mixing step can be incorporated into the standard primary manufacturing process for tobacco material, for instance using the add-back line and a flavour mixing cylinder.
  • This method maybe suited to larger quantities of material.
  • a continuous rotary drum blender can be used, which is fed by two weigh conveyors, each feeding one component (tobacco material or cut amorphous solid material, such as shredded gel) at the correct relative kg/hr rate to achieve the desired inclusion level of amorphous solid in the aerosol-generating material.
  • the components are blended in the rotating drum blender during their passage, and collected at the exit.
  • Typical dimensions and operating conditions of a continuous rotary drum blender are an RPM of 12 - 15 RPM, a drum diameter of 0.6 - 0.8m, a drum length of 2.0 - 3.0 m.
  • FIG. 9 illustrates a second method of manufacturing an aerosol-generating material, for instance and aerosol-generating material for use in an article for use in a non combustible aerosol provision system.
  • the second method can be performed using equipment as described in relation to the first method above, and the skilled person would be aware that the steps of the first and second methods can be combined as appropriate.
  • the method includes a step (S201) of cutting a first portion of amorphous solid material to form a first component comprising a plurality of strips of amorphous solid material having a first length.
  • the method also includes a step (S202) of cutting a second portion of amorphous solid material to form a second component comprising a plurality of strips of amorphous solid material having a second length different to the first length.
  • step S203 the cut strips of amorphous solid material are mixed with a tobacco material comprising strips and/or strands of tobacco material.
  • Using two or more different lengths of amorphous solid material can enable the size of the strips of the amorphous solid material to more closely match the material size distribution of the tobacco material, resulting in better mixing of the amorphous solid and tobacco material.

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  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Manufacture Of Tobacco Products (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Medicinal Preparation (AREA)
  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)
  • Manufacturing Of Micro-Capsules (AREA)
  • Packaging Of Annular Or Rod-Shaped Articles, Wearing Apparel, Cassettes, Or The Like (AREA)
  • Packages (AREA)
PCT/GB2021/050222 2020-01-30 2021-02-01 Aerosol-generating material WO2021152334A1 (en)

Priority Applications (11)

Application Number Priority Date Filing Date Title
JP2022544808A JP2023511955A (ja) 2020-01-30 2021-02-01 エアロゾル生成材料
IL294813A IL294813A (en) 2020-01-30 2021-02-01 material for creating a spray
BR112022015248A BR112022015248A2 (pt) 2020-01-30 2021-02-01 Material gerador de aerossol, artigo, pacotes, consumível, sistema e métodos
KR1020227029503A KR20220130785A (ko) 2020-01-30 2021-02-01 에어로졸 생성 재료
EP21703544.3A EP4096443A1 (en) 2020-01-30 2021-02-01 Aerosol-generating material
AU2021213960A AU2021213960B2 (en) 2020-01-30 2021-02-01 Aerosol-generating material
US17/759,847 US20230143930A1 (en) 2020-01-30 2021-02-01 Aerosol-generating material
CA3164907A CA3164907A1 (en) 2020-01-30 2021-02-01 Aerosol-generating material
CN202180024436.2A CN115666277A (zh) 2020-01-30 2021-02-01 气溶胶发生材料
MX2022009211A MX2022009211A (es) 2020-01-30 2021-02-01 Material generador de aerosol.
JP2024079917A JP2024105585A (ja) 2020-01-30 2024-05-16 エアロゾル生成材料

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GBGB2001294.4A GB202001294D0 (en) 2020-01-30 2020-01-30 Aerosol-generating material
GB2001294.4 2020-01-30

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KR (1) KR20220130785A (ja)
CN (1) CN115666277A (ja)
AU (1) AU2021213960B2 (ja)
BR (1) BR112022015248A2 (ja)
CA (1) CA3164907A1 (ja)
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WO2023118855A1 (en) * 2021-12-20 2023-06-29 Nicoventures Trading Limited A consumable for use in an aerosol provision system
WO2023148484A3 (en) * 2022-02-03 2023-10-05 Nicoventures Trading Limited Method and apparatus for shredding a sheet of material

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CN115721040A (zh) * 2021-08-25 2023-03-03 上海烟草集团有限责任公司 一种再造烟叶以及再造烟叶的制造工艺
GB202303668D0 (en) * 2023-03-13 2023-04-26 Nicoventures Trading Ltd A consumable

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WO2023148484A3 (en) * 2022-02-03 2023-10-05 Nicoventures Trading Limited Method and apparatus for shredding a sheet of material

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CA3164907A1 (en) 2021-08-05
EP4096443A1 (en) 2022-12-07
KR20220130785A (ko) 2022-09-27
GB202001294D0 (en) 2020-03-18
BR112022015248A2 (pt) 2022-10-11
JP2024105585A (ja) 2024-08-06
US20230143930A1 (en) 2023-05-11
CN115666277A (zh) 2023-01-31
AU2021213960A1 (en) 2022-08-25
JP2023511955A (ja) 2023-03-23
IL294813A (en) 2022-09-01
MX2022009211A (es) 2022-08-17

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