WO2021082224A1 - Natural gas hydrate mineral fracturing experiment device - Google Patents

Natural gas hydrate mineral fracturing experiment device Download PDF

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Publication number
WO2021082224A1
WO2021082224A1 PCT/CN2019/126577 CN2019126577W WO2021082224A1 WO 2021082224 A1 WO2021082224 A1 WO 2021082224A1 CN 2019126577 W CN2019126577 W CN 2019126577W WO 2021082224 A1 WO2021082224 A1 WO 2021082224A1
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reactor
fracturing
cylinder
gas
valve
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PCT/CN2019/126577
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French (fr)
Chinese (zh)
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李栋梁
姚远欣
梁德青
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中国科学院广州能源研究所
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Publication of WO2021082224A1 publication Critical patent/WO2021082224A1/en

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/24Earth materials
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/08Investigating permeability, pore-volume, or surface area of porous materials
    • G01N15/082Investigating permeability by forcing a fluid through a sample
    • G01N15/0826Investigating permeability by forcing a fluid through a sample and measuring fluid flow rate, i.e. permeation rate or pressure change

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  • the invention relates to a fracturing experiment device for natural gas hydrate deposits.
  • the device is a device that can synthesize natural gas hydrate deposits in situ under high pressure and low temperature conditions, perform fracturing experiments on the deposits, and measure the permeability .
  • Natural gas hydrate is an ice-like solid formed by alkanes (such as methane, ethane, etc.) and water under certain high pressure and low temperature conditions. It is commonly known as combustible ice and is widely distributed below the surface of the tundra and under the seabed of the continental margin. In the sediment. The global reserves of natural gas hydrate are huge, equivalent to 210.5 billion tons of oil equivalent, which is twice the total carbon content of conventional fossil energy in the world, and is regarded as an important alternative energy source after the oil age.
  • the permeability of the reservoir will directly affect the flow rate of gas and water between the pores after the hydrate is decomposed. This in turn affects the efficiency of gas production and recovery, so increasing the permeability of the reservoir is of great significance to the commercial exploitation of natural gas hydrates.
  • the hydraulic fracturing stimulation technology in the reservoir reconstruction technology has been widely used in the oil and gas industry, which can greatly increase the permeability of oil and gas reservoirs and realize the increase in oil and gas production in low-permeability and ultra-low-permeability oil and gas fields. Since the low permeability of natural gas hydrate reservoirs is similar to that of low-permeability gas fields such as shale gas fields, in order to increase the production of natural gas in natural gas hydrate deposits, some studies are currently exploring the use of hydraulic fracturing to increase the permeability of hydrate reservoirs.
  • the present invention provides a fracturing experimental device for natural gas hydrate deposits.
  • a fracturing experiment device for natural gas hydrate deposits comprising a support and a reactor set on the support for synthesizing samples and fracturing and reforming them, and the reactor is provided with a sample synthesis system, a permeability testing system, and data An acquisition and control system.
  • the reactor is also provided with a hydraulic fracturing system for fracturing reformation.
  • the reactor includes a reactor cylinder and a reactor end cover arranged at one end of the reactor cylinder, the reactor cylinder is used to place a sample of hydrate sediment, and the sample synthesis system is arranged in the reactor.
  • the end of the cylinder is far away from the end cover of the reactor, the space between the sample synthesis system, the reactor cylinder and the end cover of the reactor forms an inner cavity, and a second is arranged between the end cover of the reactor and the hydrate sediment sample.
  • a water-permeable plate, and a second water-permeable plate is arranged between the sample synthesis system and the hydrate sediment sample.
  • the sample synthesis system includes a piston that abuts against the second water-permeable plate, a sealing plug arranged at an end of the reactor cylinder away from the end cover of the reactor, and a side of the reactor cylinder connected between the piston and the sealing plug.
  • the manual booster pump on the wall is provided with a booster valve between the manual booster pump and the reactor cylinder.
  • the permeability test system includes a first gas pipeline connected to the inner cavity of one end of the reactor end cover, a first constant pressure system connected to the first gas pipeline, and one end connected to the sample synthesis system
  • the first gas pipeline is provided with a first valve
  • the second gas pipeline is provided with a second valve
  • the first constant pressure system and the first gas pipeline support are provided with a constant pressure valve
  • the flow meter is connected with a flow valve
  • the first constant pressure system and A differential pressure sensor is connected between the second constant pressure system
  • the differential pressure sensor and the flow meter are both connected to the data acquisition and control system.
  • the permeability test system is also connected with an evacuation system and a gas cylinder for supplying gas to the reaction and providing gas for testing the permeability, and the evacuation system and the gas cylinder are both connected to the first gas pipeline, so A vacuum valve is arranged between the vacuum system and the first gas pipeline, and an air supply valve is arranged between the gas cylinder and the first gas pipeline.
  • the hydraulic fracturing system includes a hydraulic jet tube connected from the side wall of the reactor barrel to the inner cavity, and a fracturing pump system connected with the hydraulic jet tube.
  • the outlet direction of the hydraulic jet tube is the same as that of the reactor.
  • the axial directions of the reactor are consistent, the water jet pipe is provided with a sanding device, and a fracturing valve is provided between the sanding device and the side wall of the reactor cylinder.
  • the data acquisition and control system includes a computer and a temperature sensor and a pressure sensor connected to the computer, the temperature sensor is arranged on the end cover of the reactor to collect temperature parameter data inside the cavity, and the pressure sensor is connected It is set on the sample synthesis system, permeability testing system and hydraulic fracturing system to collect the pressure parameter data of each system.
  • the photographic lighting system also includes a photographic lighting system arranged on the side wall at the corresponding position of the inner cavity of the reactor barrel, and the photographic lighting system includes a side wall of the reactor barrel for observing the internal condition of the inner cavity.
  • the sapphire tube and the camera and illuminating lamp connected to the reactor tube body, the lens of the camera is directly facing the sapphire tube, so as to observe the internal situation of the inner cavity.
  • the present invention has the following advantages:
  • the invention can synthesize natural gas hydrate deposits in situ under high-pressure and low-temperature conditions, perform fracturing experiments on the deposits, and measure the permeability, which expands the scope of use of existing experimental testing devices and improves the accuracy of experimental testing And convenience.
  • the design of this application supports in-situ synthesis of hydrate sediment samples, can reasonably simulate reservoir stress and temperature and pressure conditions, and can more completely restore conventional hydraulic fracturing steps such as fluid injection, fracturing, and proppant addition.
  • Figure 1 is a schematic diagram of the overall connection structure of the fracturing experimental device for natural gas hydrate deposits
  • Fig. 2 is an enlarged schematic diagram of the connection structure of the permeability test system of part A in Fig. 1;
  • Fracturing pump system 53, Sand adding device; 54, Fracturing valve; 6.
  • Data acquisition And control system 61, computer; 62, temperature sensor; 63, pressure sensor; 7, photographic lighting system; 71, camera; 72, lighting; 73, sapphire tube.
  • an experimental device for fracturing a natural gas hydrate deposit includes a support 1 and a reactor 2 set on the support 1 for synthesizing samples and fracturing them.
  • the reactor 2 is equipped with a sample synthesis System 3, permeability test system 4, photographic lighting system 7 and data acquisition and control system 6.
  • the reactor 2 is also provided with a hydraulic fracturing system 5 for fracturing reformation.
  • the structure of the reactor 2 includes a reactor barrel 21 and a reactor end cover 22 arranged at one end of the reactor barrel 21.
  • the reactor barrel 21 is a cylindrical cylindrical structure and is vertically fixed on the support 1.
  • the reactor The end cap 22 is arranged on the top of the reactor cylinder 21, and the reactor cylinder 21 is used to place a hydrate sediment sample 23.
  • the reactor end cover 22 and the reactor cylinder 21 are fixedly connected by bolts, and the reactor cylinder 21 and the support 1 are fixedly connected by nuts and bolts to ensure that the reactor cylinder 21 is in the process of synthesizing samples and conducting permeability tests. And it can be kept fixed during hydraulic fracturing. Wheels are added to the bottom of the bracket 1 to facilitate the overall movement. In order to improve the stability of the device during use, the wheels can be equipped with brakes to avoid slippage.
  • the sample synthesis system 3 includes a piston 31 slidably arranged inside the reactor cylinder 21, a sealing plug 32 sealingly arranged at the bottom of the reactor cylinder 21, a manual booster pump 33, and a reactor cylinder between the piston 31 and the sealing plug 32
  • the internal space of the body 21 forms a closed space.
  • the manual booster pump 33 is connected to the sealed space.
  • the piston 31 moves upwards when pressurizing, and the piston 31 moves downwards when depressurizing.
  • the manual booster pump 33 and the reactor cylinder 21 are connected with each other.
  • a booster valve 34 is also provided.
  • the internal space between the piston 31, the reactor cylinder 21 and the reactor end cover 22 forms an inner cavity, which is used to place the hydrate deposit sample 23 of the synthetic hydrate deposit, and the reactor end cover 22 and the hydrate deposit
  • a first water-permeable plate 25 is provided between the sample 23 and a second water-permeable plate 24 is provided between the piston 31 and the hydrate deposit sample 23.
  • the permeability of the first permeable plate 25 and the second permeable plate 24 is much higher than that of the hydrate sediment, which can well block the sediment and gravel from entering the pipeline and effectively transmit the axial pressure.
  • the permeability test system 4 includes a first gas pipeline 41 connected to the inner cavity of one end of the reactor end cover 22, a first constant pressure system 43 connected to the first gas pipeline 41, and a connection
  • the system 43 and the second constant pressure system 44 are used to adjust the internal pressure values at both ends of the reactor 2, and the flow meter is used for permeability testing to record the flow rate to calculate the sediment permeability.
  • the first gas pipeline 41 is provided with a first valve 411
  • the second gas pipeline 42 is provided with a second valve 421.
  • Both the first valve 411 and the second valve 421 are used to control the sealing of the internal space of the reactor 2.
  • a constant pressure system 43 and the first gas pipeline 41 are provided with a constant pressure valve 431, the flow meter is connected with a flow valve, and a differential pressure sensor 45 is connected between the first constant pressure system 43 and the second constant pressure system 44, The differential pressure sensor 45 is used to reflect the pressure difference between the top and the bottom of the reactor 2.
  • the differential pressure sensor 45 and the flow meter are both connected to the data acquisition and control system 6 to facilitate overall data monitoring and testing.
  • the permeability testing system 4 is also connected to a vacuuming system 46 and a gas cylinder 47 for supplying gas to the reaction and providing gas for testing the permeability.
  • the gas provided by the gas cylinder 47 is a supersaturated gas (such as methane), and the vacuuming system 46
  • Both the gas cylinder and the gas cylinder 47 are connected to the first gas pipeline 41, a vacuum valve 461 is provided between the vacuum system 46 and the first gas pipeline 41, and a gas supply valve is provided between the gas cylinder 47 and the first gas pipeline 41 471.
  • the vacuum system 46 is used to extract the air inside the reactor 2 and then use the gas cylinder 47 to supply air to the inside of the reactor 2 to ensure the purity of the gas inside and exhaust the interference of other gases.
  • the hydraulic fracturing system 5 is arranged on the side of the reactor barrel 21, which includes a hydraulic jet tube 51 connected from the side wall of the reactor barrel 21 to the inner cavity and connected with the hydraulic jet tube 51
  • the fracturing pump system 52 is equipped with a sand adding device 53 on the hydraulic jet tube 51.
  • the fracturing pump system 52 sets the fracturing fluid and proppant into the hydrate sediment through the hydraulic jet tube 51 at high pressure.
  • the outlet direction of 51 should be consistent with the axial direction of the reactor 2, and a fracturing valve 54 is provided between the sand adding device 53 and the side wall of the reactor cylinder 21.
  • the photographic lighting system 7 is arranged on the side wall at the corresponding position of the inner cavity of the reactor cylinder 21, which includes a sapphire cylinder 73 arranged on the side wall of the reactor cylinder 21 for observing the internal conditions of the inner cavity and connected to the reaction
  • the camera 71 and the illuminating lamp 72 on the cylinder 21, the side wall of the reactor cylinder 21 at the end is directly replaced by the sapphire cylinder 73, and the sapphire cylinder 73 is fixed to the reactor 2 with bolts and nuts to make it It is fixed at the corresponding position to better observe the internal situation.
  • the lens of the camera 71 is facing the sapphire tube 73 to observe and record the internal situation of the inner cavity.
  • the data acquisition and control system 6 includes a computer 61 and a temperature sensor 62 and a pressure sensor 63 connected to the computer 61.
  • the temperature sensor 62 is arranged on the end cover 22 of the reactor to collect temperature parameter data inside the cavity.
  • the pressure sensor 63 is connected and arranged On the sample synthesis system 3, the permeability test system 4 and the hydraulic fracturing system 5, the pressure parameter data of each system is collected.
  • the computer 61 is also connected with the differential pressure sensor 45 and the flow meter, which can photograph the test process in the whole process to record the pressure. Fracturing fracture changes and fracturing effects during the fracturing process.
  • the constant pressure valve 431, the air supply valve 471, the fracturing valve 54, the boost valve 34, and the second valve 421, connect the vacuum system 46 to the first air pipeline 41, and open the vacuum pump.
  • the vacuum system 46, the first valve 411 and the vacuum valve 461 start to vacuum the device, and the vacuum is completed after about 15 minutes; after the vacuum is completed, the vacuum system 46 and the vacuum valve 461 are closed.
  • Open the gas supply valve 471, the constant pressure valve 431 and the constant pressure system connect the gas cylinder 47 to inject supersaturated gas (such as methane), and maintain a certain pore pressure.
  • the gas valve 471 pumps a certain pressure of gas into the reactor 2, and then simultaneously opens the first constant pressure system 43, the second constant pressure system 44 and the valves located at both ends of the reactor 2, and opens the differential pressure sensor 45.
  • the sensor 45 constantly adjusts the constant pressure at both ends of the reactor 2 so that the upper end of the reactor 2 is always greater than the lower end of the reactor 2 by a certain stable pressure value, and the gas percolation experiment is performed.
  • the exhaust flow rate displayed by the flowmeter is stable, the average flow rate is calculated , Used to calculate sediment permeability.
  • Constant pressure system 43, second constant pressure system 44, constant pressure valve 431 and second valve 421, open the differential pressure sensor 45, and constantly adjust the constant pressure at both ends of the reactor 2 by observing the differential pressure sensor 45 to make the upper end of the reactor 2 Always a certain stable pressure value greater than the lower end of the reactor 2 for gas percolation experiments.
  • part of the fracturing fluid will be discharged.
  • the average flow rate is measured to calculate the sediment permeability.
  • the invention can synthesize natural gas hydrate deposits in situ under high pressure and low temperature conditions, perform fracturing experiments on the deposits, and measure the permeability, which expands the existing experimental test devices.
  • the range of use improves the accuracy and convenience of experimental testing.
  • the design of this application supports the in-situ synthesis of hydrate sediment sample 23, can reasonably simulate the reservoir stress and temperature and pressure conditions, and can more completely restore the conventional hydraulic fracturing operation steps such as fluid injection, fracturing, and proppant addition. It can also measure the changes in reservoir permeability before and after fracturing and under different fracturing conditions and observe the fracturing effect. It provides certain guidance for the study of the fracturing mechanism of gas hydrate sediments and the changes in reservoir permeability before and after fracturing. effect.

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Abstract

A natural gas hydrate mineral fracturing experiment device, comprising a support (1) and a reactor (2) disposed on the support (1) for synthesizing a sample and performing fracturing transformation on the sample. The reactor (2) is provided with a sample synthesis system (3), a permeability testing system (4), and a data acquisition and control system (6). A hydraulic fracturing system (5) used for performing the fracturing transformation is further disposed in the reactor (2). The device can synthesize natural gas hydrate sediments in situ under high-pressure and low-temperature conditions, perform fracturing experiments on the sediments, and measure the permeability thereof, thereby expanding the application range of existing experimental testing devices. In addition, the device can reasonably simulate reservoir ground stress and temperature and pressure conditions, can relatively completely restore conventional hydraulic fracturing operation steps such as liquid injection, fracturing, and propping agent addition, and can also measure changes in reservoir permeability before and after the fracturing and under different fracturing conditions and observe the fracturing effect.

Description

一种天然气水合物矿藏压裂实验装置Fracturing experimental device for natural gas hydrate deposit 技术领域Technical field
本发明涉及到一种天然气水合物矿藏压裂实验装置,其装置是一种可以在高压低温条件下原位合成天然气水合物沉积物,对沉积物进行压裂实验,并测量其渗透率的装置。The invention relates to a fracturing experiment device for natural gas hydrate deposits. The device is a device that can synthesize natural gas hydrate deposits in situ under high pressure and low temperature conditions, perform fracturing experiments on the deposits, and measure the permeability .
背景技术Background technique
天然气水合物是一种由烷烃(如甲烷、乙烷等)与水在一定的高压低温条件下形成的冰状固体,俗称可燃冰,广泛分布于冻土带地表以下和大陆边缘海底之下的沉积物中。全球范围内天然气水合物储量巨大,相当于2×105亿吨油当量,是全球常规化石能源总碳量的2倍,被视为石油时代之后重要的替代能源。Natural gas hydrate is an ice-like solid formed by alkanes (such as methane, ethane, etc.) and water under certain high pressure and low temperature conditions. It is commonly known as combustible ice and is widely distributed below the surface of the tundra and under the seabed of the continental margin. In the sediment. The global reserves of natural gas hydrate are huge, equivalent to 210.5 billion tons of oil equivalent, which is twice the total carbon content of conventional fossil energy in the world, and is regarded as an important alternative energy source after the oil age.
在天然气水合物开采过程中,利用降压、注热、注化学试剂等开采方法使水合物分解后,其储层的渗透率大小会直接影响水合物分解后孔隙间气、水的渗流速率,进而影响产气开采效率,所以提高储层渗透率对实现天然气水合物的商业化开采有着重要意义。In the process of natural gas hydrate development, after the hydrate is decomposed by mining methods such as pressure reduction, heat injection, and chemical injection, the permeability of the reservoir will directly affect the flow rate of gas and water between the pores after the hydrate is decomposed. This in turn affects the efficiency of gas production and recovery, so increasing the permeability of the reservoir is of great significance to the commercial exploitation of natural gas hydrates.
储层改造技术中的水力压裂增产技术在石油天然气工业中已得到了广泛应用,可以极大提高油气储层的渗透率,实现了低渗、特低渗油气田油气生产中的增产增注。由于天然气水合物储层的低渗特性与页岩气田等低渗气田的性质类似,为了实现天然气水合物矿藏的天然气增产,当前已有一些研究正在探索利用水力压裂法提高水合物储层渗透率的可行性,而现有对天然气水合物沉积物进行水力压裂的模拟实验较少,并且缺乏较完整水力压裂过程的模拟并可以测量压裂后储层渗透率变化的实验装置,也无法模拟真实的地应力以及储层温压条件,制约着天然气水合物矿藏水力压裂法增产技术的发展。天然气水合物沉积物在常规贮藏条件下的渗透率非常低,不利于天然气生产,因此需要实验装置模拟使用水力压裂法对天然气水合物矿藏进行储层改造,产生高渗透率的压裂通道以提高储层渗透率。The hydraulic fracturing stimulation technology in the reservoir reconstruction technology has been widely used in the oil and gas industry, which can greatly increase the permeability of oil and gas reservoirs and realize the increase in oil and gas production in low-permeability and ultra-low-permeability oil and gas fields. Since the low permeability of natural gas hydrate reservoirs is similar to that of low-permeability gas fields such as shale gas fields, in order to increase the production of natural gas in natural gas hydrate deposits, some studies are currently exploring the use of hydraulic fracturing to increase the permeability of hydrate reservoirs. However, there are few existing simulation experiments for hydraulic fracturing of gas hydrate sediments, and there is a lack of experimental devices that can simulate the complete hydraulic fracturing process and can measure changes in reservoir permeability after fracturing. The inability to simulate the real in-situ stress and reservoir temperature and pressure conditions restricts the development of hydraulic fracturing stimulation technology for natural gas hydrate deposits. The permeability of natural gas hydrate deposits under conventional storage conditions is very low, which is not conducive to natural gas production. Therefore, an experimental device is required to simulate the use of hydraulic fracturing to reconstruct the gas hydrate deposits to produce high-permeability fracturing channels. Improve reservoir permeability.
发明内容Summary of the invention
针对现有技术的不足,本发明提供一种天然气水合物矿藏压裂实验装置。Aiming at the shortcomings of the prior art, the present invention provides a fracturing experimental device for natural gas hydrate deposits.
为实现上述目的,本发明的技术方案为:In order to achieve the above objective, the technical solution of the present invention is:
一种天然气水合物矿藏压裂实验装置,包括支架以及设置在支架上用于合成样品并对其进行压裂改造的反应器,所述反应器上设置有样品合成系统、渗透率测试系统以及数据采集及控制系统,所述反应器中上还设有用于进行压裂改造的水力压裂系统。A fracturing experiment device for natural gas hydrate deposits, comprising a support and a reactor set on the support for synthesizing samples and fracturing and reforming them, and the reactor is provided with a sample synthesis system, a permeability testing system, and data An acquisition and control system. The reactor is also provided with a hydraulic fracturing system for fracturing reformation.
进一步地,所述反应器包括反应器筒体和设置在反应器筒体一端的反应器端盖,所述反 应器筒体内用于放置水合物沉积物样品,所述样品合成系统设置在反应器筒体远离反应器端盖的一端,所述样品合成系统、反应器筒体以及反应器端盖之间的空间形成内腔,所述反应器端盖与水合物沉积物样品之间设置有第一透水板,所述样品合成系统与水合物沉积物样品之间设置有第二透水板。Further, the reactor includes a reactor cylinder and a reactor end cover arranged at one end of the reactor cylinder, the reactor cylinder is used to place a sample of hydrate sediment, and the sample synthesis system is arranged in the reactor. The end of the cylinder is far away from the end cover of the reactor, the space between the sample synthesis system, the reactor cylinder and the end cover of the reactor forms an inner cavity, and a second is arranged between the end cover of the reactor and the hydrate sediment sample. A water-permeable plate, and a second water-permeable plate is arranged between the sample synthesis system and the hydrate sediment sample.
进一步地,所述样品合成系统包括与第二透水板相抵的活塞、设置在反应器筒体远离反应器端盖的一端的密封塞以及连接在活塞与密封塞之间的反应器筒体的侧壁上的手动增压泵,所述手动增压泵与反应器筒体之间设置有增压阀门。Further, the sample synthesis system includes a piston that abuts against the second water-permeable plate, a sealing plug arranged at an end of the reactor cylinder away from the end cover of the reactor, and a side of the reactor cylinder connected between the piston and the sealing plug. The manual booster pump on the wall is provided with a booster valve between the manual booster pump and the reactor cylinder.
进一步地,所述渗透率测试系统包括连接至反应器端盖的一端的内腔内的第一输气管道、与第一输气管道连接的第一恒压系统、连接至样品合成系统一端的内腔内的第二输气管道、与第二输气管道连接的第二恒压系统以及与第二恒压系统连接的流量计,所述第一输气管道上设有第一阀门,所述第二输气管道上设有第二阀门,所述第一恒压系统与第一输气管道支架设有恒压阀门,所述流量计连接有流量阀门,所述第一恒压系统和第二恒压系统之间连接有差压传感器,所述差压传感器和流量计均连接至数据采集及控制系统。Further, the permeability test system includes a first gas pipeline connected to the inner cavity of one end of the reactor end cover, a first constant pressure system connected to the first gas pipeline, and one end connected to the sample synthesis system A second gas pipeline in the inner cavity, a second constant pressure system connected to the second gas pipeline, and a flow meter connected to the second constant pressure system, the first gas pipeline is provided with a first valve, so The second gas pipeline is provided with a second valve, the first constant pressure system and the first gas pipeline support are provided with a constant pressure valve, the flow meter is connected with a flow valve, the first constant pressure system and A differential pressure sensor is connected between the second constant pressure system, and the differential pressure sensor and the flow meter are both connected to the data acquisition and control system.
进一步地,所述渗透率测试系统还连接有抽真空系统和用以给反应供气和提供测试渗透率的气体的气瓶,所述抽真空系统和气瓶均连接至第一输气管道,所述抽真空系统与第一输气管道之间设置有抽真空阀门,所述气瓶与第一输气管道之间设置有供气阀门。Further, the permeability test system is also connected with an evacuation system and a gas cylinder for supplying gas to the reaction and providing gas for testing the permeability, and the evacuation system and the gas cylinder are both connected to the first gas pipeline, so A vacuum valve is arranged between the vacuum system and the first gas pipeline, and an air supply valve is arranged between the gas cylinder and the first gas pipeline.
进一步地,所述水力压裂系统包括从反应器筒体的侧壁连接至内腔内的水力射流管以及与水力射流管连接的压裂泵系统,所述水力射流管的出口方向与反应器的轴线方向一致,所述水力射流管上设有加砂装置,所述加砂装置和反应器筒体的侧壁之间设有压裂阀门。Further, the hydraulic fracturing system includes a hydraulic jet tube connected from the side wall of the reactor barrel to the inner cavity, and a fracturing pump system connected with the hydraulic jet tube. The outlet direction of the hydraulic jet tube is the same as that of the reactor. The axial directions of the reactor are consistent, the water jet pipe is provided with a sanding device, and a fracturing valve is provided between the sanding device and the side wall of the reactor cylinder.
进一步地,所述数据采集及控制系统包括计算机以及与计算机连接的温度传感器和压力传感器,所述温度传感器设置在反应器端盖上,以采集内腔内部的温度参数数据,所述压力传感器连接设置在样品合成系统、渗透率测试系统以及水力压裂系统上,以采集各系统压力参数数据。Further, the data acquisition and control system includes a computer and a temperature sensor and a pressure sensor connected to the computer, the temperature sensor is arranged on the end cover of the reactor to collect temperature parameter data inside the cavity, and the pressure sensor is connected It is set on the sample synthesis system, permeability testing system and hydraulic fracturing system to collect the pressure parameter data of each system.
进一步地,还包括设置在反应器筒体上内腔对应位置处的侧壁上的摄影照明系统,所述摄影照明系统包括设置在反应器筒体的侧壁的用于观测内腔内部情况的蓝宝石筒以及连接在反应器筒体上的摄像机和照明灯,所述摄像机的镜头正对蓝宝石筒,以观测内腔内部情况。Further, it also includes a photographic lighting system arranged on the side wall at the corresponding position of the inner cavity of the reactor barrel, and the photographic lighting system includes a side wall of the reactor barrel for observing the internal condition of the inner cavity. The sapphire tube and the camera and illuminating lamp connected to the reactor tube body, the lens of the camera is directly facing the sapphire tube, so as to observe the internal situation of the inner cavity.
本发明与现有技术相比,具有如下优点:Compared with the prior art, the present invention has the following advantages:
本发明可以在高压低温条件下原位合成天然气水合物沉积物,对沉积物进行压裂实验,并测量其渗透率,扩展了目前所存在实验测试装置的使用范围,提高了实验测试的精确度和便利度。本申请这样的设计支持原位合成水合物沉积物样品,能合理模拟储层地应力以及温 压条件,可以较完整地还原出注液、压裂、加支撑剂等水力压裂常规操作步骤,还可以测量压裂前后和不同压裂条件下储层渗透率的变化并观察压裂效果,对天然气水合物沉积物的压裂机理和压裂前后储层渗透率变化的研究有一定的指导作用。The invention can synthesize natural gas hydrate deposits in situ under high-pressure and low-temperature conditions, perform fracturing experiments on the deposits, and measure the permeability, which expands the scope of use of existing experimental testing devices and improves the accuracy of experimental testing And convenience. The design of this application supports in-situ synthesis of hydrate sediment samples, can reasonably simulate reservoir stress and temperature and pressure conditions, and can more completely restore conventional hydraulic fracturing steps such as fluid injection, fracturing, and proppant addition. It can also measure the changes in reservoir permeability before and after fracturing and under different fracturing conditions and observe the fracturing effect, which has a certain guiding role in the study of the fracturing mechanism of gas hydrate sediments and the changes in reservoir permeability before and after fracturing. .
附图说明Description of the drawings
图1为天然气水合物矿藏压裂实验装置的整体连接结构示意图;Figure 1 is a schematic diagram of the overall connection structure of the fracturing experimental device for natural gas hydrate deposits;
图2为图1中A部分渗透率测试系统的连接结构放大示意图;Fig. 2 is an enlarged schematic diagram of the connection structure of the permeability test system of part A in Fig. 1;
附图标记说明:1、支架;2、反应器;21、反应器筒体;22、反应器端盖;23、水合物沉积物样品;24、第二透水板;25、第一透水板;3、样品合成系统;31、活塞;32、密封塞;33、手动增压泵;34、增压阀门;4、渗透率测试系统;41、第一输气管道;411、第一阀门;42、第二输气管道;421、第二阀门;43、第一恒压系统;431、恒压阀门;44、第二恒压系统;45、差压传感器;46、抽真空系统;461、抽真空阀门;47、气瓶;471、供气阀门;5、水力压裂系统;51、水力射流管;52、压裂泵系统;53、加砂装置;54、压裂阀门;6、数据采集及控制系统;61、计算机;62、温度传感器;63、压力传感器;7、摄影照明系统;71、摄像机;72、照明灯;73、蓝宝石筒。Description of Reference Signs: 1. Support; 2. Reactor; 21. Reactor cylinder; 22. Reactor end cover; 23. Hydrate sediment sample; 24. Second permeable plate; 25. First permeable plate; 3. Sample synthesis system; 31. Piston; 32. Seal plug; 33. Manual booster pump; 34. Pressure booster valve; 4. Permeability test system; 41. First gas pipeline; 411. First valve; 42 , The second gas pipeline; 421, the second valve; 43, the first constant pressure system; 431, the constant pressure valve; 44, the second constant pressure system; 45, the differential pressure sensor; 46, the vacuum system; 461, the pumping Vacuum valve; 47. Gas cylinder; 471. Gas supply valve; 5. Hydraulic fracturing system; 51. Hydraulic jet tube; 52. Fracturing pump system; 53, Sand adding device; 54, Fracturing valve; 6. Data acquisition And control system; 61, computer; 62, temperature sensor; 63, pressure sensor; 7, photographic lighting system; 71, camera; 72, lighting; 73, sapphire tube.
具体实施方式Detailed ways
为使本发明的上述目的、特征和优点能够更加明显易懂,下面结合附图和具体实施方式对本发明作进一步详细的说明。In order to make the above objectives, features and advantages of the present invention more obvious and understandable, the present invention will be further described in detail below in conjunction with the accompanying drawings and specific embodiments.
实施例Example
如图1所示,一种天然气水合物矿藏压裂实验装置,包括支架1以及设置在支架1上用于合成样品并对其进行压裂改造的反应器2,反应器2上设置有样品合成系统3、渗透率测试系统4、摄影照明系统7以及数据采集及控制系统6,反应器2中上还设有用于进行压裂改造的水力压裂系统5。As shown in Figure 1, an experimental device for fracturing a natural gas hydrate deposit includes a support 1 and a reactor 2 set on the support 1 for synthesizing samples and fracturing them. The reactor 2 is equipped with a sample synthesis System 3, permeability test system 4, photographic lighting system 7 and data acquisition and control system 6. The reactor 2 is also provided with a hydraulic fracturing system 5 for fracturing reformation.
反应器2的结构包括反应器筒体21和设置在反应器筒体21一端的反应器端盖22,反应器筒体21为圆柱筒状结构,并竖直固定设置在支架1上,反应器端盖22设置在反应器筒体21的顶部,反应器筒体21内用于放置水合物沉积物样品23。反应器端盖22与反应器筒体21之间通过螺栓固定连接,反应器筒体21与支架1之间通过螺母和螺栓固定连接,以确保反应器筒体21在合成样品、进行渗透率测试以及水力压裂的时候能保持固定,支架1底部加设有轮子,以便于整体的移动,为了使提高装置使用时的稳定,轮子可以加设有刹车,以避 免滑动。The structure of the reactor 2 includes a reactor barrel 21 and a reactor end cover 22 arranged at one end of the reactor barrel 21. The reactor barrel 21 is a cylindrical cylindrical structure and is vertically fixed on the support 1. The reactor The end cap 22 is arranged on the top of the reactor cylinder 21, and the reactor cylinder 21 is used to place a hydrate sediment sample 23. The reactor end cover 22 and the reactor cylinder 21 are fixedly connected by bolts, and the reactor cylinder 21 and the support 1 are fixedly connected by nuts and bolts to ensure that the reactor cylinder 21 is in the process of synthesizing samples and conducting permeability tests. And it can be kept fixed during hydraulic fracturing. Wheels are added to the bottom of the bracket 1 to facilitate the overall movement. In order to improve the stability of the device during use, the wheels can be equipped with brakes to avoid slippage.
样品合成系统3包括滑动设置在反应器筒体21内部的活塞31、密封设置在反应器筒体21底部的密封塞32以及手动增压泵33,活塞31和密封塞32之间的反应器筒体21内部空间形成一个密闭空间,手动增压泵33与该密闭空间链接,加压时活塞31向上活动,减压时活塞31向下活动,手动增压泵33与反应器筒体21之间还设置有增压阀门34。The sample synthesis system 3 includes a piston 31 slidably arranged inside the reactor cylinder 21, a sealing plug 32 sealingly arranged at the bottom of the reactor cylinder 21, a manual booster pump 33, and a reactor cylinder between the piston 31 and the sealing plug 32 The internal space of the body 21 forms a closed space. The manual booster pump 33 is connected to the sealed space. The piston 31 moves upwards when pressurizing, and the piston 31 moves downwards when depressurizing. The manual booster pump 33 and the reactor cylinder 21 are connected with each other. A booster valve 34 is also provided.
活塞31、反应器筒体21以及反应器端盖22之间的内部空间形成内腔,内腔用于放置合成水合物沉淀物的水合物沉积物样品23,反应器端盖22与水合物沉积物样品23之间设置有第一透水板25,活塞31与水合物沉积物样品23之间设置有第二透水板24。第一透水板25和第二透水板24的渗透率远大于水合物沉积物的渗透率,可以很好地阻挡沉积物砂砾进入管道并有效传递轴压。The internal space between the piston 31, the reactor cylinder 21 and the reactor end cover 22 forms an inner cavity, which is used to place the hydrate deposit sample 23 of the synthetic hydrate deposit, and the reactor end cover 22 and the hydrate deposit A first water-permeable plate 25 is provided between the sample 23 and a second water-permeable plate 24 is provided between the piston 31 and the hydrate deposit sample 23. The permeability of the first permeable plate 25 and the second permeable plate 24 is much higher than that of the hydrate sediment, which can well block the sediment and gravel from entering the pipeline and effectively transmit the axial pressure.
如图2所示,渗透率测试系统4包括连接至反应器端盖22的一端的内腔内的第一输气管道41、与第一输气管道41连接的第一恒压系统43、连接至样品合成系统3一端的内腔内的第二输气管道42、与第二输气管道42连接的第二恒压系统44以及与第二恒压系统44连接的流量计,第一恒压系统43与第二恒压系统44分部用于调节反应器2两端内部的压力值,流量计则是用于渗透率测试的时候,记录流速,以计算沉积物渗透率。第一输气管道41上设有第一阀门411,第二输气管道42上设有第二阀门421,第一阀门411与第二阀门421均用于控制反应器2内部空间的密闭,第一恒压系统43与第一输气管道41支架1设有恒压阀门431,流量计连接有流量阀门,第一恒压系统43和第二恒压系统44之间连接有差压传感器45,差压传感器45用于反映反应器2的顶部与底部之间的压差,差压传感器45和流量计均连接至数据采集及控制系统6,以便于整体数据的监控与测试。As shown in Figure 2, the permeability test system 4 includes a first gas pipeline 41 connected to the inner cavity of one end of the reactor end cover 22, a first constant pressure system 43 connected to the first gas pipeline 41, and a connection The second gas pipeline 42 in the inner cavity at one end of the sample synthesis system 3, the second constant pressure system 44 connected to the second gas pipeline 42 and the flow meter connected to the second constant pressure system 44, the first constant pressure The system 43 and the second constant pressure system 44 are used to adjust the internal pressure values at both ends of the reactor 2, and the flow meter is used for permeability testing to record the flow rate to calculate the sediment permeability. The first gas pipeline 41 is provided with a first valve 411, and the second gas pipeline 42 is provided with a second valve 421. Both the first valve 411 and the second valve 421 are used to control the sealing of the internal space of the reactor 2. A constant pressure system 43 and the first gas pipeline 41 are provided with a constant pressure valve 431, the flow meter is connected with a flow valve, and a differential pressure sensor 45 is connected between the first constant pressure system 43 and the second constant pressure system 44, The differential pressure sensor 45 is used to reflect the pressure difference between the top and the bottom of the reactor 2. The differential pressure sensor 45 and the flow meter are both connected to the data acquisition and control system 6 to facilitate overall data monitoring and testing.
渗透率测试系统4还连接有抽真空系统46和用以给反应供气和提供测试渗透率的气体的气瓶47,气瓶47提供的气体为过饱和气体(如甲烷),抽真空系统46和气瓶47均连接至第一输气管道41,抽真空系统46与第一输气管道41之间设置有抽真空阀门461,气瓶47与第一输气管道41之间设置有供气阀门471。抽真空系统46用于将反应器2内部的空气抽出,然后利用气瓶47对反应器2内部进行供气,以保证内部的气体的纯净,排出其他气体的干扰。The permeability testing system 4 is also connected to a vacuuming system 46 and a gas cylinder 47 for supplying gas to the reaction and providing gas for testing the permeability. The gas provided by the gas cylinder 47 is a supersaturated gas (such as methane), and the vacuuming system 46 Both the gas cylinder and the gas cylinder 47 are connected to the first gas pipeline 41, a vacuum valve 461 is provided between the vacuum system 46 and the first gas pipeline 41, and a gas supply valve is provided between the gas cylinder 47 and the first gas pipeline 41 471. The vacuum system 46 is used to extract the air inside the reactor 2 and then use the gas cylinder 47 to supply air to the inside of the reactor 2 to ensure the purity of the gas inside and exhaust the interference of other gases.
如图1所示,水力压裂系统5设置在反应器筒体21的侧边,其包括从反应器筒体21的侧壁连接至内腔内的水力射流管51以及与水力射流管51连接的压裂泵系统52,水力射流管51上设有加砂装置53,压裂泵系统52将压裂液与支撑剂通过水力射流管51高压设入打入水合物沉积物内,水力射流管51的出口方向应与反应器2的轴线方向一致,加砂装置53和反应器筒体21的侧壁之间设有压裂阀门54。As shown in Figure 1, the hydraulic fracturing system 5 is arranged on the side of the reactor barrel 21, which includes a hydraulic jet tube 51 connected from the side wall of the reactor barrel 21 to the inner cavity and connected with the hydraulic jet tube 51 The fracturing pump system 52 is equipped with a sand adding device 53 on the hydraulic jet tube 51. The fracturing pump system 52 sets the fracturing fluid and proppant into the hydrate sediment through the hydraulic jet tube 51 at high pressure. The hydraulic jet tube The outlet direction of 51 should be consistent with the axial direction of the reactor 2, and a fracturing valve 54 is provided between the sand adding device 53 and the side wall of the reactor cylinder 21.
摄影照明系统7设置在反应器筒体21上内腔对应位置处的侧壁上,其包括设置在反应器筒体21的侧壁的用于观测内腔内部情况的蓝宝石筒73以及连接在反应器筒体21上的摄像机71和照明灯72,该端部为的反应器筒体21的侧壁直接采用蓝宝石筒73来替代,并利用螺栓螺母将蓝宝石筒73与反应器2固定,使其固定在相应的位置处,以更好地观测内部情况,摄像机71的镜头正对蓝宝石筒73,用以观测并记录内腔内部情况。The photographic lighting system 7 is arranged on the side wall at the corresponding position of the inner cavity of the reactor cylinder 21, which includes a sapphire cylinder 73 arranged on the side wall of the reactor cylinder 21 for observing the internal conditions of the inner cavity and connected to the reaction The camera 71 and the illuminating lamp 72 on the cylinder 21, the side wall of the reactor cylinder 21 at the end is directly replaced by the sapphire cylinder 73, and the sapphire cylinder 73 is fixed to the reactor 2 with bolts and nuts to make it It is fixed at the corresponding position to better observe the internal situation. The lens of the camera 71 is facing the sapphire tube 73 to observe and record the internal situation of the inner cavity.
数据采集及控制系统6包括计算机61以及与计算机61连接的温度传感器62和压力传感器63,温度传感器62设置在反应器端盖22上,以采集内腔内部的温度参数数据,压力传感器63连接设置在样品合成系统3、渗透率测试系统4以及水力压裂系统5上,以采集各系统压力参数数据,同时计算机61还与差压传感器45和流量计连接,可全程拍摄测试过程,以记录压裂过程中的压裂裂缝变化和压裂效果。The data acquisition and control system 6 includes a computer 61 and a temperature sensor 62 and a pressure sensor 63 connected to the computer 61. The temperature sensor 62 is arranged on the end cover 22 of the reactor to collect temperature parameter data inside the cavity. The pressure sensor 63 is connected and arranged On the sample synthesis system 3, the permeability test system 4 and the hydraulic fracturing system 5, the pressure parameter data of each system is collected. At the same time, the computer 61 is also connected with the differential pressure sensor 45 and the flow meter, which can photograph the test process in the whole process to record the pressure. Fracturing fracture changes and fracturing effects during the fracturing process.
本装置具体的实验步骤分为以下6步:The specific experimental steps of this device are divided into the following 6 steps:
(1)装样(1) Sample loading
测试前先拧紧固定蓝宝石筒73的螺栓,卸开反应器端盖22外的螺栓,取下反应器端盖22,安装好反应器2下部的第二透水板24。将水力射流管51管孔包覆一层薄橡胶膜防止沉积物砂进入水力射流管51,之后向内腔中放入一定含水率的水合物沉积物样品23,堆实并安装好反应器2上部的第一透水板25,盖上反应器端盖22拧紧螺栓,数据采集和控制系统和计算机61开始监测反应进程。Before testing, tighten the bolts fixing the sapphire cylinder 73, remove the bolts outside the reactor end cover 22, remove the reactor end cover 22, and install the second permeable plate 24 at the bottom of the reactor 2. Cover the hole of the hydraulic jet tube 51 with a thin rubber film to prevent sediment sand from entering the hydraulic jet tube 51, and then put a hydrate sediment sample 23 with a certain moisture content into the inner cavity, pile up and install the reactor 2 The upper first water-permeable plate 25 is covered with the reactor end cap 22 and the bolts are tightened. The data acquisition and control system and the computer 61 start to monitor the reaction process.
(2)样品合成(2) Sample synthesis
为排除装置中残余空气的干扰,关闭恒压阀门431、供气阀门471、压裂阀门54、增压阀门34、第二阀门421,连接抽真空系统46到第一输气管道41,打开抽真空系统46、第一阀门411和抽真空阀门461开始对装置抽真空,约15分钟后抽真空完毕;抽真空完毕后,关闭抽真空系统46和抽真空阀门461。打开供气阀门471、恒压阀门431和恒压系统,连接气瓶47打入过饱和气体(例如甲烷),并维持一定的孔隙压力。之后打开增压阀门34,并利用手动调压泵推进活塞31,对水合物沉积物样品23施加一定的轴压,形成水合物沉积物样品23,将反应器2内温度降至1℃,等压力平衡后,打开恒温浴。In order to eliminate the interference of residual air in the device, close the constant pressure valve 431, the air supply valve 471, the fracturing valve 54, the boost valve 34, and the second valve 421, connect the vacuum system 46 to the first air pipeline 41, and open the vacuum pump. The vacuum system 46, the first valve 411 and the vacuum valve 461 start to vacuum the device, and the vacuum is completed after about 15 minutes; after the vacuum is completed, the vacuum system 46 and the vacuum valve 461 are closed. Open the gas supply valve 471, the constant pressure valve 431 and the constant pressure system, connect the gas cylinder 47 to inject supersaturated gas (such as methane), and maintain a certain pore pressure. Then open the booster valve 34, and use the manual pressure regulating pump to push the piston 31 to apply a certain axial pressure to the hydrate deposit sample 23 to form the hydrate deposit sample 23, and reduce the temperature in the reactor 2 to 1°C, etc. After the pressure is equalized, turn on the constant temperature bath.
(3)压裂前水合物沉积物渗透率测试(3) Permeability test of hydrate sediment before fracturing
反应完成后,关闭供气阀门471、增压阀门34和第一阀门411,将水合物沉积物预冷一段时间,打开第一阀门411、第二阀门421、流量计和流量阀门,并打开供气阀门471将一定压力的气体打入反应器2内,然后同时打开位于反应器2两端的第一恒压系统43、第二恒压系统44以及阀门,打开差压传感器45,通过观察差压传感器45不断调整反应器2两端的恒 压压力,使反应器2上端始终比反应器2下端大出一定的稳定压力值,进行气体渗流实验,当流量计显示的排气流量稳定后测算平均流速,用以计算沉积物渗透率。After the reaction is completed, close the gas supply valve 471, the booster valve 34 and the first valve 411, pre-cool the hydrate deposits for a period of time, open the first valve 411, the second valve 421, the flow meter and the flow valve, and open the supply valve. The gas valve 471 pumps a certain pressure of gas into the reactor 2, and then simultaneously opens the first constant pressure system 43, the second constant pressure system 44 and the valves located at both ends of the reactor 2, and opens the differential pressure sensor 45. By observing the differential pressure The sensor 45 constantly adjusts the constant pressure at both ends of the reactor 2 so that the upper end of the reactor 2 is always greater than the lower end of the reactor 2 by a certain stable pressure value, and the gas percolation experiment is performed. When the exhaust flow rate displayed by the flowmeter is stable, the average flow rate is calculated , Used to calculate sediment permeability.
(4)水力压裂测试(4) Hydraulic fracturing test
渗透率测试结束后,关闭气瓶47,供气阀门471、流量计、流量阀门、第二阀门421、第一阀门411,等到反应器2两端压力再次相等,打开照明灯72和摄像机71,打开连接压裂泵系统52的压裂阀门54,然后迅速打开压裂泵系统52和加砂装置53,控制加砂速率,压裂泵系统52以一定压力将已着色的压裂液和支撑剂打入水力射流管51,水力射流管51射出的高压液流冲破薄橡胶膜,冲击水合物沉积物样品23,将水合物沉积物样品23压裂出裂缝,摄像机71在蓝宝石筒73前记录下压裂的过程,之后停止压裂作业,关闭阀门和压裂泵系统52。After the permeability test is over, close the gas cylinder 47, the gas supply valve 471, the flow meter, the flow valve, the second valve 421, and the first valve 411. When the pressure at both ends of the reactor 2 is equal again, turn on the illumination lamp 72 and the camera 71. Open the fracturing valve 54 connected to the fracturing pump system 52, and then quickly open the fracturing pump system 52 and the sanding device 53 to control the sanding rate, and the fracturing pump system 52 will discharge the colored fracturing fluid and proppant at a certain pressure Into the hydraulic jet tube 51, the high-pressure liquid jet from the hydraulic jet tube 51 breaks through the thin rubber film and impacts the hydrate sediment sample 23, fracturing the hydrate sediment sample 23 out of cracks, and the camera 71 records in front of the sapphire tube 73 After the fracturing process, the fracturing operation is stopped, and the valve and the fracturing pump system 52 are closed.
(5)压裂后水合物沉积物渗透率测试(5) Permeability test of hydrate sediment after fracturing
压裂测试完成后,打开气瓶47阀门将一定压力的气体打入反应器2,打开流量计阀门,然后同时打开反应器2两端恒压系统,通过观察差压传感器45不断调整两端恒压压力,使反应器2上端始终比反应器2下端大出一定的稳定压力值,进行气体渗流实验,起初会排出部分压裂液,当流量计排气流量稳定后测算平均流速,以计算沉积物渗透率。After the fracturing test is completed, open the valve of the gas cylinder 47 to pump a certain pressure of gas into the reactor 2, open the flow meter valve, and then open the constant pressure system at both ends of the reactor 2 at the same time, and constantly adjust the constant pressure at both ends by observing the differential pressure sensor 45. The upper end of the reactor 2 is always higher than the lower end of the reactor 2 by a certain stable pressure value. The gas percolation experiment is carried out. At first, part of the fracturing fluid will be discharged. When the exhaust flow of the flowmeter is stable, the average flow rate is calculated to calculate the deposition.物Permeability.
压裂测试完成后,打开第一阀门411、第二阀门421、流量计和流量阀门,并打开供气阀门471将一定压力的气体打入反应器2,然后同时打开反应器2两端第一恒压系统43、第二恒压系统44、恒压阀门431和第二阀门421,打开差压传感器45,通过观察差压传感器45不断调整反应器2两端恒压压力,使反应器2上端始终比反应器2下端大出一定的稳定压力值,进行气体渗流实验。起初将排出部分压裂液,当流量计排气流量稳定后测算平均流速,用以计算沉积物渗透率。After the fracturing test is completed, open the first valve 411, the second valve 421, the flow meter and the flow valve, and open the gas supply valve 471 to pump a certain pressure of gas into the reactor 2, and then open the first two ends of the reactor 2 at the same time. Constant pressure system 43, second constant pressure system 44, constant pressure valve 431 and second valve 421, open the differential pressure sensor 45, and constantly adjust the constant pressure at both ends of the reactor 2 by observing the differential pressure sensor 45 to make the upper end of the reactor 2 Always a certain stable pressure value greater than the lower end of the reactor 2 for gas percolation experiments. At first, part of the fracturing fluid will be discharged. When the exhaust flow of the flow meter is stable, the average flow rate is measured to calculate the sediment permeability.
(6)改变温压条件(6) Change the temperature and pressure conditions
改变沉积物和压裂液的温度或压力,进行下一轮测试。Change the temperature or pressure of the sediment and fracturing fluid, and proceed to the next round of testing.
以上则是本装置具体的所有使用步骤,本发明可以在高压低温条件下原位合成天然气水合物沉积物,对沉积物进行压裂实验,并测量其渗透率,扩展了目前所存在实验测试装置的使用范围,提高了实验测试的精确度和便利度。本申请这样的设计支持原位合成水合物沉积物样品23,能合理模拟储层地应力以及温压条件,可以较完整地还原出注液、压裂、加支撑剂等水力压裂常规操作步骤,还可以测量压裂前后和不同压裂条件下储层渗透率的变化并观察压裂效果,对天然气水合物沉积物的压裂机理和压裂前后储层渗透率变化的研究有一定的指导作用。The above are all the specific use steps of this device. The invention can synthesize natural gas hydrate deposits in situ under high pressure and low temperature conditions, perform fracturing experiments on the deposits, and measure the permeability, which expands the existing experimental test devices. The range of use improves the accuracy and convenience of experimental testing. The design of this application supports the in-situ synthesis of hydrate sediment sample 23, can reasonably simulate the reservoir stress and temperature and pressure conditions, and can more completely restore the conventional hydraulic fracturing operation steps such as fluid injection, fracturing, and proppant addition. It can also measure the changes in reservoir permeability before and after fracturing and under different fracturing conditions and observe the fracturing effect. It provides certain guidance for the study of the fracturing mechanism of gas hydrate sediments and the changes in reservoir permeability before and after fracturing. effect.
上述实施例只是为了说明本发明的技术构思及特点,其目的是在于让本领域内的普通技术人员能够了解本发明的内容并据以实施,并不能以此限制本发明的保护范围。凡是根据本发明内容的实质所做出的等效的变化或修饰,都应涵盖在本发明的保护范围内。The above-mentioned embodiments are only to illustrate the technical concept and characteristics of the present invention, and their purpose is to enable those of ordinary skill in the art to understand the content of the present invention and implement them accordingly, and should not limit the protection scope of the present invention. All equivalent changes or modifications made according to the essence of the present invention should be covered by the protection scope of the present invention.

Claims (8)

  1. 一种天然气水合物矿藏压裂实验装置,其特征在于:包括支架(1)以及设置在支架(1)上用于合成样品并对其进行压裂改造的反应器(2),所述反应器(2)上设置有样品合成系统(3)、渗透率测试系统(4)以及数据采集及控制系统(6),所述反应器(2)中上还设有用于进行压裂改造的水力压裂系统(5)。An experimental device for fracturing a natural gas hydrate deposit, which is characterized by comprising a support (1) and a reactor (2) arranged on the support (1) for synthesizing samples and fracturing them. (2) A sample synthesis system (3), a permeability test system (4), and a data acquisition and control system (6) are provided on the reactor (2). The reactor (2) is also provided with hydraulic pressure for fracturing reformation. Split system (5).
  2. 根据权利要求1所述的天然气水合物矿藏压裂实验装置,其特征在于:所述反应器(2)包括反应器筒体(21)和设置在反应器筒体(21)一端的反应器端盖(22),所述反应器筒体(21)内用于放置水合物沉积物样品(23),所述样品合成系统(3)设置在反应器筒体(21)远离反应器端盖(22)的一端,所述样品合成系统(3)、反应器筒体(21)以及反应器端盖(22)之间的空间形成内腔,所述反应器端盖(22)与水合物沉积物样品(23)之间设置有第一透水板(25),所述样品合成系统(3)与水合物沉积物样品(23)之间设置有第二透水板(24)。The fracturing experimental device for natural gas hydrate deposits according to claim 1, characterized in that: the reactor (2) comprises a reactor cylinder (21) and a reactor end arranged at one end of the reactor cylinder (21) A cover (22) for placing a hydrate sediment sample (23) in the reactor cylinder (21), and the sample synthesis system (3) is arranged on the reactor cylinder (21) away from the reactor end cover ( 22), the space between the sample synthesis system (3), the reactor cylinder (21) and the reactor end cover (22) forms an inner cavity, and the reactor end cover (22) is deposited with hydrate A first permeable plate (25) is arranged between the sample (23), and a second permeable plate (24) is arranged between the sample synthesis system (3) and the hydrate sediment sample (23).
  3. 根据权利要求2所述的天然气水合物矿藏压裂实验装置,其特征在于:所述样品合成系统(3)包括与第二透水板(24)相抵的活塞(31)、设置在反应器筒体(21)远离反应器端盖(22)的一端的密封塞(32)以及连接在活塞(31)与密封塞(32)之间的反应器筒体(21)的侧壁上的手动增压泵(33),所述手动增压泵(33)与反应器筒体(21)之间设置有增压阀门(34)。The natural gas hydrate deposit fracturing experiment device according to claim 2, characterized in that: the sample synthesis system (3) comprises a piston (31) that is opposed to the second permeable plate (24), and is arranged in the reactor cylinder (21) Manual pressurization on the sealing plug (32) at the end away from the end cover (22) of the reactor and the side wall of the reactor cylinder (21) connected between the piston (31) and the sealing plug (32) A pump (33), a boost valve (34) is arranged between the manual booster pump (33) and the reactor cylinder (21).
  4. 根据权利要求2所述的天然气水合物矿藏压裂实验装置,其特征在于:所述渗透率测试系统(4)包括连接至反应器端盖(22)的一端的内腔内的第一输气管道(41)、与第一输气管道(41)连接的第一恒压系统(43)、连接至样品合成系统(3)一端的内腔内的第二输气管道(42)、与第二输气管道(42)连接的第二恒压系统(44)以及与第二恒压系统(44)连接的流量计,所述第一输气管道(41)上设有第一阀门(411),所述第二输气管道(42)上设有第二阀门(421),所述第一恒压系统(43)与第一输气管道(41)支架(1)设有恒压阀门(431),所述流量计连接有流量阀门,所述第一恒压系统(43)和第二恒压系统(44)之间连接有差压传感器(45),所述差压传感器(45)和流量计均连接至数据采集及控制系统(6)。The natural gas hydrate deposit fracturing experiment device according to claim 2, characterized in that: the permeability test system (4) comprises a first gas transmission in the inner cavity connected to one end of the reactor end cover (22) The pipeline (41), the first constant pressure system (43) connected to the first gas pipeline (41), the second gas pipeline (42) in the cavity connected to one end of the sample synthesis system (3), and the A second constant pressure system (44) connected to the second gas pipeline (42) and a flow meter connected to the second constant pressure system (44), the first gas pipeline (41) is provided with a first valve (411) ), the second gas pipeline (42) is provided with a second valve (421), the first constant pressure system (43) and the first gas pipeline (41) bracket (1) are provided with a constant pressure valve (431), the flow meter is connected with a flow valve, and a differential pressure sensor (45) is connected between the first constant pressure system (43) and the second constant pressure system (44), the differential pressure sensor (45) ) And the flow meter are both connected to the data acquisition and control system (6).
  5. 根据权利要求4所述的天然气水合物矿藏压裂实验装置,其特征在于:所述渗透率测试系统(4)还连接有抽真空系统(46)和用以给反应供气和提供测试渗透率的气体的气瓶(47),所述抽真空系统(46)和气瓶(47)均连接至第一输气管道(41),所述抽真空系统(46)与第一输气管道(41)之间设置有抽真空阀门(461),所述气瓶(47)与第一输气管道(41)之间设置有供气阀门(471)。The natural gas hydrate deposit fracturing experiment device according to claim 4, characterized in that: the permeability test system (4) is also connected with a vacuum system (46) and used to supply gas to the reaction and provide test permeability The gas cylinder (47) of the gas, the vacuum system (46) and the gas cylinder (47) are both connected to the first gas pipeline (41), and the vacuum system (46) is connected to the first gas pipeline (41). A vacuum valve (461) is arranged between ), and an air supply valve (471) is arranged between the gas cylinder (47) and the first gas pipeline (41).
  6. 根据权利要求2所述的天然气水合物矿藏压裂实验装置,其特征在于:所述水力压裂系统(5)包括从反应器筒体(21)的侧壁连接至内腔内的水力射流管(51)以及与水力射流管(51) 连接的压裂泵系统(52),所述水力射流管(51)的出口方向与反应器(2)的轴线方向一致,所述水力射流管(51)上设有加砂装置(53),所述加砂装置(53)和反应器筒体(21)的侧壁之间设有压裂阀门(54)。The fracturing experimental device for natural gas hydrate deposits according to claim 2, characterized in that: the hydraulic fracturing system (5) comprises a hydraulic jet pipe connected from the side wall of the reactor cylinder (21) to the inner cavity (51) and a fracturing pump system (52) connected with a hydraulic jet tube (51), the outlet direction of the hydraulic jet tube (51) is consistent with the axial direction of the reactor (2), and the hydraulic jet tube (51) ) Is provided with a sanding device (53), and a fracturing valve (54) is provided between the sanding device (53) and the side wall of the reactor cylinder (21).
  7. 根据权利要求2所述的天然气水合物矿藏压裂实验装置,其特征在于:所述数据采集及控制系统(6)包括计算机(61)以及与计算机(61)连接的温度传感器(62)和压力传感器(63),所述温度传感器(62)设置在反应器端盖(22)上,以采集内腔内部的温度参数数据,所述压力传感器(63)连接设置在样品合成系统(3)、渗透率测试系统(4)以及水力压裂系统(5)上,以采集各系统压力参数数据。The natural gas hydrate deposit fracturing experiment device according to claim 2, characterized in that: the data acquisition and control system (6) comprises a computer (61) and a temperature sensor (62) connected to the computer (61) and pressure Sensor (63), the temperature sensor (62) is arranged on the end cover (22) of the reactor to collect temperature parameter data inside the cavity, and the pressure sensor (63) is connected to the sample synthesis system (3), The permeability testing system (4) and the hydraulic fracturing system (5) are used to collect the pressure parameter data of each system.
  8. 根据权利要求2所述的天然气水合物矿藏压裂实验装置,其特征在于:还包括设置在反应器筒体(21)上内腔对应位置处的侧壁上的摄影照明系统(7),所述摄影照明系统(7)包括设置在反应器筒体(21)的侧壁的用于观测内腔内部情况的蓝宝石筒(73)以及连接在反应器筒体(21)上的摄像机(71)和照明灯(72),所述摄像机(71)的镜头正对蓝宝石筒(73),以观测内腔内部情况。The natural gas hydrate deposit fracturing experiment device according to claim 2, characterized in that it further comprises a photographic lighting system (7) arranged on the side wall at the corresponding position of the inner cavity of the reactor cylinder (21), so The photographic lighting system (7) includes a sapphire cylinder (73) arranged on the side wall of the reactor cylinder (21) for observing the conditions inside the cavity and a camera (71) connected to the reactor cylinder (21) And an illuminating lamp (72), the lens of the camera (71) is directly facing the sapphire tube (73) to observe the internal situation of the inner cavity.
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CN113984531A (en) * 2021-10-22 2022-01-28 中国石油大学(北京) Experimental method and experimental device for researching influence of hydration on fracturing energy storage efficiency
CN113984531B (en) * 2021-10-22 2022-08-19 中国石油大学(北京) Experimental method for researching influence of hydration on fracturing energy storage efficiency

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