WO2021023295A1 - Zizyphus jujube slice drying method using cold plasma activated water - Google Patents
Zizyphus jujube slice drying method using cold plasma activated water Download PDFInfo
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- WO2021023295A1 WO2021023295A1 PCT/CN2020/107754 CN2020107754W WO2021023295A1 WO 2021023295 A1 WO2021023295 A1 WO 2021023295A1 CN 2020107754 W CN2020107754 W CN 2020107754W WO 2021023295 A1 WO2021023295 A1 WO 2021023295A1
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B7/00—Preservation or chemical ripening of fruit or vegetables
- A23B7/02—Dehydrating; Subsequent reconstitution
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B7/00—Preservation or chemical ripening of fruit or vegetables
- A23B7/14—Preserving or ripening with chemicals not covered by groups A23B7/08 or A23B7/10
- A23B7/153—Preserving or ripening with chemicals not covered by groups A23B7/08 or A23B7/10 in the form of liquids or solids
- A23B7/157—Inorganic compounds
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
- Y02P60/80—Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
- Y02P60/85—Food storage or conservation, e.g. cooling or drying
Definitions
- the invention relates to the technical field of agricultural products processing, in particular to a method for drying red jujube slices using cold plasma to activate water.
- Zizyphus jujube also known as jujube, belongs to the phylum Angiosperm, Dicotyledon, Rhamnaria, Rhamnaceae, and Jujube.
- Red dates are rich in sugars, amino acids, vitamin C and organic acids.
- red dates also contain a variety of biologically active substances, such as phenolic compounds, red date polysaccharides, cyclic adenylate, and triterpenoids.
- Chinese medicine believes that red dates are sweet and warm in nature, soothing the nerves, helping sleep, protecting the spleen and stomach, nourishing qi and blood, and delaying aging. Studies have shown that phenolic compounds in red dates have biological activities such as antioxidant, anti-tumor, and antibacterial.
- Dried jujube slices are a traditional processed product of red dates in my country, as well as an important product of my country's current red date processing.
- Hot air drying method processing is currently one of the most widely used methods, but hot air drying is a high-energy-consuming unit operation.
- Plasma is the fourth state of matter after solid, liquid and gaseous states.
- gas molecules are ionized to produce a mixture of electrons, ions, atoms and atomic groups.
- Cold plasma refers to a plasma with a lower overall temperature generated under atmospheric pressure (normal pressure) conditions. Due to the advantages of being able to generate under normal pressure, low gas temperature (close to or slightly higher than room temperature), high content of active components, no pollution, no waste, etc., cold plasma is used in food processing, medicine and health, environmental protection, biological Many fields such as medicine have shown broad application prospects. As an emerging non-thermal food processing technology, cold plasma technology has received widespread attention.
- the application of cold plasma technology in food processing includes the killing of harmful microorganisms in food, the processing of packaging materials, the functional modification of food ingredients, the improvement of seed germination, the improvement of the physical and chemical properties of grains, and the degradation of pesticide residues.
- cold plasma treatment of fatty foods and other sensitive foods may induce chemical changes.
- the efficiency of cold plasma treatment is largely affected by the surface morphology of the sample. Therefore, the cold plasma jet system can be used to generate plasma discharge on the water surface or directly in the water to prepare cold plasma activated water, and the cold plasma activated water is used for sample pretreatment.
- a chemical reaction occurs to form active oxygen species and active nitrogen species.
- the invention discloses a drying pretreatment method for jujube slices, which adopts cold plasma activated water to pretreat fresh jujube slices, thereby reducing the hot air drying time of the jujube slices, improving drying efficiency, reducing drying energy consumption, and increasing the content of biological active components of the jujube slices.
- the pretreatment process can increase the water diffusion efficiency, reduce the hot air drying time, effectively reduce the hot air drying time of the red date slices, and at the same time reduce the degradation of phenolic substances, thereby increasing the total phenol content in the dried red date slices.
- the technical scheme of the present invention is as follows:
- the embodiment of the invention discloses a method for drying jujube slices using cold plasma activated water, which specifically includes the following steps:
- the cold plasma equipment body is used to pretreat water to prepare cold plasma activated water; the output power of the cold plasma equipment is 600-900W, the flow rate of the cold plasma gas flow is 100-300L/min, and the pretreatment time is 5-40min.
- the cold plasma activated water used in the step (2) is the cold plasma activated water obtained in step (1) that has not been immersed and used, or the cold plasma that has been immersed and used in step (2) one or more times. Activated water.
- the cold plasma activated water is repeatedly used no more than 3 times, and it is more preferable to use it repeatedly only once.
- step (1) of the present invention Under the conditions of step (1) of the present invention, according to the content of the water to be treated, about 10-50L cold plasma activated water that meets the pretreatment requirements and has a better implementation effect can be prepared.
- the output power of the cold plasma equipment is 600-800 W
- the flow rate of the cold plasma gas flow is 100-200 L/min
- the pretreatment time is 5-20 min.
- the cold plasma activated water is kept in an ice water bath during preparation.
- the ice water bath can prevent the water temperature from rising too high during the preparation process.
- step (2) the fresh red dates are washed and then cored and sliced, and the thickness of the red date slices is 4-8 mm.
- the fresh red date slices are completely immersed in cold plasma activated water, and the immersion time is 0.5-2 min.
- the soaking temperature has no significant influence on the soaking effect. It can be carried out at room temperature, or it can be carried out in a wider temperature range (such as 0-50°C) according to the actual production environment and production conditions.
- step (2) take it out after soaking, and use absorbent paper to dry the surface moisture.
- the hot air drying temperature is 50-70° C.
- the wind speed is 1-2 m/s.
- step (3) at the end of hot air drying, the moisture content of the red date slices is controlled to not exceed 5% on a wet basis.
- the present invention has the following advantages:
- the invention adopts cold plasma activated water to pretreat the jujube slices, which is green and pollution-free.
- the jujube slices treated with cold plasma activated water have no hidden food safety hazards, and the cold plasma activated water has a sterilization function to a certain extent; the present invention optimizes the treatment time and treatment methods of the cold plasma activated water.
- the invention adopts cold plasma activated water to pretreat the jujube slices.
- the processing capacity of the jujube slices per unit time is larger and the processing efficiency is higher; the direct treatment with the cold plasma requires attention to the jujube slices and cold plasma
- the distance and the positional relationship between the plasma treatment technology require high process. If the process is not properly controlled, the pretreatment effect will be unsatisfactory, and it will also cause nutritional damage to the red jujube slices, which makes the cold plasma direct pretreatment process less efficient , Poor operability.
- cold plasma activated water in the process of the present invention can be reused many times, and it still has a good pretreatment effect (in the case of repeated 1-3 times, all have a good pretreatment effect), This greatly reduces the use cost of cold plasma equipment and improves the efficiency of pretreatment.
- cold plasma activated water treatment can reduce the drying time by up to 20% (as shown in Figure 5), and can significantly increase the polyphenols of dried jujube slices (as shown in Figure 6, up to 16%) ), flavonoids (as shown in Figure 7, up to 29%) and procyanidins (as shown in Figure 8, up to 31%).
- the experimental results show that direct cold plasma treatment will cause the destruction of vitamin C in the jujube slices. Compared with the untreated group, the vitamin C content is reduced by up to 50% (as shown in Figure 9).
- the compact fiber structure on the surface of the red date slices opens, forming more uniform holes or pores, so that the quality of the final dried red date slices is more stable and uniform, which can effectively reduce the hot air drying time; while the plasma direct treatment Later, the red date slices have uneven surface holes, and some of the surfaces are burnt, resulting in shrinkage; this makes the quality of dried shiitake mushroom products obtained in the subsequent hot air drying stage unstable; for dry red date slices with unsatisfactory quality, they often need to be selected for further drying or Processing of defective products.
- the jujube slices are evenly immersed in the activated water during the pretreatment stage. Therefore, the jujube slices are relatively uniform before entering the hot air drying, and it is easy to obtain dry red date slices with stable quality.
- the present invention finds for the first time that cold plasma activated water pretreatment can effectively increase the content of phenolic substances in hot-air dried red date slices and improve the quality of dried red date slices.
- the cold plasma activated water is rich in reactive oxygen species (ROS) and reactive nitrogen molecules (RNS).
- ROS and RNS have a peroxidation effect, which can destroy the membrane lipids of the jujube slice cells, cause the cell membrane to rupture, and release the jujube slice cell sap, thereby enhancing Drying rate.
- Cold plasma activated water pretreatment can significantly increase the active substance content of dried jujube slices.
- cold plasma activated water pretreatment can increase the hot air drying rate of red jujube slices, thereby reducing the thermal degradation of active substances; on the other hand, The cold plasma activated water pretreatment can oxidize part of the active substances on the surface of the jujube slices to form an anti-oxidation protective film. The formation of this film can reduce the oxidative degradation of the active substances in the jujube slices during the drying process.
- the invention provides a new food processing application for cold plasma activated water and expands a new application field.
- Figure 1 is a comparison diagram of the drying time of the jujube slices of Comparative Example 1-3 and Example 1-3;
- Figure 2 is a comparison diagram of the total phenol content of jujube tablets of Comparative Example 1-3 and Example 1-3;
- Figure 3 is a comparison diagram of flavonoid content of jujube tablets of Comparative Example 1-3 and Example 1-3;
- Example 4 is a comparison diagram of the proanthocyanidin content of jujube slices of Comparative Example 1-3 and Example 1-3;
- Figure 5 is a comparison diagram of the drying time of the jujube slices of Comparative Examples 4-6 and Examples 1-3;
- Figure 6 is a comparison diagram of the total phenol content of jujube tablets of Comparative Examples 4-6 and Examples 1-3;
- Figure 7 is a comparison diagram of the flavonoid content of the jujube tablets of Comparative Examples 4-6 and Examples 1-3;
- Fig. 8 is a comparison diagram of proanthocyanidin content of jujube slices of Comparative Examples 4-6 and Examples 1-3;
- Figure 9 is a comparison diagram of the vitamin C content of the jujube tablets of Comparative Example 1-6 and Example 1-3.
- the fresh red dates are washed and then cored and sliced.
- the thickness of the red dates is 6mm.
- For fresh red date slices without pretreatment preheat the temperature of the hot air dryer to 50°C, put the red date slices in for hot air drying at a wind speed of 1.0m/s, and measure the water content of the red date slices every 30 minutes. When the water content of the red date slices is lower than Stop drying at 5% (based on wet basis) to obtain dried red date flakes.
- the drying time is 1050min
- the polyphenol content in dried red date tablets is 13.56mg/g DW (dry basis)
- the flavonoid content in dried red date tablets is 3.26mg/g DW (dry basis)
- the proanthocyanidin content in dried red date tablets is 2.56 mg/g DW (dry basis)
- the vitamin C content in dried red jujube tablets is 1.38mg/g DW (dry basis).
- the fresh red dates are washed and then cored and sliced.
- the thickness of the red dates is 6mm.
- the fresh red date slices are not pre-treated, the hot air dryer temperature is preheated to 60°C, and the red date slices are put in for hot air drying at a wind speed of 1.0m/s.
- the water content of the red date slices is measured every 30 minutes. When the water content of the red date slices is lower than Stop drying at 5% (based on wet basis) to obtain dried red date flakes.
- the drying time is 630 minutes, the polyphenol content in the dried red jujube tablets is 14.26mg/g DW (dry basis), the flavonoid content in the dried jujube tablets is 4.01mg/g DW (dry basis), and the proanthocyanidin content in the dried red jujube tablets is 2.58
- the vitamin C content in mg/g DW (dry basis) dried red jujube tablets is 1.62mg/g DW (dry basis).
- the fresh red dates are washed and then cored and sliced.
- the thickness of the red dates is 6mm.
- the hot air dryer temperature is preheated to 70°C, and the red date slices are put in for hot air drying at a wind speed of 1.0m/s.
- the water content of the red date slices is measured every 30 minutes. When the water content of the red date slices is lower than Stop drying at 5% (based on wet basis) to obtain dried red date flakes.
- the drying time is 540min
- the polyphenol content in dried red date tablets is 14.33mg/g DW (dry basis)
- the flavonoid content in dried red date tablets is 3.48mg/g DW (dry basis)
- the proanthocyanidin content in dried red date tablets is 2.18
- the vitamin C content in mg/g DW (dry basis) dried red jujube tablets is 1.44mg/g DW (dry basis).
- the output power of the cold plasma equipment was adjusted to 600W, the flow rate of the cold plasma gas flow was 200L/min, and the water was pretreated for 20 minutes (the water was kept in an ice water bath during the entire treatment process) to prepare 25L of cold plasma activated water.
- the fresh red dates are washed and then cored and sliced. The thickness of the red dates is 6mm.
- the fresh red date slices are completely immersed in cold plasma activated water for 2 minutes, and then taken out after soaking, and the surface water is wiped off with absorbent paper. Preheat the temperature of the hot air dryer to 50°C, put the pretreated red date slices into hot air drying at a wind speed of 1.0m/s, and measure the water content of the red date slices every 30 minutes. When the water content of the red date slices is less than 5% (to Drying was stopped at the time of wet basis, and dried red date slices were obtained.
- the drying time is 930 minutes
- the content of polyphenols in dried red date tablets is 15.26mg/g DW (dry basis)
- the content of flavonoids in dried red date tablets is 4.95 mg/g DW (dry basis)
- the content of proanthocyanidins in dried red date tablets is 3.38 mg/g DW (dry basis)
- the vitamin C content in dried red jujube tablets is 1.37mg/g DW (dry basis).
- the fresh red dates are washed and then cored and sliced.
- the thickness of the red dates is 6mm.
- Direct cold plasma treatment is adopted, the output power of the cold plasma equipment is adjusted to 600W, the flow rate of the cold plasma gas flow is 200L/min, the cold plasma probe is 15cm away from the surface of the jujube slice, and the pretreatment is 5min.
- the drying time is 1020 minutes
- the polyphenol content in the dried red date tablets is 14.28mg/g DW (dry basis)
- the flavonoid content in the dried red date tablets is 3.85 mg/g DW (dry basis)
- the proanthocyanidin content in the dried red date tablets is 2.59 mg/g DW (dry basis)
- the vitamin C content in dried red jujube tablets is 0.69mg/g DW (dry basis).
- the output power of the cold plasma equipment was adjusted to 800W, the flow rate of the cold plasma gas flow was 150L/min, and the water was pretreated for 5 minutes (keeping in an ice water bath) to prepare 10L of cold plasma activated water.
- the fresh red dates are washed and then cored and sliced. The thickness of the red dates is 6mm.
- the fresh red date slices are completely immersed in cold plasma activated water for 0.5 min. After soaking, they are taken out, and the surface water is wiped off with absorbent paper. Preheat the temperature of the hot air dryer to 60°C, put the pretreated red date slices into hot air drying at a wind speed of 1.0m/s, and measure the water content of the red date slices every 30 minutes. When the water content of the red date slices is less than 5% (to Drying was stopped at the time of wet basis, and dried red date slices were obtained.
- the drying time is 510 minutes, the content of polyphenols in dried red date tablets is 16.29mg/g DW (dry basis), the content of flavonoids in dried red date tablets is 4.39mg/g DW (dry basis), and the content of proanthocyanidins in dried red date tablets is 2.99
- the vitamin C content in mg/g DW (dry basis) dried red jujube tablets is 1.72mg/g DW (dry basis).
- the fresh red dates are washed and then cored and sliced.
- the thickness of the red dates is 6mm.
- Direct cold plasma processing is adopted, the output power of the cold plasma equipment is adjusted to 800W, the flow rate of the cold plasma gas flow is 150L/min, the cold plasma probe is 5cm away from the surface of the jujube slice, and the pretreatment is 3min.
- the drying time is 580min
- the polyphenol content in dried red date tablets is 14.04mg/g DW (dry basis)
- the flavonoid content in dried red date tablets is 3.94mg/g DW (dry basis)
- the proanthocyanidin content in dried red date tablets is 2.66 mg/g DW (dry basis)
- the vitamin C content in dried red jujube tablets is 1.35mg/g DW (dry basis).
- the output power of the cold plasma equipment was adjusted to 700W, the flow rate of the cold plasma gas flow was 100L/min, and the water was pretreated for 10 minutes (keeping in an ice water bath) to prepare 15L of cold plasma activated water.
- the fresh red dates are washed and then cored and sliced. The thickness of the red dates is 6mm.
- the fresh red date slices are completely immersed in cold plasma activated water for 1 min. After soaking, they are taken out, and the surface water is wiped off with absorbent paper. Preheat the temperature of the hot air dryer to 70°C, put the pre-treated red date slices into hot air drying at a wind speed of 1.0m/s, and measure the water content of the red date slices every 30 minutes. When the water content of the red date slices is less than 5% (to Drying was stopped at the time of wet basis, and dried red date slices were obtained.
- the drying time is 360 minutes
- the content of polyphenols in dried red date tablets is 15.37mg/g DW (dry basis)
- the content of flavonoids in dried red date tablets is 4.15 mg/g DW (dry basis)
- the content of proanthocyanidins in dried red date tablets is 2.74 mg/g DW (dry basis)
- the vitamin C content in dried red jujube tablets is 1.40mg/g DW (dry basis).
- the fresh red dates are washed and then cored and sliced.
- the thickness of the red dates is 6mm.
- Direct treatment with cold plasma is adopted, the output power of the cold plasma equipment is adjusted to 700W, the flow rate of the cold plasma gas flow is 100L/min, the cold plasma probe is 10cm away from the surface of the jujube slice, and the pretreatment is 6min.
- the drying time is 450min
- the polyphenol content in dried red date tablets is 14.13mg/g DW (dry basis)
- the flavonoid content in dried red date tablets is 3.43mg/g DW (dry basis)
- the proanthocyanidin content in dried red dates tablets is 2.22 mg/g DW (dry basis)
- the vitamin C content in dried red jujube tablets is 0.77mg/g DW (dry basis).
- the output power of the cold plasma equipment was adjusted to 900W, the flow rate of the cold plasma gas flow was 300L/min, and the water was pretreated for 40min (keeping in an ice water bath) to prepare 50L of cold plasma activated water.
- the fresh red dates are washed and then cored and sliced. The thickness of the red dates is 10mm.
- the fresh red date slices are completely immersed in cold plasma activated water for 5 minutes, and then taken out after soaking, and the surface water is wiped dry with absorbent paper. Preheat the temperature of the hot air dryer to 55°C, put the pretreated red date slices into hot air drying at a wind speed of 1.5m/s, and measure the water content of the red date slices every 30 minutes. When the water content of the red date slices is less than 5% (to Drying was stopped at the time of wet basis, and dried red date slices were obtained.
- the drying time is 630 minutes
- the polyphenol content in the dried red date tablets is 15.26mg/g DW (dry basis)
- the flavonoid content in the dried red date tablets is 4.35 mg/g DW (dry basis)
- the proanthocyanidin content in the dried red date tablets is 3.08 mg/g DW (dry basis)
- the vitamin C content in dried red jujube tablets is 1.45mg/g DW (dry basis).
- the output power of the cold plasma equipment was adjusted to 750W, the flow rate of the cold plasma gas flow was 250L/min, and the water was pretreated for 30min (keeping in an ice water bath) to prepare 35L of cold plasma activated water.
- the fresh red dates are washed and then cored and sliced. The thickness of the red dates is 2mm.
- the fresh red date slices are completely immersed in cold plasma activated water (the cold plasma activated water is used for the first time), and the immersion time is 3 minutes. After soaking, take it out, and use absorbent paper to dry the surface water. Preheat the temperature of the hot air dryer to 65°C, put the pre-treated red date slices into hot air drying at a wind speed of 2.0m/s, and measure the water content of the red date slices every 30 minutes. When the water content of the red date slices is less than 5% (to Drying was stopped at the time of wet basis, and dried red date slices were obtained.
- the drying time is 450min
- the polyphenol content in dried red date tablets is 15.66mg/g DW (dry basis)
- the flavonoid content in dried red date tablets is 4.01mg/g DW (dry basis)
- the proanthocyanidin content in dried red date tablets is 2.63 mg/g DW (dry basis)
- the vitamin C content in dried red jujube tablets is 1.57mg/g DW (dry basis).
- the fresh red jujube slices were immersed and dried with hot air with the cold isocyanine in vitro activated water after the initial soaking in Example 5.
- the second use of cold plasma activated water completely soak the fresh red date slices in cold plasma activated water (the second use of cold plasma activated water), soaking time is 3 minutes, after soaking, take it out, use absorbent paper to dry the surface water . Preheat the temperature of the hot air dryer to 65°C, put the pre-treated red date slices into hot air drying at a wind speed of 2.0m/s, and measure the water content of the red date slices every 30 minutes. When the water content of the red date slices is less than 5% (to Drying was stopped at the time of wet basis, and dried red date slices were obtained.
- the drying time is 460min
- the content of polyphenols in dried red date tablets is 15.59mg/g DW (dry basis)
- the content of flavonoids in dried red date tablets is 4.01mg/g DW (dry basis)
- the content of proanthocyanidins in dried red date tablets is 2.68 mg/g DW (dry basis)
- the vitamin C content in dried red jujube tablets is 1.52mg/g DW (dry basis).
- the fresh red jujube slices were immersed and dried with hot air with the cold plasma activated water after the second immersion used in Example 5 (cold plasma activated water was used for the third time).
- the third use of cold plasma activated water completely immerse the fresh red date slices in cold plasma activated water (the third use of cold plasma activated water), soaking time is 3min, after soaking, take it out, use absorbent paper to dry the surface water .
- Preheat the temperature of the hot air dryer to 65°C put the pre-treated red date slices into hot air drying at a wind speed of 2.0m/s, and measure the water content of the red date slices every 30 minutes.
- the water content of the red date slices is less than 5% (to Drying was stopped at the time of wet basis, and dried red date slices were obtained.
- the drying time is 460min
- the polyphenol content in dried red date tablets is 15.56mg/g DW (dry basis)
- the flavonoid content in dried red date tablets is 3.97 mg/g DW (dry basis)
- the proanthocyanidin content in dried red date tablets is 2.56 mg/g DW (dry basis)
- the vitamin C content in dried red jujube tablets is 1.55mg/g DW (dry basis).
- the cold plasma activated water pretreatment method of Example 1-3 of the present invention is compared with the non-pretreated Comparative Example 1-3 at the same hot air drying temperature and Under wind speed conditions, the drying time can be reduced by up to 33%, the polyphenol content in dried red date tablets can be increased by 14%, the flavonoid content in dried red date tablets can be increased by 52%, and the proanthocyanidin content in dried red date tablets can be increased by 32%.
- the cold plasma activated water is rich in reactive oxygen species (ROS) and reactive nitrogen molecules (RNS).
- ROS and RNS have a peroxidation effect, which can destroy the membrane lipids of the jujube slice cells, cause the cell membrane to rupture, and release the jujube slice cell sap, thereby enhancing Drying rate.
- Cold plasma activated water pretreatment can significantly increase the active substance content of dried jujube slices.
- cold plasma activated water pretreatment can increase the hot air drying rate of red jujube slices, thereby reducing the thermal degradation of active substances;
- the cold plasma activated water pretreatment can oxidize part of the active substances on the surface of the jujube slices to form an anti-oxidation protective film. The formation of this film can reduce the oxidative degradation of the active substances in the jujube slices during the drying process.
- the cold plasma activated water treatment can reduce the drying time by up to 20% compared with the cold plasma direct treatment (as shown in Figure 5), and can significantly improve The content of dried jujube slices polyphenols (as shown in Fig. 6 up to 16%), flavonoids (as shown in Fig. 7 up to 29%) and proanthocyanidins (as shown in Fig. 8 up to 31%).
- the experimental results show that direct cold plasma treatment will cause the destruction of vitamin C in the jujube slices. Compared with the untreated group, the vitamin C content is reduced by up to 50% (as shown in Figure 9).
- the present invention adopts cold plasma activated water pretreatment to improve the hot-air drying rate and biological activity of jujube slices.
- the method of ingredient content can increase the drying rate of dried red date slices, reduce drying energy consumption, and improve the quality of dried red date slices.
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Abstract
A zizyphus jujube slice drying method using cold plasma activated water. The method comprises the following steps: preparing cold plasma activated water; using the cold plasma activated water to carry out an immersion treatment on fresh zizyphus jujube slices; and performing a hot air drying treatment on the pretreated fresh zizyphus jujube slices to obtain dried zizyphus jujube slices.
Description
本发明涉及农产品加工技术领域,特别涉及一种一种采用冷等离子体活化水的红枣片干燥方法。The invention relates to the technical field of agricultural products processing, in particular to a method for drying red jujube slices using cold plasma to activate water.
红枣(Zizyphus jujube),又名大枣,属于被子植物门,双子叶植物纲、鼠李目、鼠李科、枣属。红枣含有丰富的糖类、氨基酸、维生素C和有机酸等。此外,红枣中还含有多种生物活性物质,酚类化合物、红枣多糖、环腺苷酸、三萜类化合物等。中医认为,红枣性味甘温,有安神助眠,保健脾胃,补气养血,延缓衰老等功效。研究表明,红枣中酚类化合物具有抗氧化、抗肿瘤、抗菌等生物活性。红枣鲜果因含水量高、不易储存和运输,造成了极大的浪费,因此采摘后需要及时进行加工。目前最常用的加工贮存方式,旨在将食品中水分含量降低到安全水平,在此水平下将最大程度抑制微生物腐败和水分介导的变质反应。干枣片是我国传统的红枣加工产品,也是目前我国红枣加工的重要产品。热风干燥方法加工是目前使用最广泛的方法之一,但热风干燥是一种高耗能单元操作。Zizyphus jujube, also known as jujube, belongs to the phylum Angiosperm, Dicotyledon, Rhamnaria, Rhamnaceae, and Jujube. Red dates are rich in sugars, amino acids, vitamin C and organic acids. In addition, red dates also contain a variety of biologically active substances, such as phenolic compounds, red date polysaccharides, cyclic adenylate, and triterpenoids. Chinese medicine believes that red dates are sweet and warm in nature, soothing the nerves, helping sleep, protecting the spleen and stomach, nourishing qi and blood, and delaying aging. Studies have shown that phenolic compounds in red dates have biological activities such as antioxidant, anti-tumor, and antibacterial. Because of the high water content of the red jujube, it is difficult to store and transport, which causes great waste, so it needs to be processed in time after picking. At present, the most commonly used method of processing and storage aims to reduce the moisture content in food to a safe level, at which level it will minimize microbial spoilage and moisture-mediated deterioration reactions. Dried jujube slices are a traditional processed product of red dates in my country, as well as an important product of my country's current red date processing. Hot air drying method processing is currently one of the most widely used methods, but hot air drying is a high-energy-consuming unit operation.
等离子体是是继固态、液态、气态之后的物质第四态,当外加电压达到击穿电压时,气体分子被电离,产生包括电子、离子、原子和原子团在内的混合体。冷等离子体是指在大气压(常压)条件下产生的整体温度较低的等离子体。由于具有能够在常压下产生、气体温度低(接近或略高于室温)、活性组分含量高、无污染、无废弃物等优点,冷等离子体在食品加工、医药卫生、环境保护、生物医学等诸多领域均展现出广阔的应用前景。冷等离子体技术作为一种新兴的非热食品加工技术,受到广泛关注。在食品加工中利用冷等离子体技术的应用包括食品中有害微生物的杀灭、包装材料加工、食品成分的功能改性,种子发芽性能的提高,谷物的理化性质改善和农药残留物的降解等。然而,冷等离子体处理脂肪类食品和其他敏感食品时可能会诱发化学变化。此外,冷等离子体处理的效率很大程度上受样品表面形貌的影响。因此,可以使用冷等离子体射流系统在水面上或直接在水中产生等离子体放电来制备冷等离子体活化 水,采用冷等离子体活化水进行样品预处理。制备冷等离子体活化水时会发生化学反应,形成活性氧物质和活性氮物质。有研究表明,冷等离子体活化水可以作为微生物消毒的替代方法,促进种子萌发和植物生长(Thirumdas R,Kothakota A,Annapure U,et al.Plasma activated water(PAW):chemistry,physico-chemical properties,applications in food and agriculture[J].Trends in Food Science&Technology,2018,77:21-31.)。然而,如何有效的将等离子体活化水应用于食品干燥预处理领域尚未有报道。Plasma is the fourth state of matter after solid, liquid and gaseous states. When the applied voltage reaches the breakdown voltage, gas molecules are ionized to produce a mixture of electrons, ions, atoms and atomic groups. Cold plasma refers to a plasma with a lower overall temperature generated under atmospheric pressure (normal pressure) conditions. Due to the advantages of being able to generate under normal pressure, low gas temperature (close to or slightly higher than room temperature), high content of active components, no pollution, no waste, etc., cold plasma is used in food processing, medicine and health, environmental protection, biological Many fields such as medicine have shown broad application prospects. As an emerging non-thermal food processing technology, cold plasma technology has received widespread attention. The application of cold plasma technology in food processing includes the killing of harmful microorganisms in food, the processing of packaging materials, the functional modification of food ingredients, the improvement of seed germination, the improvement of the physical and chemical properties of grains, and the degradation of pesticide residues. However, cold plasma treatment of fatty foods and other sensitive foods may induce chemical changes. In addition, the efficiency of cold plasma treatment is largely affected by the surface morphology of the sample. Therefore, the cold plasma jet system can be used to generate plasma discharge on the water surface or directly in the water to prepare cold plasma activated water, and the cold plasma activated water is used for sample pretreatment. When preparing cold plasma activated water, a chemical reaction occurs to form active oxygen species and active nitrogen species. Studies have shown that cold plasma activated water can be used as an alternative to microbial disinfection to promote seed germination and plant growth (Thirumdas R, Kothakota A, Annapure U, et al. Plasma activated water (PAW): chemistry, physico-chemical properties, applications in food and agriculture[J].Trends in Food Science&Technology,2018,77:21-31.). However, how to effectively apply plasma activated water to the field of food drying pretreatment has not been reported yet.
发明内容Summary of the invention
本发明公开了一种红枣片干燥预处理方法,采用冷等离子活化水体预处理新鲜红枣片,从而减少红枣片热风干燥时间,提高干燥效率,降低干燥能耗,同时提高红枣片生物活性成分含量。预处理过程可以增大水分扩散效率,减少热风干燥时间,有效的缩减红枣片热风干燥时间,同时也可以减少酚类物质的降解,进而提高干燥红枣片中的总酚含量。本发明的技术方案如下:The invention discloses a drying pretreatment method for jujube slices, which adopts cold plasma activated water to pretreat fresh jujube slices, thereby reducing the hot air drying time of the jujube slices, improving drying efficiency, reducing drying energy consumption, and increasing the content of biological active components of the jujube slices. The pretreatment process can increase the water diffusion efficiency, reduce the hot air drying time, effectively reduce the hot air drying time of the red date slices, and at the same time reduce the degradation of phenolic substances, thereby increasing the total phenol content in the dried red date slices. The technical scheme of the present invention is as follows:
本发明实施例公开了一种采用冷等离子体活化水的红枣片干燥方法,具体包括如下步骤:The embodiment of the invention discloses a method for drying jujube slices using cold plasma activated water, which specifically includes the following steps:
(1)采用冷等离子设备体预处理水,制备冷等离子体活化水;冷等离子体设备输出功率为600-900W,冷等离子体气流流速为100-300L/min,预处理时间为5-40min,(1) The cold plasma equipment body is used to pretreat water to prepare cold plasma activated water; the output power of the cold plasma equipment is 600-900W, the flow rate of the cold plasma gas flow is 100-300L/min, and the pretreatment time is 5-40min.
(2)将新鲜红枣片浸泡在冷等离子体活化水中进行干燥前预处理;红枣片厚度为2-10mm,新鲜红枣片完全浸泡在冷等离子体活化水中,浸泡时间为0.5-5min。(2) Soak the fresh red date slices in cold plasma activated water for pre-drying; the thickness of the red date slices is 2-10 mm, and the fresh red date slices are completely immersed in the cold plasma activated water for 0.5-5 min.
(3)预处理后的新鲜红枣片进行热风干燥处理,获得干红枣片。(3) The pretreated fresh red date slices are dried with hot air to obtain dried red date slices.
所述步骤(2)中使用的冷等离子体活化水为步骤(1)得到的未浸泡使用过的冷等离子体活化水或者为已经经步骤(2)一次或多次浸泡使用后的冷等离子体活化水。冷等离子体活化水重复使用的次数不多于3次,较优选仅重复使用一次。The cold plasma activated water used in the step (2) is the cold plasma activated water obtained in step (1) that has not been immersed and used, or the cold plasma that has been immersed and used in step (2) one or more times. Activated water. The cold plasma activated water is repeatedly used no more than 3 times, and it is more preferable to use it repeatedly only once.
在本发明步骤(1)的条件下,根据待处理的水的含量,约可制备获得10-50L符合预处理要求并具备较好实施效果的冷等离子体活化水。作为优选,步骤(1)中,所述冷等离子体设备输出功率为600-800W,冷等离子体气流流速为100-200L/min,预处理时间为5-20min。Under the conditions of step (1) of the present invention, according to the content of the water to be treated, about 10-50L cold plasma activated water that meets the pretreatment requirements and has a better implementation effect can be prepared. Preferably, in step (1), the output power of the cold plasma equipment is 600-800 W, the flow rate of the cold plasma gas flow is 100-200 L/min, and the pretreatment time is 5-20 min.
作为优选,步骤(1)中,冷等离子体活化水在制备时,一直保持在冰水浴中。冰水浴可以防止在制备过程中水温上升过高。Preferably, in step (1), the cold plasma activated water is kept in an ice water bath during preparation. The ice water bath can prevent the water temperature from rising too high during the preparation process.
作为优选,步骤(2)中,新鲜红枣洗净后去核切片,红枣片厚度为4-8mm。Preferably, in step (2), the fresh red dates are washed and then cored and sliced, and the thickness of the red date slices is 4-8 mm.
作为优选,步骤(2)中,新鲜红枣片完全浸泡在冷等离子体活化水中,浸泡时间为0.5-2min。浸泡温度对浸泡效果影响不显著,可选择在室温下进行,也可根据实际生产环境和生产条件选择在较宽的温度范围(如0~50℃)下进行。Preferably, in step (2), the fresh red date slices are completely immersed in cold plasma activated water, and the immersion time is 0.5-2 min. The soaking temperature has no significant influence on the soaking effect. It can be carried out at room temperature, or it can be carried out in a wider temperature range (such as 0-50°C) according to the actual production environment and production conditions.
作为优选,步骤(2)中,浸泡后取出,使用吸水纸擦干表面水分。Preferably, in step (2), take it out after soaking, and use absorbent paper to dry the surface moisture.
作为优选,步骤(3)中,热风干燥温度为50-70℃,风速为1-2m/s。Preferably, in step (3), the hot air drying temperature is 50-70° C., and the wind speed is 1-2 m/s.
作为优选,步骤(3)中,热风干燥结束时,红枣片水分含量控制为以湿基计不超过5%。Preferably, in step (3), at the end of hot air drying, the moisture content of the red date slices is controlled to not exceed 5% on a wet basis.
与现有技术相比,本发明具有以下优点:Compared with the prior art, the present invention has the following advantages:
本发明采用冷等离子体活化水预处理红枣片,绿色无污染。经冷等离子体活化水处理后的红枣片不存在食品安全隐患,且冷等离子体活化水在一定程度上具有杀菌的功能;本发明优化了冷等离子体活化水的处理时间和处理方式。The invention adopts cold plasma activated water to pretreat the jujube slices, which is green and pollution-free. The jujube slices treated with cold plasma activated water have no hidden food safety hazards, and the cold plasma activated water has a sterilization function to a certain extent; the present invention optimizes the treatment time and treatment methods of the cold plasma activated water.
本发明采用冷等离子体活化水预处理红枣片,与冷等离子体直接处理相比,单位时间内红枣片处理量更大,处理效率更高;冷等离子体直接处理需关注红枣片与冷等离子体之间的距离以及位置关系,对等离子处理技术的工艺要求高,若工艺控制不当,则预处理效果不理想,还将对红枣片产生营养破坏,这使得冷等离子体直接预处理过程效率较低,可操作性差。经试验证实,本发明处理过程中的冷等离子体活化水可多次重复使用,其仍具有较好的预处理效果(重复1-3次的情况下,均具有较好的预处理效果),这大大降低了冷等离子体设备的使用成本,提高了预处理的效率。冷等离子体活化水处理与冷等离子直接处理相比,最高可减少20%干燥时间(如附图5所示),同时可以显著提高干燥枣片多酚(如附图6所示,最高16%)、黄酮(如附图7所示,最高29%)和原花青素(如附图8所示,最高31%)的含量。此外,实验结果表明,冷等离子体直接处理会造成枣片中维生素C的破坏,与未处理组相比,维生素C含量最高降低了50%(如附图9所示)。The invention adopts cold plasma activated water to pretreat the jujube slices. Compared with the direct treatment with cold plasma, the processing capacity of the jujube slices per unit time is larger and the processing efficiency is higher; the direct treatment with the cold plasma requires attention to the jujube slices and cold plasma The distance and the positional relationship between the plasma treatment technology require high process. If the process is not properly controlled, the pretreatment effect will be unsatisfactory, and it will also cause nutritional damage to the red jujube slices, which makes the cold plasma direct pretreatment process less efficient , Poor operability. Tests have confirmed that the cold plasma activated water in the process of the present invention can be reused many times, and it still has a good pretreatment effect (in the case of repeated 1-3 times, all have a good pretreatment effect), This greatly reduces the use cost of cold plasma equipment and improves the efficiency of pretreatment. Compared with cold plasma direct treatment, cold plasma activated water treatment can reduce the drying time by up to 20% (as shown in Figure 5), and can significantly increase the polyphenols of dried jujube slices (as shown in Figure 6, up to 16%) ), flavonoids (as shown in Figure 7, up to 29%) and procyanidins (as shown in Figure 8, up to 31%). In addition, the experimental results show that direct cold plasma treatment will cause the destruction of vitamin C in the jujube slices. Compared with the untreated group, the vitamin C content is reduced by up to 50% (as shown in Figure 9).
等离子体活化水预处理后,红枣片表面紧密纤维结构打开,形成较为均匀的孔洞或孔隙,使得最终干红枣片产品的品质较为稳定和均一,能有效的减少热风干燥的时间;而等离子直接处理后,红枣片表面孔洞不均一,部分表面存在灼伤现象,形成皱缩;这使得后续热风干燥阶段得到的干香菇产品品质不稳定;对于品质不理想的干红枣片往往需要挑选以进一步干燥或作为次品处理。而冷等离子体活化水预处理的阶段,红枣片在预处理阶段是均匀浸泡在活化水中的,因此进入热风干燥前红枣片较为均一,易获得品质稳定的干红枣片产品。After the plasma activated water pretreatment, the compact fiber structure on the surface of the red date slices opens, forming more uniform holes or pores, so that the quality of the final dried red date slices is more stable and uniform, which can effectively reduce the hot air drying time; while the plasma direct treatment Later, the red date slices have uneven surface holes, and some of the surfaces are burnt, resulting in shrinkage; this makes the quality of dried shiitake mushroom products obtained in the subsequent hot air drying stage unstable; for dry red date slices with unsatisfactory quality, they often need to be selected for further drying or Processing of defective products. In the cold plasma activated water pretreatment stage, the jujube slices are evenly immersed in the activated water during the pretreatment stage. Therefore, the jujube slices are relatively uniform before entering the hot air drying, and it is easy to obtain dry red date slices with stable quality.
本发明首次发现冷等离子体活化水预处理能够有效提高热风干燥红枣片酚类物质含量,提高干红枣片品质。冷等离子活化水中含有丰富的活性氧(ROS)和活性氮分子(RNS),ROS和RNS具有过氧化作用,可以破坏枣片细胞的膜脂质,引起细胞膜破裂,释放枣片细胞液,从而提升干燥速率。冷等离子体活化水预处理可以显著提升干燥枣片的活性物质含量,一方面是因为冷等离子体活化水预处理可以提高红枣片的热风干燥速率,从而降低活性物质的热降解;另一方面,冷等离子体活化水预处理可以氧化枣片表层部分活性物质,形成抗氧化保护膜,该膜的形成可以降低干燥过程中枣片内部活性物质的氧化降解。The present invention finds for the first time that cold plasma activated water pretreatment can effectively increase the content of phenolic substances in hot-air dried red date slices and improve the quality of dried red date slices. The cold plasma activated water is rich in reactive oxygen species (ROS) and reactive nitrogen molecules (RNS). ROS and RNS have a peroxidation effect, which can destroy the membrane lipids of the jujube slice cells, cause the cell membrane to rupture, and release the jujube slice cell sap, thereby enhancing Drying rate. Cold plasma activated water pretreatment can significantly increase the active substance content of dried jujube slices. On the one hand, cold plasma activated water pretreatment can increase the hot air drying rate of red jujube slices, thereby reducing the thermal degradation of active substances; on the other hand, The cold plasma activated water pretreatment can oxidize part of the active substances on the surface of the jujube slices to form an anti-oxidation protective film. The formation of this film can reduce the oxidative degradation of the active substances in the jujube slices during the drying process.
本发明为冷等离子体活化水提供了新的食品加工用途,拓展了一个新的应用领域。The invention provides a new food processing application for cold plasma activated water and expands a new application field.
图1为对比例1-3和实施例1-3的红枣片干燥时间对比图;Figure 1 is a comparison diagram of the drying time of the jujube slices of Comparative Example 1-3 and Example 1-3;
图2为对比例1-3和实施例1-3的红枣片总酚含量对比图;Figure 2 is a comparison diagram of the total phenol content of jujube tablets of Comparative Example 1-3 and Example 1-3;
图3为对比例1-3和实施例1-3的红枣片黄酮含量对比图;Figure 3 is a comparison diagram of flavonoid content of jujube tablets of Comparative Example 1-3 and Example 1-3;
图4为对比例1-3和实施例1-3的红枣片原花青素含量对比图;4 is a comparison diagram of the proanthocyanidin content of jujube slices of Comparative Example 1-3 and Example 1-3;
图5为对比例4-6和实施例1-3的红枣片干燥时间对比图;Figure 5 is a comparison diagram of the drying time of the jujube slices of Comparative Examples 4-6 and Examples 1-3;
图6为对比例4-6和实施例1-3的红枣片总酚含量对比图;Figure 6 is a comparison diagram of the total phenol content of jujube tablets of Comparative Examples 4-6 and Examples 1-3;
图7为对比例4-6和实施例1-3的红枣片黄酮含量对比图;Figure 7 is a comparison diagram of the flavonoid content of the jujube tablets of Comparative Examples 4-6 and Examples 1-3;
图8为对比例4-6和实施例1-3的红枣片原花青素含量对比图;Fig. 8 is a comparison diagram of proanthocyanidin content of jujube slices of Comparative Examples 4-6 and Examples 1-3;
图9为对比例1-6和实施例1-3的红枣片维生素C含量对比图。Figure 9 is a comparison diagram of the vitamin C content of the jujube tablets of Comparative Example 1-6 and Example 1-3.
下面结合对比例和具体实施例对本发明作进一步描述,以下列举的仅是本发明的具体实施例,但本发明的保护范围并不仅限于此:The present invention will be further described below in conjunction with comparative examples and specific embodiments. The following are only specific embodiments of the present invention, but the protection scope of the present invention is not limited to this:
对比例1Comparative example 1
新鲜红枣洗净后去核切片,红枣片厚度为6mm。新鲜红枣片不经预处理,将热风干燥机温度预热至50℃,放入红枣片进行热风干燥,风速为1.0m/s,每隔30min测定红枣片含水量,当红枣片水分含量低于5%(以湿基计)时停止干燥,获得干红枣 片。The fresh red dates are washed and then cored and sliced. The thickness of the red dates is 6mm. For fresh red date slices without pretreatment, preheat the temperature of the hot air dryer to 50℃, put the red date slices in for hot air drying at a wind speed of 1.0m/s, and measure the water content of the red date slices every 30 minutes. When the water content of the red date slices is lower than Stop drying at 5% (based on wet basis) to obtain dried red date flakes.
所述干燥时间为1050min,干红枣片中多酚含量为13.56mg/g DW(干基),干红枣片中黄酮含量为3.26mg/g DW(干基),干红枣片中原花青素含量为2.56mg/g DW(干基),干红枣片中维生素C含量为1.38mg/g DW(干基)。The drying time is 1050min, the polyphenol content in dried red date tablets is 13.56mg/g DW (dry basis), the flavonoid content in dried red date tablets is 3.26mg/g DW (dry basis), and the proanthocyanidin content in dried red date tablets is 2.56 mg/g DW (dry basis), the vitamin C content in dried red jujube tablets is 1.38mg/g DW (dry basis).
对比例2Comparative example 2
新鲜红枣洗净后去核切片,红枣片厚度为6mm。新鲜红枣片不经预处理,将热风干燥机温度预热至60℃,放入红枣片进行热风干燥,风速为1.0m/s,每隔30min测定红枣片含水量,当红枣片水分含量低于5%(以湿基计)时停止干燥,获得干红枣片。The fresh red dates are washed and then cored and sliced. The thickness of the red dates is 6mm. The fresh red date slices are not pre-treated, the hot air dryer temperature is preheated to 60℃, and the red date slices are put in for hot air drying at a wind speed of 1.0m/s. The water content of the red date slices is measured every 30 minutes. When the water content of the red date slices is lower than Stop drying at 5% (based on wet basis) to obtain dried red date flakes.
所述干燥时间为630min,干红枣片中多酚含量为14.26mg/g DW(干基),干红枣片中黄酮含量为4.01mg/g DW(干基),干红枣片中原花青素含量为2.58mg/g DW(干基)干红枣片中维生素C含量为1.62mg/g DW(干基)。The drying time is 630 minutes, the polyphenol content in the dried red jujube tablets is 14.26mg/g DW (dry basis), the flavonoid content in the dried jujube tablets is 4.01mg/g DW (dry basis), and the proanthocyanidin content in the dried red jujube tablets is 2.58 The vitamin C content in mg/g DW (dry basis) dried red jujube tablets is 1.62mg/g DW (dry basis).
对比例3Comparative example 3
新鲜红枣洗净后去核切片,红枣片厚度为6mm。新鲜红枣片不经预处理,将热风干燥机温度预热至70℃,放入红枣片进行热风干燥,风速为1.0m/s,每隔30min测定红枣片含水量,当红枣片水分含量低于5%(以湿基计)时停止干燥,获得干红枣片。The fresh red dates are washed and then cored and sliced. The thickness of the red dates is 6mm. Without pretreatment, the hot air dryer temperature is preheated to 70℃, and the red date slices are put in for hot air drying at a wind speed of 1.0m/s. The water content of the red date slices is measured every 30 minutes. When the water content of the red date slices is lower than Stop drying at 5% (based on wet basis) to obtain dried red date flakes.
所述干燥时间为540min,干红枣片中多酚含量为14.33mg/g DW(干基),干红枣片中黄酮含量为3.48mg/g DW(干基),干红枣片中原花青素含量为2.18mg/g DW(干基)干红枣片中维生素C含量为1.44mg/g DW(干基)。The drying time is 540min, the polyphenol content in dried red date tablets is 14.33mg/g DW (dry basis), the flavonoid content in dried red date tablets is 3.48mg/g DW (dry basis), and the proanthocyanidin content in dried red date tablets is 2.18 The vitamin C content in mg/g DW (dry basis) dried red jujube tablets is 1.44mg/g DW (dry basis).
实施例1Example 1
调节冷等离子体设备输出功率为600W,冷等离子体气流流速为200L/min,预处理水20min(整个处理过程中,水保持在冰水浴中),制备得到冷等离子体活化水25L。新鲜红枣洗净后去核切片,红枣片厚度为6mm。将新鲜红枣片完全浸泡在冷等离子体活化水中,浸泡时间为2min,浸泡后取出,使用吸水纸擦干表面水分。将热风干燥机温度预热至50℃,放入预处理后的红枣片进行热风干燥,风速为1.0m/s,每隔30min测定红枣片含水量,当红枣片水分含量低于5%(以湿基计)时停止干燥,获得干红 枣片。The output power of the cold plasma equipment was adjusted to 600W, the flow rate of the cold plasma gas flow was 200L/min, and the water was pretreated for 20 minutes (the water was kept in an ice water bath during the entire treatment process) to prepare 25L of cold plasma activated water. The fresh red dates are washed and then cored and sliced. The thickness of the red dates is 6mm. The fresh red date slices are completely immersed in cold plasma activated water for 2 minutes, and then taken out after soaking, and the surface water is wiped off with absorbent paper. Preheat the temperature of the hot air dryer to 50℃, put the pretreated red date slices into hot air drying at a wind speed of 1.0m/s, and measure the water content of the red date slices every 30 minutes. When the water content of the red date slices is less than 5% (to Drying was stopped at the time of wet basis, and dried red date slices were obtained.
所述干燥时间为930min,干红枣片中多酚含量为15.26mg/g DW(干基),干红枣片中黄酮含量为4.95mg/g DW(干基),干红枣片中原花青素含量为3.38mg/g DW(干基),干红枣片中维生素C含量为1.37mg/g DW(干基)。The drying time is 930 minutes, the content of polyphenols in dried red date tablets is 15.26mg/g DW (dry basis), the content of flavonoids in dried red date tablets is 4.95 mg/g DW (dry basis), and the content of proanthocyanidins in dried red date tablets is 3.38 mg/g DW (dry basis), the vitamin C content in dried red jujube tablets is 1.37mg/g DW (dry basis).
对比例4Comparative example 4
新鲜红枣洗净后去核切片,红枣片厚度为6mm。采用冷等离子体直接处理,调节冷等离子体设备输出功率为600W,冷等离子体气流流速为200L/min,冷等离子体探头距离枣片表面15cm,预处理5min。The fresh red dates are washed and then cored and sliced. The thickness of the red dates is 6mm. Direct cold plasma treatment is adopted, the output power of the cold plasma equipment is adjusted to 600W, the flow rate of the cold plasma gas flow is 200L/min, the cold plasma probe is 15cm away from the surface of the jujube slice, and the pretreatment is 5min.
将热风干燥机温度预热至50℃,放入预处理后的红枣片进行热风干燥,风速为1.0m/s,每隔30min测定红枣片含水量,当红枣片水分含量低于5%(以湿基计)时停止干燥,获得干红枣片。热风干燥用时和干红枣片中活性成分含量见图5-9。Preheat the temperature of the hot air dryer to 50℃, put the pretreated red date slices into hot air drying at a wind speed of 1.0m/s, and measure the water content of the red date slices every 30 minutes. When the water content of the red date slices is less than 5% (to Drying was stopped at the time of wet basis, and dried red date slices were obtained. Figure 5-9 shows the active ingredient content of hot air drying and dried red jujube tablets.
所述干燥时间为1020min,干红枣片中多酚含量为14.28mg/g DW(干基),干红枣片中黄酮含量为3.85mg/g DW(干基),干红枣片中原花青素含量为2.59mg/g DW(干基),干红枣片中维生素C含量为0.69mg/g DW(干基)。The drying time is 1020 minutes, the polyphenol content in the dried red date tablets is 14.28mg/g DW (dry basis), the flavonoid content in the dried red date tablets is 3.85 mg/g DW (dry basis), and the proanthocyanidin content in the dried red date tablets is 2.59 mg/g DW (dry basis), the vitamin C content in dried red jujube tablets is 0.69mg/g DW (dry basis).
实施例2Example 2
调节冷等离子体设备输出功率为800W,冷等离子体气流流速为150L/min,预处理水5min(保持在冰水浴中),制备得到冷等离子体活化水10L。新鲜红枣洗净后去核切片,红枣片厚度为6mm。将新鲜红枣片完全浸泡在冷等离子体活化水中,浸泡时间为0.5min,浸泡后取出,使用吸水纸擦干表面水分。将热风干燥机温度预热至60℃,放入预处理后的红枣片进行热风干燥,风速为1.0m/s,每隔30min测定红枣片含水量,当红枣片水分含量低于5%(以湿基计)时停止干燥,获得干红枣片。The output power of the cold plasma equipment was adjusted to 800W, the flow rate of the cold plasma gas flow was 150L/min, and the water was pretreated for 5 minutes (keeping in an ice water bath) to prepare 10L of cold plasma activated water. The fresh red dates are washed and then cored and sliced. The thickness of the red dates is 6mm. The fresh red date slices are completely immersed in cold plasma activated water for 0.5 min. After soaking, they are taken out, and the surface water is wiped off with absorbent paper. Preheat the temperature of the hot air dryer to 60℃, put the pretreated red date slices into hot air drying at a wind speed of 1.0m/s, and measure the water content of the red date slices every 30 minutes. When the water content of the red date slices is less than 5% (to Drying was stopped at the time of wet basis, and dried red date slices were obtained.
所述干燥时间为510min,干红枣片中多酚含量为16.29mg/g DW(干基),干红枣片中黄酮含量为4.39mg/g DW(干基),干红枣片中原花青素含量为2.99mg/g DW(干基)干红枣片中维生素C含量为1.72mg/g DW(干基)。The drying time is 510 minutes, the content of polyphenols in dried red date tablets is 16.29mg/g DW (dry basis), the content of flavonoids in dried red date tablets is 4.39mg/g DW (dry basis), and the content of proanthocyanidins in dried red date tablets is 2.99 The vitamin C content in mg/g DW (dry basis) dried red jujube tablets is 1.72mg/g DW (dry basis).
对比例5Comparative example 5
新鲜红枣洗净后去核切片,红枣片厚度为6mm。采用冷等离子体直接处理,调节 冷等离子体设备输出功率为800W,冷等离子体气流流速为150L/min,冷等离子体探头距离枣片表面5cm,预处理3min。The fresh red dates are washed and then cored and sliced. The thickness of the red dates is 6mm. Direct cold plasma processing is adopted, the output power of the cold plasma equipment is adjusted to 800W, the flow rate of the cold plasma gas flow is 150L/min, the cold plasma probe is 5cm away from the surface of the jujube slice, and the pretreatment is 3min.
将热风干燥机温度预热至60℃,放入预处理后的红枣片进行热风干燥,风速为1.0m/s,每隔30min测定红枣片含水量,当红枣片水分含量低于5%(以湿基计)时停止干燥,获得干红枣片。热风干燥用时和干红枣片中活性成分含量见图5-9。Preheat the temperature of the hot air dryer to 60℃, put the pretreated red date slices into hot air drying at a wind speed of 1.0m/s, and measure the water content of the red date slices every 30 minutes. When the water content of the red date slices is less than 5% (to Drying was stopped at the time of wet basis, and dried red date slices were obtained. Figure 5-9 shows the active ingredient content of hot air drying and dried red jujube tablets.
所述干燥时间为580min,干红枣片中多酚含量为14.04mg/g DW(干基),干红枣片中黄酮含量为3.94mg/g DW(干基),干红枣片中原花青素含量为2.66mg/g DW(干基),干红枣片中维生素C含量为1.35mg/g DW(干基)。The drying time is 580min, the polyphenol content in dried red date tablets is 14.04mg/g DW (dry basis), the flavonoid content in dried red date tablets is 3.94mg/g DW (dry basis), and the proanthocyanidin content in dried red date tablets is 2.66 mg/g DW (dry basis), the vitamin C content in dried red jujube tablets is 1.35mg/g DW (dry basis).
实施例3Example 3
调节冷等离子体设备输出功率为700W,冷等离子体气流流速为100L/min,预处理水10min(保持在冰水浴中),制备得到冷等离子体活化水15L。新鲜红枣洗净后去核切片,红枣片厚度为6mm。将新鲜红枣片完全浸泡在冷等离子体活化水中,浸泡时间为1min,浸泡后取出,使用吸水纸擦干表面水分。将热风干燥机温度预热至70℃,放入预处理后的红枣片进行热风干燥,风速为1.0m/s,每隔30min测定红枣片含水量,当红枣片水分含量低于5%(以湿基计)时停止干燥,获得干红枣片。The output power of the cold plasma equipment was adjusted to 700W, the flow rate of the cold plasma gas flow was 100L/min, and the water was pretreated for 10 minutes (keeping in an ice water bath) to prepare 15L of cold plasma activated water. The fresh red dates are washed and then cored and sliced. The thickness of the red dates is 6mm. The fresh red date slices are completely immersed in cold plasma activated water for 1 min. After soaking, they are taken out, and the surface water is wiped off with absorbent paper. Preheat the temperature of the hot air dryer to 70℃, put the pre-treated red date slices into hot air drying at a wind speed of 1.0m/s, and measure the water content of the red date slices every 30 minutes. When the water content of the red date slices is less than 5% (to Drying was stopped at the time of wet basis, and dried red date slices were obtained.
所述干燥时间为360min,干红枣片中多酚含量为15.37mg/g DW(干基),干红枣片中黄酮含量为4.15mg/g DW(干基),干红枣片中原花青素含量为2.74mg/g DW(干基),干红枣片中维生素C含量为1.40mg/g DW(干基)。The drying time is 360 minutes, the content of polyphenols in dried red date tablets is 15.37mg/g DW (dry basis), the content of flavonoids in dried red date tablets is 4.15 mg/g DW (dry basis), and the content of proanthocyanidins in dried red date tablets is 2.74 mg/g DW (dry basis), the vitamin C content in dried red jujube tablets is 1.40mg/g DW (dry basis).
对比例6Comparative example 6
新鲜红枣洗净后去核切片,红枣片厚度为6mm。采用冷等离子体直接处理,调节冷等离子体设备输出功率为700W,冷等离子体气流流速为100L/min,冷等离子体探头距离枣片表面10cm,预处理6min。The fresh red dates are washed and then cored and sliced. The thickness of the red dates is 6mm. Direct treatment with cold plasma is adopted, the output power of the cold plasma equipment is adjusted to 700W, the flow rate of the cold plasma gas flow is 100L/min, the cold plasma probe is 10cm away from the surface of the jujube slice, and the pretreatment is 6min.
将热风干燥机温度预热至70℃,放入预处理后的红枣片进行热风干燥,风速为1.0m/s,每隔30min测定红枣片含水量,当红枣片水分含量低于5%(以湿基计)时停止干燥,获得干红枣片。热风干燥用时和干红枣片中活性成分含量见图5-9。Preheat the temperature of the hot air dryer to 70℃, put the pre-treated red date slices into hot air drying at a wind speed of 1.0m/s, and measure the water content of the red date slices every 30 minutes. When the water content of the red date slices is less than 5% (to Drying was stopped at the time of wet basis, and dried red date slices were obtained. Figure 5-9 shows the active ingredient content of hot air drying and dried red jujube tablets.
所述干燥时间为450min,干红枣片中多酚含量为14.13mg/g DW(干基),干红 枣片中黄酮含量为3.43mg/g DW(干基),干红枣片中原花青素含量为2.22mg/g DW(干基),干红枣片中维生素C含量为0.77mg/g DW(干基)。The drying time is 450min, the polyphenol content in dried red date tablets is 14.13mg/g DW (dry basis), the flavonoid content in dried red date tablets is 3.43mg/g DW (dry basis), and the proanthocyanidin content in dried red dates tablets is 2.22 mg/g DW (dry basis), the vitamin C content in dried red jujube tablets is 0.77mg/g DW (dry basis).
实施例4Example 4
调节冷等离子体设备输出功率为900W,冷等离子体气流流速为300L/min,预处理水40min(保持在冰水浴中),制备得到冷等离子体活化水50L。新鲜红枣洗净后去核切片,红枣片厚度为10mm。将新鲜红枣片完全浸泡在冷等离子体活化水中,浸泡时间为5min,浸泡后取出,使用吸水纸擦干表面水分。将热风干燥机温度预热至55℃,放入预处理后的红枣片进行热风干燥,风速为1.5m/s,每隔30min测定红枣片含水量,当红枣片水分含量低于5%(以湿基计)时停止干燥,获得干红枣片。The output power of the cold plasma equipment was adjusted to 900W, the flow rate of the cold plasma gas flow was 300L/min, and the water was pretreated for 40min (keeping in an ice water bath) to prepare 50L of cold plasma activated water. The fresh red dates are washed and then cored and sliced. The thickness of the red dates is 10mm. The fresh red date slices are completely immersed in cold plasma activated water for 5 minutes, and then taken out after soaking, and the surface water is wiped dry with absorbent paper. Preheat the temperature of the hot air dryer to 55℃, put the pretreated red date slices into hot air drying at a wind speed of 1.5m/s, and measure the water content of the red date slices every 30 minutes. When the water content of the red date slices is less than 5% (to Drying was stopped at the time of wet basis, and dried red date slices were obtained.
所述干燥时间为630min,干红枣片中多酚含量为15.26mg/g DW(干基),干红枣片中黄酮含量为4.35mg/g DW(干基),干红枣片中原花青素含量为3.08mg/g DW(干基),干红枣片中维生素C含量为1.45mg/g DW(干基)。The drying time is 630 minutes, the polyphenol content in the dried red date tablets is 15.26mg/g DW (dry basis), the flavonoid content in the dried red date tablets is 4.35 mg/g DW (dry basis), and the proanthocyanidin content in the dried red date tablets is 3.08 mg/g DW (dry basis), the vitamin C content in dried red jujube tablets is 1.45mg/g DW (dry basis).
实施例5Example 5
调节冷等离子体设备输出功率为750W,冷等离子体气流流速为250L/min,预处理水30min(保持在冰水浴中),制备得到冷等离子体活化水35L。新鲜红枣洗净后去核切片,红枣片厚度为2mm。将新鲜红枣片完全浸泡在冷等离子体活化水中(冷等离子体活化水第一次使用),浸泡时间为3min,浸泡后取出,使用吸水纸擦干表面水分。将热风干燥机温度预热至65℃,放入预处理后的红枣片进行热风干燥,风速为2.0m/s,每隔30min测定红枣片含水量,当红枣片水分含量低于5%(以湿基计)时停止干燥,获得干红枣片。The output power of the cold plasma equipment was adjusted to 750W, the flow rate of the cold plasma gas flow was 250L/min, and the water was pretreated for 30min (keeping in an ice water bath) to prepare 35L of cold plasma activated water. The fresh red dates are washed and then cored and sliced. The thickness of the red dates is 2mm. The fresh red date slices are completely immersed in cold plasma activated water (the cold plasma activated water is used for the first time), and the immersion time is 3 minutes. After soaking, take it out, and use absorbent paper to dry the surface water. Preheat the temperature of the hot air dryer to 65℃, put the pre-treated red date slices into hot air drying at a wind speed of 2.0m/s, and measure the water content of the red date slices every 30 minutes. When the water content of the red date slices is less than 5% (to Drying was stopped at the time of wet basis, and dried red date slices were obtained.
所述干燥时间为450min,干红枣片中多酚含量为15.66mg/g DW(干基),干红枣片中黄酮含量为4.01mg/g DW(干基),干红枣片中原花青素含量为2.63mg/g DW(干基),干红枣片中维生素C含量为1.57mg/g DW(干基)。The drying time is 450min, the polyphenol content in dried red date tablets is 15.66mg/g DW (dry basis), the flavonoid content in dried red date tablets is 4.01mg/g DW (dry basis), and the proanthocyanidin content in dried red date tablets is 2.63 mg/g DW (dry basis), the vitamin C content in dried red jujube tablets is 1.57mg/g DW (dry basis).
实施例6Example 6
以实施例5初次浸泡使用后的冷等子离体活化水对新鲜红枣片进行浸泡预处理及 热风干燥。The fresh red jujube slices were immersed and dried with hot air with the cold isocyanine in vitro activated water after the initial soaking in Example 5.
冷等离子体活化水第二次使用:将新鲜红枣片完全浸泡在冷等离子体活化水中(冷等离子体活化水第二次使用),浸泡时间为3min,浸泡后取出,使用吸水纸擦干表面水分。将热风干燥机温度预热至65℃,放入预处理后的红枣片进行热风干燥,风速为2.0m/s,每隔30min测定红枣片含水量,当红枣片水分含量低于5%(以湿基计)时停止干燥,获得干红枣片。The second use of cold plasma activated water: completely soak the fresh red date slices in cold plasma activated water (the second use of cold plasma activated water), soaking time is 3 minutes, after soaking, take it out, use absorbent paper to dry the surface water . Preheat the temperature of the hot air dryer to 65℃, put the pre-treated red date slices into hot air drying at a wind speed of 2.0m/s, and measure the water content of the red date slices every 30 minutes. When the water content of the red date slices is less than 5% (to Drying was stopped at the time of wet basis, and dried red date slices were obtained.
所述干燥时间为460min,干红枣片中多酚含量为15.59mg/g DW(干基),干红枣片中黄酮含量为4.01mg/g DW(干基),干红枣片中原花青素含量为2.68mg/g DW(干基),干红枣片中维生素C含量为1.52mg/g DW(干基)。The drying time is 460min, the content of polyphenols in dried red date tablets is 15.59mg/g DW (dry basis), the content of flavonoids in dried red date tablets is 4.01mg/g DW (dry basis), and the content of proanthocyanidins in dried red date tablets is 2.68 mg/g DW (dry basis), the vitamin C content in dried red jujube tablets is 1.52mg/g DW (dry basis).
实施例7Example 7
以实施例5二次浸泡使用后的冷等子离体活化水再对新鲜红枣片进行浸泡预处理及热风干燥(冷等离子活化水第三次使用)。The fresh red jujube slices were immersed and dried with hot air with the cold plasma activated water after the second immersion used in Example 5 (cold plasma activated water was used for the third time).
冷等离子体活化水第三次使用:将新鲜红枣片完全浸泡在冷等离子体活化水中(冷等离子体活化水第三次使用),浸泡时间为3min,浸泡后取出,使用吸水纸擦干表面水分。将热风干燥机温度预热至65℃,放入预处理后的红枣片进行热风干燥,风速为2.0m/s,每隔30min测定红枣片含水量,当红枣片水分含量低于5%(以湿基计)时停止干燥,获得干红枣片。The third use of cold plasma activated water: completely immerse the fresh red date slices in cold plasma activated water (the third use of cold plasma activated water), soaking time is 3min, after soaking, take it out, use absorbent paper to dry the surface water . Preheat the temperature of the hot air dryer to 65℃, put the pre-treated red date slices into hot air drying at a wind speed of 2.0m/s, and measure the water content of the red date slices every 30 minutes. When the water content of the red date slices is less than 5% (to Drying was stopped at the time of wet basis, and dried red date slices were obtained.
所述干燥时间为460min,干红枣片中多酚含量为15.56mg/g DW(干基),干红枣片中黄酮含量为3.97mg/g DW(干基),干红枣片中原花青素含量为2.56mg/g DW(干基),干红枣片中维生素C含量为1.55mg/g DW(干基)。The drying time is 460min, the polyphenol content in dried red date tablets is 15.56mg/g DW (dry basis), the flavonoid content in dried red date tablets is 3.97 mg/g DW (dry basis), and the proanthocyanidin content in dried red date tablets is 2.56 mg/g DW (dry basis), the vitamin C content in dried red jujube tablets is 1.55mg/g DW (dry basis).
由实施例5-7的结果可知,冷等离子体活化水重复使用时,对枣片干燥时间和活性成分含量无明显影响(不超过3%),由此可知冷等离子体活化水重复使用仍能保持较好预处理效果。From the results of Examples 5-7, it can be seen that repeated use of cold plasma activated water has no significant effect on the drying time and active ingredient content of the jujube slices (not more than 3%). It can be seen that cold plasma activated water can still be used repeatedly. Maintain a better pretreatment effect.
由以上结果和附图1-9可以看出:本发明的实施例1-3利用冷等离子体活化水预处理方法相比于未预处理的对比例1-3,在相同的热风干燥温度和风速条件下,干燥时间最高可以减少33%,干红枣片中多酚含量最高可提升14%,干红枣片中黄酮含量最高可提升52%,干红枣片中原花青素含量最高可提升32%。冷等离子活化水中含有丰富的活性氧(ROS)和活性氮分子(RNS),ROS和RNS具有过氧化作用,可以破坏枣片细胞的膜脂质,引起细胞膜破裂,释放枣片细胞液,从而提升干燥速率。冷等离 子体活化水预处理可以显著提升干燥枣片的活性物质含量,一方面是因为冷等离子体活化水预处理可以提高红枣片的热风干燥速率,从而降低活性物质的热降解;另一方面,冷等离子体活化水预处理可以氧化枣片表层部分活性物质,形成抗氧化保护膜,该膜的形成可以降低干燥过程中枣片内部活性物质的氧化降解。From the above results and Figures 1-9, it can be seen that the cold plasma activated water pretreatment method of Example 1-3 of the present invention is compared with the non-pretreated Comparative Example 1-3 at the same hot air drying temperature and Under wind speed conditions, the drying time can be reduced by up to 33%, the polyphenol content in dried red date tablets can be increased by 14%, the flavonoid content in dried red date tablets can be increased by 52%, and the proanthocyanidin content in dried red date tablets can be increased by 32%. The cold plasma activated water is rich in reactive oxygen species (ROS) and reactive nitrogen molecules (RNS). ROS and RNS have a peroxidation effect, which can destroy the membrane lipids of the jujube slice cells, cause the cell membrane to rupture, and release the jujube slice cell sap, thereby enhancing Drying rate. Cold plasma activated water pretreatment can significantly increase the active substance content of dried jujube slices. On the one hand, cold plasma activated water pretreatment can increase the hot air drying rate of red jujube slices, thereby reducing the thermal degradation of active substances; on the other hand, The cold plasma activated water pretreatment can oxidize part of the active substances on the surface of the jujube slices to form an anti-oxidation protective film. The formation of this film can reduce the oxidative degradation of the active substances in the jujube slices during the drying process.
从实施例1-3与对比例4-6相比可见,冷等离子体活化水处理与冷等离子直接处理相比,最高可减少20%干燥时间(如附图5所示),同时可以显著提高干燥枣片多酚(如附图6所示,最高16%)、黄酮(如附图7所示,最高29%)和原花青素(如附图8所示,最高31%)的含量。此外,实验结果表明,冷等离子体直接处理会造成枣片中维生素C的破坏,与未处理组相比,维生素C含量最高降低了50%(如附图9所示)。Comparing Examples 1-3 with Comparative Examples 4-6, it can be seen that the cold plasma activated water treatment can reduce the drying time by up to 20% compared with the cold plasma direct treatment (as shown in Figure 5), and can significantly improve The content of dried jujube slices polyphenols (as shown in Fig. 6 up to 16%), flavonoids (as shown in Fig. 7 up to 29%) and proanthocyanidins (as shown in Fig. 8 up to 31%). In addition, the experimental results show that direct cold plasma treatment will cause the destruction of vitamin C in the jujube slices. Compared with the untreated group, the vitamin C content is reduced by up to 50% (as shown in Figure 9).
因此,相比未进行预处理的红枣片热风干燥方法和采用冷等子离体直接预处理的热风干燥方法而言,本发明采用冷等离子体活化水预处理提高红枣片热风干燥速率和生物活性成分含量的方法可提高干红枣片干燥速率,降低干燥能耗,提高干燥红枣片品质。Therefore, compared to the hot-air drying method of jujube slices without pretreatment and the hot-air drying method using cold plasma in vitro direct pretreatment, the present invention adopts cold plasma activated water pretreatment to improve the hot-air drying rate and biological activity of jujube slices. The method of ingredient content can increase the drying rate of dried red date slices, reduce drying energy consumption, and improve the quality of dried red date slices.
最后,本发明可用其他的不违背本发明的精神和主要特征的具体形式来概述。因此,无论从那一点来看,本发明的上述实施方案都只能认为是对本发明的说明而不能限制本发明,权利要求书指出了本发明的范围,而上述的说明并未指出本发明的范围,因此,在与本发明的权利要求书相当的含义和范围内的任何改变,都应认为是包括在权利要求书的范围内。Finally, the present invention can be summarized in other specific forms that do not violate the spirit and main features of the present invention. Therefore, no matter from which point of view, the above-mentioned embodiments of the present invention can only be regarded as descriptions of the present invention and cannot limit the present invention. The claims indicate the scope of the present invention, while the foregoing description does not indicate the scope of the present invention. Scope, therefore, any changes within the meaning and scope equivalent to the claims of the present invention shall be considered to be included in the scope of the claims.
Claims (10)
- 一种采用冷等离子体活化水的红枣片干燥方法,其特征在于包括如下步骤:A method for drying red date slices using cold plasma activated water, which is characterized in that it comprises the following steps:(1)采用冷等离子体设备预处理水,制备冷等离子体活化水;冷等离子体设备输出功率为600-900W,冷等离子体气流流速为100-300L/min,预处理时间为5-40min;(1) Use cold plasma equipment to pretreat water to prepare cold plasma activated water; the output power of cold plasma equipment is 600-900W, the flow rate of cold plasma gas flow is 100-300L/min, and the pretreatment time is 5-40min;(2)将新鲜红枣片浸泡在冷等离子体活化水中进行干燥前预处理;红枣片厚度为2-10mm,新鲜红枣片完全浸泡在冷等离子体活化水中,浸泡时间为0.5-5min;(2) Soak the fresh red date slices in cold plasma activated water for pre-treatment; the thickness of the red date slices is 2-10mm, and the fresh red date slices are completely immersed in cold plasma activated water for 0.5-5min;(3)预处理后的新鲜红枣片进行热风干燥处理至红枣片水含量满足设定要求,获得干红枣片。(3) The pretreated fresh jujube slices are dried with hot air until the water content of the jujube slices meets the set requirements, and dried jujube slices are obtained.
- 根据权利要求1所述采用冷等离子体活化水的红枣片干燥方法,其特征在于所述步骤(2)中使用的冷等离子体活化水为步骤(1)得到的未浸泡使用的冷等离子体活化水或者为已经经步骤(2)一次或多次浸泡使用后的冷等离子体活化水。The method for drying red jujube slices using cold plasma activated water according to claim 1, wherein the cold plasma activated water used in step (2) is the cold plasma activated water used in step (1) that is not soaked. The water may be cold plasma activated water that has been immersed in step (2) for one or more times.
- 根据权利要求2所述采用冷等离子体活化水的红枣片干燥方法,其特征在于冷等离子体活化水重复使用的次数不多于3次。The method for drying red jujube slices using cold plasma activated water according to claim 2, wherein the repeated use of cold plasma activated water is not more than 3 times.
- 根据权利要求1所述采用冷等离子体活化水的红枣片干燥方法,其特征在于步骤(1)中,冷等离子体设备输出功率为600-800W,冷等离子体气流流速为100-200L/min,预处理时间为5-20min。The method for drying jujube slices using cold plasma activated water according to claim 1, wherein in step (1), the output power of the cold plasma equipment is 600-800W, and the flow rate of the cold plasma gas flow is 100-200L/min, The pretreatment time is 5-20min.
- 根据权利要求1所述采用冷等离子体活化水的红枣片干燥方法,其特征在于步骤(1)制备冷等离子体活化水的过程中,水一直保持在冰水浴中。The method for drying red date slices using cold plasma activated water according to claim 1, wherein the water is kept in an ice water bath during the process of preparing cold plasma activated water in step (1).
- 根据权利要求1所述采用冷等离子体活化水的红枣片干燥方法,其特征在于步骤(2)所述的新鲜红枣片通过新鲜红枣洗净后去核切片制得,红枣片厚度为4-8mm。The method for drying jujube slices using cold plasma activated water according to claim 1, wherein the fresh jujube slices in step (2) are prepared by washing the fresh jujube and then cored and sliced, and the thickness of the jujube slice is 4-8mm .
- 根据权利要求1所述采用冷等离子体活化水的红枣片干燥方法,其特征在于步骤(2)中,新鲜红枣片完全浸泡在冷等离子体活化水中,浸泡时间为0.5-2min。The method for drying red date slices using cold plasma activated water according to claim 1, wherein in step (2), the fresh red date slices are completely immersed in cold plasma activated water for a soaking time of 0.5-2 min.
- 根据权利要求1所述采用冷等离子体活化水的红枣片干燥方法,其特征在于步骤(2)浸泡之后还包括擦干或吸干红枣片表面水分的步骤。The method for drying jujube slices using cold plasma activated water according to claim 1, characterized in that step (2) after soaking further comprises a step of wiping or absorbing moisture on the surface of the jujube slices.
- 根据权利要求1所述采用冷等离子体活化水的红枣片干燥方法,其特征在于步骤(3)热风干燥处理的具体操方法为:热风干燥温度为50-70℃,风速为1-2m/s。The method for drying jujube slices using cold plasma activated water according to claim 1, characterized in that the specific operation method of step (3) hot air drying treatment is: hot air drying temperature is 50-70°C, wind speed is 1-2m/s .
- 根据权利要求1所述采用冷等离子体活化水的红枣片干燥方法,其特征在于步骤(3)热风干燥结束时,要求红枣片水分含量为以湿基计不超过5%。The method for drying jujube slices using cold plasma activated water according to claim 1, characterized in that at the end of step (3) hot air drying, the moisture content of the jujube slices is required to be no more than 5% on a wet basis.
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