WO2020216275A1 - Procédé de stérilisation en continu à ultra haute température pour boisson contenant des granulés - Google Patents

Procédé de stérilisation en continu à ultra haute température pour boisson contenant des granulés Download PDF

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Publication number
WO2020216275A1
WO2020216275A1 PCT/CN2020/086319 CN2020086319W WO2020216275A1 WO 2020216275 A1 WO2020216275 A1 WO 2020216275A1 CN 2020086319 W CN2020086319 W CN 2020086319W WO 2020216275 A1 WO2020216275 A1 WO 2020216275A1
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WIPO (PCT)
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particle
tank
sterilization
pressure
beverage
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PCT/CN2020/086319
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English (en)
Chinese (zh)
Inventor
茅嘉惠
杨亚军
徐海防
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江苏新美星包装机械股份有限公司
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Publication of WO2020216275A1 publication Critical patent/WO2020216275A1/fr

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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/42Preservation of non-alcoholic beverages
    • A23L2/46Preservation of non-alcoholic beverages by heating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/96Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with openwork frames or cages

Definitions

  • the invention relates to the technical field of beverage production, in particular to a continuous ultra-high temperature sterilization process for beverages containing particles.
  • Granule-containing beverages have high nutritional value and unique taste and flavor. They are emerging in China and selling well in Southeast Asian markets. They are also widely accepted by consumers in my country. However, there is no such process equipment for continuous sterilization of high-concentration granular beverages at home and abroad. Many customers can only choose sterilization pots and sterilization kettles, but their sterilization capacity is low, and the sterilization volume of each batch is limited, and continuous Supply, the tank needs to be changed midway. At the same time, after the heating of the pot, the central temperature does not meet the standard, resulting in incomplete sterilization, and the surface of the pot wall is prone to scale and burnt, difficult to clean, and high maintenance costs are troubled by many customers. Secondly, every time the customer adjusts the product, it needs manual operation, which has low operating efficiency and high risk of misoperation.
  • beverages containing particles on the market include coconut milk beverages containing coconuts, fruit juices containing strawberry particles, juices containing yellow peach pulp, fruit juices containing aloe vera particles, and cereal beverages containing grain particles.
  • the common microorganisms and all pathogenic bacteria in such products can be killed in the pasteurization process, but some heat-resistant spores that cannot be killed by pasteurization can still affect the shelf life of the product.
  • the product In order to ensure that the product can be stored for a certain period of time at room temperature, the product must be sterilized at a higher temperature.
  • This sterilization method is called the ultra-high temperature instantaneous sterilization process.
  • the existing ultra-high temperature sterilization process for beverages containing particles still has the following problems: the problem of heating and sterilization of the core temperature of the particles, the problem of damage to the particles after the particle sterilization, the problem of the precipitation of the particles in the balance buffer tank, and the length of the material containing particles. Erosion caused by time cycle sterilization. Among them, the problem of particle damage after particle sterilization particularly affects the taste and quality of beverages containing particles.
  • the purpose of the present invention is to provide a continuous ultra-high temperature sterilization process for beverages containing particles, which can be applied to various beverages containing particles, and can completely destroy the microorganisms and spores that can grow in the particles and liquids to maximize Reduce the physical, chemical and sensory changes of the product, and the processed product can reach the level of commercial sterility. It can be stored, transported and sold under non-refrigerated conditions. It belongs to a new type of advanced processing in the field of liquid beverage processing containing particles Craft.
  • a continuous ultra-high temperature sterilization process for beverages containing particles including the following steps:
  • a liquid level sensor is arranged in the particle mixing balance tank, and the mixing speed is controlled according to the liquid level signal fed back by the liquid level sensor;
  • the outlet pressure controller is a pipe with a pipe diameter smaller than that of the output pipe of the heating system, and the pipe diameter of the pipe is greater than or equal to the particle size;
  • the opening degree of the pressure regulating diaphragm valve is adjustable, and the minimum opening degree is greater than or equal to the particle size.
  • step (4) the cooled pellet-containing beverage is passed upwards into the outlet pressure controller.
  • the opening degree of the pressure regulating diaphragm valve is adjusted according to the pressure at the inlet end of the outlet pressure controller, the opening degree is increased when the pressure increases, and the opening degree is decreased when the pressure decreases.
  • step (4) back pressure is applied to the aseptic buffer tank.
  • the heating system includes a pre-heating system and a sterilization system, and the evenly stirred particle-containing beverage in the particle stirring balance tank is sent to the pre-heating system to be pre-heated and kept for a period of time. Time to make the core temperature of the particles reach the holding temperature; then the pre-heated and insulated beverage containing particles is sent into the sterilization system for heating and sterilization and holding for a period of time.
  • step (4) the pellet-containing beverage before cooling is exchanged and cooled by a heat exchange medium, which is used for preheating the pellet-containing beverage in step (2).
  • step (1) CIP cleaning and SIP cleaning are performed on the system in advance.
  • the normally open outlet that is located between the pressure regulating diaphragm valve and the aseptic buffer tank is The pressure valve ventilates and pressurizes.
  • the RO water in the water tank is pushed into the system, and the particle-containing beverage in the system is pushed into the particle stirring balance tank for temporary storage, and then stored in the system. Circulate RO water to maintain the sterility of the system.
  • a frame agitator is used to control the rotation speed of the frame agitator according to the liquid level, so that the particle stirring balance tank can maintain the uniformity of particle suspension at different liquid level heights.
  • the present invention is a continuous ultra-high temperature sterilization process for beverages containing particles.
  • a pipeline is adopted.
  • the outlet pressure controller replaces the back pressure of the outlet back pressure valve, so that the particles can pass through the outlet pressure controller without damage, which solves the problem of damage after the particle sterilization; by setting a pressure regulating diaphragm valve at the output end of the pipeline outlet pressure controller, Under the condition of ensuring the particles pass through without damage, it plays a role of secondary pressure and pressure regulation.
  • the production process produces products with stable taste and quality, high heat exchange efficiency, simple daily maintenance, energy saving and environmental protection.
  • Figure 1 is a schematic structural diagram of a continuous ultra-high temperature sterilization production line for beverages containing particles using the process of the present invention.
  • Flow meter 19, pre-heating heat exchanger; 20, pre-heating temperature detector; 21, pre-heating Temperature control valve; 22, pre-heating holder; 23, sterilization section heat exchanger; 24, sterilization section temperature control valve; 25, sterilization section temperature detector; 26, sterilization temperature holder; 27, two sets Hot water heating system; 28. A set of hot water heating system; 29. Heat recovery heat exchanger; 30. Tower water cooling heat exchanger; 31. Discharge valve of particle balance tank; 32. Discharge valve of particle balance tank; 33. Water shut-off valve; 34. RO water inlet check valve; 35. Discharge recovery switch valve; 36. Ice water cooling heat exchanger; 37. Outlet pressure controller; 38. Outlet back pressure valve; 39.
  • System return and discharge switch Valve 40, return particle filter; 41, SIP return switch valve; 42, liquid level sensor; 43, outlet pressure detector; 44, CIP bypass valve one; 45, CIP bypass pipe; 46, small pressurized pipeline 47. Pressure regulating diaphragm valve; 48. CIP bypass valve two; 49. Backflow stop valve; 50. Tank feed stop valve; 51. Tank SIP condensate drain valve; 52. Tank pressure adjustment control valve; 53, Tank Pressure detector; 54, tank CIP cleaning pipe; 55, tank SIP steam pipe.
  • the process of the present invention is used for processing materials with a concentration of ⁇ 60%, that is, pulp particles in 100g of materials with a content of not more than 60g.
  • the materials are prepared by mixing pulp particles with a size of ⁇ 5 ⁇ 5 ⁇ 5mm and the material liquid in proportion.
  • A represents the entry of cleaning fluid from the CIP station
  • B represents the entry of particles containing materials before the deployment
  • C represents the product reflux
  • D represents the entry of the first-level RO water
  • E represents the entry of the CIP acid/alkali cleaning mother liquor
  • F represents the particles
  • G means product outlet
  • H means 7°C ice water in
  • I means 17°C ice water out
  • J means 32°C ice water in
  • K means 42°C ice water out
  • L means steam in
  • M It means SIP steam inlet
  • N means CIP liquid inlet
  • O sterilization back pressure air inlet
  • P means to the filling area.
  • a continuous ultra-high temperature sterilization process for beverages containing particles including the following steps:
  • a liquid level sensor 42 is provided in the particle mixing balance tank 14, and the mixing speed is controlled according to the liquid level signal fed back by the liquid level sensor 42;
  • a frame agitator is used, and the rotation speed of the frame agitator is controlled according to the liquid level, so that the particle stirring balance tank 14 can maintain the uniformity of particle suspension at different liquid level heights.
  • the heating system includes a pre-heating system and a sterilization system.
  • the evenly stirred particle-containing beverage in the particle stirring balance tank 14 is sent to the pre-heating system to be pre-heated and kept for a period of time, so that the core temperature of the particles reaches the heat preservation Temperature:
  • the pre-heated and insulated beverage containing particles is sent to the sterilization system for heating and sterilization and holding for a period of time, so that the core temperature of the particles reaches the sterilization temperature.
  • the outlet pressure controller 37 is a pipe whose pipe diameter is smaller than the pipe diameter of the output pipe of the heating system, and the pipe diameter is greater than or equal to the particle size; through this setting, the pressure is increased while reducing the cross section, and the particle Cause the problem of damage.
  • the cooled pellet-containing beverage is passed upwards into the outlet pressure controller 37 to further improve the boost effect.
  • the pressure controller alternately extends along an inverted U-shaped path and a U-shaped path.
  • the opening degree of the pressure regulating diaphragm valve 47 is adjustable, and its minimum opening degree is greater than or equal to the particle size. Through this setting, damage to the particles can be avoided. Adjust the opening degree of the diaphragm valve 47 according to the pressure at the inlet end of the outlet pressure controller 37. When the pressure increases, the opening degree is appropriately adjusted to allow the crowded particles to pass. When the pressure decreases, the opening degree is adjusted appropriately to increase the pressure, which is the second increase. The role of pressure and pressure regulation.
  • the outlet pressure detector 43 detects the pressure at the inlet end of the outlet pressure controller 37, and adjusts the opening of the pressure adjustment diaphragm valve 47 according to the detection result.
  • the sterilization back pressure gas Pass the sterilization back pressure gas to the back pressure of the aseptic buffer tank 1, and monitor the pressure state in the sterile buffer tank 1 in real time, adjust the flow of the sterilization back pressure gas according to the monitoring data, and make the pressure in the back pressure of the sterile buffer tank 1 Maintained within a set range, the third pressurization of the system outlet materials.
  • the pressure in the aseptic buffer tank 1 is detected by the tank pressure detector 53, and the flow rate of the sterilization back pressure gas is adjusted by the tank pressure adjustment control valve 52 according to the detection result.
  • the heat exchange medium is used to exchange heat and lower the temperature of the beverage containing particles before cooling, and the heat exchange medium is used for preheating the beverage containing particles in step (2).
  • step (1) Before step (1), perform CIP cleaning and SIP cleaning on the system in advance.
  • SIP cleaning ventilate and add air to the normally open outlet back pressure valve 38 between the pressure regulating diaphragm valve 47 and the aseptic buffer tank 1. Pressure.
  • the outlet back pressure valve 38 that is kept in the normally open state is not vented, so that the particles can pass through the outlet back pressure valve 38 without damage.
  • the RO water in the water tank is pushed into the system, and the pellet-containing beverage in the system is pushed into the particle stirring balance tank 14 for temporary storage, and the RO water is circulated in the system. Maintain the sterility of the system.
  • the processing technology of the present invention adopts a stepwise heating method of one set of hot water heating system 28 and two sets of hot water heating system 27, sets different pre-heating temperatures according to product characteristics, and enters the pre-heating heat exchanger 19 for pre-heating.
  • the temperature rises, for example, 95°C, where the temperature enters the pre-heating holder 22, holding the temperature for a specific time: for example, 10s, 20s, 30s, etc., the length of the temperature holding time is determined according to the heat transfer characteristics of the product, and real-time feedback through the pre-heating temperature detector 20 Entering the temperature of the pre-heating holder 22, the temperature deviation is adjusted by the pre-heating temperature control valve 21 to ensure that the material with a constant temperature enters the subsequent sterilization section heat exchanger 23 for final temperature control and sterilization.
  • the dual hot water heating system is used to control the temperature, and the pre-heating section and the sterilization section perform their duties to keep the system stable. This can effectively ensure the thorough sterilization of the product. At the same time, the dual hot water heating system can reduce the energy consumption of equipment operation and realize energy saving. Consumption.
  • the dual hot water heating system is used to control the temperature, so that the core temperature of the particles reaches the holding temperature during the pre-heating stage, which greatly reduces the heat absorbed by the particles during the sterilization section, so that the particles can be kept warm during the sterilization section. Effectively sterilize.
  • the outlet back pressure is designed to maintain the heating effect of the sterilization section. Only when the system is under pressure can the sterilization temperature of the sterilization section rise to above 100°C. Any form of outlet back pressure valve 38 used to produce beverages containing particles cannot avoid crushing damage when particles flow through the valve core.
  • the outlet pressure controller 37 is used for back pressure, and pipes of appropriate length and diameter are selected according to the needs. After the system cuts into the feed production, the outlet back pressure valve 38 is fully opened, and the system pressure passes through the outlet pressure controller. 37 to control. With reference to the principle of the pipeline damper, the back pressure is achieved by selecting the appropriate length and appropriate diameter pipeline for outlet damping and pressurization, thus avoiding the problem of crushing damage when particles pass through the back pressure valve spool.
  • the product balance tank provides constant processing flow and pressure for the back end, and the particle density is generally relatively large.
  • the particles are prone to sedimentation during the temporary storage of granular materials, which leads to the different ratio of the material particles sent by the discharge conveying rotor pump 17 to affect the back end
  • the uniformity of heat transfer and the concentration ratio of the final product In the process of the present invention, the particle stirring balance tank 14 and the frame agitator are adopted, which has a good anti-sedimentation effect.
  • the bottom of the tank is equipped with a liquid level sensor 42, analog detection output, through real-time detection of the level of the tank, the analog output is fed back to the tank top stirring motor to adjust the stirring speed of the frame stirrer, which not only solves the problem of particle precipitation It also effectively ensures the uniformity of particle suspension at different liquid levels, and ensures the uniformity of the back-end heat exchange and the concentration ratio of the final product.
  • a set of water tank 5, water tank 5 and particle mixing balance tank 14 are directly connected by particle balance tank discharge valve 32 and water shut-off valve 33, and the connection distance is very short, effectively reducing the mixing of products and RO water loss.
  • the RO water in the water tank 5 is directly replaced with the product materials in the system, and the materials in the system are pushed into the particle mixing balance tank 14 for temporary storage, and the RO water is used to replace the materials in the system for circulating sterilization to ensure the system
  • the normal operation of the aseptic environment also solves the problem of particle erosion in the product caused by the long-term circulation of materials by replacing the internal medium of the system.
  • the top water and water top discharge processes before and after production are very common, but during the topping process, it is necessary to ensure that all the materials in the particle mixing and balance tank 14 cannot be sucked away by the back-end conveying rotor pump 17, causing the pump to evacuate and cause no If there are risks such as bacterial environmental damage, the particle mixing balance tank 14 is generally set to a minimum protection level, once it is lower than this protection level, the top liquid process starts, but often the set storage tank protection level becomes product mixing loss again a part of. By directly replacing the product materials in the system with the RO water in the water tank 5, part of the materials can also be saved.
  • the particle-containing material enters the feed control valve group 11 through the pre-processing feeding observation mirror 10 and then enters the particle mixing balance tank 14.
  • the bottom of the tank is equipped with a liquid level sensor 42 with an analog quantity detection output, which simulates the real-time detection of the liquid level in the tank.
  • the volume output is fed back to the tank top mixing motor to adjust its mixing speed, so that it can achieve different mixing speeds at different levels of high, medium and low to achieve the consistency of the particle suspension effect in the tank.
  • the product then flows through the particle balance tank discharge valve 31, which is used for the end of production and the CIP cleaning and emptying the residual liquid in the tank. Then the product flows through the particle balance tank discharge valve 32 and is discharged to the SIP switch valve 16.
  • This valve It is used to sterilize the system with SIP ⁇ 140°C superheated water.
  • the entire system needs to be sealed with back pressure.
  • the granular stirring balance tank 14 is an atmospheric tank and cannot achieve this function. All you need to pass the SIP switch valve 16 to overheat the SIP
  • the water tank 15 is introduced into the system for SIP superheated water sterilization.
  • the product is then output through the rotor pump 17, which is a positive displacement pump, and the particle damage rate in the product can be controlled to be small during the transportation process.
  • the product then uses the back-end flow meter 18 to detect the system flow in real time and feed it back to the rotor pump 17 to change the output frequency to control the system flow.
  • the temperature control method is real-time feedback of the temperature entering the pre-heating holder 22 through the pre-heating temperature detector 20, and the temperature deviation is adjusted through the pre-heating temperature control valve 21 to ensure that the constant temperature materials enter the subsequent sterilization section heat exchanger 23 for final Temperature control and sterilization. It adopts dual hot water system for temperature control, including two hot water heating systems 27 and a hot water heating system 28.
  • Pre-heating and temperature control of the sterilization section perform their duties to keep the system stable, which can effectively ensure the thorough sterilization of the product At the same time, it reduces the energy consumption of equipment operation and realizes energy saving and consumption reduction.
  • the temperature control of the sterilization section is also real-time feedback of the temperature entering the sterilization temperature holder 26 through the sterilization section temperature detector 25, and the temperature deviation is adjusted by the temperature control valve 24 of the sterilization section to ensure the sterilization temperature entering the sterilization temperature holder 26 Constant, the product enters the heat recovery heat exchanger 29 after maintaining the sterilization, is pre-cooled by the recovered low-temperature hot water, and then passes through the tower water cooling heat exchanger 30 and the ice water cooling heat exchanger 36 in turn before entering the outlet pressure control ⁇ 37.
  • the outlet back pressure valve 38 After the system cuts into the feed production, the outlet back pressure valve 38 is fully opened, and the system pressure is controlled by the outlet pressure controller 37.
  • the outlet back pressure valve 38 will only ventilate the back pressure when the SIP system is sterilized, and will not vent during normal production.
  • the product after the system sterilization finally enters the aseptic buffer tank 1, buffered by this tank and supplied to the back-end filling equipment for filling.
  • the system When the system is CIP cleaned, the residual liquid in the tank is discharged through the water tank discharge valve 2 and the particle balance tank discharge valve 31; then the chemical agent is added to the water tank 5 through the CIP liquid inlet pipe and the stop valve 3, and the cleaning liquid passes through the water After the tank 5 is prepared, it enters the water shut-off valve 33, and then enters the rotor pump 17 through the discharge valve 32 of the particle balance tank, and is transported to the rear end for cyclic cleaning.
  • the concentration of the cleaning solution is detected by the CIP cleaning conductivity detector 13, and then enters the tank reflux switching valve 9, which is switched at intervals for cleaning and entering the particle mixing
  • the balance tank 14 return line, and then the cleaning fluid passes through the system backflow discharge switch valve 39, then enters the backflow particle filter 40 to filter particulates to prevent the back-end cleaner from clogging, and then enters the SIP backflow switch valve 41, which is used for When SIP is sterilized, it is directly switched back to SIP superheated water tank 15 for use; then the cleaning liquid enters the water tank return valve 4, this valve is used to open the cleaning return pipe at intervals, and the cleaning liquid passes through the tank CIP stop valve 6, this valve and water
  • the tank reflux valve 4 switches to each other for cleaning, and then the cleaning liquid enters the CIP switching valve 7, which is used for the interval cleaning tank and the feed pipe of the feed control valve group 11.
  • CIP bypass valve 44 CIP bypass pipe 45, small pressurized pipe 46, pressure regulating diaphragm valve 47, CIP bypass valve 48, must be in Open or circulate state, so that 143°C superheated water can flow through to ensure complete sterilization;
  • the system pressure control needs to open the outlet back pressure valve 38 to adjust and control the system pressure of 2.5bar and above when SIP;
  • 143°C superheat After passing through the outlet back pressure valve 38, it flows through the tank feed shut-off valve 50 and the return shut-off valve 49 for high-temperature sterilization, and then flows back to the particle stirring balance tank 14 for 30-minute cycle timing sterilization.
  • the sterilization of the aseptic buffer tank 1 provides SIP high temperature steam separately through the tank SIP steam pipe 55 for heat sterilization.
  • the steam condensate is automatically drained through the tank SIP condensate drain valve 51, and goes to the back-end filling area for circulating steam sterilization together.
  • the internal materials of the system can be separately recovered to the front deployment.
  • the system backflow discharge switching valve 39 switch down to enter the discharge recovery switching valve 35, and you can choose to discharge to the trench or directly switch to the front deployment. Can be used.

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Chemical Kinetics & Catalysis (AREA)
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Abstract

L'invention concerne un procédé de stérilisation en continu à ultra haute température pour une boisson contenant des granulés. Le processus consiste à : (1) fournir un capteur de niveau de liquide dans un réservoir d'équilibrage d'agitation de granulés, et selon un signal de niveau de liquide renvoyé par le capteur de niveau de liquide, commander une vitesse de rotation d'agitation ; (2) transporter une boisson contenant des granulés, laquelle est agitée jusqu'à obtenir un résultat uniforme dans le réservoir d'agitation de granulés, dans un système de chauffage pour la chauffer et la stériliser, et réaliser une conservation à chaud pendant un certain temps ; (3) refroidir la boisson contenant des granulés après que celle-ci a été stérilisée et soumise à une conservation à chaud ; et (4) permettre à la boisson contenant des granulés refroidie de passer successivement à travers un dispositif de commande de pression de sortie et une soupape à membrane de réglage de pression, puis la transporter dans un réservoir tampon aseptique, le dispositif de commande de pression de sortie étant une conduite qui a un diamètre de conduite plus petit que celui d'une conduite de sortie du système de chauffage mais supérieur ou égal aux diamètres des granulés ; et un degré d'ouverture de la soupape à membrane de réglage de pression est réglable, et son degré d'ouverture minimal est supérieur ou égal aux diamètres des granulés. Le procédé résout le problème selon lequel les granulés sont brisés après stérilisation, garantissant ainsi le goût et la qualité de la boisson contenant des granulés.
PCT/CN2020/086319 2019-04-24 2020-04-23 Procédé de stérilisation en continu à ultra haute température pour boisson contenant des granulés WO2020216275A1 (fr)

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CN201910333938.8 2019-04-24
CN201910333938.8A CN110140849A (zh) 2019-04-24 2019-04-24 一种用于含颗粒饮料的连续性超高温灭菌工艺

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CN112602871B (zh) * 2020-10-23 2023-08-29 江苏新美星包装机械股份有限公司 一种无菌果粒饮料混合系统

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WO2023194070A1 (fr) * 2022-04-07 2023-10-12 Tetra Laval Holdings & Finance S.A. Unité de nettoyage en place, système de nettoyage en place et procédé associé

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