WO2020206826A1 - Ultra-thin atomic force microscope head - Google Patents

Ultra-thin atomic force microscope head Download PDF

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Publication number
WO2020206826A1
WO2020206826A1 PCT/CN2019/089280 CN2019089280W WO2020206826A1 WO 2020206826 A1 WO2020206826 A1 WO 2020206826A1 CN 2019089280 W CN2019089280 W CN 2019089280W WO 2020206826 A1 WO2020206826 A1 WO 2020206826A1
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Prior art keywords
probe
laser beam
laser
cantilever
reflecting
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PCT/CN2019/089280
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French (fr)
Chinese (zh)
Inventor
吴森
卢念航
胡晓东
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天津大学
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Publication of WO2020206826A1 publication Critical patent/WO2020206826A1/en

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01QSCANNING-PROBE TECHNIQUES OR APPARATUS; APPLICATIONS OF SCANNING-PROBE TECHNIQUES, e.g. SCANNING PROBE MICROSCOPY [SPM]
    • G01Q60/00Particular types of SPM [Scanning Probe Microscopy] or microscopes; Essential components thereof
    • G01Q60/24AFM [Atomic Force Microscopy] or apparatus therefor, e.g. AFM probes
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01QSCANNING-PROBE TECHNIQUES OR APPARATUS; APPLICATIONS OF SCANNING-PROBE TECHNIQUES, e.g. SCANNING PROBE MICROSCOPY [SPM]
    • G01Q60/00Particular types of SPM [Scanning Probe Microscopy] or microscopes; Essential components thereof
    • G01Q60/24AFM [Atomic Force Microscopy] or apparatus therefor, e.g. AFM probes
    • G01Q60/38Probes, their manufacture, or their related instrumentation, e.g. holders

Definitions

  • the invention belongs to the technical field of atomic force microscopes, and in particular relates to a probe fixing module with an ultra-thin thickness in the vertical direction and an atomic force microscope probe based on the probe fixing module.
  • the current mainstream atomic force microscope systems generally use micro cantilever probes to sense samples.
  • the force between the tip and the sample causes the micro cantilever to bend and deform. This small deformation is caused by the optical lever in the probe.
  • the optical path is amplified and converted into electrical signals by the photodetector.
  • the probe is usually large in size, and its thickness in the Z direction can reach several centimeters.
  • the working distance between the electron microscope and the optical microscope (the distance between the exit of the electron gun or the lower surface of the optical objective lens and the sample) is generally only a few millimeters to ten millimeters, which makes it difficult for the existing atomic force microscope probe devices to be directly integrated into the electron microscope and optical microscope.
  • Most of the existing atomic force microscope-electron microscope combined systems on the market use self-inducing tuning fork probes or piezoresistive probes. This type of probe does not require an additional detection light path and occupies a small space, but it is susceptible to interference in the atmospheric environment and has many application restrictions.
  • the atomic force microscope-Raman/fluorescence microscope combination equipment introduced by some companies mostly adopts an inverted optical microscope system. This solution can avoid the mechanical interference between the optical microscope and the atomic force probe in structure, but the disadvantage is that it can only detect Transparent sample.
  • the volume of the atomic force probe mainly depends on the design of the optical lever optical path.
  • the existing optical lever optical path can be roughly divided into several typical forms as shown in Figures 1 to 4.
  • the laser beam passes through the right-angle prism 20 or lens group 23 and strikes the cantilever probe vertically downwards along the Z direction.
  • the light reflected by the cantilever beam passes through one or more plane mirrors 21. Reflected on the photodetector.
  • optical microscopes can be installed above or on the side.
  • a low-power objective lens with a long working distance must be used.
  • the optical lever and the optical microscope optical path share an objective lens.
  • the optical lever laser beam is focused on the probe cantilever beam through the objective lens.
  • the reflected light of the cantilever beam is collected by the objective lens and converted into parallel light, and then passes through
  • the polarization beam splitter 24 and other elements located above the objective lens are projected onto the photodetector (the optical path between the objective lens and the polarization beam splitter is provided with a dichroic mirror 22 and a quarter wave plate 25).
  • This form of optical path can minimize the space occupied by the atomic force probe, allowing the use of high magnification objectives with large numerical apertures and short working distances.
  • the atomic force probe cannot be integrated with a packaged commercial optical system.
  • optical elements are arranged directly above the probe and the sample, which will hinder the propagation of the electron beam, so these three types of atomic force probes are not suitable for integration with an electron microscope.
  • the laser beam is incident on the probe obliquely, and the reflected light is symmetrically emitted to the photodetector.
  • the advantage of this design is that the area directly above the probe is released, which can be installed with either an optical microscope or an electron microscope or other types of equipment.
  • the laser beam in order to prevent the laser beam from being blocked by the optical objective lens housing or the electron microscope pole piece, the laser beam must be directed toward the cantilever probe with a large inclination angle.
  • the inclination angle is too large, the shape and intensity of the reflected light spot on the cantilever beam will deteriorate, which will affect the output signal quality of the photodetector. Therefore, the atomic force probe in Figure 4 can only be used for low magnification systems with long working distances.
  • the existing several optical path forms make the Z-direction of the probe part of the atomic force microscope occupy too much space, which is not conducive to the integration of optical microscopes (especially upright high-power optical microscopes), electron microscopes and other equipment.
  • optical microscopes especially upright high-power optical microscopes
  • electron microscopes especially electron microscopes and other equipment.
  • the purpose of the present invention is to provide a probe fixing module which can reduce the Z-direction thickness of the probe of the atomic force microscope.
  • Another object of the present invention is to provide an atomic force microscope probe, which is based on the above-mentioned probe fixing module and can be directly installed on the workbench of high-power optical microscopes, electron microscopes and other equipment without affecting the original equipment's own functions And performance indicators.
  • a probe fixing module comprising: a cantilever beam probe, a piezoelectric ceramic, a probe holder, a first reflection surface, a first reflection device and a second reflection device, the cantilever beam probe is mounted on the probe holder In the holder, the tip of the cantilever beam probe is located at the lowest point of the probe fixing module, and the first reflective surface is located on one side of the cantilever beam probe for receiving the cantilever beam probe on the other side.
  • the first laser beam emitted by the laser reflects the first laser beam to form a second laser beam, and the acute angle between the first reflective surface and the first laser beam is 60°-67.5°;
  • the reflection device is located between the cantilever beam probe and the first reflection surface, and the second laser beam is reflected by the first reflection device and irradiated on the cantilever beam probe and reflected by the cantilever beam probe to form a third laser beam
  • the second reflecting device is located between the cantilever beam probe and the laser, the third laser beam is reflected by the second reflecting device and then emitted from the probe fixing module to form a fourth laser bundle.
  • the first reflecting device is a second reflecting surface parallel to the first laser beam
  • the second reflecting surface and the cantilever probe are respectively located on both sides of the first laser beam and the second
  • the mirror surface of the reflecting surface faces the first laser beam
  • the second laser beam is reflected by the second reflecting surface and irradiated on the cantilever beam probe.
  • the first reflective device is a first reflective structure and a second reflective structure
  • the first reflective structure is one reflective surface or multiple reflective surfaces located on the same plane and the number is greater than one
  • the second reflective structure is one reflective surface or multiple reflective surfaces located on the same plane and the number is greater than one
  • the first reflective structure and the second reflective structure are parallel to each other and mirror-faced.
  • the second reflecting device is a fourth reflecting surface parallel to the first laser beam, and the fourth reflecting surface and the cantilever probe are respectively located on both sides of the first laser beam and the fourth reflecting surface
  • the mirror surface of the reflecting surface faces the first laser beam, and the third laser beam is reflected by the fourth reflecting surface to form the fourth laser beam.
  • the second reflecting device is a third reflecting structure and a fourth reflecting structure
  • the third reflecting structure is one reflecting surface or a plurality of reflecting surfaces located on the same plane and the number is greater than 1
  • the fourth reflective structure is one reflective surface or multiple reflective surfaces located on the same plane and the number is greater than one, and the third reflective structure and the fourth reflective structure are parallel to each other and mirror-faced.
  • a light through hole is formed between the first reflecting device and the second reflecting device for passing through the imaging light path.
  • a first adjustment frame mounted with the first reflection surface, for adjusting the angle between the first reflection surface and the first laser beam.
  • it further includes: piezoelectric ceramics fixed to the probe holder, used to excite the cantilever beam probe to vibrate or perform Z-direction scanning.
  • An atomic force microscope measuring head comprising: the probe fixing module and a laser transceiving module, the laser transceiving module includes: a laser emitting structure and a laser receiving structure, the laser emitting structure includes: the laser and the first laser A first converging lens on the beam path, so that the first laser beam passes through the first converging lens and the second laser beam is focused on the cantilever probe; the laser receiving structure includes: a photodetector And a second convergent lens located on the optical path of the fourth laser beam, so that the fourth laser beam passes through the second convergent lens and is projected on the photosensitive surface of the photodetector.
  • a filter is installed on the optical path after the fourth laser beam passes through the second condensing lens to reduce stray light interference.
  • the photodetector is installed on a two-dimensional adjustment table, and the two-dimensional adjustment table is used to adjust the position of the photodetector.
  • it further includes: a second adjustment frame on which the laser is installed, and the second adjustment frame is used to adjust the position and angle of the laser.
  • the Z-direction effective thickness (the vertical distance from the upper surface of the second reflecting surface 5 to the tip of the cantilever probe 1) of the probe fixing module in the atomic force microscope probe of the present invention is only a few millimeters, which can be directly installed at the working distance
  • the integrated use of different devices can be realized under an optical or electron microscope larger than this thickness.
  • the probe of the atomic force microscope has a compact structure, and the Z-direction thickness is significantly reduced compared with the conventional atomic force microscope, and it is easy to integrate with other equipment.
  • the AFM probe When the AFM probe is integrated with an optical microscope or an electron microscope, it can be directly installed between the optical objective lens or electron microscope pole piece and the sample without modifying the existing microscope body. The optical paths of the two are not coupled, and their functions are not affected. influences.
  • each module is relatively independent, easy to install, debug, maintain and upgrade.
  • Figure 1 is a schematic diagram of the probe structure 1 of an atomic force microscope
  • Figure 2 is a schematic diagram of the probe structure 2 of an atomic force microscope
  • Figure 3 is a schematic diagram of the probe structure 3 of the atomic force microscope:
  • Figure 4 is a schematic diagram of the probe structure 4 of the atomic force microscope:
  • FIG. 5 is a schematic diagram of the structure of the probe of the atomic force microscope of the present invention.
  • Fig. 6 is a schematic diagram of the structure of the probe of the atomic force microscope of the present invention.
  • Probe fixed module II Laser transceiver module
  • a probe fixing module includes: a cantilever beam probe 1, a piezoelectric ceramic 2, a probe holder 3, a first reflection surface 4, a first reflection device and a second reflection device.
  • the cantilever beam probe 1 is installed on In the probe holder 3, the tip of the cantilever probe 1 is located at the lowest point of the probe fixing module I, and the first reflective surface 4 is located on one side of the cantilever probe 1 for receiving another
  • the first laser beam emitted by the laser 10 on one side reflects the first laser beam to form a second laser beam, and the acute angle between the first reflective surface 4 and the first laser beam is 60°-67.5°.
  • the first reflection device is located between the cantilever beam probe 1 and the first reflection surface 4.
  • the second laser beam is reflected by the first reflection device and irradiated on the cantilever beam probe 1 at an inclination angle of 45°-60° and is The probe 1 reflects to form a third laser beam; the second reflecting device is located between the cantilever beam probe 1 and the laser 10.
  • the third laser beam is reflected by the second reflecting device and then emitted from the probe fixing module I and forms a fourth laser beam .
  • a light through hole is formed between the first reflecting device and the second reflecting device for passing through the imaging light path;
  • a first adjustment frame 9 mounted with a first reflective surface 4, for adjusting the angle between the first reflective surface 4 and the first laser beam;
  • the first reflection device is a first reflection structure and a second reflection structure
  • the first reflection structure is a reflection surface
  • the second reflection structure is a reflection surface.
  • the first reflective structure is the second reflective surface 5
  • the second reflective structure is the third reflective surface 6
  • the first reflective structure and the second reflective structure are parallel to each other
  • the second reflective surface 5 and the third reflective surface 6 They are located on the upper and lower sides of the first laser beam and the distance between them is 3.7 mm.
  • the second reflection device is a third reflection structure and a fourth reflection structure
  • the third reflection structure is a reflection surface
  • the fourth reflection structure is a reflection surface
  • the third reflection structure is a fourth reflection surface 7, and the fourth reflection structure It is the fifth reflective surface 8, and the third reflective structure and the fourth reflective structure are parallel to each other.
  • the fourth reflection surface 7 and the fifth reflection surface 8 are respectively located on the upper and lower sides of the first laser beam with a vertical distance of 3.7 mm; the second reflection surface 5 and the fourth reflection surface 7 have a horizontal distance of 7.5 mm as light passing holes.
  • the first to fifth reflective surfaces are all silver-coated flat mirrors.
  • the silver-plated plane mirror used for the first reflecting surface 4 has a size of 15mm ⁇ 4.5mm ⁇ 1mm, which is pasted on a fixed inclined surface at an angle of 112.5° with the horizontal plane, and the reflection surface faces the second upper right side.
  • the reflecting surface 5 (as shown in Figure 5); the second reflecting surface 5 and the fourth reflecting surface 7 can belong to different areas of the same reflecting mirror (that is, integrated), or they can be two different reflecting mirrors.
  • the size can be 15mm ⁇ 20mm ⁇ 1mm, placed horizontally above the cantilever probe, and a through hole with a diameter of 7.5mm is processed in the middle of the reflector for light transmission Hole, the second reflection surface 5 and the fourth reflection surface 7 are located on the left and right sides of the through hole.
  • the size of the reflector used for the fifth reflecting surface 8 is 15mm ⁇ 20mm ⁇ 1mm, and it is placed horizontally on the right side of the cantilever probe 1.
  • the first laser beam is emitted from the first condensing lens 12 and then passes through the first reflection surface 4, the first reflection surface 5, the third reflection surface 6 and the second reflection surface 5, and then converges on
  • the third laser beam reflected by the cantilever beam probe 1 passes through the first reflection of the fourth reflection surface 7, the second reflection of the fifth reflection surface 8 and the fourth reflection surface 7 in turn.
  • the probe fixing module 1 emits and forms a fourth laser beam at the bottom right.
  • the distance between the two reflection points on each of the second reflection surface 5 and the fourth reflection surface 7 is about 14 mm.
  • the thickness of the probe fixing module in this embodiment is 6.8 mm.
  • the first reflecting device is a second reflecting surface 5 parallel to the first laser beam
  • the second reflecting surface 5 and the cantilever beam probe 1 are respectively located at the side of the first laser beam.
  • the upper and lower sides and the mirror surfaces of the second reflection surface 5 face the first laser beam, and the second laser beam is reflected by the second reflection surface 5 and irradiated on the cantilever probe 1.
  • the second reflection device is a third reflection structure and a fourth reflection structure
  • the third reflection structure is a reflection surface
  • the fourth reflection structure is a reflection surface
  • the third reflection structure is a fourth reflection surface 7
  • the fourth reflection structure It is the fifth reflection surface 8.
  • the third reflection structure and the fourth reflection structure are respectively located on the upper and lower sides of the first laser beam and are parallel to each other and mirror-faced.
  • the size of the first reflective surface 4 is 12mm (width) x 5mm (length) x 1mm (thickness); the angle between the first reflective surface 4 and the horizontal plane is 112.5°; the size of the second reflective surface 5 is 20mm (width) x 9mm (Length) x 1mm (thickness); the size of the fourth reflective surface 7 is 20mm (width) x 5.5mm (length) x 1mm (thickness); the size of the fifth reflective surface 8 is 20mm (width) x 9mm (length) x 1mm (thickness); the vertical distance between the fourth reflective surface 7 and the fifth reflective surface 8 is 3.7mm; the horizontal distance between the second reflective surface 5 and the fourth reflective surface 7 is 7.5mm.
  • the thickness of the probe fixing module in this embodiment is 6.8 mm.
  • An atomic force microscope probe including: the probe fixing module I and the laser transceiver module II of the above-mentioned embodiment 3.
  • the laser transceiver module II includes: a laser emitting structure and a laser receiving structure, the laser emitting structure includes: a laser 10 and a laser The first condensing lens 12 on the optical path of the laser beam (the first condensing lens 12 is located outside the probe fixing module), so that the first laser beam passes through the first condensing lens 12 and the second laser beam is projected on the cantilever probe 1
  • the laser receiving structure includes: a photodetector 14 and a second converging lens 13 located on the optical path of the fourth laser beam, so that the fourth laser beam passes through the second converging lens 13 and is projected on the photosensitive surface of the photodetector 14.
  • a filter (not shown in the figure) is installed on the optical path of the fourth laser beam after passing through the second condensing lens 13 to reduce stray light interference.
  • the photodetector 14 is installed on a two-dimensional adjustment table 15, and the two-dimensional adjustment table 15 is used to adjust the position of the photodetector 14;
  • It also includes a second adjustment frame 11 on which the laser 10 is installed, and the second adjustment frame 11 is used to adjust the position and angle of the laser 10.
  • the laser uses a diode laser with a wavelength of 780 nm and a power of 4.5 mW, and its exit spot is a circle with a diameter of 2.5 mm.
  • the first convergent lens is installed at the exit of the laser, using a precision polished aspheric lens plated with a 780nm antireflection coating, with an effective focal length of 79mm and a numerical aperture of 0.143.
  • the second convergent lens is an ordinary spherical lens with a 780nm antireflection coating, with an effective focal length of 25mm and a numerical aperture of 0.23.
  • the photodetector uses Hamamatsu's four-quadrant photodetector, and the photosensitive surface is a square area with a side length of 10mm.
  • the photodetector is fixed on the two-dimensional adjustment table 15.
  • the two-dimensional adjustment stage is a two-dimensional manual translation stage, and its X and Y strokes are both 6mm, and the displacement resolution is better than 10 ⁇ m.
  • the effective Z-direction thickness of the probe fixing module that is, the vertical distance from the upper surface of the second reflective surface 5 to the tip of the cantilever probe 1 is 6.8 mm.
  • the optical microscope above the probe of the atomic force microscope can use Mitutoyo's 50X plan apochromatic objective lens with a working distance of 13mm and a numerical aperture of 0.55.
  • the fourth laser beam emitted from the probe fixing module I enters the second convergent lens 13 in the laser transceiver module II and is projected onto the photodetector 14.
  • An atomic force microscope comprising: the probe of the atomic force microscope in embodiment 5, a motor coarse positioning platform 16, a piezoelectric scanner 17, a sample stage 18, and an objective lens 19 located outside the probe of the atomic force microscope, and the objective lens 19 is fixed on the probe Just above the module I, the tip of the cantilever probe 1 is positioned in the field of view of the objective lens 19 through the light-passing hole.
  • the motor coarse positioning platform 16, the piezoelectric scanner 17, and the sample stage 18 are located below the probe fixing module I, which can drive the sample to move three-dimensionally relative to the needle tip and scan and image.
  • the sample stage is installed on a piezoelectric ceramic scanner (piezoelectric scanner) with three-dimensional scanning capability.
  • the piezoelectric ceramic scanner is installed on the motor coarse positioning platform.
  • the atomic force microscope probe is located above the sample stage, and the probe is fixed
  • Module I is located directly above the sample, and laser transceiver module II is located on the side of probe fixing module I (the right side is shown in Figure 5).
  • the motor coarse positioning platform 16 adopts a combined stepping motor, and the three-axis stepping resolution is less than 1 ⁇ m.
  • the piezoelectric ceramic scanner uses PI's three-dimensional nano-positioning stage P-517.3C, with a closed loop stroke of 100 ⁇ m in the X and Y directions, a displacement resolution of 0.3nm, and a closed loop stroke of 20 ⁇ m in the Z direction and a displacement resolution of 0.1nm.
  • the cantilever beam probe is installed in the probe holder and the cantilever beam is inclined at 10° with the horizontal plane to ensure that the needle tip is located at the lowest point of the probe fixing module 1.
  • the probe holder is fixed on the bottom of the piezoelectric ceramic.
  • the size of the piezoelectric ceramic is 5mm ⁇ 5mm ⁇ 1mm.
  • the probe of the atomic force microscope proposed by the present invention must cooperate with an external three-dimensional scanner (motor coarse positioning platform 16 and piezoelectric scanner 17) to realize the scanning imaging function.
  • an external three-dimensional scanner motor coarse positioning platform 16 and piezoelectric scanner 17
  • the probe of the atomic force microscope is fixed and the piezoelectric scanner carries the sample for three-dimensional scanning.
  • the probe of the atomic force microscope is used in conjunction with other instruments such as an optical microscope, the probe of the atomic force microscope is located between the sample and the objective lens, and the Z-direction thickness of the probe of the atomic force microscope is smaller than the working distance of the objective lens used.

Abstract

An ultra-thin atomic force microscope head. The atomic force microscope head employs an ultra-thin probe fixing module (I). The probe fixing module (I) comprises a cantilever probe (1), piezoelectric ceramic (2), a probe holder (3), a first reflecting surface (4), a first reflecting unit, and a second reflecting unit. The cantilever probe (1) is mounted in the probe holder (3), and the tip of the cantilever probe (1) is located at the lowest portion of the probe fixing module (I). The first reflecting surface (4) is located on one side of the cantilever probe (1). The first reflecting unit is located between the cantilever probe (1) and the first reflecting surface (4). The second reflecting unit is located between the cantilever probe (1) and a laser. A third laser beam is reflected by the second reflecting unit and then is emitted from the probe fixing module (I) to form a fourth laser beam. The Z-direction effective thickness of the probe fixing module (I) in the atomic force microscope head is only several millimeters, and therefore, the atomic force microscope head can be directly mounted below an optical or electron microscope having a working distance greater than the thickness to achieve integrated combination of different devices.

Description

一种超薄原子力显微镜测头An ultra-thin atomic force microscope probe 技术领域Technical field
本发明属于原子力显微镜技术领域,具体涉及一种竖直方向厚度超薄的探针固定模块以及基于该探针固定模块的原子力显微镜测头。The invention belongs to the technical field of atomic force microscopes, and in particular relates to a probe fixing module with an ultra-thin thickness in the vertical direction and an atomic force microscope probe based on the probe fixing module.
背景技术Background technique
20世纪80年代原子力显微镜的出现使人们得以突破衍射极限对传统光学显微镜的限制,能够以亚纳米级的分辨力实现对各种材料的三维形貌表征。不仅如此,这一技术还能进行材料物理特性的原位检测甚至原子级的操纵与加工。经过三十余年的发展,原子力显微镜目前已被广泛应用于半导体工业、新材料、生命科学等领域,是微纳米尺度科学研究的必备工具之一。The emergence of atomic force microscopes in the 1980s allowed people to break through the limitations of the diffraction limit on traditional optical microscopes, and to realize the three-dimensional characterization of various materials with sub-nanometer resolution. Not only that, this technology can also perform in-situ detection of material physical properties and even atomic-level manipulation and processing. After more than 30 years of development, atomic force microscopes have been widely used in the semiconductor industry, new materials, life sciences and other fields, and are one of the necessary tools for micro- and nano-scale scientific research.
通过集成不同种类的检测装置以实现原位多物理场探测是当前仪器行业发展的重要趋势之一。原子力显微镜与各类光学显微镜及电子显微镜相结合能够进行原位高分辨形貌、成分和理化特性表征,可以显著提高检测效率,在生命科学、微电子等领域有着十分广阔的应用前景。然而由于结构尺寸上的限制,原子力显微镜与其他类型显微镜的集成存在一定的技术困难。The integration of different types of detection devices to achieve in-situ multi-physics detection is one of the important trends in the development of the current instrument industry. The combination of atomic force microscope and various optical microscopes and electron microscopes can perform in-situ high-resolution characterization of morphology, composition and physical and chemical properties, and can significantly improve detection efficiency. It has very broad application prospects in life sciences, microelectronics and other fields. However, due to the limitation of the size of the structure, there are certain technical difficulties in integrating the atomic force microscope with other types of microscopes.
当前主流原子力显微镜系统普遍采用微悬臂梁探针感知样品,当探针在样品表面扫描时,针尖与样品间的作用力使得微悬臂梁产生弯曲形变,这一微小形变经测头中的光杠杆光路放大并由光电探测器转换为电信号。作为原子力显微镜的核心部分,其测头通常体积较大,其Z向厚度尺寸可达数厘米。而电镜和光学显微镜的工作距离(电子枪出口或光学物镜下表面到样品的距离)一般只有几毫米到十几毫米,这就使得现有的原子力显微镜测头装置很难直接集成在电镜和光学显微镜工作台上。市面上现有的原子力显微镜-电镜联用系统大多采用自感应的音叉式探针或压阻探针。这类探针无需额外的检测光路,占用空间小,但在大气环境中易受干扰,应用限制较多。近年一些公司推出的原子力显微镜-拉曼/荧光显微镜联用设备则大多采用倒置式光学显微系统,这一方案可从结构上避免光学显微镜与原子力测头的机械干涉,但不足在于只能检测透明样品。The current mainstream atomic force microscope systems generally use micro cantilever probes to sense samples. When the probe is scanned on the surface of the sample, the force between the tip and the sample causes the micro cantilever to bend and deform. This small deformation is caused by the optical lever in the probe. The optical path is amplified and converted into electrical signals by the photodetector. As the core part of the atomic force microscope, the probe is usually large in size, and its thickness in the Z direction can reach several centimeters. The working distance between the electron microscope and the optical microscope (the distance between the exit of the electron gun or the lower surface of the optical objective lens and the sample) is generally only a few millimeters to ten millimeters, which makes it difficult for the existing atomic force microscope probe devices to be directly integrated into the electron microscope and optical microscope. On the workbench. Most of the existing atomic force microscope-electron microscope combined systems on the market use self-inducing tuning fork probes or piezoresistive probes. This type of probe does not require an additional detection light path and occupies a small space, but it is susceptible to interference in the atmospheric environment and has many application restrictions. In recent years, the atomic force microscope-Raman/fluorescence microscope combination equipment introduced by some companies mostly adopts an inverted optical microscope system. This solution can avoid the mechanical interference between the optical microscope and the atomic force probe in structure, but the disadvantage is that it can only detect Transparent sample.
原子力测头的体积主要取决于光杠杆光路的设计。现有的光杠杆光路大致可分为如 图1~4所示的几种典型形式。在图1、2所示的光路中,激光经过直角棱镜20或透镜组23之后沿Z向竖直向下打在悬臂梁探针上,悬臂梁反射的光经一片或多片平面反射镜21反射至光电探测器上。对于采用此类光路的原子力显微镜,可在其上方或侧面安装光学显微镜。但为了不与光杠杆光路中的光学元件发生机械干涉,必须使用工作距离较长的低倍物镜。在图3所示的光路中,光杠杆与光学显微镜光路共用一个物镜,光杠杆激光束通过物镜聚焦在探针悬臂梁上,悬臂梁的反射光又被物镜收集并转换为平行光,再通过位于物镜上方的偏振分光镜24等元件投射到光电探测器上(物镜和偏振分光镜之间光路上设置有二向色镜22和四分之一波片25)。这种形式的光路能够最大限度地减小原子力测头所占空间,允许使用大数值孔径、短工作距离的高倍物镜。但由于需要将光杠杆光路耦合到光学显微镜中,该原子力测头无法与已封装好的商品化光学系统集成。此外,在图1~3所示的方案中,探针和样品的正上方设置有光学元件,会阻碍电子束的传播,因而这三种原子力测头均不适合与电子显微镜集成。在图4所示的结构中,激光束倾斜入射至探针上,反射光对称出射至光电探测器。这一设计的优势在于探针正上方的区域得到了释放,既可以安装光学显微镜也可以安装电子显微镜或其他类型设备。但为避免激光束被光学物镜外壳或电镜极靴遮挡,激光束必须以较大的倾角射向悬臂梁探针。当倾角过大时,悬臂梁上的反射光斑形状和反射强度会变差,进而影响光电探测器的输出信号质量。因此图4中的原子力测头只能用于工作距离较长的低放大倍率系统。The volume of the atomic force probe mainly depends on the design of the optical lever optical path. The existing optical lever optical path can be roughly divided into several typical forms as shown in Figures 1 to 4. In the light path shown in Figures 1 and 2, the laser beam passes through the right-angle prism 20 or lens group 23 and strikes the cantilever probe vertically downwards along the Z direction. The light reflected by the cantilever beam passes through one or more plane mirrors 21. Reflected on the photodetector. For atomic force microscopes using this type of optical path, optical microscopes can be installed above or on the side. However, in order not to mechanically interfere with the optical components in the optical path of the optical lever, a low-power objective lens with a long working distance must be used. In the optical path shown in Figure 3, the optical lever and the optical microscope optical path share an objective lens. The optical lever laser beam is focused on the probe cantilever beam through the objective lens. The reflected light of the cantilever beam is collected by the objective lens and converted into parallel light, and then passes through The polarization beam splitter 24 and other elements located above the objective lens are projected onto the photodetector (the optical path between the objective lens and the polarization beam splitter is provided with a dichroic mirror 22 and a quarter wave plate 25). This form of optical path can minimize the space occupied by the atomic force probe, allowing the use of high magnification objectives with large numerical apertures and short working distances. However, due to the need to couple the optical lever optical path to the optical microscope, the atomic force probe cannot be integrated with a packaged commercial optical system. In addition, in the solutions shown in Figures 1 to 3, optical elements are arranged directly above the probe and the sample, which will hinder the propagation of the electron beam, so these three types of atomic force probes are not suitable for integration with an electron microscope. In the structure shown in Figure 4, the laser beam is incident on the probe obliquely, and the reflected light is symmetrically emitted to the photodetector. The advantage of this design is that the area directly above the probe is released, which can be installed with either an optical microscope or an electron microscope or other types of equipment. However, in order to prevent the laser beam from being blocked by the optical objective lens housing or the electron microscope pole piece, the laser beam must be directed toward the cantilever probe with a large inclination angle. When the inclination angle is too large, the shape and intensity of the reflected light spot on the cantilever beam will deteriorate, which will affect the output signal quality of the photodetector. Therefore, the atomic force probe in Figure 4 can only be used for low magnification systems with long working distances.
如上所述,现有的几种光路形式使得原子力显微镜测头部分的Z向占用空间过大,不利于与光学显微镜(特别是正置高倍光学显微镜)、电子显微镜等设备集成。为减小原子力测头的体积,使之具有更好的兼容性和可集成性,有必要设计一种竖直方向(Z向)尺寸更为紧凑的新型测头结构。As mentioned above, the existing several optical path forms make the Z-direction of the probe part of the atomic force microscope occupy too much space, which is not conducive to the integration of optical microscopes (especially upright high-power optical microscopes), electron microscopes and other equipment. In order to reduce the volume of the atomic force probe and make it have better compatibility and integration, it is necessary to design a new type of probe structure with a more compact vertical (Z-direction) size.
发明内容Summary of the invention
针对原子力显微镜因尺寸原因而难以与其他类型设备集成的问题,本发明的目的在于提供一种探针固定模块,该探针固定模块能够减小原子力显微镜测头的Z向厚度。Aiming at the problem that the atomic force microscope is difficult to integrate with other types of equipment due to its size, the purpose of the present invention is to provide a probe fixing module which can reduce the Z-direction thickness of the probe of the atomic force microscope.
本发明的另一目的是提供一种原子力显微镜测头,该原子力显微镜测头基于上述探针固定模块,能够直接安装在高倍光学显微镜、电子显微镜等设备工作台上,且不影响原设备自身功能和性能指标。Another object of the present invention is to provide an atomic force microscope probe, which is based on the above-mentioned probe fixing module and can be directly installed on the workbench of high-power optical microscopes, electron microscopes and other equipment without affecting the original equipment's own functions And performance indicators.
本发明的目的是通过下述技术方案予以实现的。The purpose of the present invention is achieved through the following technical solutions.
一种探针固定模块,包括:悬臂梁探针、压电陶瓷、探针夹持器、第一反射面、第一反射装置和第二反射装置,所述悬臂梁探针安装在探针夹持器中,悬臂梁探针的针尖位于探针固定模块的最低处,所述第一反射面位于所述悬臂梁探针的一侧,用于接收位于所述悬臂梁探针另一侧的激光器发射的第一激光束并将该第一激光束反射形成第二激光束,所述第一反射面与所述第一激光束之间所夹锐角为60°~67.5°;所述第一反射装置位于所述悬臂梁探针和所述第一反射面之间,第二激光束被第一反射装置反射后照射在所述悬臂梁探针上并被悬臂梁探针反射形成第三激光束;所述第二反射装置位于所述悬臂梁探针和所述激光器之间,所述第三激光束被所述第二反射装置反射后从所述探针固定模块射出并形成第四激光束。A probe fixing module, comprising: a cantilever beam probe, a piezoelectric ceramic, a probe holder, a first reflection surface, a first reflection device and a second reflection device, the cantilever beam probe is mounted on the probe holder In the holder, the tip of the cantilever beam probe is located at the lowest point of the probe fixing module, and the first reflective surface is located on one side of the cantilever beam probe for receiving the cantilever beam probe on the other side. The first laser beam emitted by the laser reflects the first laser beam to form a second laser beam, and the acute angle between the first reflective surface and the first laser beam is 60°-67.5°; The reflection device is located between the cantilever beam probe and the first reflection surface, and the second laser beam is reflected by the first reflection device and irradiated on the cantilever beam probe and reflected by the cantilever beam probe to form a third laser beam The second reflecting device is located between the cantilever beam probe and the laser, the third laser beam is reflected by the second reflecting device and then emitted from the probe fixing module to form a fourth laser bundle.
在上述技术方案中,所述第一反射装置为平行于第一激光束的第二反射面,所述第二反射面与悬臂梁探针分别位于所述第一激光束的两侧且第二反射面的镜面朝向该第一激光束,所述第二激光束被第二反射面反射后照射在所述悬臂梁探针上。In the above technical solution, the first reflecting device is a second reflecting surface parallel to the first laser beam, and the second reflecting surface and the cantilever probe are respectively located on both sides of the first laser beam and the second The mirror surface of the reflecting surface faces the first laser beam, and the second laser beam is reflected by the second reflecting surface and irradiated on the cantilever beam probe.
在上述技术方案中,所述第一反射装置为第一反射结构和第二反射结构,所述第一反射结构为1个反射面或位于同一平面上且数量大于1的多个反射面,所述第二反射结构为1个反射面或位于同一平面上且数量大于1的多个反射面,所述第一反射结构和第二反射结构相互平行且镜面相对。In the above technical solution, the first reflective device is a first reflective structure and a second reflective structure, and the first reflective structure is one reflective surface or multiple reflective surfaces located on the same plane and the number is greater than one, so The second reflective structure is one reflective surface or multiple reflective surfaces located on the same plane and the number is greater than one, and the first reflective structure and the second reflective structure are parallel to each other and mirror-faced.
在上述技术方案中,所述第二反射装置为平行于第一激光束的第四反射面,所述第四反射面与悬臂梁探针分别位于所述第一激光束的两侧且第四反射面的镜面朝向该第一激光束,所述第三激光束被第四反射面反射后形成所述第四激光束。In the above technical solution, the second reflecting device is a fourth reflecting surface parallel to the first laser beam, and the fourth reflecting surface and the cantilever probe are respectively located on both sides of the first laser beam and the fourth reflecting surface The mirror surface of the reflecting surface faces the first laser beam, and the third laser beam is reflected by the fourth reflecting surface to form the fourth laser beam.
在上述技术方案中,所述第二反射装置为第三反射结构和第四反射结构,所述第三反射结构为1个反射面或位于同一平面上且数量大于1的多个反射面,所述第四反射结构为1个反射面或位于同一平面上且数量大于1的多个反射面,所述第三反射结构和第四反射结构相互平行且镜面相对。In the above technical solution, the second reflecting device is a third reflecting structure and a fourth reflecting structure, and the third reflecting structure is one reflecting surface or a plurality of reflecting surfaces located on the same plane and the number is greater than 1, so The fourth reflective structure is one reflective surface or multiple reflective surfaces located on the same plane and the number is greater than one, and the third reflective structure and the fourth reflective structure are parallel to each other and mirror-faced.
在上述技术方案中,在所述第一反射装置和所述第二反射装置之间形成有通光孔,用于通过成像光路。In the above technical solution, a light through hole is formed between the first reflecting device and the second reflecting device for passing through the imaging light path.
在上述技术方案中,还包括:安装有所述第一反射面的第一调整架,用于调整该第一反射面与所述第一激光束的夹角。In the above technical solution, it further includes: a first adjustment frame mounted with the first reflection surface, for adjusting the angle between the first reflection surface and the first laser beam.
在上述技术方案中,还包括:与所述探针夹持器固装的压电陶瓷,用于激励悬臂梁探针产生振动或做Z向扫描。In the above technical solution, it further includes: piezoelectric ceramics fixed to the probe holder, used to excite the cantilever beam probe to vibrate or perform Z-direction scanning.
一种原子力显微镜测头,包括:所述探针固定模块和激光收发模块,所述激光收发模块包括:激光发射结构和激光接收结构,所述激光发射结构包括:所述激光器以及位于第一激光束光路上的第一会聚透镜,以使所述第一激光束穿过所述第一会聚透镜且第二激光束聚焦在所述悬臂梁探针上;所述激光接收结构包括:光电探测器和位于第四激光束光路上的第二会聚透镜,以使所述第四激光束穿过所述第二会聚透镜后投射在所述光电探测器的感光面上。An atomic force microscope measuring head, comprising: the probe fixing module and a laser transceiving module, the laser transceiving module includes: a laser emitting structure and a laser receiving structure, the laser emitting structure includes: the laser and the first laser A first converging lens on the beam path, so that the first laser beam passes through the first converging lens and the second laser beam is focused on the cantilever probe; the laser receiving structure includes: a photodetector And a second convergent lens located on the optical path of the fourth laser beam, so that the fourth laser beam passes through the second convergent lens and is projected on the photosensitive surface of the photodetector.
在上述技术方案中,在所述第四激光束穿过所述第二会聚透镜后的光路上安装有滤光片,用于减少杂散光干扰。In the above technical solution, a filter is installed on the optical path after the fourth laser beam passes through the second condensing lens to reduce stray light interference.
在上述技术方案中,所述光电探测器安装在二维调整台上,该二维调整台用于调整该光电探测器的位置。In the above technical solution, the photodetector is installed on a two-dimensional adjustment table, and the two-dimensional adjustment table is used to adjust the position of the photodetector.
在上述技术方案中,还包括:第二调整架,所述激光器安装在第二调整架上,该第二调整架用于调整该激光器的位置和角度。In the above technical solution, it further includes: a second adjustment frame on which the laser is installed, and the second adjustment frame is used to adjust the position and angle of the laser.
1.本发明原子力显微镜测头中探针固定模块的Z向有效厚度(从第二反射面5的上表面到悬臂梁探针1的针尖的垂直距离)仅为数毫米,可直接安装在工作距离大于该厚度的光学或电子显微镜下实现不同设备的集成联用。1. The Z-direction effective thickness (the vertical distance from the upper surface of the second reflecting surface 5 to the tip of the cantilever probe 1) of the probe fixing module in the atomic force microscope probe of the present invention is only a few millimeters, which can be directly installed at the working distance The integrated use of different devices can be realized under an optical or electron microscope larger than this thickness.
2.原子力显微镜测头结构紧凑,Z向厚度较之常规原子力显微镜显著减小,易于与其他设备集成。2. The probe of the atomic force microscope has a compact structure, and the Z-direction thickness is significantly reduced compared with the conventional atomic force microscope, and it is easy to integrate with other equipment.
3.该原子力显微镜测头与光学显微镜或电子显微镜集成时,可直接安装在光学物镜或电镜极靴与样品之间,无需对既有显微镜主体进行改动,二者光路无耦合,各自功能不受影响。3. When the AFM probe is integrated with an optical microscope or an electron microscope, it can be directly installed between the optical objective lens or electron microscope pole piece and the sample without modifying the existing microscope body. The optical paths of the two are not coupled, and their functions are not affected. influences.
4.该原子力显微镜测头采用模块化设计,各模块相对独立,易于安装调试和维修升级。4. The probe of the atomic force microscope adopts modular design, each module is relatively independent, easy to install, debug, maintain and upgrade.
附图说明Description of the drawings
图1为原子力显微镜测头结构1示意图;Figure 1 is a schematic diagram of the probe structure 1 of an atomic force microscope;
图2为原子力显微镜测头结构2示意图;Figure 2 is a schematic diagram of the probe structure 2 of an atomic force microscope;
图3为原子力显微镜测头结构3示意图:Figure 3 is a schematic diagram of the probe structure 3 of the atomic force microscope:
图4为原子力显微镜测头结构4示意图:Figure 4 is a schematic diagram of the probe structure 4 of the atomic force microscope:
图5为本发明原子力显微镜测头的结构示意图;5 is a schematic diagram of the structure of the probe of the atomic force microscope of the present invention;
图6为本发明原子力显微镜测头的结构示意图。Fig. 6 is a schematic diagram of the structure of the probe of the atomic force microscope of the present invention.
其中,among them,
Ⅰ:探针固定模块          Ⅱ:激光收发模块Ⅰ: Probe fixed module Ⅱ: Laser transceiver module
1:悬臂梁探针;           2:压电陶瓷;1: Cantilever beam probe; 2: Piezoelectric ceramic;
3:探针夹持器;           4:第一反射面;3: Probe holder; 4: The first reflective surface;
5:第二反射面;           6:第三反射面;5: Second reflective surface; 6: Third reflective surface;
7:第四反射面;           8:第五反射面;7: Fourth reflecting surface; 8: Fifth reflecting surface;
9:第一调整架;           10:激光器;9: First adjustment frame; 10: Laser;
11:第二调整架;          12:第一会聚透镜;11: Second adjustment frame; 12: First convergent lens;
13:第二会聚透镜;        14:光电探测器;13: Second convergent lens; 14: Photodetector;
15:二维调整台;          16:电机粗定位平台;15: Two-dimensional adjustment platform; 16: Motor coarse positioning platform;
17:压电扫描器;          18:样品台;17: Piezoelectric scanner; 18: Sample stage;
19:物镜;                20:直角棱镜;19: Objective lens; 20: Right-angle prism;
21:平面反射镜;          22:二向色镜;21: Plane mirror; 22: Dichroic mirror;
23:透镜组;              24:偏振分光镜;23: Lens group; 24: Polarization beam splitter;
25:四分之一波片。25: Quarter wave plate.
具体实施方式detailed description
下面结合具体实施例进一步说明本发明的技术方案。The technical solution of the present invention will be further described below in conjunction with specific embodiments.
实施例1Example 1
一种探针固定模块,包括:悬臂梁探针1、压电陶瓷2、探针夹持器3、第一反射面4、第一反射装置和第二反射装置,悬臂梁探针1安装在探针夹持器3中,悬臂梁探针1的针尖位于探针固定模块Ⅰ的最低处,第一反射面4位于悬臂梁探针1的一侧,用于接收位于悬臂梁探针1另一侧的激光器10发射的第一激光束并将该第一激光束反射形成第二激光束,第一反射面4与第一激光束之间所夹锐角为60°~67.5°。A probe fixing module includes: a cantilever beam probe 1, a piezoelectric ceramic 2, a probe holder 3, a first reflection surface 4, a first reflection device and a second reflection device. The cantilever beam probe 1 is installed on In the probe holder 3, the tip of the cantilever probe 1 is located at the lowest point of the probe fixing module I, and the first reflective surface 4 is located on one side of the cantilever probe 1 for receiving another The first laser beam emitted by the laser 10 on one side reflects the first laser beam to form a second laser beam, and the acute angle between the first reflective surface 4 and the first laser beam is 60°-67.5°.
第一反射装置位于悬臂梁探针1和第一反射面4之间,第二激光束被第一反射装置反射后以45°~60°的倾角照射在悬臂梁探针1上并被悬臂梁探针1反射形成第三激光束;第二反射装置位于悬臂梁探针1和激光器10之间,第三激光束被第二反射装置反射后从探针固定模块Ⅰ射出并形成第四激光束。The first reflection device is located between the cantilever beam probe 1 and the first reflection surface 4. The second laser beam is reflected by the first reflection device and irradiated on the cantilever beam probe 1 at an inclination angle of 45°-60° and is The probe 1 reflects to form a third laser beam; the second reflecting device is located between the cantilever beam probe 1 and the laser 10. The third laser beam is reflected by the second reflecting device and then emitted from the probe fixing module I and forms a fourth laser beam .
实施例2Example 2
在实施例1的基础上,在第一反射装置和第二反射装置之间形成有通光孔,用于通过成像光路;On the basis of Embodiment 1, a light through hole is formed between the first reflecting device and the second reflecting device for passing through the imaging light path;
还包括:安装有第一反射面4的第一调整架9,用于调整该第一反射面4与第一激光束的夹角;It also includes: a first adjustment frame 9 mounted with a first reflective surface 4, for adjusting the angle between the first reflective surface 4 and the first laser beam;
还包括:与探针夹持器3固装的压电陶瓷2,用于激励悬臂梁探针1产生振动或做Z向扫描(Z向:与第一激光束垂直的方向)。It also includes: the piezoelectric ceramic 2 fixed to the probe holder 3, which is used to excite the cantilever beam probe 1 to vibrate or perform Z-direction scanning (Z-direction: the direction perpendicular to the first laser beam).
实施例3Example 3
如图5所示,在实施例2的基础上,第一反射装置为第一反射结构和第二反射结构,第一反射结构为1个反射面,第二反射结构为1个反射面,在本实施例中,第一反射结构为第二反射面5,第二反射结构为第三反射面6,第一反射结构和第二反射结构相互平行,第二反射面5和第三反射面6分别位于第一激光束的上下两侧且其之间的距离为3.7mm。As shown in FIG. 5, on the basis of Embodiment 2, the first reflection device is a first reflection structure and a second reflection structure, the first reflection structure is a reflection surface, and the second reflection structure is a reflection surface. In this embodiment, the first reflective structure is the second reflective surface 5, the second reflective structure is the third reflective surface 6, the first reflective structure and the second reflective structure are parallel to each other, and the second reflective surface 5 and the third reflective surface 6 They are located on the upper and lower sides of the first laser beam and the distance between them is 3.7 mm.
第二反射装置为第三反射结构和第四反射结构,第三反射结构为1个反射面,第四反射结构为1个反射面,第三反射结构为第四反射面7,第四反射结构为第五反射面8,第三反射结构和第四反射结构相互平行。第四反射面7和第五反射面8分别位于第一激光束的上下两侧且垂直间距为3.7mm;第二反射面5和第四反射面7水平间距为7.5mm作为通光孔。The second reflection device is a third reflection structure and a fourth reflection structure, the third reflection structure is a reflection surface, the fourth reflection structure is a reflection surface, the third reflection structure is a fourth reflection surface 7, and the fourth reflection structure It is the fifth reflective surface 8, and the third reflective structure and the fourth reflective structure are parallel to each other. The fourth reflection surface 7 and the fifth reflection surface 8 are respectively located on the upper and lower sides of the first laser beam with a vertical distance of 3.7 mm; the second reflection surface 5 and the fourth reflection surface 7 have a horizontal distance of 7.5 mm as light passing holes.
在本实施例中,第一~第五反射面均采用镀银膜平面反射镜。其中,第一反射面4所用的镀银膜平面反射镜尺寸为15mm×4.5mm×1mm,粘贴在与水平面成112.5°角的固定斜面上,且用于反射的一面朝向其右上方的第二反射面5(如图5所示);第二反射面5和第四反射面7可以属于同一个反射镜的不同区域(即一体构成),也可以为2块不同的反射镜,当第二反射面5和第四反射面7为一体构成时,其尺寸可以为15mm×20mm×1mm,水平放置于悬臂梁探针的上方,反射镜中间加工有一个直径为7.5mm的通孔作为通光孔,第二反射面5和第四反射面7分居该通孔左右两侧。In this embodiment, the first to fifth reflective surfaces are all silver-coated flat mirrors. Among them, the silver-plated plane mirror used for the first reflecting surface 4 has a size of 15mm×4.5mm×1mm, which is pasted on a fixed inclined surface at an angle of 112.5° with the horizontal plane, and the reflection surface faces the second upper right side. The reflecting surface 5 (as shown in Figure 5); the second reflecting surface 5 and the fourth reflecting surface 7 can belong to different areas of the same reflecting mirror (that is, integrated), or they can be two different reflecting mirrors. When the reflecting surface 5 and the fourth reflecting surface 7 are integrally formed, the size can be 15mm×20mm×1mm, placed horizontally above the cantilever probe, and a through hole with a diameter of 7.5mm is processed in the middle of the reflector for light transmission Hole, the second reflection surface 5 and the fourth reflection surface 7 are located on the left and right sides of the through hole.
第五反射面8所用的反射镜尺寸为15mm×20mm×1mm,水平放置于悬臂梁探针1右侧。第一激光束从第一会聚透镜12射出后依次经过第一反射面4、第二反射面5的第一次反射、第三反射面6和第二反射面5的第二次反射后会聚在悬臂梁探针1上,悬臂梁探针1反射的第三激光束再依次经过第四反射面7的第一次反射、第五反射面8和第四 反射面7的第二次反射后向探针固定模块I右下方射出且形成第四激光束。第二反射面5和第四反射面7中每一反射面上的两个反射点相距约14mm。The size of the reflector used for the fifth reflecting surface 8 is 15mm×20mm×1mm, and it is placed horizontally on the right side of the cantilever probe 1. The first laser beam is emitted from the first condensing lens 12 and then passes through the first reflection surface 4, the first reflection surface 5, the third reflection surface 6 and the second reflection surface 5, and then converges on On the cantilever beam probe 1, the third laser beam reflected by the cantilever beam probe 1 passes through the first reflection of the fourth reflection surface 7, the second reflection of the fifth reflection surface 8 and the fourth reflection surface 7 in turn. The probe fixing module 1 emits and forms a fourth laser beam at the bottom right. The distance between the two reflection points on each of the second reflection surface 5 and the fourth reflection surface 7 is about 14 mm.
经测量,本实施例中探针固定模块的厚度为6.8mm。After measurement, the thickness of the probe fixing module in this embodiment is 6.8 mm.
实施例4Example 4
如图6所示,在实施例2的基础上,第一反射装置为平行于第一激光束的第二反射面5,第二反射面5与悬臂梁探针1分别位于第一激光束的上下两侧且第二反射面5的镜面朝向该第一激光束,第二激光束被第二反射面5反射后照射在悬臂梁探针1上。As shown in FIG. 6, on the basis of Embodiment 2, the first reflecting device is a second reflecting surface 5 parallel to the first laser beam, and the second reflecting surface 5 and the cantilever beam probe 1 are respectively located at the side of the first laser beam. The upper and lower sides and the mirror surfaces of the second reflection surface 5 face the first laser beam, and the second laser beam is reflected by the second reflection surface 5 and irradiated on the cantilever probe 1.
第二反射装置为第三反射结构和第四反射结构,第三反射结构为1个反射面,第四反射结构为1个反射面,第三反射结构为第四反射面7,第四反射结构为第五反射面8,第三反射结构和第四反射结构分别位于第一激光束的上下两侧且相互平行、镜面相对。The second reflection device is a third reflection structure and a fourth reflection structure, the third reflection structure is a reflection surface, the fourth reflection structure is a reflection surface, the third reflection structure is a fourth reflection surface 7, and the fourth reflection structure It is the fifth reflection surface 8. The third reflection structure and the fourth reflection structure are respectively located on the upper and lower sides of the first laser beam and are parallel to each other and mirror-faced.
第一反射面4的尺寸是12mm(宽)x 5mm(长)x 1mm(厚);第一反射面4和水平面的角度为112.5°;第二反射面5的尺寸是20mm(宽)x 9mm(长)x 1mm(厚);第四反射面7的尺寸是20mm(宽)x 5.5mm(长)x 1mm(厚);第五反射面8的尺寸是20mm(宽)x 9mm(长)x 1mm(厚);第四反射面7和第五反射面8的垂直间距为3.7mm;第二反射面5和第四反射面7水平间距为7.5mm。The size of the first reflective surface 4 is 12mm (width) x 5mm (length) x 1mm (thickness); the angle between the first reflective surface 4 and the horizontal plane is 112.5°; the size of the second reflective surface 5 is 20mm (width) x 9mm (Length) x 1mm (thickness); the size of the fourth reflective surface 7 is 20mm (width) x 5.5mm (length) x 1mm (thickness); the size of the fifth reflective surface 8 is 20mm (width) x 9mm (length) x 1mm (thickness); the vertical distance between the fourth reflective surface 7 and the fifth reflective surface 8 is 3.7mm; the horizontal distance between the second reflective surface 5 and the fourth reflective surface 7 is 7.5mm.
经测量,本实施例中探针固定模块的厚度为6.8mm。After measurement, the thickness of the probe fixing module in this embodiment is 6.8 mm.
实施例5Example 5
一种原子力显微镜测头,包括:上述实施例3的探针固定模块Ⅰ和激光收发模块Ⅱ,激光收发模块Ⅱ包括:激光发射结构和激光接收结构,激光发射结构包括:激光器10以及位于第一激光束光路上的第一会聚透镜12(第一会聚透镜12位于探针固定模块外部),以使第一激光束穿过第一会聚透镜12且第二激光束投射在悬臂梁探针1上;激光接收结构包括:光电探测器14和位于第四激光束光路上的第二会聚透镜13,以使第四激光束穿过第二会聚透镜13后投射在光电探测器14的感光面上。An atomic force microscope probe, including: the probe fixing module I and the laser transceiver module II of the above-mentioned embodiment 3. The laser transceiver module II includes: a laser emitting structure and a laser receiving structure, the laser emitting structure includes: a laser 10 and a laser The first condensing lens 12 on the optical path of the laser beam (the first condensing lens 12 is located outside the probe fixing module), so that the first laser beam passes through the first condensing lens 12 and the second laser beam is projected on the cantilever probe 1 The laser receiving structure includes: a photodetector 14 and a second converging lens 13 located on the optical path of the fourth laser beam, so that the fourth laser beam passes through the second converging lens 13 and is projected on the photosensitive surface of the photodetector 14.
作为优选,在第四激光束穿过第二会聚透镜13后的光路上安装有滤光片(图中未示出),用于减少杂散光干扰。Preferably, a filter (not shown in the figure) is installed on the optical path of the fourth laser beam after passing through the second condensing lens 13 to reduce stray light interference.
作为优选,光电探测器14安装在二维调整台15上,二维调整台15用于调整该光电探测器14的位置;Preferably, the photodetector 14 is installed on a two-dimensional adjustment table 15, and the two-dimensional adjustment table 15 is used to adjust the position of the photodetector 14;
还包括:第二调整架11,激光器10安装在第二调整架11上,第二调整架11用于调整该激光器10的位置和角度。It also includes a second adjustment frame 11 on which the laser 10 is installed, and the second adjustment frame 11 is used to adjust the position and angle of the laser 10.
在本实施例中,激光器采用波长780nm,功率4.5mW的二极管激光器,其出射光斑为直径2.5mm的圆形。第一会聚透镜安装在激光器出口,采用镀有780nm增透膜的精密抛光非球面透镜,有效焦距为79mm,数值孔径0.143。第二会聚透镜选用带780nm增透膜的普通球面透镜,有效焦距25mm,数值孔径0.23。光电探测器采用滨松公司的四象限光电探测器,感光面为边长10mm的正方形区域。光电探测器固定在二维调整台15上。二维调整台为二维手动平移台,其X、Y行程均为6mm,位移分辨力优于10μm。本方案中,探针固定模块的有效Z向厚度即第二反射面5的上表面至悬臂梁探针1针尖处的垂直距离为6.8mm。原子力显微镜测头上方的光学显微镜可采用三丰公司的50X平场复消色差物镜,其工作距离为13mm,数值孔径0.55。In this embodiment, the laser uses a diode laser with a wavelength of 780 nm and a power of 4.5 mW, and its exit spot is a circle with a diameter of 2.5 mm. The first convergent lens is installed at the exit of the laser, using a precision polished aspheric lens plated with a 780nm antireflection coating, with an effective focal length of 79mm and a numerical aperture of 0.143. The second convergent lens is an ordinary spherical lens with a 780nm antireflection coating, with an effective focal length of 25mm and a numerical aperture of 0.23. The photodetector uses Hamamatsu's four-quadrant photodetector, and the photosensitive surface is a square area with a side length of 10mm. The photodetector is fixed on the two-dimensional adjustment table 15. The two-dimensional adjustment stage is a two-dimensional manual translation stage, and its X and Y strokes are both 6mm, and the displacement resolution is better than 10μm. In this solution, the effective Z-direction thickness of the probe fixing module, that is, the vertical distance from the upper surface of the second reflective surface 5 to the tip of the cantilever probe 1 is 6.8 mm. The optical microscope above the probe of the atomic force microscope can use Mitutoyo's 50X plan apochromatic objective lens with a working distance of 13mm and a numerical aperture of 0.55.
从探针固定模块I出射的第四激光束进入激光收发模块II中的第二会聚透镜13后投射到光电探测器14上。The fourth laser beam emitted from the probe fixing module I enters the second convergent lens 13 in the laser transceiver module II and is projected onto the photodetector 14.
实施例6Example 6
一种原子力显微镜,包括:实施例5中的原子力显微镜测头以及位于原子力显微镜测头外部的电机粗定位平台16、压电扫描器17、样品台18和物镜19,物镜19安装在探针固定模块Ⅰ的正上方,通过通光孔使悬臂梁探针1的针尖位于物镜19的视场内。An atomic force microscope, comprising: the probe of the atomic force microscope in embodiment 5, a motor coarse positioning platform 16, a piezoelectric scanner 17, a sample stage 18, and an objective lens 19 located outside the probe of the atomic force microscope, and the objective lens 19 is fixed on the probe Just above the module I, the tip of the cantilever probe 1 is positioned in the field of view of the objective lens 19 through the light-passing hole.
电机粗定位平台16、压电扫描器17和样品台18位于探针固定模块Ⅰ的下方,可带动样品相对于针尖做三维移动及扫描成像。The motor coarse positioning platform 16, the piezoelectric scanner 17, and the sample stage 18 are located below the probe fixing module I, which can drive the sample to move three-dimensionally relative to the needle tip and scan and image.
样品台安装于具有三维扫描能力的压电陶瓷扫描器(压电扫描器)上,压电陶瓷扫描器安装于电机粗定位平台上,原子力显微镜测头位于样品台的上方,其中,探针固定模块Ⅰ位于样品正上方,激光收发模块Ⅱ位于探针固定模块Ⅰ的一侧(图5所示为右侧)。The sample stage is installed on a piezoelectric ceramic scanner (piezoelectric scanner) with three-dimensional scanning capability. The piezoelectric ceramic scanner is installed on the motor coarse positioning platform. The atomic force microscope probe is located above the sample stage, and the probe is fixed Module I is located directly above the sample, and laser transceiver module II is located on the side of probe fixing module I (the right side is shown in Figure 5).
电机粗定位平台16采用组合式步进电机,三轴步进分辨力小于1μm。The motor coarse positioning platform 16 adopts a combined stepping motor, and the three-axis stepping resolution is less than 1μm.
压电陶瓷扫描器采用PI公司的三维纳米定位台P-517.3C,其X、Y方向的闭环行程为100μm,位移分辨力0.3nm,Z方向的闭环行程为20μm,位移分辨力0.1nm。The piezoelectric ceramic scanner uses PI's three-dimensional nano-positioning stage P-517.3C, with a closed loop stroke of 100μm in the X and Y directions, a displacement resolution of 0.3nm, and a closed loop stroke of 20μm in the Z direction and a displacement resolution of 0.1nm.
悬臂梁探针安装在探针夹持器内且悬臂梁与水平面成10°倾角以确保针尖位于探针固定模块I的最低点。The cantilever beam probe is installed in the probe holder and the cantilever beam is inclined at 10° with the horizontal plane to ensure that the needle tip is located at the lowest point of the probe fixing module 1.
探针夹持器固定在压电陶瓷底部,压电陶瓷的尺寸为5mm×5mm×1mm,当原子力显微镜工作在动态模式下时,压电陶瓷谐振可驱动悬臂梁探针1产生谐振。The probe holder is fixed on the bottom of the piezoelectric ceramic. The size of the piezoelectric ceramic is 5mm×5mm×1mm. When the atomic force microscope works in the dynamic mode, the piezoelectric ceramic resonance can drive the cantilever beam probe 1 to generate resonance.
本发明提出的原子力显微镜测头须与外部三维扫描器(电机粗定位平台16和压电扫描器17)配合实现扫描成像功能。扫描成像时,原子力显微镜测头固定不动,压电扫描 器搭载样品做三维扫描。该原子力显微镜与其他仪器如光学显微镜联用时,原子力显微镜测头位于样品和物镜之间,原子力显微镜测头的Z向厚度小于所用物镜的工作距离。The probe of the atomic force microscope proposed by the present invention must cooperate with an external three-dimensional scanner (motor coarse positioning platform 16 and piezoelectric scanner 17) to realize the scanning imaging function. When scanning imaging, the probe of the atomic force microscope is fixed and the piezoelectric scanner carries the sample for three-dimensional scanning. When the atomic force microscope is used in conjunction with other instruments such as an optical microscope, the probe of the atomic force microscope is located between the sample and the objective lens, and the Z-direction thickness of the probe of the atomic force microscope is smaller than the working distance of the objective lens used.
以上对本发明做了示例性的描述,应该说明的是,在不脱离本发明的核心的情况下,任何简单的变形、修改或者其他本领域技术人员能够不花费创造性劳动的等同替换均落入本发明的保护范围。The present invention has been exemplarily described above. It should be noted that, without departing from the core of the present invention, any simple deformation, modification, or other equivalent substitutions that can be made without creative labor by those skilled in the art fall into this The scope of protection of the invention.

Claims (12)

  1. 一种探针固定模块,其特征在于,包括:悬臂梁探针(1)、压电陶瓷(2)、探针夹持器(3)、第一反射面(4)、第一反射装置和第二反射装置,所述悬臂梁探针(1)安装在探针夹持器(3)中,悬臂梁探针(1)的针尖位于探针固定模块(Ⅰ)的最低处,所述第一反射面(4)位于所述悬臂梁探针(1)的一侧,用于接收位于所述悬臂梁探针(1)另一侧的激光器(10)发射的第一激光束并将该第一激光束反射形成第二激光束,所述第一反射面(4)与所述第一激光束之间所夹锐角为60~67.5°;所述第一反射装置位于所述悬臂梁探针(1)和所述第一反射面(4)之间,第二激光束被第一反射装置反射后照射在所述悬臂梁探针(1)上并被悬臂梁探针(1)反射形成第三激光束;所述第二反射装置位于所述悬臂梁探针(1)和所述激光器(10)之间,所述第三激光束被所述第二反射装置反射后从所述探针固定模块(Ⅰ)射出并形成第四激光束。A probe fixing module, which is characterized by comprising: a cantilever beam probe (1), a piezoelectric ceramic (2), a probe holder (3), a first reflecting surface (4), a first reflecting device and The second reflecting device, the cantilever beam probe (1) is installed in the probe holder (3), the tip of the cantilever beam probe (1) is located at the lowest point of the probe fixing module (I), and the first A reflecting surface (4) is located on one side of the cantilever probe (1), and is used to receive the first laser beam emitted by the laser (10) on the other side of the cantilever probe (1) The first laser beam is reflected to form a second laser beam, and the acute angle between the first reflecting surface (4) and the first laser beam is 60-67.5°; the first reflecting device is located in the cantilever beam probe Between the needle (1) and the first reflecting surface (4), the second laser beam is reflected by the first reflecting device and irradiated on the cantilever probe (1) and reflected by the cantilever probe (1) A third laser beam is formed; the second reflection device is located between the cantilever probe (1) and the laser (10), and the third laser beam is reflected by the second reflection device from the The probe fixing module (I) emits and forms a fourth laser beam.
  2. 根据权利要求1所述的探针固定模块,其特征在于,所述第一反射装置为平行于第一激光束的第二反射面(5),所述第二反射面(5)与悬臂梁探针(1)分别位于所述第一激光束的两侧且第二反射面(5)的镜面朝向该第一激光束,所述第二激光束被第二反射面(5)反射后照射在所述悬臂梁探针(1)上。The probe fixing module according to claim 1, wherein the first reflecting device is a second reflecting surface (5) parallel to the first laser beam, and the second reflecting surface (5) is connected to the cantilever beam. The probes (1) are respectively located on both sides of the first laser beam and the mirror surface of the second reflection surface (5) faces the first laser beam, and the second laser beam is reflected by the second reflection surface (5) and then irradiated On the cantilever probe (1).
  3. 根据权利要求1所述的探针固定模块,其特征在于,所述第一反射装置为第一反射结构和第二反射结构,所述第一反射结构为1个反射面或位于同一平面上且数量大于1的多个反射面,所述第二反射结构为1个反射面或位于同一平面上且数量大于1的多个反射面,所述第一反射结构和第二反射结构相互平行且镜面相对。The probe fixing module according to claim 1, wherein the first reflecting device is a first reflecting structure and a second reflecting structure, and the first reflecting structure is a reflecting surface or is located on the same plane and A number of reflective surfaces greater than 1, the second reflective structure is one reflective surface or multiple reflective surfaces located on the same plane with a number greater than 1, the first reflective structure and the second reflective structure are parallel to each other and mirrored relatively.
  4. 根据权利要求2或3所述的探针固定模块,其特征在于,所述第二反射装置为平行于第一激光束的第四反射面(7),所述第四反射面(7)与悬臂梁探针(1)分别位于所述第一激光束的两侧且第四反射面(7)的镜面朝向该第一激光束,所述第三激光束被第四反射面(7)反射后形成所述第四激光束。The probe fixing module according to claim 2 or 3, wherein the second reflecting device is a fourth reflecting surface (7) parallel to the first laser beam, and the fourth reflecting surface (7) is connected to The cantilever probes (1) are respectively located on both sides of the first laser beam and the mirror surface of the fourth reflection surface (7) faces the first laser beam, and the third laser beam is reflected by the fourth reflection surface (7) Then, the fourth laser beam is formed.
  5. 根据权利要求2或3所述的探针固定模块,其特征在于,所述第二反射装置为第三反射结构和第四反射结构,所述第三反射结构为1个反射面或位于同一平面上且数量大于1的多个反射面,所述第四反射结构为1个反射面或位于同一平面上且数量大于1的多个反射面,所述第三反射结构和第四反射结构相互平行且镜面相对。The probe fixing module according to claim 2 or 3, wherein the second reflection device is a third reflection structure and a fourth reflection structure, and the third reflection structure is a reflection surface or is located on the same plane The fourth reflective structure is one reflective surface or multiple reflective surfaces on the same plane with a number greater than 1, and the third reflective structure and the fourth reflective structure are parallel to each other And the mirror faces are opposite.
  6. 根据权利要求4或5所述的探针固定模块,其特征在于,在所述第一反射装置和 所述第二反射装置之间形成有通光孔,用于通过成像光路。The probe fixing module according to claim 4 or 5, wherein a light through hole is formed between the first reflecting device and the second reflecting device for passing through the imaging light path.
  7. 根据权利要求6所述的探针固定模块,其特征在于,还包括:安装有所述第一反射面(4)的第一调整架(9),用于调整该第一反射面(4)与所述第一激光束的夹角。The probe fixing module according to claim 6, further comprising: a first adjusting frame (9) mounted with the first reflecting surface (4), for adjusting the first reflecting surface (4) The included angle with the first laser beam.
  8. 根据权利要求7所述的探针固定模块,其特征在于,还包括:与所述探针夹持器(3)固装的压电陶瓷(2),用于激励悬臂梁探针(1)产生振动或做Z向扫描。The probe fixing module according to claim 7, further comprising: a piezoelectric ceramic (2) fixed to the probe holder (3) for exciting the cantilever beam probe (1) Vibrate or scan in Z direction.
  9. 一种原子力显微镜测头,其特征在于,包括:如权利要求1中所述探针固定模块(Ⅰ)和激光收发模块(Ⅱ),所述激光收发模块(Ⅱ)包括:激光发射结构和激光接收结构,所述激光发射结构包括:所述激光器(10)以及位于第一激光束光路上的第一会聚透镜(12),以使所述第一激光束穿过所述第一会聚透镜(12)且第二激光束聚焦在所述悬臂梁探针(1)上;所述激光接收结构包括:光电探测器(14)和位于第四激光束光路上的第二会聚透镜(13),以使所述第四激光束穿过所述第二会聚透镜(13)后投射在所述光电探测器(14)的感光面上。An atomic force microscope probe, characterized by comprising: the probe fixing module (I) and the laser transceiver module (II) as claimed in claim 1, the laser transceiver module (II) comprising: a laser emitting structure and a laser A receiving structure, the laser emitting structure includes: the laser (10) and a first converging lens (12) located on the optical path of the first laser beam, so that the first laser beam passes through the first converging lens ( 12) And the second laser beam is focused on the cantilever beam probe (1); the laser receiving structure includes: a photodetector (14) and a second converging lens (13) located on the optical path of the fourth laser beam, So that the fourth laser beam passes through the second condensing lens (13) and is projected on the photosensitive surface of the photodetector (14).
  10. 根据权利要求9所述的原子力显微镜测头,其特征在于,在所述第四激光束穿过所述第二会聚透镜(13)后的光路上安装有滤光片,用于减少杂散光干扰。The AFM probe according to claim 9, characterized in that a filter is installed on the optical path after the fourth laser beam passes through the second condensing lens (13) to reduce stray light interference .
  11. 根据权利要求10所述的原子力显微镜测头,其特征在于,所述光电探测器(14)安装在二维调整台(15)上,二维调整台(15)用于调整该光电探测器(14)的位置。The atomic force microscope probe according to claim 10, wherein the photodetector (14) is installed on a two-dimensional adjustment table (15), and the two-dimensional adjustment table (15) is used to adjust the photodetector ( 14) Location.
  12. 根据权利要求11所述的原子力显微镜测头,其特征在于,还包括:第二调整架(11),所述激光器(10)安装在第二调整架(11)上,第二调整架(11)用于调整该激光器(10)的位置和角度。The AFM probe according to claim 11, further comprising: a second adjustment frame (11), the laser (10) is mounted on the second adjustment frame (11), and the second adjustment frame (11) ) Is used to adjust the position and angle of the laser (10).
PCT/CN2019/089280 2019-04-09 2019-05-30 Ultra-thin atomic force microscope head WO2020206826A1 (en)

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