WO2019104769A1 - 一种防静电的印染助剂的制备方法 - Google Patents

一种防静电的印染助剂的制备方法 Download PDF

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WO2019104769A1
WO2019104769A1 PCT/CN2017/116885 CN2017116885W WO2019104769A1 WO 2019104769 A1 WO2019104769 A1 WO 2019104769A1 CN 2017116885 W CN2017116885 W CN 2017116885W WO 2019104769 A1 WO2019104769 A1 WO 2019104769A1
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water
preparing
printing
agent
ratio
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蒋宏
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蒋宏
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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/38—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using reactive dyes
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/46—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing natural macromolecular substances or derivatives thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/46—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing natural macromolecular substances or derivatives thereof
    • D06P1/48—Derivatives of carbohydrates
    • D06P1/50—Derivatives of cellulose
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/52—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing synthetic macromolecular substances
    • D06P1/5207—Macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/52—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing synthetic macromolecular substances
    • D06P1/5207—Macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • D06P1/525—Polymers of unsaturated carboxylic acids or functional derivatives thereof
    • D06P1/5257—(Meth)acrylic acid
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/52—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing synthetic macromolecular substances
    • D06P1/5264—Macromolecular compounds obtained otherwise than by reactions involving only unsaturated carbon-to-carbon bonds

Definitions

  • the invention belongs to the technical field of textile auxiliaries and fine chemicals, and in particular relates to a preparation method of an antistatic auxiliaries.
  • Printing and dyeing auxiliaries can improve the printing and dyeing effects.
  • the production and market development of China's dyes, auxiliaries and organic pigments industry has been healthy and rapid, and the consumption of dye chemicals has increased initially.
  • the rapid development of the textile industry has greatly increased the demand for dye textile chemicals.
  • the mutual support of the dye industry and the textile industry means that the Chinese dye industry has a huge market prospect.
  • the technical problem to be solved by the present invention is to provide a method for preparing an antistatic printing and dyeing auxiliary agent against the deficiencies of the prior art.
  • a method for preparing an antistatic printing and dyeing auxiliary comprises the following steps:
  • Stop heating add to the stainless steel container after cooling, then add the bactericidal anti-mold agent, then add the water in proportion, stir at 1000 rpm, and dissolve it all;
  • the ratio of the aqueous thickener, hydrotrope, emulsion mixture, filler and bactericidal anti-mold agent is 7:7:5:1:1 based on the total weight of the auxiliary.
  • the aqueous thickener comprises a mixture of a reactive dye in a ratio of 1:3 and a natural, semi-synthetic and synthetic water-soluble polymer; the mixture comprises water in a ratio of 1:1:3:2, Natural water soluble polymers, semi-synthetic water soluble polymers and synthetic water soluble polymers.
  • the hydrotrope comprises a reducing agent, a wetting agent, an emulsifier and a dispersing agent in a ratio of 1:2:3:1.
  • the emulsion mixture includes a film forming aid in a ratio of 1:2:2, a flame retardant, and a water-soluble conductive polyaniline solution.
  • the filler comprises polyoxyethylene diamine, ammonium persulfate, flaky mica powder, light calcium and talc in a ratio of 1:1:3:4:3:.
  • the natural water-soluble polymer is a dry matter of a natural gum or a derivative thereof, and the semi-synthetic water-soluble polymer is carboxymethylcellulose having a degree of substitution of 0.6 to 3.
  • the synthetic water-soluble The polymer is a polymerization product of an ethylenically unsaturated monomer.
  • the beneficial effects of the present invention are: by using a reactive dye, the chromatogram is wide, the color is bright, the performance is excellent, and the applicability is strong. By using the mixing of three different kinds of thickeners and adjusting the proportions appropriately, it is possible to adapt to the printing and printing state under different conditions. At the same time, the water-soluble conductive polyaniline solution is used as an antistatic filler, which can maintain the antistatic function after printing and dyeing.
  • a method for preparing an antistatic printing and dyeing auxiliary comprises the following steps:
  • Stop heating add to the stainless steel container after cooling, then add the bactericidal anti-mold agent, then add the water in proportion, stir at 1000 rpm, and dissolve it all;
  • the ratio of the aqueous thickener, hydrotrope, emulsion mixture, filler and bactericidal anti-mold agent is based on the total weight of the auxiliaries: 7:7:5:1:1.
  • the aqueous thickener comprises a mixture of reactive dyes in a ratio of 1:3 and natural, semi-synthetic and synthetic water-soluble polymers; the mixture comprises water in a ratio of 1:1:3:2, natural water-soluble polymers, semi-synthetic Water soluble polymers and synthetic water soluble polymers.
  • the hydrotrope includes a reducing agent, a wetting agent, an emulsifier and a dispersing agent in a ratio of 1:2:3:1.
  • the emulsion mixture includes a film forming aid in a ratio of 1:2:2, a flame retardant, and a water-soluble conductive polyaniline solution.
  • the filler includes polyoxyethylene diamine, ammonium persulfate, flaky mica powder, light calcium and talc in a ratio of 1:1:3:4:3:.
  • the natural water-soluble polymer is a dry matter of natural gum or a derivative thereof, the semi-synthetic water-soluble polymer is carboxymethyl cellulose having a degree of substitution of 0.6-3, and the synthetic water-soluble polymer is an ethylenically unsaturated monomer. Polymerization product.

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Molecular Biology (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Coloring (AREA)

Abstract

一种防静电的印染助剂的制备方法。包括以下步骤：添加水溶助长剂、水性增稠剂、杀菌防霉助剂，然后按比例加入水，使之全部溶解；将填料充分搅拌，再转入砂磨机中研磨，待分散均匀后过滤，添加乳液混合物，然后按比例加入水。所述印染助剂能够适应不同条件下的印花印染状态。同时以水溶性导电聚苯胺溶液为防静电填料，能够在印染之后保持防静电功能。

Description

一种防静电的印染助剂的制备方法 技术领域
本发明属于纺织助剂和精细化工技术领域，具体涉及一种防静电的印染助剂的制备方法。
背景技术
印染助剂能够提高印花和染色的效果。近年来，中国染料、助剂和有机颜料行业的生产与市场发展健康而迅速，染料化学品消费初步增长。纺织业的快速发展大大提高了对染料纺织化学品的需求，染料行业与纺织业的相互依托意味着中国染料行业有着巨大的市场前景。
尽管现有技术中已存在多种染色助剂，但其防静电功能仍然不够理想。
发明内容
本发明要解决的技术问题是，针对现有技术不足，提出一种防静电的印染助剂的制备方法。
本发明为解决上述技术问题提出的技术方案是：
一种防静电的印染助剂的制备方法，包括以下步骤：
1)制备第一组成分：在反应釜A中，添加还原剂、润湿剂、乳化剂和分散剂以及它们的混合物组成的水溶助长剂，升温至60℃，添加水性增稠剂，并搅拌，2小时；
停止加热，冷却后加入不锈钢容器中，然后加入杀菌防霉助剂，然后按比例加入水，以1000转/分搅拌，使之全部溶解；
2)制备第二组成分：将聚氧乙烯二胺、过硫酸铵、片状云母粉、轻钙和滑石粉组成的填料充分搅拌，再转入砂磨机中研磨，待分散均匀后过滤，添加成膜助剂、阻燃剂和水溶性导电聚苯胺溶液组成的乳液混合物，然后按比例加入水，以900转/分搅拌，使之全部溶解；
3)将所述第一组成分与所述第二组成分搅拌并充分混合。
本发明中，基于助剂的总重量，所述水性增稠剂、水溶助长剂、乳液混合物、填料和杀菌防霉助剂的比例是：7:7:5:1:1。
本发明中，所述水性增稠剂包括比例为1:3的活性染料和天然、半合成和合成的水溶性聚合物的混合物；所述混合物包括比例为1:1:3:2的水、天然水溶性聚合物、半合成水溶性聚合物和合成水溶性聚合物。
本发明中，所述水溶助长剂包括比例为1:2:3:1的还原剂、润湿剂、乳化剂和分散剂。
本发明中，所述乳液混合物包括比例为1:2:2的成膜助剂、阻燃剂和水溶性导电聚苯胺溶液。
本发明中，所述填料包括比例为:1:1:3:4:3:的聚氧乙烯二胺、过硫酸铵、片状云母粉、轻钙和滑石粉。
本发明中，所述天然水溶性聚合物为天然胶或其衍生物的干物质，所述半合成水溶性聚合物为取代度在0.6-3之间的羧甲基纤维素，所述合成水溶性聚合物为烯属不饱和单体的聚合产物。
本发明的有益效果在于：通过使用活性染料，色谱广、色泽鲜艳、性能优异、适用性强。通过使用三种不同种类的增稠剂的混合并适当调整比例，能够适应不同条件下的印花印染状态。同时以水溶性导电聚苯胺溶液为防静电填料，能够在印染之后保持防静电功能。
具体实施方式
下面通过具体的实施例对本发明进行详细说明，但这些例举性实施方式的用途和目的仅用来例举本发明，并非对本发明的实际保护范围构成任何形式的任何限定，更非将本发明的保护范围局限于此。
一种防静电的印染助剂的制备方法，包括以下步骤：
1)制备第一组成分：在反应釜A中，添加还原剂、润湿剂、乳化剂和分散剂以及它们的混合物组成的水溶助长剂，升温至60℃，添加水性增稠剂，并搅拌，2小时；
停止加热，冷却后加入不锈钢容器中，然后加入杀菌防霉助剂，然后按比例加入水，以1000转/分搅拌，使之全部溶解；
2)制备第二组成分：将聚氧乙烯二胺、过硫酸铵、片状云母粉、轻钙和滑石粉组成的填料充分搅拌，再转入砂磨机中研磨，待分散均匀后过滤，添加成膜助剂、阻燃剂和水溶性导电聚苯胺溶液组成的乳液混合物，然后按比例加入水，以900转/分搅拌，使之全部溶解；
3)将第一组成分与第二组成分搅拌并充分混合。
基于助剂的总重量，水性增稠剂、水溶助长剂、乳液混合物、填料和杀菌防霉助剂的比例是：7:7:5:1:1。
水性增稠剂包括比例为1:3的活性染料和天然、半合成和合成的水溶性聚合物的混合物；混合物包括比例为1:1:3:2的水、天然水溶性聚合物、半合成水溶性聚合物和合成水溶性聚合物。
水溶助长剂包括比例为1:2:3:1的还原剂、润湿剂、乳化剂和分散剂。
乳液混合物包括比例为1:2:2的成膜助剂、阻燃剂和水溶性导电聚苯胺溶液。
填料包括比例为:1:1:3:4:3:的聚氧乙烯二胺、过硫酸铵、片状云母粉、轻钙和滑石粉。
天然水溶性聚合物为天然胶或其衍生物的干物质，半合成水溶性聚合物为取代度在0.6-3之间的羧甲基纤维素，合成水溶性聚合物为烯属不饱和单体的聚合产物。
本发明不局限于上述实施例，凡采用等同替换形成的技术方案，均落在本发明的保护范围。

Claims (7)

  1. 一种防静电的印染助剂的制备方法，其特征在于包括以下步骤：
    1)制备第一组成分：在反应釜A中，添加还原剂、润湿剂、乳化剂和分散剂以及它们的混合物组成的水溶助长剂，升温至60℃，添加水性增稠剂，并搅拌，2小时；
    停止加热，冷却后加入不锈钢容器中，然后加入杀菌防霉助剂，然后按比例加入水，以1000转/分搅拌，使之全部溶解；
    2)制备第二组成分：将聚氧乙烯二胺、过硫酸铵、片状云母粉、轻钙和滑石粉组成的填料充分搅拌，再转入砂磨机中研磨，待分散均匀后过滤，添加成膜助剂、阻燃剂和水溶性导电聚苯胺溶液组成的乳液混合物，然后按比例加入水，以900转/分搅拌，使之全部溶解；
    3)将所述第一组成分与所述第二组成分搅拌并充分混合。
  2. 根据权利要求1所述一种防静电的印染助剂的制备方法，其特征在于：基于助剂的总重量，所述水性增稠剂、水溶助长剂、乳液混合物、填料和杀菌防霉助剂的比例是：7:7:5:1:1。
  3. 根据权利要求1和2所述一种防静电的印染助剂的制备方法，其特征在于：所述水性增稠剂包括比例为1:3的活性染料和天然、半合成和合成的水溶性聚合物的混合物；所述混合物包括比例为1:1:3:2的水、天然水溶性聚合物、半合成水溶性聚合物和合成水溶性聚合物。
  4. 根据权利要求1所述一种防静电的印染助剂的制备方法，其特征在于：所述水溶助长剂包括比例为1:2:3:1的还原剂、润湿剂、乳化剂和分散剂。
  5. 根据权利要求1所述一种防静电的印染助剂的制备方法，其特征在于：所述乳液混合物包括比例为1:2:2的成膜助剂、阻燃剂和水溶性导电聚苯胺溶液。
  6. 根据权利要求1所述一种防静电的印染助剂的制备方法，其特征在于：所述填料包括比例为:1:1:3:4:3:的聚氧乙烯二胺、过硫酸铵、片状云母粉、轻钙和滑石粉。
  7. 根据权利要求3所述一种防静电的印染助剂的制备方法，其特征在于：所述天然水溶性聚合物为天然胶或其衍生物的干物质，所述半合成水溶性聚合物为取代度在0.6-3之间的羧甲基纤维素，所述合成水溶性聚合物为烯属不饱和单体的聚合产物。
PCT/CN2017/116885 2017-11-29 2017-12-18 一种防静电的印染助剂的制备方法 WO2019104769A1 (zh)

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