WO2019071910A1 - Smoke generation product, preparation method therefor and use thereof - Google Patents

Smoke generation product, preparation method therefor and use thereof Download PDF

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Publication number
WO2019071910A1
WO2019071910A1 PCT/CN2018/078791 CN2018078791W WO2019071910A1 WO 2019071910 A1 WO2019071910 A1 WO 2019071910A1 CN 2018078791 W CN2018078791 W CN 2018078791W WO 2019071910 A1 WO2019071910 A1 WO 2019071910A1
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WIPO (PCT)
Prior art keywords
smoking article
tobacco
mixed
inorganic
water
Prior art date
Application number
PCT/CN2018/078791
Other languages
French (fr)
Chinese (zh)
Inventor
艾明欢
陈超英
杨菁
陆诚玮
赵文涛
Original Assignee
上海新型烟草制品研究院有限公司
上海烟草集团有限责任公司
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Application filed by 上海新型烟草制品研究院有限公司, 上海烟草集团有限责任公司 filed Critical 上海新型烟草制品研究院有限公司
Publication of WO2019071910A1 publication Critical patent/WO2019071910A1/en

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Classifications

    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/16Chemical features of tobacco products or tobacco substitutes of tobacco substitutes

Definitions

  • the invention belongs to the technical field of tobacco, and in particular relates to a smoking article, a preparation method thereof and use thereof.
  • the suction-heated non-combustible tobacco product includes tobacco cut tobacco, tobacco chips, tobacco particles, smoke, and the like as compared to conventional cigarettes.
  • the non-combustion type heating tobacco product is heated, the temperature of the tobacco portion is low, and only the tobacco is heated without burning the tobacco, so that the generation of tar can be greatly reduced or even avoided.
  • the consumer sucks and heats the non-combustion type of tobacco product, no flue gas is generated, and smoke that enters the environment is hardly generated, so-called "second-hand smoke", which greatly reduces environmental pollution.
  • Heating non-combustible tobacco products is being welcomed by some tobacco consumers because of its extremely low tar content and environmental friendliness, and is gradually being accepted by cigarette consumers in most countries.
  • Existing heated non-combustible tobacco products are mainly in the form of filaments, granules or powders.
  • ploom's heating non-burning smoking products are powder or granules, using aluminum can heating (Public No. 101951796A); Philip Morris Production Company's company's silk-like smoking products (Public No. 103841844A); Tobacco Particles of Tobacco LLC (Publication No. 102325472A).
  • These forms of heating tobacco products are not of an integrated construction and are therefore disadvantageous for being placed and removed from the heating non-combustion device.
  • these forms of heating tobacco products are prone to generate powders and granules after heating, causing contamination of the heating chamber of the non-combustion device, and even some fine dust is generated, which is disadvantageous for keeping the cavity clean.
  • the object of the present invention is to provide a smoking article, a preparation method and a use thereof, which can be used for heating non-combustion type cigarettes, and the smoking article is an integrated structure, and has high strength and convenience.
  • the insertion or removal of the heating non-combustion device overcomes the drawbacks of the prior art.
  • the present invention provides a smoking article comprising an inorganic binder, an inorganic adsorbent material, tobacco, an atomizing agent, water, and flavor.
  • the mass ratio of the inorganic binder, inorganic adsorbent material, tobacco, atomizing agent, water and flavor is (400 to 700): (100 to 400): (100 to 400): (400 to 1000) : (100 ⁇ 300): (1 ⁇ 30).
  • the mass ratio of the inorganic binder, the inorganic adsorbent material, the tobacco, the atomizing agent, the water and the flavor is (400 to 600): (200 to 400): (200 to 300): (600 to 900): (100 ⁇ 300): (1 ⁇ 30).
  • the inorganic binder is selected from one or more of kaolin, bentonite, and clay.
  • the inorganic adsorbent material is selected from one or more of diatomaceous earth, zeolite, alumina, silica, carbon, molecular sieve.
  • the inorganic binder and the inorganic adsorbent have a particle diameter of not more than 48 ⁇ m.
  • the tobacco is selected from one or more of flue-cured tobacco, oriental tobacco, burley tobacco, air-cured tobacco, and tobacco sheets.
  • the tobacco should have a particle size of not more than 250 ⁇ m.
  • the atomizing agent is selected from one or more of glycerol (glycerol), propylene glycol, butylene glycol, and butyl tributol.
  • the fragrance is selected from one or more of the edible natural flavor, the edible synthetic flavor, the natural flavor for tobacco, and the synthetic flavor for tobacco.
  • the edible natural flavor is selected from the group consisting of lemon oil, vanilla bean curd, Asian peppermint oil, cocoa butter, and geranium oil.
  • the edible synthetic fragrance is selected from the group consisting of vanillin, citral, menthol, ethyl butyrate, and linalool.
  • the natural flavor for tobacco is selected from the group consisting of clove bud oil, apple juice, Lai Baidang oil, fenugreek extract, and Peruvian balm.
  • the synthetic flavor for tobacco is selected from one of 2-acetylpyrazine, ethyl acetate, furanone, eugenol, and ethyl maltol.
  • the mass ratio of bentonite, diatomaceous earth, flue-cured tobacco, glycerin, water, flavor is (400-500): (300-400): (200 ⁇ 300): (600 ⁇ 800): (100 ⁇ 200): (10 ⁇ 30);
  • the mass ratio of kaolin, zeolite, oriental tobacco, glycerin, water, and flavor is (500 to 600): (200 to 300): (200 to 300): (700 to 900): (100 to 200): (10 ⁇ 30);
  • the mass ratio of clay, silica, flue-cured tobacco, glycerin, water, and flavor is (500-600): (200-400): (200-300): (700-900): (100-200) : (10 ⁇ 30).
  • the invention also discloses a preparation method of the smoking article as described above, which comprises uniformly mixing the raw material components according to the ratio, and then performing extrusion molding, cutting and drying to obtain a smoking article.
  • the mixing order of each raw material component is: first mixing the atomizing agent, water and flavor to obtain a mixed solution; then mixing the inorganic binder, the inorganic adsorbing material and the tobacco uniformly to obtain a mixed dry material; finally mixing A mixed solution is added to the dry material.
  • the extrusion molding is performed by a screw extruder, and the cross-sectional shape and cross-sectional area of the extruded smoking article are determined by a template matched with the extruder, and different templates can be selected as needed.
  • the smoking article can be cut to a certain size, preferably, the cutting length is 10 to 16 mm.
  • the drying treatment temperature is 100 to 150 ° C and the time is 10 min to 180 min. More preferably, the drying treatment is carried out at a temperature of from 105 to 130 ° C for a period of from 0.5 h to 1.5 h.
  • a third aspect of the invention also provides the use of the smoking article described above for heating a non-burning cigarette.
  • the integrated smoking article When the smoking article of the present invention is applied to heating non-combustion cigarettes, the integrated smoking article is placed in a heating non-combustion device, heated to 150-400 ° C and then suctioned.
  • the smoking article of the invention does not burn at the above heating temperature, and can enable the user to obtain a good suction feeling.
  • the temperature reaches 150 ° C, the smoke can be generated, and when the temperature exceeds 400 ° C, the harmful substances generated by the thermal cracking are large. Increase is not conducive to the health of consumers.
  • the smoking article of the invention is provided with an inorganic binder, so that the smoking article is integrally formed, and has sufficient bending strength, so that the consumer can easily put in or take out the smoking article from the heating non-combustion device;
  • the binder does not produce a taste under heating to 150 to 400 ° C and does not affect the flavor of tobacco and flavor.
  • the addition of water can make the bonding effect of the inorganic binder better, not only to effectively bond the inorganic binder, but also to prevent the surface of the smoking article from being too moist.
  • the inorganic adsorbing material added by the invention can adsorb the atomizing agent and moisture, improve the liquid adsorption amount of the smoking article, and does not generate odor at 150-400 ° C, and does not affect the flavor of tobacco and flavor, thereby ensuring Obtain sufficient smoke and tobacco aroma at 150-400 °C.
  • the inorganic binder and the inorganic adsorbing material it is convenient to control the proportion of the tobacco, so that the nicotine and the tobacco flavor are effectively regulated.
  • the smoking article prepared by the invention is an integrated structure after extrusion molding, and is applied to heating non-burning tobacco products, convenient to put in and take out the heating non-combustion device, and does not generate powder and particles, and is convenient for cleaning.
  • the inorganic binder since the inorganic binder is added, the strength of the integrated smoking article can be improved, and the intrinsic aroma of the tobacco can be prevented from being affected by the bad odor of the external bonding agent.
  • the inorganic adsorbing material can adsorb a large amount of the atomizing agent and the fragrance, a large amount of smoke and aroma substances can be generated to enhance the suction feeling of the consumer.
  • the smoking article of the invention has high strength, is not easy to be damaged in structure, can accurately control the tobacco content, and extracts aroma substances in the tobacco raw material by heat to release nicotine.
  • the method for preparing the integrated smoking article of the invention has simple molding process and is different from the traditional silk making process.
  • the tobacco used in the examples of the present invention has a particle diameter of not more than 250 ⁇ m.
  • the inorganic binder and the inorganic adsorbing material used have a particle diameter of not more than 48 ⁇ m.
  • the inorganic binder used is bentonite, and the particle diameter is not more than 48 ⁇ m.
  • the inorganic adsorbing material used is diatomaceous earth, and the particle diameter is not more than 48 ⁇ m.
  • the tobacco used is Yunnan flue-cured tobacco powder with a particle size of not more than 250 ⁇ m.
  • the atomizing agent is glycerol and the flavor is vanillin.
  • the mass ratio of bentonite, diatomaceous earth, flue-cured tobacco powder, glycerin, water, and vanillin is 400:400:100:1000:300:30.
  • the preparation method of the smoking article in the embodiment mixing glycerin, water and vanillin uniformly to obtain a mixed solution, and standby; mixing the bentonite, diatomaceous earth and Yunnan flue-cured tobacco powder uniformly to obtain a mixed dry material; The solution is added to the mixed dry material to obtain a mixed wet material. Then, a long rod-shaped smoking article having a diameter of 7 mm was extruded by a screw extruder and cut into a length of 16 mm. A long rod-shaped smoking article having a length of 16 mm and a diameter of 7 mm was dried, and the drying temperature was 150 ° C, and the drying time was 30 min to obtain an integrated smoking article.
  • the inorganic binder used is bentonite, and the particle diameter is not more than 48 ⁇ m.
  • the inorganic adsorbing material used is diatomaceous earth, and the particle diameter is not more than 48 ⁇ m.
  • the tobacco used is Yunnan flue-cured tobacco powder with a particle size of not more than 250 ⁇ m.
  • the atomizing agent is glycerol and the flavor is vanillin.
  • the mass ratio of bentonite, diatomaceous earth, flue-cured tobacco powder, glycerin, water, and vanillin is 400:400:100:600:300:30.
  • the preparation method of the smoking article in the embodiment mixing glycerin, water and vanillin uniformly to obtain a mixed solution, and standby; mixing the bentonite, diatomaceous earth and Yunnan flue-cured tobacco powder uniformly to obtain a mixed dry material; The solution is added to the mixed dry material to obtain a mixed wet material. Then, a long rod-shaped smoking article having a diameter of 7 mm was extruded by a screw extruder and cut into a length of 16 mm. A long rod-shaped smoking article having a length of 16 mm and a diameter of 7 mm was dried, and the drying temperature was 150 ° C, and the drying time was 30 min to obtain an integrated smoking article.
  • the inorganic binder used is bentonite, and the particle diameter is not more than 48 ⁇ m.
  • the inorganic adsorbing material used is diatomaceous earth, and the particle diameter is not more than 48 ⁇ m.
  • the tobacco used is Yunnan flue-cured tobacco powder with a particle size of not more than 250 ⁇ m.
  • the atomizing agent is glycerol and the flavor is cocoa.
  • the mass ratio of bentonite, diatomaceous earth, flue-cured tobacco powder, glycerin, water and cocoa is 500:300:200:800:200:10.
  • the preparation method of the smoking article in the embodiment mixing glycerin, water and cocoa glutinous uniformly to obtain a mixed solution for use; mixing the bentonite, diatomaceous earth and Yunnan flue-cured tobacco powder uniformly to obtain a mixed dry material; It is added to the mixed dry material to obtain a mixed wet material. Then, a long rod-shaped smoking article having a diameter of 7 mm was extruded by a screw extruder and cut into a length of 16 mm. A long rod-shaped smoking article having a length of 16 mm and a diameter of 7 mm was dried, and the drying temperature was 100 ° C, and the drying time was 3 hours to obtain an integrated smoking article.
  • the inorganic binder used is bentonite, and the particle diameter is not more than 48 ⁇ m.
  • the inorganic adsorbing material used is diatomaceous earth, and the particle diameter is not more than 48 ⁇ m.
  • the tobacco used is Yunnan flue-cured tobacco powder with a particle size of not more than 250 ⁇ m.
  • the atomizing agent is glycerol and the fragrance is 2-acetylpyrazine.
  • the mass ratio of bentonite, diatomaceous earth, flue-cured tobacco powder, glycerol, water, 2-acetylpyrazine is 600:350:300:700:150:20.
  • the preparation method of the smoking article in the embodiment mixing glycerin, water and 2-acetylpyrazine uniformly to obtain a mixed solution for use; mixing bentonite, diatomaceous earth and Yunnan flue-cured tobacco powder to obtain a mixed dry material.
  • the mixed solution is added to the mixed dry material to obtain a mixed wet material.
  • a long rod-shaped smoking article having a diameter of 7 mm was extruded by a screw extruder and cut into a length of 16 mm.
  • a long rod-shaped smoking article having a length of 16 mm and a diameter of 7 mm was dried, and the drying temperature was 120 ° C and the drying time was 90 min to obtain an integrated smoking article.
  • the inorganic binder used is kaolin, and the particle diameter is not more than 48 ⁇ m.
  • the inorganic adsorbing material used is zeolite, and the particle diameter is not more than 48 ⁇ m.
  • the tobacco used was Yunnan flue-cured tobacco powder and Hunan flue-cured tobacco powder (mass ratio 1:1), and the particle size was not more than 250 ⁇ m.
  • the atomizing agent is glycerol, and the essence is clove flower bud oil.
  • the mass ratio of kaolin, zeolite, flue-cured tobacco powder, glycerin, water, and clove flower bud oil is 500:300:200:900:200:30.
  • the preparation method of the smoking article in the embodiment mixing glycerin, water and clove flower bud oil uniformly to obtain a mixed solution for use; mixing kaolin, zeolite and flue-cured tobacco powder uniformly to obtain a mixed dry material; adding the mixed solution to In the mixed dry material, a mixed wet material is obtained. Then, a long rod-shaped smoking article having a diameter of 7 mm was extruded by a screw extruder and cut into a length of 16 mm. A long rod-shaped smoking article having a length of 16 mm and a diameter of 7 mm was dried, and the drying temperature was 150 ° C, and the drying time was 10 min to obtain an integrated smoking article.
  • the inorganic binder used is clay, and the particle diameter is not more than 48 ⁇ m.
  • the inorganic adsorbing material used is silica, and the particle diameter is not more than 48 ⁇ m.
  • the tobacco used is Hunan flue-cured tobacco powder with a particle size of not more than 250 ⁇ m.
  • the atomizing agent is glycerol and the flavor is vanillin.
  • the mass ratio of clay, silica, flue-cured tobacco, glycerin, water, and vanillin is 600:200:200:900:100:10.
  • the preparation method of the smoking article in the embodiment mixing glycerin, water and vanillin uniformly to obtain a mixed solution for use; mixing the clay, the silica and the flue-cured tobacco powder uniformly to obtain a mixed dry material; adding the mixed solution Into the mixed dry material, a mixed wet material is obtained. Then, a long rod-shaped smoking article having a diameter of 8 mm was extruded by a screw extruder and cut into a length of 10 mm. A long rod-shaped smoking article having a length of 10 mm and a diameter of 8 mm was dried, and the drying temperature was 130 ° C, and the drying time was 0.5 h to obtain an integrated smoking article.
  • the inorganic binder used is clay, and the particle diameter is not more than 48 ⁇ m.
  • the inorganic adsorbing material used is silica, and the particle diameter is not more than 48 ⁇ m.
  • the tobacco used was Yunnan flue-cured tobacco powder and Hunan flue-cured tobacco powder (mass ratio 1:2), and the particle size was not more than 250 ⁇ m.
  • the atomizing agent is glycerol and the essence is eugenol.
  • the mass ratio of clay, silica, flue-cured tobacco, glycerol, water, and eugenol is 500:400:300:700:200:30.
  • the preparation method of the smoking article in the embodiment mixing glycerin, water and eugenol to obtain a mixed solution for use; mixing clay, silica and flue-cured tobacco powder uniformly to obtain a mixed dry material; adding the mixed solution Into the mixed dry material, a mixed wet material is obtained. Then, a long rod-shaped smoking article having a diameter of 7 mm was extruded by a screw extruder and cut into a length of 16 mm. A long rod-shaped smoking article having a length of 16 mm and a diameter of 7 mm was dried, and the drying temperature was 105 ° C, and the drying time was 1 h to obtain an integrated smoking article.
  • the inorganic binder used is kaolin, and the particle diameter is not more than 48 ⁇ m.
  • the inorganic adsorbing material used is zeolite, and the particle diameter is not more than 48 ⁇ m.
  • the tobacco used was Shandong flue-cured tobacco powder and Hunan flue-cured tobacco powder (mass ratio 1:2), and the particle size was not more than 250 ⁇ m.
  • the atomizing agent is glycerol, and the flavor is vanilla bean meal.
  • the mass ratio of kaolin, zeolite, flue-cured tobacco powder, glycerol, water, and vanilla bean meal is 600:200:300:700:100:30.
  • the preparation method of the smoking article in the embodiment mixing glycerin, water and vanilla bean meal uniformly to obtain a mixed solution for use; mixing kaolin, zeolite and flue-cured tobacco powder uniformly to obtain a mixed dry material; adding the mixed solution Into the mixed dry material, a mixed wet material is obtained. Then, a long rod-shaped smoking article having a diameter of 5 mm was extruded by a screw extruder and cut into a length of 10 mm. A long rod-shaped smoking article having a length of 10 mm and a diameter of 5 mm was dried, and the drying temperature was 110 ° C, and the drying time was 1 h to obtain an integrated smoking article.
  • the inorganic binder used is kaolin, and the particle diameter is not more than 48 ⁇ m.
  • the inorganic adsorbing material used is diatomaceous earth, and the particle diameter is not more than 48 ⁇ m.
  • the tobacco used is oriental tobacco and has a particle size of not more than 250 ⁇ m.
  • the atomizing agent is glycerol and butylene glycol (mass ratio is 2:1), and the flavor is citral.
  • the mass ratio of kaolin, diatomaceous earth, oriental tobacco, atomizing agent, water, and citral is 700:100:400:800:200:1.
  • the preparation method of the smoking article in the embodiment mixing the atomizing agent, water and citral to obtain a mixed solution for use; mixing kaolin, diatomaceous earth and oriental tobacco to obtain a dry material; adding the mixed solution to the mixture; In the mixed dry material, a mixed wet material is obtained. Then, a long rod-shaped smoking article having a diameter of 5 mm was extruded by a screw extruder and cut into a length of 10 mm. A long rod-shaped smoking article having a length of 10 mm and a diameter of 5 mm was dried, and the drying temperature was 110 ° C, and the drying time was 1 h to obtain an integrated smoking article.
  • the inorganic binder used is kaolin, and the particle diameter is not more than 48 ⁇ m.
  • the inorganic adsorbent material used is carbon and has a particle diameter of not more than 48 ⁇ m.
  • the tobacco used is a sun-cured tobacco with a particle size of not more than 250 ⁇ m.
  • the atomizing agent is butyl triol, and the flavor is apple juice.
  • the mass ratio of kaolin, carbon, sun-cured tobacco, atomizing agent, water and apple juice is 400:400:300:1000:200:10.
  • the atomizing agent, the water and the apple juice are uniformly mixed to obtain a mixed solution for use; the kaolin, the carbon and the oriental tobacco are uniformly mixed to obtain a mixed dry material; and the mixed solution is added to the mixing.
  • a mixed wet material is obtained.
  • a long rod-shaped smoking article having a diameter of 5 mm was extruded by a screw extruder and cut into a length of 10 mm.
  • a long rod-shaped smoking article having a length of 10 mm and a diameter of 5 mm was dried, and the drying temperature was 100 ° C, and the drying time was 1 h to obtain an integrated smoking article.
  • the performances of the smoking articles prepared in the examples and the comparative examples were evaluated respectively, and the evaluation indexes included the flexural strength, the amount of smoke, the heating odor, the tobacco flavor, and the aroma amount.
  • the flexural strength is tested by a universal material testing machine by applying a stress from any radial direction of the center of the length of the smoking article to test the stress value of the smoking article when it is broken.
  • the amount of smoke, the smell of heating, the flavor of tobacco, and the amount of aroma were scored using a 5-point evaluation form.
  • the meanings of the scores of each indicator are shown in Table 1.
  • the evaluation group consisted of 9 people. After smoking the smoking products, the sensory quality of the smoking products was comprehensively scored.
  • Example 1 The smoking products prepared in Example 1 and the smoking articles prepared in Comparative Examples 1, 2, and 3 were respectively subjected to sensory quality evaluation and strength comparison. The results are shown in Table 2, and the scores of the evaluation indexes in Table 2 were respectively shown. The arithmetic average score for the effective rating of 9 reviewers.
  • the smoking article in the embodiment of the present invention uses an inorganic binder to ensure the molding strength of the integrated smoking article, and to ensure that the taste, smoke amount, and the like of the integrated smoking article are not affected.
  • Example 2 The smoking articles prepared in Example 2 were compared with the smoking articles prepared in Comparative Examples 4, 5, and 6, respectively, and the results are shown in Table 2.
  • Table 3 shows the sensory performance evaluation and strength evaluation of the integrated smoking articles prepared in Examples 3-10.
  • Example 3 43.7N 4.72 4.79 4.77 4.80
  • Example 4 41.3N 4.75 4.82 4.72 4.80
  • Example 5 45.0N 4.70 4.81 4.80 4.83
  • Example 6 47.1N 4.72 4.80 4.85 4.79
  • Example 7 48.7N 4.76 4.77 4.73 4.86
  • Example 8 39.9N 4.80 4.85 4.75 4.78
  • Example 9 40.1N 4.79 4.69 4.87 4.82
  • Example 10 49.4N 4.82 4.83 4.79 4.84

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture Of Tobacco Products (AREA)
  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)

Abstract

A smoke generation product, comprising an inorganic binder, an inorganic adsorbing material, tobacco, an atomizing agent, water and an essence. Further provided are a preparation method for the smoke generation product and use of same. The smoke generation product is an integrated structure after extrusion molding, has large bending strength, has a damage resistant structure, and is used for heating non-burning tobacco products, is convenient for a non-burning device to be inserted therein and removed therefrom, and does not produce powders and particles, and is easy to clean, could produce a large amount of smoke and aroma materials, improving the suction feeling for the consumer, and in the smoke generation product, the content of tobacco can be accurately controlled, and the aroma material in the tobacco raw material is extracted by means of heat to release nicotine. The preparation method has a simple molding process.

Description

一种发烟制品及其制备方法和用途Cigarette product, preparation method and use thereof 技术领域Technical field
本发明属于烟草技术领域,具体涉及一种发烟制品及其制备方法和用途。The invention belongs to the technical field of tobacco, and in particular relates to a smoking article, a preparation method thereof and use thereof.
背景技术Background technique
抽吸加热不燃烧型烟草制品与抽吸传统卷烟相比,两者抽吸的烟草均包括烟丝、烟草碎片、烟草颗粒、烟末等。但是,加热不燃烧型加热用烟草制品抽吸时烟草部位温度较低,仅加热烟草而不燃烧烟草,因而能够极大降低甚至避免焦油的产生。消费者抽吸加热不燃烧型烟草制品时不会产生测流烟气,且几乎不产生进入环境的烟气,即所谓的“二手烟”,大大降低了环境污染。加热不燃烧型烟草制品正因其焦油量极低和环境友好而受到部分烟草消费者的欢迎,正逐步被大多数国家的卷烟消费者所接受。The suction-heated non-combustible tobacco product includes tobacco cut tobacco, tobacco chips, tobacco particles, smoke, and the like as compared to conventional cigarettes. However, when the non-combustion type heating tobacco product is heated, the temperature of the tobacco portion is low, and only the tobacco is heated without burning the tobacco, so that the generation of tar can be greatly reduced or even avoided. When the consumer sucks and heats the non-combustion type of tobacco product, no flue gas is generated, and smoke that enters the environment is hardly generated, so-called "second-hand smoke", which greatly reduces environmental pollution. Heating non-combustible tobacco products is being welcomed by some tobacco consumers because of its extremely low tar content and environmental friendliness, and is gradually being accepted by cigarette consumers in most countries.
现有加热不燃烧烟草制品主要为丝片状、颗粒状或粉末状。如ploom公司的加热不燃烧发烟制品为粉末或颗粒状,使用铝罐加热方式(公开号101951796A);菲利普莫里斯生产公司的公司的丝片状发烟制品(公开号103841844A);美国无烟烟草有限责任公司的烟草颗粒(公开号102325472A)。这些形态的加热用烟草制品并不是一体化的构造,因此不利于从加热不燃烧装置中置入和取出。另外,这些形态的加热用烟草制品在加热使用后容易产生粉末和颗粒,造成加热不燃烧装置加热腔的污染,甚至会产生一些及其细小的粉尘,不利于保持腔体的清洁。Existing heated non-combustible tobacco products are mainly in the form of filaments, granules or powders. For example, ploom's heating non-burning smoking products are powder or granules, using aluminum can heating (Public No. 101951796A); Philip Morris Production Company's company's silk-like smoking products (Public No. 103841844A); Tobacco Particles of Tobacco LLC (Publication No. 102325472A). These forms of heating tobacco products are not of an integrated construction and are therefore disadvantageous for being placed and removed from the heating non-combustion device. In addition, these forms of heating tobacco products are prone to generate powders and granules after heating, causing contamination of the heating chamber of the non-combustion device, and even some fine dust is generated, which is disadvantageous for keeping the cavity clean.
发明内容Summary of the invention
鉴于以上所述现有技术的缺点,本发明的目的在于提供一种发烟制品及其制备方法和用途,可用于加热不燃烧型卷烟中,且发烟制品为一体化结构,强度大,便于置入或取出加热不燃烧装置中,克服现有技术中存在的缺陷。In view of the above-mentioned shortcomings of the prior art, the object of the present invention is to provide a smoking article, a preparation method and a use thereof, which can be used for heating non-combustion type cigarettes, and the smoking article is an integrated structure, and has high strength and convenience. The insertion or removal of the heating non-combustion device overcomes the drawbacks of the prior art.
为了实现上述目的或者其他目的,本发明是通过以下技术方案实现的。In order to achieve the above object or other objects, the present invention is achieved by the following technical solutions.
本发明提供了一种发烟制品,所述发烟制品包括无机粘结剂、无机吸附材料、烟草、雾化剂、水和香精。The present invention provides a smoking article comprising an inorganic binder, an inorganic adsorbent material, tobacco, an atomizing agent, water, and flavor.
优选地,所述无机粘结剂、无机吸附材料、烟草、雾化剂、水和香精的质量比为(400~700):(100~400):(100~400):(400~1000):(100~300):(1~30)。Preferably, the mass ratio of the inorganic binder, inorganic adsorbent material, tobacco, atomizing agent, water and flavor is (400 to 700): (100 to 400): (100 to 400): (400 to 1000) : (100 ~ 300): (1 ~ 30).
更优选地,无机粘结剂、无机吸附材料、烟草、雾化剂、水和香精的质量比为(400~600):(200~400):(200~300):(600~900):(100~300):(1~30)。More preferably, the mass ratio of the inorganic binder, the inorganic adsorbent material, the tobacco, the atomizing agent, the water and the flavor is (400 to 600): (200 to 400): (200 to 300): (600 to 900): (100~300): (1~30).
优选地,所述无机粘结剂选自高岭土、膨润土、黏土中的一种或多种。Preferably, the inorganic binder is selected from one or more of kaolin, bentonite, and clay.
优选地,所述无机吸附材料选自硅藻土、沸石、氧化铝、二氧化硅、碳素、分子筛中的 一种或多种。Preferably, the inorganic adsorbent material is selected from one or more of diatomaceous earth, zeolite, alumina, silica, carbon, molecular sieve.
更优选地,所述无机粘结剂和无机吸附材料的粒径均不大于48μm。More preferably, the inorganic binder and the inorganic adsorbent have a particle diameter of not more than 48 μm.
优选地,所述烟草选自烤烟、香料烟、白肋烟、晾晒烟、烟草薄片中的一种或多种。所述烟草的粒径应不大于250μm。Preferably, the tobacco is selected from one or more of flue-cured tobacco, oriental tobacco, burley tobacco, air-cured tobacco, and tobacco sheets. The tobacco should have a particle size of not more than 250 μm.
优选地,所述雾化剂选自丙三醇(甘油)、丙二醇、丁二醇、丁三醇中的一种或多种。Preferably, the atomizing agent is selected from one or more of glycerol (glycerol), propylene glycol, butylene glycol, and butyl tributol.
优选地,所述香精选自食用天然香料、食用合成香料、烟用天然香料、烟用合成香料中的一种或多种。所述食用天然香料选自柠檬油、香荚兰豆酊、亚洲薄荷油、可可酊、香叶油中的一种。所述食用合成香料选自香兰素、柠檬醛、薄荷脑、丁酸乙酯、芳樟醇中的一种。所述烟用天然香料选自丁香花蕾油、苹果汁、赖百当净油、葫芦巴提取物、秘鲁香膏中的一种。所述烟用合成香料选自2-乙酰基吡嗪、乙酸乙酯、呋喃酮、丁香酚、乙基麦芽酚中的一种。Preferably, the fragrance is selected from one or more of the edible natural flavor, the edible synthetic flavor, the natural flavor for tobacco, and the synthetic flavor for tobacco. The edible natural flavor is selected from the group consisting of lemon oil, vanilla bean curd, Asian peppermint oil, cocoa butter, and geranium oil. The edible synthetic fragrance is selected from the group consisting of vanillin, citral, menthol, ethyl butyrate, and linalool. The natural flavor for tobacco is selected from the group consisting of clove bud oil, apple juice, Lai Baidang oil, fenugreek extract, and Peruvian balm. The synthetic flavor for tobacco is selected from one of 2-acetylpyrazine, ethyl acetate, furanone, eugenol, and ethyl maltol.
更优选地,本发明所述发烟制品的原料成分中,膨润土、硅藻土、烤烟、丙三醇、水、香精的质量比为(400~500):(300~400):(200~300):(600~800):(100~200):(10~30);More preferably, in the raw material component of the smoking article of the present invention, the mass ratio of bentonite, diatomaceous earth, flue-cured tobacco, glycerin, water, flavor is (400-500): (300-400): (200~ 300): (600 ~ 800): (100 ~ 200): (10 ~ 30);
或,高岭土、沸石、香料烟、丙三醇、水、香精的质量比为(500~600):(200~300):(200~300):(700~900):(100~200):(10~30);Or, the mass ratio of kaolin, zeolite, oriental tobacco, glycerin, water, and flavor is (500 to 600): (200 to 300): (200 to 300): (700 to 900): (100 to 200): (10~30);
或,黏土、二氧化硅、烤烟、丙三醇、水、香精的质量比为(500~600):(200~400):(200~300):(700~900):(100~200):(10~30)。Or, the mass ratio of clay, silica, flue-cured tobacco, glycerin, water, and flavor is (500-600): (200-400): (200-300): (700-900): (100-200) : (10 ~ 30).
本发明还公开了如上述所述发烟制品的制备方法,将各原料组分按配比混合均匀后,进行挤压成型,切割,干燥处理后即得发烟制品。The invention also discloses a preparation method of the smoking article as described above, which comprises uniformly mixing the raw material components according to the ratio, and then performing extrusion molding, cutting and drying to obtain a smoking article.
优选地,各原料组分的混合顺序为,先将雾化剂、水和香精混合,得混合溶液;然后将无机粘结剂、无机吸附材料和烟草混合均匀,得混合干料;最后向混合干料中加入混合溶液。Preferably, the mixing order of each raw material component is: first mixing the atomizing agent, water and flavor to obtain a mixed solution; then mixing the inorganic binder, the inorganic adsorbing material and the tobacco uniformly to obtain a mixed dry material; finally mixing A mixed solution is added to the dry material.
优选地,挤压成型采用螺杆挤出机进行挤出,所挤出的发烟制品的截面形状和截面面积由挤出机配套的模板所决定,可按需选用不同的模板。挤出成型后,可将发烟制品切割成一定尺寸,优选地,切割长度为10~16mm。Preferably, the extrusion molding is performed by a screw extruder, and the cross-sectional shape and cross-sectional area of the extruded smoking article are determined by a template matched with the extruder, and different templates can be selected as needed. After extrusion molding, the smoking article can be cut to a certain size, preferably, the cutting length is 10 to 16 mm.
由于干燥处理的温度和时间会影响一体化发烟制品的抽吸品质,因此,本发明中优选地,干燥处理的温度为100~150℃,时间为10min~180min。更优选地,干燥处理的温度为105~130℃,时间为0.5h~1.5h。Since the temperature and time of the drying treatment affect the suction quality of the integrated smoking article, in the present invention, preferably, the drying treatment temperature is 100 to 150 ° C and the time is 10 min to 180 min. More preferably, the drying treatment is carried out at a temperature of from 105 to 130 ° C for a period of from 0.5 h to 1.5 h.
本发明第三方面还提供了上述所述发烟制品在加热不燃烧香烟中的用途。A third aspect of the invention also provides the use of the smoking article described above for heating a non-burning cigarette.
本发明的发烟制品应用于加热不燃烧卷烟中时,将一体化发烟制品置于加热不燃烧装置中,加热至150~400℃后抽吸。本发明的发烟制品在上述加热温度下不燃烧,且能够使使用 者获得良好的抽吸感受,当温度到达150℃,烟雾才能产生,而温度超过400℃,热裂解产生的有害物质会大量增加,不利于消费者的健康。When the smoking article of the present invention is applied to heating non-combustion cigarettes, the integrated smoking article is placed in a heating non-combustion device, heated to 150-400 ° C and then suctioned. The smoking article of the invention does not burn at the above heating temperature, and can enable the user to obtain a good suction feeling. When the temperature reaches 150 ° C, the smoke can be generated, and when the temperature exceeds 400 ° C, the harmful substances generated by the thermal cracking are large. Increase is not conducive to the health of consumers.
本发明的发烟制品,加入无机粘结剂,使得发烟制品一体化成型,且拥有足够的抗折强度,使消费者便于从加热不燃烧装置中放入或取出发烟制品;所述无机粘结剂在加热至150~400℃的条件下不产生味道,不会影响烟草和香精的香味。而水的加入,可使无机粘结剂的粘结效果更好,既能使无机粘结剂有效粘结,又避免发烟制品表面过于湿润。本发明所加入的无机吸附材料,可对雾化剂和水分进行吸附,提高发烟制品的液体吸附量,同时在150~400℃下也不产生气味,不影响烟草和香精的香味,从而保证在150~400℃下获得足够的烟雾和烟草香气。通过无机粘结剂和无机吸附材料的加入,便于控制烟草的比例,从而使烟碱和烟草本香得到有效调控。The smoking article of the invention is provided with an inorganic binder, so that the smoking article is integrally formed, and has sufficient bending strength, so that the consumer can easily put in or take out the smoking article from the heating non-combustion device; The binder does not produce a taste under heating to 150 to 400 ° C and does not affect the flavor of tobacco and flavor. The addition of water can make the bonding effect of the inorganic binder better, not only to effectively bond the inorganic binder, but also to prevent the surface of the smoking article from being too moist. The inorganic adsorbing material added by the invention can adsorb the atomizing agent and moisture, improve the liquid adsorption amount of the smoking article, and does not generate odor at 150-400 ° C, and does not affect the flavor of tobacco and flavor, thereby ensuring Obtain sufficient smoke and tobacco aroma at 150-400 °C. Through the addition of the inorganic binder and the inorganic adsorbing material, it is convenient to control the proportion of the tobacco, so that the nicotine and the tobacco flavor are effectively regulated.
本发明所制备的发烟制品,挤压成型后是一体化构造,应用于加热不燃烧烟草制品,方便置入和取出加热不燃烧装置,也不会产生粉末和颗粒,便于清洁。另外,由于添加了无机粘接剂,既可以提高一体化发烟制品的强度,又可以避免烟草本征香气受到外加粘接剂加热条件的不良气味影响。同时,由于无机吸附材料可以大量吸附雾化剂和香精,因此可以产生大量的烟雾和香气物质,提升消费者的抽吸感受。本发明的发烟制品的强度大,结构不易损坏,能精确控制烟草含量,利用热作用提取烟草原料中的香气物质,释放烟碱。本发明的一体化发烟制品制备方法成型工艺简单,有别于传统卷烟的制丝工艺。The smoking article prepared by the invention is an integrated structure after extrusion molding, and is applied to heating non-burning tobacco products, convenient to put in and take out the heating non-combustion device, and does not generate powder and particles, and is convenient for cleaning. In addition, since the inorganic binder is added, the strength of the integrated smoking article can be improved, and the intrinsic aroma of the tobacco can be prevented from being affected by the bad odor of the external bonding agent. At the same time, since the inorganic adsorbing material can adsorb a large amount of the atomizing agent and the fragrance, a large amount of smoke and aroma substances can be generated to enhance the suction feeling of the consumer. The smoking article of the invention has high strength, is not easy to be damaged in structure, can accurately control the tobacco content, and extracts aroma substances in the tobacco raw material by heat to release nicotine. The method for preparing the integrated smoking article of the invention has simple molding process and is different from the traditional silk making process.
具体实施方式Detailed ways
以下由特定的具体实施例说明本发明的实施方式,熟悉此技术的人士可由本说明书所揭露的内容轻易地了解本发明的其他优点及功效。The embodiments of the present invention are described below by way of specific embodiments, and those skilled in the art can readily understand other advantages and functions of the present invention from the disclosure.
在进一步描述本发明具体实施方式之前,应理解,本发明的保护范围不局限于下述特定的具体实施方案;还应当理解,本发明实施例中使用的术语是为了描述特定的具体实施方案,而不是为了限制本发明的保护范围。下列实施例中未注明具体条件的试验方法,通常按照常规条件,或者按照各制造商所建议的条件。Before the present invention is further described, it is to be understood that the scope of the present invention is not limited to the specific embodiments described below; It is not intended to limit the scope of the invention. The test methods which do not specify the specific conditions in the following examples are usually carried out according to conventional conditions or according to the conditions recommended by each manufacturer.
当实施例给出数值范围时,应理解,除非本发明另有说明,每个数值范围的两个端点以及两个端点之间任何一个数值均可选用。除非另外定义,本发明中使用的所有技术和科学术语与本技术领域技术人员通常理解的意义相同。除实施例中使用的具体方法、设备、材料外,根据本技术领域的技术人员对现有技术的掌握及本发明的记载,还可以使用与本发明实施例中所述的方法、设备、材料相似或等同的现有技术的任何方法、设备和材料来实现本发明。When the numerical values are given by the examples, it is to be understood that the two endpoints of each numerical range and any one of the two. Unless otherwise defined, all technical and scientific terms used in the present invention have the same meaning meaning In addition to the specific methods, devices, and materials used in the embodiments, the methods, devices, and materials described in the embodiments of the present invention may also be used according to the prior art and the description of the present invention by those skilled in the art. Any method, apparatus, and material of the prior art, similar or equivalent, is used to practice the invention.
本发明实施例中所采用的烟草的粒径不大于250μm。所采用的无机粘结剂和无机吸附材 料的粒径不大于48μm。The tobacco used in the examples of the present invention has a particle diameter of not more than 250 μm. The inorganic binder and the inorganic adsorbing material used have a particle diameter of not more than 48 μm.
实施例1Example 1
本实施例中,所采用的无机粘结剂为膨润土,粒径不大于48μm。所采用的无机吸附材料为硅藻土,粒径不大于48μm。所采用的烟草为云南烤烟烟粉,粒径不大于250μm。本实施例中,雾化剂为丙三醇,香精为香兰素。In the present embodiment, the inorganic binder used is bentonite, and the particle diameter is not more than 48 μm. The inorganic adsorbing material used is diatomaceous earth, and the particle diameter is not more than 48 μm. The tobacco used is Yunnan flue-cured tobacco powder with a particle size of not more than 250 μm. In this embodiment, the atomizing agent is glycerol and the flavor is vanillin.
膨润土、硅藻土、烤烟烟粉、丙三醇、水、香兰素的质量比为400:400:100:1000:300:30。The mass ratio of bentonite, diatomaceous earth, flue-cured tobacco powder, glycerin, water, and vanillin is 400:400:100:1000:300:30.
本实施例中发烟制品的制备方法:将丙三醇、水和香兰素混合均匀,得混合溶液,备用;将膨润土、硅藻土和云南烤烟烟粉混合均匀,得混合干料;将混合溶液加入到混合干料中,获得混合湿料。然后利用螺杆挤出机挤出直径为7mm的长棒状发烟制品,切割成长度为16mm。将长度为16mm,直径为7mm的长棒状发烟制品进行干燥,干燥温度为150℃,干燥时间30min,制得一体化发烟制品。The preparation method of the smoking article in the embodiment: mixing glycerin, water and vanillin uniformly to obtain a mixed solution, and standby; mixing the bentonite, diatomaceous earth and Yunnan flue-cured tobacco powder uniformly to obtain a mixed dry material; The solution is added to the mixed dry material to obtain a mixed wet material. Then, a long rod-shaped smoking article having a diameter of 7 mm was extruded by a screw extruder and cut into a length of 16 mm. A long rod-shaped smoking article having a length of 16 mm and a diameter of 7 mm was dried, and the drying temperature was 150 ° C, and the drying time was 30 min to obtain an integrated smoking article.
实施例2Example 2
本实施例中,所采用的无机粘结剂为膨润土,粒径不大于48μm。所采用的无机吸附材料为硅藻土,粒径不大于48μm。所采用的烟草为云南烤烟烟粉,粒径不大于250μm。本实施例中,雾化剂为丙三醇,香精为香兰素。In the present embodiment, the inorganic binder used is bentonite, and the particle diameter is not more than 48 μm. The inorganic adsorbing material used is diatomaceous earth, and the particle diameter is not more than 48 μm. The tobacco used is Yunnan flue-cured tobacco powder with a particle size of not more than 250 μm. In this embodiment, the atomizing agent is glycerol and the flavor is vanillin.
膨润土、硅藻土、烤烟烟粉、丙三醇、水、香兰素的质量比为400:400:100:600:300:30。The mass ratio of bentonite, diatomaceous earth, flue-cured tobacco powder, glycerin, water, and vanillin is 400:400:100:600:300:30.
本实施例中发烟制品的制备方法:将丙三醇、水和香兰素混合均匀,得混合溶液,备用;将膨润土、硅藻土和云南烤烟烟粉混合均匀,得混合干料;将混合溶液加入到混合干料中,获得混合湿料。然后利用螺杆挤出机挤出直径为7mm的长棒状发烟制品,切割成长度为16mm。将长度为16mm,直径为7mm的长棒状发烟制品进行干燥,干燥温度为150℃,干燥时间30min,制得一体化发烟制品。The preparation method of the smoking article in the embodiment: mixing glycerin, water and vanillin uniformly to obtain a mixed solution, and standby; mixing the bentonite, diatomaceous earth and Yunnan flue-cured tobacco powder uniformly to obtain a mixed dry material; The solution is added to the mixed dry material to obtain a mixed wet material. Then, a long rod-shaped smoking article having a diameter of 7 mm was extruded by a screw extruder and cut into a length of 16 mm. A long rod-shaped smoking article having a length of 16 mm and a diameter of 7 mm was dried, and the drying temperature was 150 ° C, and the drying time was 30 min to obtain an integrated smoking article.
实施例3Example 3
本实施例中,所采用的无机粘结剂为膨润土,粒径不大于48μm。所采用的无机吸附材料为硅藻土,粒径不大于48μm。所采用的烟草为云南烤烟烟粉,粒径不大于250μm。本实施例中,雾化剂为丙三醇,香精为可可酊。In the present embodiment, the inorganic binder used is bentonite, and the particle diameter is not more than 48 μm. The inorganic adsorbing material used is diatomaceous earth, and the particle diameter is not more than 48 μm. The tobacco used is Yunnan flue-cured tobacco powder with a particle size of not more than 250 μm. In this embodiment, the atomizing agent is glycerol and the flavor is cocoa.
膨润土、硅藻土、烤烟烟粉、丙三醇、水、可可酊的质量比为500:300:200:800:200:10。The mass ratio of bentonite, diatomaceous earth, flue-cured tobacco powder, glycerin, water and cocoa is 500:300:200:800:200:10.
本实施例中发烟制品的制备方法:将丙三醇、水和可可酊混合均匀,得混合溶液备用; 将膨润土、硅藻土和云南烤烟烟粉混合均匀,得混合干料;将混合溶液加入到混合干料中,获得混合湿料。然后利用螺杆挤出机挤出直径为7mm的长棒状发烟制品,切割成长度为16mm。将长度为16mm,直径为7mm的长棒状发烟制品进行干燥,干燥温度为100℃,干燥时间3h,制得一体化发烟制品。The preparation method of the smoking article in the embodiment: mixing glycerin, water and cocoa glutinous uniformly to obtain a mixed solution for use; mixing the bentonite, diatomaceous earth and Yunnan flue-cured tobacco powder uniformly to obtain a mixed dry material; It is added to the mixed dry material to obtain a mixed wet material. Then, a long rod-shaped smoking article having a diameter of 7 mm was extruded by a screw extruder and cut into a length of 16 mm. A long rod-shaped smoking article having a length of 16 mm and a diameter of 7 mm was dried, and the drying temperature was 100 ° C, and the drying time was 3 hours to obtain an integrated smoking article.
实施例4Example 4
本实施例中,所采用的无机粘结剂为膨润土,粒径不大于48μm。所采用的无机吸附材料为硅藻土,粒径不大于48μm。所采用的烟草为云南烤烟烟粉,粒径不大于250μm。本实施例中,雾化剂为丙三醇,香精为2-乙酰基吡嗪。In the present embodiment, the inorganic binder used is bentonite, and the particle diameter is not more than 48 μm. The inorganic adsorbing material used is diatomaceous earth, and the particle diameter is not more than 48 μm. The tobacco used is Yunnan flue-cured tobacco powder with a particle size of not more than 250 μm. In this embodiment, the atomizing agent is glycerol and the fragrance is 2-acetylpyrazine.
膨润土、硅藻土、烤烟烟粉、丙三醇、水、2-乙酰基吡嗪的质量比为600:350:300:700:150:20。The mass ratio of bentonite, diatomaceous earth, flue-cured tobacco powder, glycerol, water, 2-acetylpyrazine is 600:350:300:700:150:20.
本实施例中发烟制品的制备方法:将丙三醇、水和2-乙酰基吡嗪混合均匀,得混合溶液备用;将膨润土、硅藻土和云南烤烟烟粉混合均匀,得混合干料;将混合溶液加入到混合干料中,获得混合湿料。然后利用螺杆挤出机挤出直径为7mm的长棒状发烟制品,切割成长度为16mm。将长度为16mm,直径为7mm的长棒状发烟制品进行干燥,干燥温度为120℃,干燥时间90min,制得一体化发烟制品。The preparation method of the smoking article in the embodiment: mixing glycerin, water and 2-acetylpyrazine uniformly to obtain a mixed solution for use; mixing bentonite, diatomaceous earth and Yunnan flue-cured tobacco powder to obtain a mixed dry material. The mixed solution is added to the mixed dry material to obtain a mixed wet material. Then, a long rod-shaped smoking article having a diameter of 7 mm was extruded by a screw extruder and cut into a length of 16 mm. A long rod-shaped smoking article having a length of 16 mm and a diameter of 7 mm was dried, and the drying temperature was 120 ° C and the drying time was 90 min to obtain an integrated smoking article.
实施例5Example 5
本实施例中,所采用的无机粘结剂为高岭土,粒径不大于48μm。所采用的无机吸附材料为沸石,粒径不大于48μm。所采用的烟草为云南烤烟烟粉和湖南烤烟烟粉(质量比1:1),粒径不大于250μm。本实施例中,雾化剂为丙三醇,香精为丁香花蕾油。In the present embodiment, the inorganic binder used is kaolin, and the particle diameter is not more than 48 μm. The inorganic adsorbing material used is zeolite, and the particle diameter is not more than 48 μm. The tobacco used was Yunnan flue-cured tobacco powder and Hunan flue-cured tobacco powder (mass ratio 1:1), and the particle size was not more than 250 μm. In this embodiment, the atomizing agent is glycerol, and the essence is clove flower bud oil.
高岭土、沸石、烤烟烟粉、丙三醇、水、丁香花蕾油的质量比为500:300:200:900:200:30。The mass ratio of kaolin, zeolite, flue-cured tobacco powder, glycerin, water, and clove flower bud oil is 500:300:200:900:200:30.
本实施例中发烟制品的制备方法:将丙三醇、水和丁香花蕾油混合均匀,得混合溶液备用;将高岭土、沸石和烤烟烟粉混合均匀,得混合干料;将混合溶液加入到混合干料中,获得混合湿料。然后利用螺杆挤出机挤出直径为7mm的长棒状发烟制品,切割成长度为16mm。将长度为16mm,直径为7mm的长棒状发烟制品进行干燥,干燥温度为150℃,干燥时间10min,制得一体化发烟制品。The preparation method of the smoking article in the embodiment: mixing glycerin, water and clove flower bud oil uniformly to obtain a mixed solution for use; mixing kaolin, zeolite and flue-cured tobacco powder uniformly to obtain a mixed dry material; adding the mixed solution to In the mixed dry material, a mixed wet material is obtained. Then, a long rod-shaped smoking article having a diameter of 7 mm was extruded by a screw extruder and cut into a length of 16 mm. A long rod-shaped smoking article having a length of 16 mm and a diameter of 7 mm was dried, and the drying temperature was 150 ° C, and the drying time was 10 min to obtain an integrated smoking article.
实施例6Example 6
本实施例中,所采用的无机粘结剂为黏土,粒径不大于48μm。所采用的无机吸附材料为二氧化硅,粒径不大于48μm。所采用的烟草为湖南烤烟烟粉,粒径不大于250μm。本实施例中,雾化剂为丙三醇,香精为香兰素。In this embodiment, the inorganic binder used is clay, and the particle diameter is not more than 48 μm. The inorganic adsorbing material used is silica, and the particle diameter is not more than 48 μm. The tobacco used is Hunan flue-cured tobacco powder with a particle size of not more than 250 μm. In this embodiment, the atomizing agent is glycerol and the flavor is vanillin.
黏土、二氧化硅、烤烟烟粉、丙三醇、水、香兰素的质量比为600:200:200:900:100:10。The mass ratio of clay, silica, flue-cured tobacco, glycerin, water, and vanillin is 600:200:200:900:100:10.
本实施例中发烟制品的制备方法:将丙三醇、水和香兰素混合均匀,得混合溶液备用;将黏土、二氧化硅和烤烟烟粉混合均匀,得混合干料;将混合溶液加入到混合干料中,获得混合湿料。然后利用螺杆挤出机挤出直径为8mm的长棒状发烟制品,切割成长度为10mm。将长度为10mm,直径为8mm的长棒状发烟制品进行干燥,干燥温度为130℃,干燥时间0.5h,制得一体化发烟制品。The preparation method of the smoking article in the embodiment: mixing glycerin, water and vanillin uniformly to obtain a mixed solution for use; mixing the clay, the silica and the flue-cured tobacco powder uniformly to obtain a mixed dry material; adding the mixed solution Into the mixed dry material, a mixed wet material is obtained. Then, a long rod-shaped smoking article having a diameter of 8 mm was extruded by a screw extruder and cut into a length of 10 mm. A long rod-shaped smoking article having a length of 10 mm and a diameter of 8 mm was dried, and the drying temperature was 130 ° C, and the drying time was 0.5 h to obtain an integrated smoking article.
实施例7Example 7
本实施例中,所采用的无机粘结剂为黏土,粒径不大于48μm。所采用的无机吸附材料为二氧化硅,粒径不大于48μm。所采用的烟草为云南烤烟烟粉和湖南烤烟烟粉(质量比1:2),粒径不大于250μm。本实施例中,雾化剂为丙三醇,香精为丁香酚。In this embodiment, the inorganic binder used is clay, and the particle diameter is not more than 48 μm. The inorganic adsorbing material used is silica, and the particle diameter is not more than 48 μm. The tobacco used was Yunnan flue-cured tobacco powder and Hunan flue-cured tobacco powder (mass ratio 1:2), and the particle size was not more than 250 μm. In this embodiment, the atomizing agent is glycerol and the essence is eugenol.
黏土、二氧化硅、烤烟烟粉、丙三醇、水、丁香酚的质量比为500:400:300:700:200:30。The mass ratio of clay, silica, flue-cured tobacco, glycerol, water, and eugenol is 500:400:300:700:200:30.
本实施例中发烟制品的制备方法:将丙三醇、水和丁香酚混合均匀,得混合溶液备用;将黏土、二氧化硅和烤烟烟粉混合均匀,得混合干料;将混合溶液加入到混合干料中,获得混合湿料。然后利用螺杆挤出机挤出直径为7mm的长棒状发烟制品,切割成长度为16mm。将长度为16mm,直径为7mm的长棒状发烟制品进行干燥,干燥温度为105℃,干燥时间1h,制得一体化发烟制品。The preparation method of the smoking article in the embodiment: mixing glycerin, water and eugenol to obtain a mixed solution for use; mixing clay, silica and flue-cured tobacco powder uniformly to obtain a mixed dry material; adding the mixed solution Into the mixed dry material, a mixed wet material is obtained. Then, a long rod-shaped smoking article having a diameter of 7 mm was extruded by a screw extruder and cut into a length of 16 mm. A long rod-shaped smoking article having a length of 16 mm and a diameter of 7 mm was dried, and the drying temperature was 105 ° C, and the drying time was 1 h to obtain an integrated smoking article.
实施例8Example 8
本实施例中,所采用的无机粘结剂为高岭土,粒径不大于48μm。所采用的无机吸附材料为沸石,粒径不大于48μm。所采用的烟草为山东烤烟烟粉和湖南烤烟烟粉(质量比1:2),粒径不大于250μm。本实施例中,雾化剂为丙三醇,香精为香荚兰豆酊。In the present embodiment, the inorganic binder used is kaolin, and the particle diameter is not more than 48 μm. The inorganic adsorbing material used is zeolite, and the particle diameter is not more than 48 μm. The tobacco used was Shandong flue-cured tobacco powder and Hunan flue-cured tobacco powder (mass ratio 1:2), and the particle size was not more than 250 μm. In this embodiment, the atomizing agent is glycerol, and the flavor is vanilla bean meal.
高岭土、沸石、烤烟烟粉、丙三醇、水、香荚兰豆酊的质量比为600:200:300:700:100:30。The mass ratio of kaolin, zeolite, flue-cured tobacco powder, glycerol, water, and vanilla bean meal is 600:200:300:700:100:30.
本实施例中发烟制品的制备方法:将丙三醇、水和香荚兰豆酊混合均匀,得混合溶液备用;将高岭土、沸石和烤烟烟粉混合均匀,得混合干料;将混合溶液加入到混合干料中,获得混合湿料。然后利用螺杆挤出机挤出直径为5mm的长棒状发烟制品,切割成长度为10mm。将长度为10mm,直径为5mm的长棒状发烟制品进行干燥,干燥温度为110℃,干燥时间1h,制得一体化发烟制品。The preparation method of the smoking article in the embodiment: mixing glycerin, water and vanilla bean meal uniformly to obtain a mixed solution for use; mixing kaolin, zeolite and flue-cured tobacco powder uniformly to obtain a mixed dry material; adding the mixed solution Into the mixed dry material, a mixed wet material is obtained. Then, a long rod-shaped smoking article having a diameter of 5 mm was extruded by a screw extruder and cut into a length of 10 mm. A long rod-shaped smoking article having a length of 10 mm and a diameter of 5 mm was dried, and the drying temperature was 110 ° C, and the drying time was 1 h to obtain an integrated smoking article.
实施例9Example 9
本实施例中,所采用的无机粘结剂为高岭土,粒径不大于48μm。所采用的无机吸附材料为硅藻土,粒径不大于48μm。所采用的烟草为香料烟,粒径不大于250μm。本实施例中,雾化剂为丙三醇和丁二醇(质量比为2:1),香精为柠檬醛。In the present embodiment, the inorganic binder used is kaolin, and the particle diameter is not more than 48 μm. The inorganic adsorbing material used is diatomaceous earth, and the particle diameter is not more than 48 μm. The tobacco used is oriental tobacco and has a particle size of not more than 250 μm. In this embodiment, the atomizing agent is glycerol and butylene glycol (mass ratio is 2:1), and the flavor is citral.
高岭土、硅藻土、香料烟、雾化剂、水、柠檬醛的质量比为700:100:400:800:200:1。The mass ratio of kaolin, diatomaceous earth, oriental tobacco, atomizing agent, water, and citral is 700:100:400:800:200:1.
本实施例中发烟制品的制备方法:将雾化剂、水和柠檬醛混合均匀,得混合溶液备用;将高岭土、硅藻土和香料烟混合均匀,得混合干料;将混合溶液加入到混合干料中,获得混合湿料。然后利用螺杆挤出机挤出直径为5mm的长棒状发烟制品,切割成长度为10mm。将长度为10mm,直径为5mm的长棒状发烟制品进行干燥,干燥温度为110℃,干燥时间1h,制得一体化发烟制品。The preparation method of the smoking article in the embodiment: mixing the atomizing agent, water and citral to obtain a mixed solution for use; mixing kaolin, diatomaceous earth and oriental tobacco to obtain a dry material; adding the mixed solution to the mixture; In the mixed dry material, a mixed wet material is obtained. Then, a long rod-shaped smoking article having a diameter of 5 mm was extruded by a screw extruder and cut into a length of 10 mm. A long rod-shaped smoking article having a length of 10 mm and a diameter of 5 mm was dried, and the drying temperature was 110 ° C, and the drying time was 1 h to obtain an integrated smoking article.
实施例10Example 10
本实施例中,所采用的无机粘结剂为高岭土,粒径不大于48μm。所采用的无机吸附材料为碳素,粒径不大于48μm。所采用的烟草为晒晾烟,粒径不大于250μm。本实施例中,雾化剂为丁三醇,香精为苹果汁。In the present embodiment, the inorganic binder used is kaolin, and the particle diameter is not more than 48 μm. The inorganic adsorbent material used is carbon and has a particle diameter of not more than 48 μm. The tobacco used is a sun-cured tobacco with a particle size of not more than 250 μm. In this embodiment, the atomizing agent is butyl triol, and the flavor is apple juice.
高岭土、碳素、晒晾烟、雾化剂、水、苹果汁的质量比为400:400:300:1000:200:10。The mass ratio of kaolin, carbon, sun-cured tobacco, atomizing agent, water and apple juice is 400:400:300:1000:200:10.
本实施例中发烟制品的制备方法:将雾化剂、水和苹果汁混合均匀,得混合溶液备用;将高岭土、碳素和香料烟混合均匀,得混合干料;将混合溶液加入到混合干料中,获得混合湿料。然后利用螺杆挤出机挤出直径为5mm的长棒状发烟制品,切割成长度为10mm。将长度为10mm,直径为5mm的长棒状发烟制品进行干燥,干燥温度为100℃,干燥时间1h,制得一体化发烟制品。In the method for preparing the smoking article in the embodiment, the atomizing agent, the water and the apple juice are uniformly mixed to obtain a mixed solution for use; the kaolin, the carbon and the oriental tobacco are uniformly mixed to obtain a mixed dry material; and the mixed solution is added to the mixing. In the dry material, a mixed wet material is obtained. Then, a long rod-shaped smoking article having a diameter of 5 mm was extruded by a screw extruder and cut into a length of 10 mm. A long rod-shaped smoking article having a length of 10 mm and a diameter of 5 mm was dried, and the drying temperature was 100 ° C, and the drying time was 1 h to obtain an integrated smoking article.
对比例1Comparative example 1
搅拌混合1000g丙三醇、300g水和30g香兰素均匀后作为混合溶液待用,搅拌混合400g硅藻土和100g云南烤烟烟粉形成混合干料,将混合溶液倒入混合干料中获得混合湿料。用螺杆挤出机挤出直径7mm的长棒状发烟制品,然后将发烟制品长度切割为16mm。最后对长16mm,直径7mm的发烟制品进行干燥,干燥温度150℃,干燥时间30min。制得一体化发烟制品A1。Mix 1000g of glycerin, 300g of water and 30g of vanillin to be mixed and used as a mixed solution for use. Mix 400g of diatomaceous earth and 100g of Yunnan flue-cured tobacco powder to form a mixed dry material, and pour the mixed solution into the mixed dry material to obtain a mixture. Wet material. A long rod-shaped smoking article having a diameter of 7 mm was extruded by a screw extruder, and then the length of the smoking article was cut to 16 mm. Finally, the smoking article having a length of 16 mm and a diameter of 7 mm was dried, and the drying temperature was 150 ° C and the drying time was 30 min. An integrated smoking article A1 is produced.
对比例2Comparative example 2
搅拌混合1000g丙三醇、300g水和30g香兰素均匀后作为混合溶液待用,搅拌混合400g瓜尔豆胶、400g硅藻土和100g云南烤烟烟粉形成混合干料,将混合溶液倒入混合干料中获 得混合湿料。用螺杆挤出机挤出直径7mm的长棒状发烟制品,然后将发烟制品长度切割为16mm。最后对长16mm,直径7mm的发烟制品进行干燥,干燥温度150℃,干燥时间30min。制得一体化发烟制品A2。Mix 1000g of glycerin, 300g of water and 30g of vanillin to be mixed and used as a mixed solution. Mix 400g of guar gum, 400g of diatomaceous earth and 100g of Yunnan flue-cured tobacco to form a mixed dry material. Pour the mixed solution into the mixture. A mixed wet material is obtained in the mixed dry material. A long rod-shaped smoking article having a diameter of 7 mm was extruded by a screw extruder, and then the length of the smoking article was cut to 16 mm. Finally, the smoking article having a length of 16 mm and a diameter of 7 mm was dried, and the drying temperature was 150 ° C and the drying time was 30 min. An integrated smoking article A2 is produced.
对比例3Comparative example 3
搅拌混合1000g丙三醇、300g水和30g香兰素均匀后作为混合溶液待用,搅拌混合40g黄原胶、400g硅藻土和100g云南烤烟烟粉形成混合干料,将混合溶液倒入混合干料中获得混合湿料。用螺杆挤出机挤出直径7mm的长棒状发烟制品,然后将发烟制品长度切割为16mm。最后对长16mm,直径7mm的发烟制品进行干燥,干燥温度150℃,干燥时间30min。制得一体化发烟制品A3。Mix 1000g of glycerin, 300g of water and 30g of vanillin to be mixed and used as a mixed solution for use. Mix 40g of xanthan gum, 400g of diatomaceous earth and 100g of Yunnan flue-cured tobacco powder to form a mixed dry material, and pour the mixed solution into the mixture. A mixed wet material is obtained in the dry material. A long rod-shaped smoking article having a diameter of 7 mm was extruded by a screw extruder, and then the length of the smoking article was cut to 16 mm. Finally, the smoking article having a length of 16 mm and a diameter of 7 mm was dried, and the drying temperature was 150 ° C and the drying time was 30 min. An integrated smoking article A3 is produced.
对比例4Comparative example 4
搅拌混合600g丙三醇、300g水和30g香兰素均匀后作为混合溶液待用,搅拌混合400g膨润土和100g云南烤烟烟粉形成混合干料,将混合溶液倒入混合干料中获得混合湿料。用螺杆挤出机挤出直径7mm的长棒状发烟制品,然后将发烟制品长度切割为16mm。最后对长16mm,直径7mm的发烟制品进行干燥,干燥温度150℃,干燥时间30min。制得一体化发烟制品B1。600 g of glycerin, 300 g of water and 30 g of vanillin were mixed and mixed uniformly as a mixed solution, and 400 g of bentonite and 100 g of Yunnan flue-cured tobacco powder were mixed and mixed to form a mixed dry material, and the mixed solution was poured into the mixed dry material to obtain a mixed wet material. . A long rod-shaped smoking article having a diameter of 7 mm was extruded by a screw extruder, and then the length of the smoking article was cut to 16 mm. Finally, the smoking article having a length of 16 mm and a diameter of 7 mm was dried, and the drying temperature was 150 ° C and the drying time was 30 min. An integrated smoking article B1 is produced.
对比例5Comparative example 5
搅拌混合600g丙三醇、300g水和30g香兰素均匀后作为混合溶液待用,搅拌混合400g膨润土、400g木粉和100g云南烤烟烟粉形成混合干料,将混合溶液倒入混合干料中获得混合湿料。用螺杆挤出机挤出直径7mm的长棒状发烟制品,然后将发烟制品长度切割为16mm。最后对长16mm,直径7mm的发烟制品进行干燥,干燥温度150℃,干燥时间30min。制得一体化发烟制品B2。600 g of glycerin, 300 g of water and 30 g of vanillin were mixed and mixed as a mixed solution, and 400 g of bentonite, 400 g of wood powder and 100 g of Yunnan flue-cured tobacco powder were mixed and mixed to form a mixed dry material, and the mixed solution was poured into the mixed dry material. A mixed wet material is obtained. A long rod-shaped smoking article having a diameter of 7 mm was extruded by a screw extruder, and then the length of the smoking article was cut to 16 mm. Finally, the smoking article having a length of 16 mm and a diameter of 7 mm was dried, and the drying temperature was 150 ° C and the drying time was 30 min. The integrated smoking article B2 is obtained.
对比例6Comparative example 6
搅拌混合600g丙三醇、300g水和30g香兰素均匀后作为混合溶液待用,搅拌混合400g膨润土、100g淀粉和100g云南烤烟烟粉形成混合干料,将混合溶液倒入混合干料中获得混合湿料。用螺杆挤出机挤出直径7mm的长棒状发烟制品,然后将发烟制品长度切割为16mm。最后对长16mm,直径7mm的发烟制品进行干燥,干燥温度150℃,干燥时间30min。制得一体化发烟制品B3。600 g of glycerin, 300 g of water and 30 g of vanillin were mixed and mixed uniformly as a mixed solution, and 400 g of bentonite, 100 g of starch and 100 g of Yunnan flue-cured tobacco powder were mixed and mixed to form a mixed dry material, and the mixed solution was poured into the mixed dry material. Mix wet materials. A long rod-shaped smoking article having a diameter of 7 mm was extruded by a screw extruder, and then the length of the smoking article was cut to 16 mm. Finally, the smoking article having a length of 16 mm and a diameter of 7 mm was dried, and the drying temperature was 150 ° C and the drying time was 30 min. An integrated smoking article B3 is produced.
性能试验Performance test
分别对实施例及对比例中制得的发烟制品进行性能评价,评价指标包括抗折强度、发烟量、加热气味、烟草本香、香气量。The performances of the smoking articles prepared in the examples and the comparative examples were evaluated respectively, and the evaluation indexes included the flexural strength, the amount of smoke, the heating odor, the tobacco flavor, and the aroma amount.
抗折强度是采用万能材料试验机进行测试,具体方法为:从发烟制品长度中心位置的任意径向施加应力,测试发烟制品折断时的应力值。The flexural strength is tested by a universal material testing machine by applying a stress from any radial direction of the center of the length of the smoking article to test the stress value of the smoking article when it is broken.
发烟量、加热气味、烟草本香、香气量采用5分制评价表进行打分,各指标打分值含义见表1。评吸组由9人组成,分别抽吸发烟制品后,对发烟制品的感官质量进行综合评分。The amount of smoke, the smell of heating, the flavor of tobacco, and the amount of aroma were scored using a 5-point evaluation form. The meanings of the scores of each indicator are shown in Table 1. The evaluation group consisted of 9 people. After smoking the smoking products, the sensory quality of the smoking products was comprehensively scored.
表1一体化发烟制品感官质量评价指标分值含义表Table 1 Table of meanings of sensory quality evaluation indicators for integrated smoking products
Figure PCTCN2018078791-appb-000001
Figure PCTCN2018078791-appb-000001
分别将实施例1制得的发烟制品与对比例1、2、3所制得的发烟制品进行感官质量评价及强度对比,结果如表2所示,表2中各项评价指标的评分为9位评吸员有效评分的算术平均分。The smoking products prepared in Example 1 and the smoking articles prepared in Comparative Examples 1, 2, and 3 were respectively subjected to sensory quality evaluation and strength comparison. The results are shown in Table 2, and the scores of the evaluation indexes in Table 2 were respectively shown. The arithmetic average score for the effective rating of 9 reviewers.
表2一体化发烟制品性能对比情况表Table 2 Performance comparison of integrated smoking products
项目project 抗折强度Flexural strength 发烟量(200℃)Smoke (200 ° C) 加热气味(200℃)Heating odor (200 ° C) 香气量Aroma amount 烟草本香Tobacco
实施例1Example 1 50.3N50.3N 4.674.67 4.894.89 4.754.75 4.794.79
对比例1Comparative example 1 1.2N1.2N 4.324.32 4.754.75 4.124.12 4.104.10
对比例2Comparative example 2 30.7N30.7N 4.014.01 1.501.50 3.763.76 4.214.21
对比例3Comparative example 3 10.9N10.9N 4.304.30 2.672.67 4.214.21 4.134.13
由表1可知,本发明实施例中的发烟制品选用无机粘接剂,既能保证一体化发烟制品成型强度,又能确保一体化发烟制品的味道、发烟量等不受影响。It can be seen from Table 1 that the smoking article in the embodiment of the present invention uses an inorganic binder to ensure the molding strength of the integrated smoking article, and to ensure that the taste, smoke amount, and the like of the integrated smoking article are not affected.
分别将实施例2制得的发烟制品与对比例4、5、6所制得的发烟制品进行对比,结果如表2所示。The smoking articles prepared in Example 2 were compared with the smoking articles prepared in Comparative Examples 4, 5, and 6, respectively, and the results are shown in Table 2.
表2一体化发烟制品性能对比情况表Table 2 Performance comparison of integrated smoking products
项目project 抗折强度Flexural strength 发烟量(200℃)Smoke (200 ° C) 加热气味(200℃)Heating odor (200 ° C) 香气量Aroma amount 烟草本香Tobacco
实施例2Example 2 55.8N55.8N 4.724.72 4.794.79 4.774.77 4.804.80
对比例4Comparative example 4 40.2N40.2N 4.254.25 4.824.82 4.124.12 4.104.10
对比例5Comparative example 5 3.3N3.3N 4.104.10 2.652.65 3.763.76 4.214.21
对比例6Comparative example 6 42.1N42.1N 4.324.32 2.572.57 4.214.21 4.134.13
由表2可知,本发明实施例的发烟制品选用无机吸附材料既能保证一体化发烟制品发烟量,又能确保一体化发烟制品的味道不受影响。It can be seen from Table 2 that the use of the inorganic adsorbing material in the smoking article of the embodiment of the present invention can ensure the smoke amount of the integrated smoking article and ensure the taste of the integrated smoking article is not affected.
表3为实施例3-10制得的一体化发烟制品的感官性能评价及强度评价。Table 3 shows the sensory performance evaluation and strength evaluation of the integrated smoking articles prepared in Examples 3-10.
表3实施例3-10的一体化发烟制品性能情况Table 3 Performance of the integrated smoking articles of Examples 3-10
项目project 强度strength 发烟量(200℃)Smoke (200 ° C) 加热气味(200℃)Heating odor (200 ° C) 香气量Aroma amount 烟草本香Tobacco
实施例3Example 3 43.7N43.7N 4.724.72 4.794.79 4.774.77 4.804.80
实施例4Example 4 41.3N41.3N 4.754.75 4.824.82 4.724.72 4.804.80
实施例5Example 5 45.0N45.0N 4.704.70 4.814.81 4.804.80 4.834.83
实施例6Example 6 47.1N47.1N 4.724.72 4.804.80 4.854.85 4.794.79
实施例7Example 7 48.7N48.7N 4.764.76 4.774.77 4.734.73 4.864.86
实施例8Example 8 39.9N39.9N 4.804.80 4.854.85 4.754.75 4.784.78
实施例9Example 9 40.1N40.1N 4.794.79 4.694.69 4.874.87 4.824.82
实施例10Example 10 49.4N49.4N 4.824.82 4.834.83 4.794.79 4.844.84
上述实施例仅例示性说明本发明的原理及其功效,而非用于限制本发明。任何熟悉此技术的人士皆可在不违背本发明的精神及范畴下,对上述实施例进行修饰或改变。因此,举凡所属技术领域中具有通常知识者在未脱离本发明所揭示的精神与技术思想下所完成的一切等效修饰或改变,仍应由本发明的权利要求所涵盖。The above-described embodiments are merely illustrative of the principles of the invention and its effects, and are not intended to limit the invention. Modifications or variations of the above-described embodiments may be made by those skilled in the art without departing from the spirit and scope of the invention. Therefore, all equivalent modifications or changes made by those skilled in the art without departing from the spirit and scope of the invention are still to be covered by the appended claims.

Claims (10)

  1. 一种发烟制品,其特征在于,所述发烟制品包括无机粘结剂、无机吸附材料、烟草、雾化剂、水和香精。A smoking article, characterized in that the smoking article comprises an inorganic binder, an inorganic adsorbent material, tobacco, an atomizing agent, water and a fragrance.
  2. 如权利要求1所述的发烟制品,其特征在于,所述无机粘结剂、无机吸附材料、烟草、雾化剂、水和香精的质量比为(400~700):(100~400):(100~400):(400~1000):(100~300):(1~30)。The smoking article according to claim 1, wherein the mass ratio of said inorganic binder, inorganic adsorbent material, tobacco, atomizing agent, water and flavor is (400 to 700): (100 to 400) : (100 to 400): (400 to 1000): (100 to 300): (1 to 30).
  3. 如权利要求1所述的发烟制品,其特征在于,所述无机粘结剂选自高岭土、膨润土、黏土中的一种或多种。The smoking article according to claim 1, wherein the inorganic binder is one or more selected from the group consisting of kaolin, bentonite, and clay.
  4. 如权利要求1所述的发烟制品,其特征在于,所述无机吸附材料选自硅藻土、沸石、氧化铝、二氧化硅、碳素和分子筛中的一种或多种。A smoking article according to claim 1 wherein said inorganic adsorbent material is selected from the group consisting of diatomaceous earth, zeolite, alumina, silica, carbon and molecular sieves.
  5. 如权利要求1所述的发烟制品,其特征在于,所述烟草选自烤烟、香料烟、白肋烟、晾晒烟、烟草薄片中的一种或多种。The smoking article of claim 1 wherein said tobacco is selected from the group consisting of flue-cured tobacco, oriental tobacco, burley tobacco, air-cured tobacco, and tobacco flakes.
  6. 如权利要求1所述的发烟制品,其特征在于,所述雾化剂选自丙三醇、丙二醇、丁二醇、丁三醇中的一种或多种。The smoking article according to claim 1, wherein the atomizing agent is one or more selected from the group consisting of glycerol, propylene glycol, butylene glycol, and butyl triol.
  7. 一种如权利要求1至6任一项所述发烟制品的制备方法,将各原料组分按配比混合均匀后,进行挤压成型,切割,干燥处理后即得发烟制品。A method for preparing a smoking article according to any one of claims 1 to 6, wherein each of the raw material components is uniformly mixed according to a ratio, and then extruded, cut, and dried to obtain a smoking article.
  8. 如权利要求7所述的制备方法,其特征在于,各原料组分的混合顺序为,先将雾化剂、水和香精混合,得混合溶液;然后将无机粘结剂、无机吸附材料和烟草混合均匀,得混合干料;最后向混合干料中加入混合溶液。The preparation method according to claim 7, wherein the mixing order of the raw material components is such that the atomizing agent, water and flavor are first mixed to obtain a mixed solution; then the inorganic binder, the inorganic adsorbent material and the tobacco are added. The mixture is uniformly mixed to obtain a dry material; finally, the mixed solution is added to the mixed dry material.
  9. 如权利要求7所述的制备方法,其特征在于,干燥处理的温度为100~150℃,时间为10min~180min。The production method according to claim 7, wherein the drying treatment is carried out at a temperature of from 100 to 150 ° C for a period of from 10 min to 180 min.
  10. 一种如权利要求1至6任一项所述发烟制品在加热不燃烧香烟中的用途。Use of a smoking article according to any one of claims 1 to 6 in heating a non-burning cigarette.
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