WO2019045483A2 - Cosmetic composition comprising centella asiatica extract or triterpene derived therefrom in high content and method for producing same - Google Patents

Abstract

The present invention relates to a cosmetic composition containing high content of a Centella asiatica extract or Centella asiatica selec. triterpene, which is a poorly soluble plant extract ingredient. More specifically, the present invention relates to an oil-in-water cosmetic composition containing high content of a Centella asiatica extract and/or Centella asiatica selec. triterpene and in a stable manner, by dispersing a Centella asiatica extract and/or Centella asiatica selec. triterpene at a high temperature together with certain polymer polyols to prepare a water phase comprising a Centella asiatica extract and/or a triterpene, upon preparation of the water phase.

Description

A cosmetic composition comprising a centilla extract or a triterpene derived therefrom in a high content and a process for producing the same

Cross reference of related application

The present application claims priority to Korean Patent Application No. 10-2017-0111339 (filed on August 31, 2017) and Korean Patent Application No. 10-2018-0099138 (filed on August 24, 2018) The two above-mentioned applications are incorporated herein by reference in their entirety.

The present invention relates to a cosmetic composition containing a large amount of Centella asiatica selec. Triterpene, which is a poorly soluble plant extract component, or Centella asiatica selec. Triterpene derived from centella asiatica extract. More particularly, (O / W) which can contain tritaper in a high amount and stably in a high concentration and can stably contain Triticum annuum extract-derived tritaper, by dispersing triterpenes with specific polymer polyols at a high temperature, To a cosmetic composition.

The Centella asiatica selec. Triterpene, which is a plant extract component or Centella asiatica selec. Triterpene derived from it, has excellent functions such as anti-inflammation, soothing, antibacterial, scar relaxation, promotion of collagen production and whitening effect. .

However, tritaperpenes derived from the centilla sp. Extract are generally poorly soluble in water and have low solubility in oil. Therefore, it is difficult to uniformly disperse in cosmetics, especially in oil-in-water cosmetics, There is a great restriction on the use of a high content due to precipitation by the skin,

As a method of blending tritaper with an extract of Kukushuko extract from an existing water-in-oil type cosmetic formulation, 1) a method of finely triturating the Tentairpen derived from Kukushuka extract with a smaller and uniform powder using a pulverizer or the like, and then adding to the formulation WO 2008/058755), 2) a method of dissolving with an amine-based pH adjusting agent at a higher pH (10 or higher) and / or dispersing in a solvent such as ethanol (Patent No. 10-0795512, -0024932), and 3) a method in which an excess amount of a PEG surfactant is dispersed (WO97 / 39734). However, these methods have the following drawbacks: 1) high mass production of cosmetics necessitates the use of an external grinder separately, resulting in poor temporal and spatial efficiency, high raw material loss rate during the grinding process, A formulation having a pH of at least 10 or a formulation containing an excess of ethanol using a system pH adjuster is difficult to use as a cosmetic to be applied to the skin due to severe skin irritation and has a legal problem; and 3) by using a PEG surfactant There is a problem in that customers are reluctant to use due to inhibition of formulation safety.

Due to these problems, most cosmetic products on the market have a limitation that they can not provide sufficient functionality to customers by adding only a small amount of tritaper in the extracts of Kunchuk extract. In addition, a high-cost, low-efficiency process is applied to produce a large amount of tritaper It is necessary to be improved because it is likely to cause problems such as increase of cost and decrease of productivity to producers and problems of skin irritation and safety in use.

The present invention relates to a method for stabilizing a large amount of centella ash extract or a triterpene derived therefrom in an aquatic-type cosmetic formulation, comprising the steps of subjecting to an additional pulverizing step in the manufacturing process or adding an excessive amount of stimulating substance such as ethanol, PEG surfactant, There is provided a method for producing a cosmetic composition containing a centistallophylla extract or tallpox extract-derived tritanthrene in a high content and stably without using any formulations and the like, and to provide an underwater-type cosmetic composition prepared by such a method Purpose .

On the other hand, by minimizing or not using the amount of toxic chemicals in the cosmetic production process, it is possible to guarantee the health of workers in the production line, and also to easily and rapidly mass-concentrate the extracts of chimpanzee or triterpene derived therefrom And a method for producing a cosmetic composition of the present invention.

On the other hand, by minimizing the amount and / or residual amount of some harmful chemicals used for stabilizing triterpenes derived from Centella asiatica or Centella asiatica extracts from the cosmetic preparation process and final cosmetic products, And to provide a cosmetic composition which relieves anxiety of consumers about harmful chemical substances while enhancing the functionality of the cosmetic composition and enhances safety and cosmetic satisfaction of products.

In order to achieve the above object, the present invention provides an underwater type cosmetic composition comprising an aqueous phase and an oil phase, wherein 0.05 to 2.0% by weight of a centistallophylla extract or tritaper Thereby providing a cosmetic composition.

The present invention relates to a cosmetic composition and / or a cosmetic composition containing at least one of C ₃ -C ₆ trihydric alcohols, C ₂ -C ₅ divalent alcohols and C ₆ -C ₁₀ Lt; RTI ID = 0.0 > alcohol. ≪ / RTI > More particularly, the present invention is C ₃ as the active ingredient for in the production of in-water type cosmetic composition and / or cosmetics containing high Centella asiatica Urban extract, or Centella asiatica Urban extract derived triterpene, can stabilize the Centella asiatica Urban extract, or Centella asiatica Urban extract derived triterpene the upper A mixture of a trivalent alcohol of -C ₆ , a _divalent alcohol of C ₂ -C _{5 and} a divalent alcohol of C ₆ -C ₁₀ .

Further, according to the present invention,

1) 0.05 to 2.0% by weight of tentapenes derived from Centaurea extract or Centella asiatica extract from Centella asiatica extracts, and 5 to 37.5% by weight of C ₃ -C ₆ trihydric alcohols are mixed at a temperature of 75 ° C or more to prepare a first mixture step;

2) adding to the first mixture 5 to 37.5% by weight of divalent alcohol of C ₂ -C ₅ , based on the total weight of the composition, followed by mixing at a temperature of 75 ° C or higher to prepare a second mixture;

3) adding to the second mixture from 0.25 to 3.25% by weight of divalent C ₆ -C ₁₀ alcohol based on the total weight of the composition, followed by mixing at a temperature of 85 ° C or less to prepare a third mixture; And

4) preparing a water-in-oil cosmetic composition composition comprising an aqueous-type cosmetic composition comprising a third mixture, more precisely, a method for stabilizing a tricerpene from a centipede extract or a centipede extract from a top portion thereof.

The cosmetic composition according to the present invention can provide a high content and stable content of the centilla extract or tricterpene derived from the centilla spp. Extract, without giving any stimulation to the skin, And it is possible to provide satisfaction and relief by solving the anxiety of consumers about toxic chemicals in cosmetics. In addition, the manufacturing method according to the present invention is characterized in that, unlike cosmetic formulations utilizing tricorder, derived from Centella asiatica extract and / or Centella asiatica extract, the extracts of Centella asiatica And can stably provide an underwater type cosmetic composition.

1: A photograph showing a time-dependent foreign object sensation (a: Example 2; b: Comparative Example 4) of an embodiment (a) and a comparative example (below; b) according to the present invention.

2: Comparative Example 1 (Fig. 2 (b): Comparative Example 2; Fig. 2 (c): Comparative Example 3) Scale unit: 10 mu m).

3 (a), 3 (b) and 3 (c) show comparative examples 3 and 4, respectively. FIG. 3 is a photograph showing the dispersion state of the compositions of the examples and comparative examples according to the present invention, : Example 1; Fig. 3b: Example 2; Fig. 3c: Example 3) (unit of scale: 10 占 퐉).

Unless otherwise defined, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. In general, the nomenclature used herein is well known and commonly used in the art.

Hereinafter, the present invention will be described in more detail.

As used herein, the term " about " used to describe volume, time (period), concentration, volume (content, etc.), area, temperature, etc. has a tolerance of up to 10%, typically 5% It means that it exists.

Unless otherwise indicated, the units "% " used to denote the concentration of a particular substance throughout this specification are percentages by weight of solids / solids (weight / weight) And the liquid / liquid is (volume / volume)%.

An aspect of the present invention relates to a cosmetic composition which stably contains a high amount of centella as an extract or tritaeniorhana extract derived from centipede.

More particularly, the present invention relates to an underwater-type cosmetic composition comprising a water-in-oil and an oil-in-water composition, wherein a high content of centilla sp.

In the present invention, "stably containing a high amount of centistallium extract or centrilobular extract derived from centistocellular extract" means that the centistallium extract or centrilobular extract derived from centistocellular extract is used in an amount of 0.05 to 2.0% by weight, based on the total weight of the composition constituting the cosmetic composition, By weight, preferably from 0.5% by weight to 2.0% by weight, more preferably from 1% by weight to 2.0% by weight, with precipitation of at least 6 months, preferably at least 12 months, more preferably at least 18 months, It means that the problem such as discoloration does not occur.

The centilla extracts used in the present invention may be prepared by a general method known in the art, or commercially available ones may be used.

Unless otherwise defined herein, Tritterpen derived from Centaurea tumefaciens extract means a triterpene obtained by isolating and / or purifying from a Centaurea or Centella asiatica extract, and may be manufactured using conventional extraction methods or commercially available .

In the present invention, T. terpenes derived from Centaurea or Centella asiatica extracts are used in conventional cosmetics in the form of an alcoholic solvent (e.g., ethanol), an amine-based pH adjusting agent (e.g., ethanolamine (For example, sorbitan isostearate (SORBITAN ISOSTEARATE)), a PEG-based surfactant (e.g., PEG-100 stearate, PEG 40 stearate and the like), other harmful surfactants BEHENETH-based surfactants such as BEHENETH-5, BEHENETH-10, BEHENETH-20 and BEHENETH-25 and steareth surfactants such as Steareth-2 and Steareth- -20, Steareth-21, Steareth-25, Steareth-27, Steareth-30, Steareth-40, Steareth-50, Steareth-80, Steareth-100, Steareth-200), the PEG surfactant and / Without moisturizers or thickeners containing surfactants, Type cosmetic composition.

In the water-in-oil type cosmetic composition according to the present invention, the water phase can be used by mixing three kinds of polyhydric alcohol components in order to stabilize T. terpenes derived from Centella asiatica or Centella asiatica (composition total weight):

a. From 5.0 to 37.5% by weight, preferably from 10 to 35% by weight, more preferably from 10 to 30% by weight and most preferably from 10 to 25% by weight of a C ₃ -C ₆ trivalent alcohol;

b. From 5.0 to 37.5% by weight, preferably from 10 to 35% by weight, more preferably from 10 to 30% by weight, most preferably from 10 to 25% by weight, of a C ₂ -C ₅ divalent alcohol; And

c. 0.25 to 3.25% by weight, preferably 0.5 to 3.0% by weight, more preferably 1.0 to 2.5% by weight, most preferably 1.0 to 2.0% by weight of a C ₆ -C ₁₀ divalent alcohol.

In the present invention, the C ₃ -C ₆ trihydric alcohol as the a component is preferably glycerin. When the C ₃ -C ₆ tricarboxylic alcohol is less than 5.0 wt%, the centilla annulus extract or Triticum annulare extract-derived tritaper can not be sufficiently dispersed in the water, and when it is more than 37.5 wt%, it becomes too sticky, The attractiveness as a product is low. In addition, the emulsifying agent dispersed in the water does not act sufficiently to lower the stability of emulsification, and excessive surfactant or emulsion stabilizer should be used in the oil phase, thereby reducing skin safety.

In the present invention, the divalent alcohol of C ₂ -C ₅ as the component b is preferably butylene glycol or propanediol. When the C ₂ -C ₅ divalent alcohol is less than 5.0% by weight, the centilla annulus extract or the trita flower extract derived from the centistallos extract can not be sufficiently dispersed in the water, and when it is more than 37.5% by weight, The attractiveness as a product is low. In addition, the emulsifying agent dispersed in the water does not act sufficiently to lower the stability of emulsification, and excessive surfactant or emulsion stabilizer should be used in the oil phase, thereby reducing skin safety.

In the present invention, as the c component, the C ₆ -C ₁₀ divalent alcohol is preferably hexanediol. When the C ₆ -C ₁₀ divalent alcohol is less than 0.25% by weight, the centilla annulus extract or tritaeniorhana extract derived from the centistalles extract can not be sufficiently dispersed in the water, and when it exceeds 3.25% by weight, skin irritation may be caused, There is a risk that the viscosity of the emulsion is lowered by lowering the viscosity.

In the present invention, the three polyhydric alcohol components may be mixed in a mixing ratio of a: b: c = 20 to 11: 20 to 11: 1, preferably 14 to 12: 41 to 12: 1, In the present invention, the water phase part does not contain an alcoholic solvent such as ethanol, an amine-based pH adjusting agent such as ethanolamine for stabilizing T. terpenes derived from Centaurea or Centella asiatica.

In the water-in-oil type cosmetic composition according to the present invention, the water-pervious portion contains 78 wt% to 90 wt%, preferably 80.5 wt% to 88.5 wt%, more preferably 83.0 wt% To 88.0% by weight.

The oily portion of the cosmetic composition for underwater type according to the present invention can be prepared by appropriately selecting and adjusting the ingredients and the content used in a typical underwater type cosmetic formulation.

In the present invention, the oily phase does not contain a PEG surfactant in order to stabilize T. terpenes derived from Centaurea or Centella asiatica.

In the submerged cosmetic composition according to the present invention, the oily portion may be from 8 wt% to 15 wt%, preferably from 11.5 wt% to 14.5 wt%, more preferably from 12.0 wt% to 13.0 wt% based on the total weight of the composition have.

The water-in-oil type cosmetic composition according to the present invention may further contain fragrance, plant extract, natural preservative and the like in a range of about 10.0% by weight or less.

According to another aspect of the present invention, the present invention provides a method for stabilizing a centilla extract or a centilla extract derived from a centilla sp. Extract in an underwater type cosmetic composition,

1) 0.05 to 2.0% by weight tritaperbene derived from Centaal incipienta extract and 5 to 37.5% by weight of C ₃ -C ₆ trihydric alcohol based on the total weight of the composition are premixed at a temperature of at least about 75 캜 to prepare a first mixture step;

2) adding to the first mixture 5 to 37.5% by weight of a divalent alcohol of C ₂ -C ₅ , based on the total weight of the composition, followed by secondary mixing at a temperature of at least about 75 ° C to produce a second mixture;

3) adding to the second mixture from 0.25 to 3.25% by weight of divalent C ₆ -C ₁₀ alcohol based on the total weight of the composition, followed by tertiary mixing at a temperature of about 85 ° C or less to produce a third mixture; And

4) adding a residual amount of water to the third mixture, and mixing the fourth mixture to prepare a water phase of an underwater type cosmetic composition.

In the above method, the first mixing step is performed for at least 1 minute, preferably from 2 minutes to 30 minutes, the second mixing step is at least 1 minute, preferably from 2 minutes to 30 minutes, the tertiary mixing step is at least one minute, Preferably 2 to 10 minutes, and the fourth mixing step is preferably carried out for 1 minute or more, preferably 2 to 10 minutes.

When the water-in-oil type cosmetic composition containing T. terpenes derived from Centella asiatica or Centella asiatica extract is produced by the above method according to the present invention, the composition is stable for a long period of time, preferably for 6 months or more, have. On the other hand, if the mixing step of the method according to the present invention is not followed, precipitation of tritaeniornephrine extract or Triticum pertussis derived from the centipede extract in the composition occurs within a short period of time, for example, 1 to 2 days after the preparation of the cosmetic composition, .

The composition of the present invention can provide excellent antiinflammation, soothing, antibacterial, scar relaxation, stimulation of collagen production, and whitening effect by containing a centistallophylla extract or a centistrophene extract derived from a centistocellular extract.

The water-in-oil type cosmetic composition of the present invention can be prepared into a suitable formulation as desired. For example, skin lotion, skin softener, skin toner, astringent, lotion, milky lotion, moisturizing lotion, nutrition lotion, massage cream, nutritional cream, moisturizing cream, hand cream, foundation, essence, nutrition essence, pack, soap, cleansing But the present invention is not limited thereto, and may be manufactured by any one or more formulations selected from the group consisting of a foam, a cleansing lotion, a cleansing cream, a body lotion and a body cleanser.

When the formulation of the composition of the present invention is a paste, a cream or a gel, an animal fiber, a plant fiber, a wax, a paraffin, a starch, a tracer, a cellulose derivative, polyethylene glycol, silicon, bentonite, silica, talc, Can be used.

When the formulation of the composition of the present invention is a solution or an emulsion, a solvent, a solvent or an emulsifier is used as a carrier component, and examples thereof include water, isopropanol, ethyl carbonate, ethyl acetate, benzyl alcohol, benzyl benzoate, propylene glycol, , 3-butyl glycol oil, glycerol aliphatic ester, polyethylene glycol or sorbitan fatty acid esters.

The composition of the present invention may further include components included in functional additives and common cosmetic compositions, in addition to centistallium extracts or tritaeniorhana extracts derived from centipedes extracts. The functional additives may include water-soluble vitamins, oil-soluble vitamins, polymer peptides, polymeric polysaccharides, sphingolipids and seaweed extracts.

The composition of the present invention may further contain, in addition to the above-described functional additive, components contained in a general cosmetic composition as required. Examples of the other ingredients that can be included in the composition include humectants, emollients, surfactants, organic and inorganic pigments, organic powders, ultraviolet absorbents, preservatives, bactericides, antioxidants, plant extracts, pH adjusters, alcohols, Accelerators, coolants, antiperspirants, purified water, and the like.

Hereinafter, the constitution and effects of the present invention will be described in more detail with reference to examples and test examples. However, these examples and test examples are provided for illustrative purposes only in order to facilitate understanding of the present invention, and the scope and scope of the present invention are not limited by the following examples.

[Preparation Example 1] Preparation of an underwater type cosmetic composition of Examples 1 to 3

An underwater-type cosmetic composition (Examples 1 to 3) according to the present invention having the components and contents shown in the following Table 1 was prepared according to the following manufacturing process:

I. Manufacturing

(1) Centella asiatica Urban extract, or Centella asiatica Urban extract derived triterpene the upper preparative reactor (Asia Tycho side (ASIATICOSIDE) * Asiatic Acid (ASIATIC ACID) * Madeira homogeneous dispersion of kasik Acid (MADECASSIC ACID)) (manufactured by: Indena ^ⓡ) Followed by addition of a C ₃ -C ₆ trihydric alcohol, followed by primary mixing at a temperature of about 75 ° C (± 5 ° C) for about 15 minutes using a homomixer (manufactured by Tokushu Kika Kogyo Co., LTD) ;

(2) C ₂ -C ₅ divalent alcohol was added to the reaction vessel, followed by secondary mixing using a homomixer at a temperature of about 75 ° C (± 5 ° C) for about 15 minutes;

(3) C ₆ -C ₁₀ divalent alcohol was added to the reaction vessel and mixed at a temperature of about 85 ° C (± 5 ° C) for about 10 minutes using a homomixer;

(4) Water is added to the mixture obtained through the processes of (1) to (3), and the mixture is quadrature mixed for about 10 minutes to prepare an aqueous phase.

II. Manufacturing

(5) An oil, a fat component, a surfactant or an emulsion stabilizer, and an emollient were put into a melting tank together and mixed and dissolved at a temperature of about 75 ° C or higher. The oily part manufacturing process can be carried out without any particular limitation by modifying the oily part manufacturing process and the manufacturing conditions in a water-in-oil type cosmetic preparation process generally known in the art.

III. Mixing / dispersing emulsification / stabilization of water and oil phase

(6) The oil phase produced through the above step (5) was added to the reaction vessel containing the water phase unit manufactured through the above steps (1) to (4), and the mixture was mixed. : Tokushu Kika Kogyo Co., Ltd.) for about 3 minutes or more and then stabilized by allowing to stand for a certain time. The cosmetic obtained through the dispersion emulsification / stabilization process was degassed and cooled to finally obtain an underwater type cosmetic composition. The present process can be suitably modified and applied to water and oil phase mixing / dispersion, emulsification / stabilization processes and conditions of each process in an underwater type cosmetic preparation process generally known in the art.

[Production Example 2] Preparation of an underwater type cosmetic composition of Comparative Examples 1 to 4

[Comparative Examples 1 to 4] Preparation of an underwater-type cosmetic material containing a centilla extract or a centilla extract derived from a centilla sp.

An underwater type cosmetic composition of Comparative Examples 1 to 4 in the following Table 1 was prepared by the same manufacturing process as the manufacturing processes of Examples 1 to 3 except that the components and contents of water and oil were different.

Water top		Example 1	Example 2	Example 3	Comparative Example 1	Comparative Example 2	Comparative Example 3	Comparative Example 4
	Purified water	Balance	Balance	Balance	Balance	Balance	Balance	Balance
	glycerin	10	17.5	25	17.5	17.5	17.5	4.5
	Butylene glycol or propanediol	10 *	17.5 **	25 **	17.5 **	17.5 **	17.5 **	4.5 **
	Hexanediol	0.5	1.25	2	1.25	1.25	1.25	0.1
	Centipede extract or triterpene	0.5	One	2	One	One	One	One
	ethanol	-	-	-	5	-	-	-
	Triethanolamine	-	-	-	-	0.5	-	-
Floating	Squalane	10	10	10	10	10	10	10
	Cetylaryl alcohol	1.6	1.6	1.6	1.6	1.6	1.6	1.6
	Cetylaryl glucoside	0.4	0.4	0.4	0.4	0.4	0.4	0.4
	Glyceryl stearate	0.5	0.5	0.5	0.5	0.5	0.5	0.5
	FAGE -100 stearate	-	-	-	-	-	2	One

Note) *: Butylene glycol; **: Propanediol

[Test Example 1] Stability of formulation over time and evaluation of foreign body sensation

The formulation stability and the foreign body sensation of the underwater type cosmetic compositions of Examples 1 to 3 according to Production Example 1 and Comparative Examples 1 to 4 according to Production Example 2 were evaluated.

The time-dependent formulation stability was evaluated by observing with time the changes of the composition of the examples and comparative examples from the time immediately after the preparation to the elapse of time (2 weeks) at room temperature (room temperature), that is, the formation of the formulations, discoloration and precipitation. Table 2 summarizes the results.

The compositions of the examples and the comparative examples were immediately poured into a glass plate (width * length * thickness =) immediately after the preparation to obtain a temporal foreign body feel of the formulation (that is, a centistokes extract or tritulifene ASIATIC ACID * homogeneous dispersion of MADECASSIC ACID), and the results are summarized in Table 2.

	Example 1	Example 2	Example 3	Comparative Example 1	Comparative Example 2	Comparative Example 3	Comparative Example 4
Over time stability	○	○	○	○	○	○	×
Over time paint (homogeneous dispersion)	+++	++++	+++	++ -	++ -	++ -	- + -

<Evaluation Criteria for Time Stability>

X: unstable (at least one of the formation of the formulations, the discoloration and the precipitation)

○: Stable (formation of formulations, discoloration, no precipitation

<Evaluation Criteria for Time-Dependent Foreign Objects>

+++: Coated on a glass plate but neat, rarely coarse, occasional foreign body is rarely observed;

++++: The condition applied on the glass plate is clean as a whole, no time-dependent foreign matter is observed;

++ -: The coated state on the glass plate is smooth, some coarse portions are observed, and a temporal foreign body is rarely observed;

- + -: The state of the coating on the glass plate is rough as a whole, and some of the time-dependent foreign matter is observed;

---: The state of the coating on the glass plate is rough as a whole, and the foreign matter feeling over time is observed as a whole

In the case of Examples 1, 2 and 3, a time-dependent foreign matter was not observed at all or rarely observed, and the state of being coated on the surface of the glass sheet was smooth and clean.

On the other hand, in the case of Comparative Examples 1, 2 and 3, the rough surface was present on the surface of the glass plate, but the surface appeared smooth, and the foreign matter could not be confirmed with time. However, in Comparative Example 4, it was not possible to properly disperse or dissolve tritterone derived from Centella asiatica or Centella asiatica extract, and it was possible to confirm a foreign object with a naked eye, and the coated state was rough and uneven (Fig. 1). In comparison with Comparative Example 4 in Fig. 1, it can be visually confirmed that Example 2 according to the present invention shows that tentapenes derived from Centaurea or Centella asiatica are well dispersed or dissolved and stably maintained.

[Test Example 2] Evaluation of precipitation by polarization observation

Since the cosmetic compositions of Examples 1, 2, and 3 and Comparative Examples 1, 2, and 3 were unable to confirm the temporal foreign matter sensation of the T. terpenes derived from Centaurea or Centella asiatica extracts, Respectively.

As a result, in Examples 1, 2 and 3, precipitation was not observed at the time of observing the polarized light, but it was confirmed that the compositions of Comparative Examples 1, 2, and 3 had the precipitation of T. periplan 2).

[Test Example 3] Evaluation of the dispersion state of Kunchuk extract by optical microscope observation

In order to confirm the long-term stability of T. terpenes derived from Centella asiatica or Centella asiatica in the cosmetic compositions of Examples 1, 2 and 3 and Comparative Examples 1, 2 and 3, they were sealed at room temperature for 2 weeks after the preparation and then stained with Nikon ECRIPSE 80i (Magnification: 400) using an optical microscope.

As a result, as can be seen from FIG. 3, precipitation did not occur at all in the compositions of Examples 1, 2, and 3, but precipitation occurred in the compositions of Comparative Examples 1, 2, and 3.

The present invention is not limited to the process of manufacturing a cosmetic composition containing tritaper in an extract of Centella asiatica and / or Centella asiatica extract derived from Centella asiatica extract, which has been developed in the past, without using harmful chemicals that consumers are reluctant to use, The present invention can provide a manufacturing process capable of producing an underwater type cosmetic composition containing the composition. Since the cosmetic composition produced by the manufacturing process according to the present invention contains the core extract or the core extract of tsukerutepen in a high amount and stably even without using harmful chemicals that consumers are reluctant to use, It is possible to sufficiently provide the functionality of terpenes and to relieve consumers' anxiety about harmful chemicals in cosmetics, thereby making it possible to improve make-up relief and satisfaction, and as a result, Cosmetics products are expected to have high consumer preference.

Claims (4)

1. An underwater-type cosmetic composition comprising 0.05 to 2.0% by weight of Centella asiatica extract or Triticum persicae extract derived from Centella asiatica in a water-in-oil type cosmetic composition comprising an aqueous phase and an oil phase.
2. 2. The composition of claim 1, wherein the water-

   0.05 to 2.0% by weight of triterpene isolated from Centella asiatica or Centella asiatica extract,

   5 to 37.5% by weight of a C ₃ -C ₆ trivalent alcohol,

   5 to 37.5% by weight of divalent alcohol of C ₂ -C ₅ ,

   From 0.25 to 3.25% by weight of a divalent alcohol of C ₆ -C ₁₀ ; And

   Wherein the water-in-oil type cosmetic composition comprises water.
3. The underwater type cosmetic composition according to claim 1 or 2,

   1) preparing a first mixture by firstly mixing T. terpenes derived from Centella asiatica or Centella asiatica extracts and C ₃ -C ₆ trihydric alcohols at a temperature of 75 ° C or higher;

   2) preparing a second mixture by adding a C ₂ -C ₅ divalent alcohol to the first mixture, followed by secondary mixing at a temperature of 75 ° C or higher;

   3) adding a C ₆ -C ₁₀ divalent alcohol to the second mixture, followed by tertiary mixing at a temperature of 85 ° C or lower to prepare a third mixture; And

   And 4) adding water to the third mixture to prepare a water phase by mixing the water to form a water phase. The method according to claim 1, wherein the water phase is selected from the group consisting of a centilla sp. Cosmetic composition.
4. 1) preparing a first mixture by first mixing 0.05 to 2.0% by weight of triterpenes derived from Centaalinae sp. Extract and 5 to 37.5% by weight of C ₃ -C ₆ trihydric alcohol at a temperature of 75 ° C or more, based on the total weight of the composition; ;

   2) adding to the first mixture 5 to 37.5% by weight of a divalent alcohol of C ₂ -C ₅ , based on the total weight of the composition, followed by secondary mixing at a temperature of 75 ° C or higher to prepare a second mixture;

   3) adding to the second mixture 0.25 to 3.25% by weight of divalent C ₆ -C ₁₀ alcohol based on the total weight of the composition, followed by tertiary mixing at a temperature of 85 ° C or less to prepare a third mixture; And

   4) adding water to the third mixture, and then mixing the mixture to form a water phase; and 4) stabilizing the T. terpenes derived from Centella asiatica or Centella asiaticus on top of water in the water type cosmetic composition.

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