WO2014156398A1 - Method for producing air filter material, air filter material, and air filter pack - Google Patents
Method for producing air filter material, air filter material, and air filter pack Download PDFInfo
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- WO2014156398A1 WO2014156398A1 PCT/JP2014/054118 JP2014054118W WO2014156398A1 WO 2014156398 A1 WO2014156398 A1 WO 2014156398A1 JP 2014054118 W JP2014054118 W JP 2014054118W WO 2014156398 A1 WO2014156398 A1 WO 2014156398A1
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- air filter
- nonwoven fabric
- porous membrane
- filter medium
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- 238000004519 manufacturing process Methods 0.000 title claims description 22
- 239000000463 material Substances 0.000 title abstract description 16
- 239000004745 nonwoven fabric Substances 0.000 claims abstract description 109
- 229920001343 polytetrafluoroethylene Polymers 0.000 claims abstract description 84
- 239000004810 polytetrafluoroethylene Substances 0.000 claims abstract description 84
- 238000010438 heat treatment Methods 0.000 claims abstract description 35
- -1 polytetrafluoroethylene Polymers 0.000 claims abstract description 18
- 239000012528 membrane Substances 0.000 claims description 74
- 238000004049 embossing Methods 0.000 claims description 28
- 238000003825 pressing Methods 0.000 claims description 4
- 238000000034 method Methods 0.000 description 12
- 239000000835 fiber Substances 0.000 description 9
- 239000002245 particle Substances 0.000 description 8
- 238000003475 lamination Methods 0.000 description 5
- 238000002844 melting Methods 0.000 description 5
- 230000008018 melting Effects 0.000 description 5
- 238000004364 calculation method Methods 0.000 description 4
- 239000010687 lubricating oil Substances 0.000 description 4
- 238000000879 optical micrograph Methods 0.000 description 4
- 239000004698 Polyethylene Substances 0.000 description 3
- 239000000853 adhesive Substances 0.000 description 3
- 230000001070 adhesive effect Effects 0.000 description 3
- 239000000306 component Substances 0.000 description 3
- 239000002131 composite material Substances 0.000 description 3
- 238000010030 laminating Methods 0.000 description 3
- 229920000139 polyethylene terephthalate Polymers 0.000 description 3
- 239000005020 polyethylene terephthalate Substances 0.000 description 3
- 238000005096 rolling process Methods 0.000 description 3
- 238000009823 thermal lamination Methods 0.000 description 3
- MQIUGAXCHLFZKX-UHFFFAOYSA-N Di-n-octyl phthalate Natural products CCCCCCCCOC(=O)C1=CC=CC=C1C(=O)OCCCCCCCC MQIUGAXCHLFZKX-UHFFFAOYSA-N 0.000 description 2
- 239000004743 Polypropylene Substances 0.000 description 2
- BJQHLKABXJIVAM-UHFFFAOYSA-N bis(2-ethylhexyl) phthalate Chemical compound CCCCC(CC)COC(=O)C1=CC=CC=C1C(=O)OCC(CC)CCCC BJQHLKABXJIVAM-UHFFFAOYSA-N 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 238000005520 cutting process Methods 0.000 description 2
- 230000006378 damage Effects 0.000 description 2
- SNRUBQQJIBEYMU-UHFFFAOYSA-N dodecane Chemical compound CCCCCCCCCCCC SNRUBQQJIBEYMU-UHFFFAOYSA-N 0.000 description 2
- 239000000428 dust Substances 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 229920001155 polypropylene Polymers 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 239000011347 resin Substances 0.000 description 2
- 229920005989 resin Polymers 0.000 description 2
- 125000006850 spacer group Chemical group 0.000 description 2
- 229920001410 Microfiber Polymers 0.000 description 1
- 239000004952 Polyamide Substances 0.000 description 1
- 239000000443 aerosol Substances 0.000 description 1
- 238000004378 air conditioning Methods 0.000 description 1
- 239000004760 aramid Substances 0.000 description 1
- 229920003235 aromatic polyamide Polymers 0.000 description 1
- 239000011324 bead Substances 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 239000008358 core component Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000010410 dusting Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000003365 glass fiber Substances 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000003658 microfiber Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- 229920002647 polyamide Polymers 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 229920000098 polyolefin Polymers 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 239000012779 reinforcing material Substances 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
- 238000009423 ventilation Methods 0.000 description 1
- 238000004804 winding Methods 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
- B01D69/12—Composite membranes; Ultra-thin membranes
- B01D69/1216—Three or more layers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
- B01D69/12—Composite membranes; Ultra-thin membranes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D39/00—Filtering material for liquid or gaseous fluids
- B01D39/14—Other self-supporting filtering material ; Other filtering material
- B01D39/16—Other self-supporting filtering material ; Other filtering material of organic material, e.g. synthetic fibres
- B01D39/1607—Other self-supporting filtering material ; Other filtering material of organic material, e.g. synthetic fibres the material being fibrous
- B01D39/1623—Other self-supporting filtering material ; Other filtering material of organic material, e.g. synthetic fibres the material being fibrous of synthetic origin
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D71/00—Semi-permeable membranes for separation processes or apparatus characterised by the material; Manufacturing processes specially adapted therefor
- B01D71/06—Organic material
- B01D71/30—Polyalkenyl halides
- B01D71/32—Polyalkenyl halides containing fluorine atoms
- B01D71/36—Polytetrafluoroethene
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2239/00—Aspects relating to filtering material for liquid or gaseous fluids
- B01D2239/06—Filter cloth, e.g. knitted, woven non-woven; self-supported material
- B01D2239/065—More than one layer present in the filtering material
- B01D2239/0668—The layers being joined by heat or melt-bonding
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Filtering Materials (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
Abstract
Description
ポリテトラフルオロエチレン多孔質膜の一面側に第1不織布を重ね、前記ポリテトラフルオロエチレン多孔質膜の他面側に第2不織布を重ねる工程(a)と、
前記ポリテトラフルオロエチレン多孔質膜、前記第1不織布および前記第2不織布を重ねた状態で、前記第2不織布に加熱ロールを接触させ、前記ポリテトラフルオロエチレン多孔質膜、前記第1不織布および前記第2不織布に前記加熱ロールを押圧する工程(b)と、を含むエアフィルタ濾材の製造方法であって、
前記第1不織布として前記一面側に接する面のエンボス比率が12%以上18%以下である不織布を用い、
前記第2不織布として前記他面側に接する面のエンボス比率が18%よりも大きい不織布を用いるエアフィルタ濾材の製造方法を提供する。 That is, the present invention
A step (a) of superposing a first non-woven fabric on one side of the polytetrafluoroethylene porous membrane and superposing a second non-woven fabric on the other side of the polytetrafluoroethylene porous membrane;
In a state where the polytetrafluoroethylene porous membrane, the first nonwoven fabric and the second nonwoven fabric are stacked, a heating roll is brought into contact with the second nonwoven fabric, the polytetrafluoroethylene porous membrane, the first nonwoven fabric and the A step (b) of pressing the heating roll against the second nonwoven fabric, and a method for producing an air filter medium,
Using a non-woven fabric having an embossing ratio of 12% or more and 18% or less as the first non-woven fabric in contact with the one surface side,
Provided is a method for producing an air filter medium using a nonwoven fabric having an embossing ratio of a surface in contact with the other surface as the second nonwoven fabric that is greater than 18%.
続けて、前記PTFE多孔質膜、前記第1不織布および前記第2不織布を重ねた状態で前記第2不織布に加熱ロールを接触させ、全体を加熱ロール4に沿わせて押圧する(工程b)。加熱ロール4に沿わせた状態でPTFE多孔質膜2、不織布1aおよび1bを含む全体を加熱ロール4により所定の温度にまで加熱し、不織布1aおよび1bとPTFE多孔質膜2とを接着、積層させ、得られた積層体をロール5に引き取ることで、加熱ロール4から分離し、エアフィルタ濾材Aを得ることができる。 More specifically, as shown in FIG. 1, first, the
Subsequently, a heating roll is brought into contact with the second nonwoven fabric in a state where the PTFE porous membrane, the first nonwoven fabric and the second nonwoven fabric are stacked, and the whole is pressed along the heating roll 4 (step b). The entire structure including the PTFE
特に、不織布1aとしてエンボス比率が12%以上18%以下である不織布を用い、不織布1bとしてエンボス比率が19%以上50%以下である不織布をそれぞれ用いることが好ましい。
In particular, it is preferable to use a nonwoven fabric with an embossing ratio of 12% or more and 18% or less as the
このため、不織布1aが加熱ロール4に向かって、加熱された状態で押し付けられる圧力は、不織布1bが加熱ロール4に向かって押し付けられる圧力よりも高くなる。 When the
For this reason, the pressure with which the
特に、PTFE多孔質膜2として、HEPA、ULPA等のエアフィルタ濾材を構成する、より捕集効率は高いが、非常に損傷しやすいPTFE多孔質膜を用いる場合に、本発明の効果は顕著である。
HEPA、ULPA等のエアフィルタ濾材用のPTFE多孔質膜は、PTFE多孔質膜2の繊維へのダメージが、エアフィルタ濾材の捕集効率の低下に反映されやすいからである。 Therefore, when the number of contact points between the
In particular, when the PTFE
This is because in the PTFE porous membrane for air filter media such as HEPA and ULPA, damage to the fibers of the PTFE
本実施形態のエアパックとしては、例えば、エアフィルタ濾材が複数箇所で屈曲されてひだ状に形成されてなるエアパック等が挙げられる。
かかるエアパックは、例えば、前記エアフィルタ濾材が一方向に沿って屈曲されて形成される屈曲部と、前記屈曲部以外の領域が板状に形成されてなる平板部と、エアフィルタ濾材の一方の面側および他方の面側における各平板部の間に形成されて隣り合う屈曲部同士の間隔を保持する複数の間隔保持部とを備えてなるものであってもよい。 The air pack of this embodiment is formed by forming an air filter medium obtained by the manufacturing method of this embodiment into a predetermined shape or size.
Examples of the air pack of the present embodiment include an air pack in which an air filter medium is bent at a plurality of locations and formed into a pleat shape.
Such an air pack includes, for example, a bent portion formed by bending the air filter medium along one direction, a flat plate formed by forming a region other than the bent portion in a plate shape, and one of the air filter medium. It may be provided with a plurality of interval holding portions that are formed between the flat plate portions on the surface side and the other surface side and hold intervals between adjacent bent portions.
まず、エアフィルタ濾材がプリーツ加工される。具体的には、帯状のエアフィルタ濾材が長手方向に直交する幅方向に沿って複数箇所で屈曲されてひだ状に形成される。これにより、エアフィルタ濾材には複数の屈曲部と複数の平板部とが形成される(プリーツ加工する工程)。
次に、ひだ状にプリーツ加工したエアフィルタ濾材が、プリーツ加工前の平らな状態に伸ばされ、エアフィルタ濾材の両面に接着剤等のスペーサー樹脂(一般に「ビード」と呼ばれる)が塗布されて間隔保持部が形成される(スペーサー樹脂を塗布する工程)。
間隔保持部は、隣り合う平板部におけるひだ状に形成された際に対向する一対の対向面の間に配置される。
さらに、エアフィルタ濾材が再度屈曲されてひだ状に形成される(再度プリーツ加工する工程)。
必要に応じて、プリーツ加工されたエアフィルタ濾材が所定の大きさに切断されてもよい(切断工程)。 Examples of a method for manufacturing such an air pack include the following methods.
First, the air filter medium is pleated. Specifically, the band-shaped air filter medium is bent at a plurality of locations along the width direction orthogonal to the longitudinal direction to form a pleat. As a result, a plurality of bent portions and a plurality of flat plate portions are formed in the air filter medium (step of pleating).
Next, the air filter medium pleated into pleats is stretched to a flat state before pleating, and spacer resin (generally called “bead”) such as adhesive is applied to both sides of the air filter medium, and the interval is applied. A holding part is formed (step of applying a spacer resin).
The interval holding portion is disposed between a pair of opposing surfaces that face each other when formed in a pleat shape in adjacent flat plate portions.
Further, the air filter medium is bent again to form a pleat (step of pleating again).
If necessary, the pleated air filter medium may be cut into a predetermined size (cutting step).
エアフィルタユニットは、前記エアフィルタパックの四方を囲むようなフレームとエアフィルタパックとをシールすることで製造される。
このように製造されたエアフィルタユニットは、空気清浄装置やクリーンルームの空調設備などに用いられる。 The air filter pack may be attached to a frame and formed as an air filter unit.
The air filter unit is manufactured by sealing a frame surrounding the four sides of the air filter pack and the air filter pack.
The air filter unit manufactured in this way is used for an air purifier or an air conditioning facility in a clean room.
例えば、
(1)液状潤滑剤の混合された分子量の異なるPTFEファインパウダーを、層状に分布させたのちに、層構造を保ったまま押出して圧延し、さらに延伸することでPTFE複層多孔質膜を得る方法(日本国特開平3-179038号公報に記載)、
(2)液状潤滑剤を含んだ複数のPTFE圧延シートを重ねて圧延し、さらに延伸することでPTFE複層多孔質膜を得る方法(日本国特開昭59-49935号公報に記載)、
(3)孔径の異なる未焼成のPTFE多孔質膜を圧着することにより積層化し、PTFEの融点以上の温度で焼成することでPTFE複層多孔質膜を得る方法(日本国特開昭54-97686号公報に記載)、
などが挙げられる。 If necessary, a PTFE multilayer porous membrane having a structure in which a plurality of PTFE porous membranes are laminated may be used as the PTFE
For example,
(1) A PTFE fine powder mixed with a liquid lubricant and having different molecular weights is distributed in layers, then extruded and rolled while maintaining the layer structure, and further stretched to obtain a PTFE multilayer porous membrane. Method (described in Japanese Patent Application Laid-Open No. 3-17938),
(2) A method of obtaining a PTFE multi-layer porous film by rolling a plurality of PTFE rolled sheets containing a liquid lubricant, and further stretching (described in JP-A-59-49935),
(3) A method of obtaining a PTFE multilayer porous membrane by laminating unfired PTFE porous membranes having different pore diameters by pressure bonding and firing at a temperature equal to or higher than the melting point of PTFE (Japanese Patent Laid-Open No. 54-97686). ),
Etc.
この条件を満たすものであれば、不織布1aおよび1bは、特に限定されるものではないが、PTFE多孔質膜より通気性に優れているものが好ましい。
また、PTFE多孔質膜との接着が容易であることなどから、不織布を構成する一部あるいは全部の繊維が芯鞘構造の複合繊維であり、芯成分が鞘成分より相対的に融点が高い合成繊維であることがより好ましい。
As long as this condition is satisfied, the
In addition, because it is easy to adhere to the PTFE porous membrane, some or all of the fibers constituting the nonwoven fabric are composite fibers having a core-sheath structure, and the core component has a relatively higher melting point than the sheath component. More preferably, it is a fiber.
不織布のエンボス比率は、単位面積当たりの不織布の凹部の面積の割合として求めた。算出方法は、倍率5倍で不織布表面(例えば、図3および図4を参照)の光学顕微鏡写真を撮影して、この写真を印刷し、印刷された写真全体の重量を測定した後、印刷された写真から凹部を切り抜き、切り抜かれた紙片の重量を測定することで計算する。なお、図3は実施例1の不織布1a、図4は実施例1の不織布1bの表面の光学顕微鏡写真である。 (Non-woven embossing ratio)
The embossing ratio of the nonwoven fabric was determined as a ratio of the area of the concave portion of the nonwoven fabric per unit area. The calculation method is to take an optical micrograph of the surface of the nonwoven fabric (for example, see FIGS. 3 and 4) at a magnification of 5 times, print this photo, measure the weight of the entire printed photo, and then print it. The calculation is performed by cutting out the concave portion from the photograph and measuring the weight of the cut paper piece. 3 is an optical micrograph of the surface of the
圧力損失(Pa)の測定は、JIS K 0901の「気体中のダスト試料補集用濾過材」に準じ、PTFE多孔質膜およびエアフィルタ濾材の測定サンプルを、面積100mm2のホルダーにセットし、コンプレッサーで入口側を加圧し、流量計で空気の透過する流量を5.3cm/秒に調整した。この時の圧力損失をマノメーターで測定した。結果を表1及び2に示す。 (Measurement of pressure loss of PTFE porous membrane and air filter medium)
The pressure loss (Pa) is measured according to JIS K 0901 “filtering material for collecting dust sample in gas”, and a PTFE porous membrane and a measuring sample of air filter medium are set in a holder having an area of 100 mm 2 . The inlet side was pressurized with a compressor, and the flow rate of air through the flow meter was adjusted to 5.3 cm / sec. The pressure loss at this time was measured with a manometer. The results are shown in Tables 1 and 2.
捕集効率は、JIS K 3803の「除菌用空気濾過デプスフィルタのエアロゾル捕集性能試験方法」により、粒子径0.3~0.5μmのDOP(ジオクチルフタレート)の粒子を、粒子の濃度が約108個/リットルとなるように混入して測定し、次式(1)で計算した。なお、式(1)中の、NLは下流側の粒子数(個/L)、NUは上流側の粒子数(個/L)、Pは粒子捕集効率(%)を表す。結果を表1及び2に示す。
P=(1-NL/NU)×100 ・・・(1) (Measurement of collection efficiency of PTFE porous membrane and air filter medium)
The collection efficiency is determined according to JIS K 3803 “Method for testing aerosol collection performance of an air filtration depth filter for sterilization” with DOP (dioctyl phthalate) particles having a particle size of 0.3 to 0.5 μm and a particle concentration of It mixed and measured so that it might become about 10 < 8 > piece / liter, and calculated by following Formula (1). In the formula (1), NL represents the number of particles on the downstream side (number / L), NU represents the number of particles on the upstream side (number / L), and P represents the particle collection efficiency (%). The results are shown in Tables 1 and 2.
P = (1-NL / NU) × 100 (1)
エアフィルタ濾材の性能を表すPF値は、次式(2)により算出した。結果を表1及び2に示す。
PF値=-Log(1-捕集効率(%)/100)/圧力損失(mmH2O)×100・・・(2) (PF value of air filter media)
The PF value representing the performance of the air filter medium was calculated by the following formula (2). The results are shown in Tables 1 and 2.
PF value = −Log (1−capturing efficiency (%) / 100) / pressure loss (mmH 2 O) × 100 (2)
2 PTFE多孔質膜
3 ガイドロール
4 加熱ロール
5 巻取ロール
6 ガイドロール
A エアフィルタ濾材 1a,
Claims (4)
- ポリテトラフルオロエチレン多孔質膜の一面側に第1不織布を重ね、前記ポリテトラフルオロエチレン多孔質膜の他面側に第2不織布を重ねる工程(a)と、
前記ポリテトラフルオロエチレン多孔質膜、前記第1不織布および前記第2不織布を重ねた状態で、前記第2不織布に加熱ロールを接触させ、前記ポリテトラフルオロエチレン多孔質膜、前記第1不織布および前記第2不織布に前記加熱ロールを押圧する工程(b)と、を含むエアフィルタ濾材の製造方法であって、
前記第1不織布として前記一面側に接する面のエンボス比率が12%以上18%以下である不織布を用い、
前記第2不織布として前記他面側に接する面のエンボス比率が18%よりも大きい不織布を用いるエアフィルタ濾材の製造方法。 A step (a) of superposing a first non-woven fabric on one side of the polytetrafluoroethylene porous membrane and superposing a second non-woven fabric on the other side of the polytetrafluoroethylene porous membrane;
In a state where the polytetrafluoroethylene porous membrane, the first nonwoven fabric and the second nonwoven fabric are stacked, a heating roll is brought into contact with the second nonwoven fabric, the polytetrafluoroethylene porous membrane, the first nonwoven fabric and the A step (b) of pressing the heating roll against the second nonwoven fabric, and a method for producing an air filter medium,
Using a non-woven fabric having an embossing ratio of 12% or more and 18% or less as the first non-woven fabric in contact with the one surface side,
The manufacturing method of the air filter medium which uses the nonwoven fabric whose embossing ratio of the surface which contact | connects the said other surface side as said 2nd nonwoven fabric is larger than 18%. - 前記第2不織布の前記他面側に接する面のエンボス比率が19%以上50%以下である、請求項1に記載のエアフィルタ濾材の製造方法。 The method for producing an air filter medium according to claim 1, wherein an embossing ratio of a surface in contact with the other surface side of the second nonwoven fabric is 19% or more and 50% or less.
- 請求項1または2に記載の製造方法で得られたエアフィルタ濾材。 An air filter medium obtained by the production method according to claim 1 or 2.
- 請求項3に記載のエアフィルタ濾材を備えたエアフィルタパック。 An air filter pack comprising the air filter medium according to claim 3.
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KR1020157025428A KR102255737B1 (en) | 2013-03-29 | 2014-02-21 | Method for producing air filter material, air filter material, and air filter pack |
CN201480014084.2A CN105188878B (en) | 2013-03-29 | 2014-02-21 | The manufacture method of air filter filter medium, air filter filter medium and air filter element |
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KR (1) | KR102255737B1 (en) |
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CN105879826B (en) * | 2016-06-08 | 2018-03-13 | 河南科高辐射化工科技有限公司 | One kind is used for radiation grafted rear heating solid-liquid reaction device |
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KR102326322B1 (en) * | 2018-10-30 | 2021-11-12 | 주식회사 엘지화학 | Multi-layer film for air purification filter |
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CN105188878A (en) | 2015-12-23 |
TW201446323A (en) | 2014-12-16 |
TWI618572B (en) | 2018-03-21 |
JP6292920B2 (en) | 2018-03-14 |
JP2014208326A (en) | 2014-11-06 |
KR20150138845A (en) | 2015-12-10 |
CN105188878B (en) | 2017-04-05 |
KR102255737B1 (en) | 2021-05-26 |
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