WO2013044599A1 - Method for achieving high-pressure shearing deformation in tube materials by wedge principle and apparatus therefor - Google Patents

Method for achieving high-pressure shearing deformation in tube materials by wedge principle and apparatus therefor Download PDF

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Publication number
WO2013044599A1
WO2013044599A1 PCT/CN2012/070157 CN2012070157W WO2013044599A1 WO 2013044599 A1 WO2013044599 A1 WO 2013044599A1 CN 2012070157 W CN2012070157 W CN 2012070157W WO 2013044599 A1 WO2013044599 A1 WO 2013044599A1
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workpiece
pressure
rigid
principle
mandrel
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PCT/CN2012/070157
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French (fr)
Chinese (zh)
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王经涛
李政
王进
安钰坤
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南京理工大学
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21JFORGING; HAMMERING; PRESSING METAL; RIVETING; FORGE FURNACES
    • B21J1/00Preparing metal stock or similar ancillary operations prior, during or post forging, e.g. heating or cooling
    • B21J1/02Preliminary treatment of metal stock without particular shaping, e.g. salvaging segregated zones, forging or pressing in the rough
    • B21J1/025Preliminary treatment of metal stock without particular shaping, e.g. salvaging segregated zones, forging or pressing in the rough affecting grain orientation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21CMANUFACTURE OF METAL SHEETS, WIRE, RODS, TUBES OR PROFILES, OTHERWISE THAN BY ROLLING; AUXILIARY OPERATIONS USED IN CONNECTION WITH METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL
    • B21C23/00Extruding metal; Impact extrusion
    • B21C23/001Extruding metal; Impact extrusion to improve the material properties, e.g. lateral extrusion
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21JFORGING; HAMMERING; PRESSING METAL; RIVETING; FORGE FURNACES
    • B21J5/00Methods for forging, hammering, or pressing; Special equipment or accessories therefor
    • B21J5/06Methods for forging, hammering, or pressing; Special equipment or accessories therefor for performing particular operations
    • B21J5/063Friction heat forging
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D7/00Modifying the physical properties of iron or steel by deformation
    • C21D7/02Modifying the physical properties of iron or steel by deformation by cold working
    • C21D7/04Modifying the physical properties of iron or steel by deformation by cold working of the surface
    • C21D7/08Modifying the physical properties of iron or steel by deformation by cold working of the surface by burnishing or the like
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D9/00Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
    • C21D9/08Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for tubular bodies or pipes

Definitions

  • the invention relates to the field of material processing engineering, in particular to a method and a device for realizing high-pressure shear plastic deformation of a tubular material by using a tipping principle, which are mainly applied to various metal and alloy materials, inorganic non-metal materials and polymer materials, etc. To achieve plastic deformation of these materials under high hydrostatic pressure conditions, thereby controlling and optimizing its microstructure and improving its performance.
  • Severe plastic deformation The method of deformation (SPD) is a general term for a series of plastic processing techniques with large deformation.
  • the SPD method refines the grain effect obviously, and can refine the internal structure of the material to sub-micron, nano-scale or even amorphous [R. Z. Valiev. Nature materials. 2004 (3): 511-516.; R. Z. Valiev, A. K. Mukherjee. Scripta mater. 2001 (44): 1747–1750.].
  • SPD method refines the grain effect obviously, and can refine the internal structure of the material to sub-micron, nano-scale or even amorphous [R. Z. Valiev. Nature materials. 2004 (3): 511-516.; R. Z. Valiev, A. K. Mukherjee. Scripta mater. 2001 (44): 1747–1750.].
  • the technology of preparing bulk nanostructured materials by SPD method has received widespread attention from experts and scholar in the field of materials science.
  • the most popular SPD method at present is mainly cumulative rolling (accumulative Roll-bonding (abbreviated ARB) technology, equal-channel angular pressing (ECAP) technology, and high-pressure torsion (high-pressure torsion, referred to as HPT) Technology, etc.
  • ARB cumulative rolling
  • ECAP equal-channel angular pressing
  • HPT high-pressure torsion
  • the ARB technology is shown in Figure 1. It can continuously prepare thin-plate ultrafine-grained structural materials, and is easy to implement on traditional rolling mills. The equipment is simple and practical. However, in the ARB process, in order to achieve good rolling compounding, lubricants are often not used, which is detrimental to the service life of the rolls.
  • HPT technology shown in Figure 4 is the most suitable condition for the preparation of ultrafine grained materials in accordance with the SPD method mentioned in the previous section.
  • SPD technology has the strongest grain refinement capability.
  • the thickness of the specimen that HPT can process is small [A. P. Zhilyaev, T. G. Langdon. Progress in Materials Science. 2008 (53) : 893-979.], the processed disc-shaped sample has a large strain gradient in the radial direction, the deformation is uneven, and the degree of grain refinement is not uniform.
  • the radial expansion of the mandrel creates radial pressure on the inner wall of the tubular workpiece, while the rigid disk creates a radial pressure in the opposite direction to the outer wall of the tubular workpiece, thereby creating hydrostatic pressure in the tubular workpiece.
  • the ring sleeve is rotated, and the tubular workpiece is sheared under the surface friction.
  • This method is very good.
  • the main problem is that the method of loading the sample is radial loading. That is to say, the method directly applies axial pressure to the mandrel, and the mandrel produces a diameter on the sample. To the pressure.
  • the pressure is not directly loaded in the axial direction of the tubular material, and the hydrostatic pressure of the specimen is derived from the elastic deformation of the mandrel after being pressed. Since the elastic deformation of the mandrel is unlikely to be large, it is difficult to produce high The hydrostatic pressure, therefore, provides limited friction and is only suitable for pure metals with lower strength. For materials with higher strength, the frictional force that can be generated does not reach the yield strength of the material, and slipping and the like are likely to occur, and the required deformation cannot be achieved.
  • baffle at the two ends of the tubular workpiece is a cantilever beam structure, and the constraint on the axial deformation of the sample is insufficient.
  • hydrostatic pressure of the sample is high, the material is easily extruded from the gap, affecting Processing process.
  • the invention proposes a technology for realizing high-pressure shear deformation of a tubular material by using the tip principle, and the principle of the wedge applied by the technology is also called the wedge effect or the principle of the beveling force.
  • This principle can be used with the Lamy's theorem (Lami's Theorem) to explain: in the same plane, when the resultant force of the three co-point forces is zero, the ratio of any one of the forces to the sine of the other two forces is equal [R.K. Bansal (2005). Laxmi Publications. p. 4.].
  • the small angled bevel of the tip or wedge can be seen as a force amplifying device.
  • the high hydrostatic pressure of the invention utilizes the force amplification effect of the tip principle, so that the technology satisfies many conditions that should be satisfied by the SPD method for preparing the ultrafine grain material, such as large plastic deformation amount and relatively low deformation temperature. And the high hydrostatic pressure inside the deformed material.
  • the method avoids the complicated process of multi-channel operation such as ARB, ECAP and back pressure ECAP.
  • the method also overcomes the problems of insufficient hydrostatic pressure of Tóth et al.
  • it can provide high hydrostatic pressure conditions similar to HPT technology, which is suitable for the processing of difficult-to-deform metals and alloys, to achieve the effect of controlling and optimizing the structure of the material and improving its performance.
  • the technical solution for achieving the object of the present invention is: a method for realizing high-pressure shearing of a pipe by using a tipping principle, first selecting a machined workpiece, the workpiece is a tapered pipe, and the inner wall and the outer wall of the workpiece are respectively restrained by the restraining body; Applying axial pressure to one end of the restraining body, using the pressure-increasing and force-increasing characteristics of the tipping principle (also called the wedge effect or the principle of the beveling force), a high pressure is generated in a direction perpendicular to the inner and outer walls of the workpiece, so that the workpiece is elastically deformed.
  • the deformation of the workpiece is hindered by the reverse frictional force with the deformation trend, thereby generating a high hydrostatic pressure in the workpiece; then providing a torque to a restraining body in contact with the inner and outer walls of the workpiece to surround the center of the workpiece
  • the shaft rotates while fixing the other restraint body; or the opposite direction torque is provided to the two restraint bodies at the same time.
  • the materials at different thicknesses in the radial direction of the workpiece have different angular velocities. Rotate to achieve shear deformation of the workpiece.
  • a device for realizing high-pressure shearing of a pipe by using a tipping principle comprising a press having a constant pressure function, a torque reducer providing torque, and a mold having a transfer pressure, a constraining deformation, and a partial rotation function;
  • the mold includes: fixed or a rotatable rigid mandrel and a rotatable or fixed rigid collar; the workpiece is coaxially placed in the rigid collar, the inner surface of the rigid collar is in contact with the outer wall of the workpiece, and the interior of the workpiece is coaxially provided with a rigid mandrel, rigid core
  • the outer surface of the shaft is in contact with the inner wall of the workpiece, and the rigid mandrel and the rigid ring sleeve are respectively mounted along the central axis or placed on the upper and lower bottom plates of the press, and the displacement of the rigid ring sleeve and the rigid mandrel is limited, only along Move axially or around the central axis.
  • the invention has significant advantages: (1) the processing procedure is simple.
  • the method for realizing high-pressure shearing of pipe by using the tip principle of the invention is a severe plastic deformation method which can be realized in a single pass on a conventional pressure device having a constant pressure function.
  • ARB cumulative rolling
  • ECAP equal-angle extrusion
  • back pressure ECAP method etc.
  • the method utilizes the friction between the rigid ring sleeve, the tubular workpiece and the mandrel and the tubular workpiece, so that the rigid ring sleeve and the rigid mandrel rotate relative to each other, and the outer layer region of the tubular workpiece contacting the rigid ring sleeve is opposite to the mandrel. Shearing between the inner regions of the contact, thereby achieving severe plastic deformation under a single process pass.
  • the true strain is 1 ⁇ 10 or even higher.
  • the method of the severe plastic deformation proposed by the present invention is simple in principle and easy to obtain, and can be realized in a general pressure processing factory and a plastic forming laboratory.
  • the high-pressure shearing method proposed by the present invention does not directly pressurize the tubular material axially, and does not restrain the end of the workpiece. Therefore, there is no central pressure that may occur after the workpiece is too long. Insufficient, pressure instability and other issues. Hydrostatic pressure can be generated more evenly inside the material up to 15 GPa. This is currently not possible with other processes including HPTT. Moreover, with the development of mold materials and the improvement of design, the hydrostatic pressure that can be provided will be higher.
  • Plastic deformation under such high hydrostatic pressure conditions effectively suppresses the generation and development of material surfaces and internal cracks, thereby improving the workability of many difficult-to-machine materials such as magnesium alloys with poor plasticity.
  • materials such as magnesium alloys are densely packed due to the crystal structure, and the slip coefficient is limited, and the plasticity is often poor.
  • ARB or ECAP is processed on difficult-to-deform materials such as magnesium alloy, the sample often cracks.
  • it is often necessary to increase the processing temperature which will inevitably increase the processing cost. More importantly, as the processing temperature increases, the grain refining effect of the material becomes worse and the grains become coarser, which improves the material properties.
  • the method can achieve plastic processing of many materials such as aluminum, copper, nickel, magnesium, titanium, tungsten and their alloys, and low carbon steel at room temperature or at a lower heating temperature, thereby controlling and improving. Its organizational structure improves its performance.
  • the size of the tubular product that can be obtained is large.
  • the method for realizing the high-pressure shearing of the pipe by using the tipping principle of the invention has a tubular shape, and the size thereof is limited only by the scale of the equipment. Even in the laboratory, the tubular material of ⁇ 100mm height can be obtained by this method, which has good performance and can be applied in many fields after a little subsequent treatment. In addition, the obtained tubular material is cut along the axial direction and is rolled. High performance sheeting is obtained.
  • Figure 1 is a schematic diagram of the principle of cumulative composite rolling (ARB) technology.
  • FIG. 2 is a schematic diagram of the principle of equal channel angular extrusion (ECAP) technology.
  • FIG. 3 is a schematic diagram of the principle of back pressure ECAP (BP-ECAP) technology.
  • FIG. 4 is a schematic diagram of the principle of high voltage torsion (HPT) technology.
  • Figure 5 is a high-pressure tube twist Twisting-HPTT) Schematic diagram of the technical principle.
  • FIG. 6 is a schematic diagram of the tip principle (or wedge effect, ramping force amplification principle).
  • the so-called tip principle is shown in Figure 2.
  • the input force is P
  • FIGS. 7(a) to 7(d) are schematic diagrams showing the principle of the method for realizing high-pressure shearing of pipes by using the tip principle of the present invention, wherein 1-rigid mandrel, 2-rigid ring sleeve, 3-tube workpiece with taper h is the height of the tubular workpiece; r i , r e are the inner and outer radii of the lower end surface of the tubular workpiece; ⁇ is the half cone angle; P is the main power provided by the press; T is the active torque provided by the power unit.
  • the constrained reaction force and the constrained counter torque are not marked; the high pressure shear of the tubular specimen is achieved by applying the main power and the active torque shown in Figure 8 to the rigid collar and the mandrel or a combination thereof (the two main power directions are opposite in the figure). , respectively, acting on the rigid mandrel and the collar; the two active torques are opposite in direction, acting on the rigid collar and the mandrel respectively).
  • FIGS. 8(a) to (c) are schematic views of several constraint forms of the end portion of the workpiece of the present invention: the inner and outer walls of the workpiece are always constrained by a 1-rigid mandrel and a 2-rigid cuff, and (a) the end is unconstrained; (b) end semi-constraint; (c) end full constraint.
  • FIG. 9 is a schematic view of a device for implementing a method for realizing high-pressure shearing of a pipe by using a tipping principle, wherein (a) is an exploded view: 90-upper head, 93-rigid mandrel, 95-tubular workpiece, 96-rigid ring sleeve, 97-ring sleeve gear, 98-thrust bearing, 100-mandrel base; in addition, the following features: 91-upper head lower square section Quadrangular prism, 92-rigid mandrel at the upper end of the square mandrel, 94-rigid mandrel at the lower end of the square section quadrangular prism, 99-core shaft base upper end square section recessed hole; (b) for assembly effect diagram.
  • Figure 11 is a cross-sectional optical microscopic metallographic diagram of a pure aluminum sample: (a) an initial extruded pure aluminum sample near the inner diameter of the anodic laminar polarized metallographic phase with an average grain size of about 40 ⁇ m; (b) high pressure shear After the deformation, the pure aluminum sample is close to the inner diameter of the anodic laminar polarized metallographic phase. The grain boundary of the deformed sample is not shown. No estimation of the average grain size is given, but it can be clearly seen that the grain is elongated and broken. Refined.
  • the material processing object of the present invention can be realized on a conventional extruder having a constant pressure function: the rigid ring is placed in the lower bottom plate or the lower pressing head plate.
  • the tapered tubular workpiece is placed coaxially in a rigid collar that is connected to the upper or upper ram at a centered position and passes through the center of the tapered tubular workpiece.
  • the rigid mandrel, the workpiece and the rigid ring sleeve are coaxially matched. After the rigid mandrel and rigid ring sleeve are coaxially assembled with the workpiece between the upper and lower plates (or indenters) of the press, displacement in the radial direction is not allowed (no horizontal displacement is allowed).
  • the axial pressure provided by the press is then transmitted to the inner wall of the workpiece by a rigid mandrel or rigid collar attached to the upper and lower base plates (or rams).
  • the inner wall of the workpiece is a small angle cone with respect to the axial direction.
  • the tubular workpiece generates a large pressure perpendicular to the inner or outer wall of the workpiece under the axial pressure.
  • the rigid ring sleeve and the mandrel constrain the radial deformation of the workpiece.
  • the invention enables the tubular material to undergo shear plastic deformation under high hydrostatic pressure (up to ⁇ 15 GPa) (true should be up to 10 ⁇ ). Thereby, the plastic structure is controlled to control and optimize the structure of the material and improve its performance.
  • the present invention only needs to install a simple combined mold composed of a rigid mandrel and a rigid ring sleeve on a conventional pressing device having a constant pressure function, that is, at a lower temperature (such as room temperature or lower).
  • the heating temperature achieves a new method of severe plastic deformation (SPD) processing - the use of the tipping principle (also known as the wedge effect or the principle of beveling force) to achieve high-pressure shearing of the pipe.
  • SPD severe plastic deformation
  • the technology is highly feasible, there are no special requirements for operation, and the required equipment is simple and easy to obtain.
  • the present invention is a new plastic working method realized by a conventional extrusion apparatus, the function of the conventional extrusion apparatus is expanded.
  • the invention is suitable for experimental research and industrial production of bulk ultrafine crystal and nanocrystalline materials prepared by vigorous plastic deformation.
  • high-performance metals, alloys, inorganic non-metallic materials, and polymer materials can be prepared.
  • the method of using the tip of the tip to realize the high-pressure shearing of the pipe has a shape of a cone-shaped tube, which has high practical application potential and value.
  • the present invention utilizes the tipping principle to realize the method of high pressure shearing of the pipe.
  • the workpiece is processed, and the shape is a tapered pipe, and the inner wall and the outer wall of the workpiece are respectively restrained by the restraining body; then the inner wall is passed through the inner wall.
  • the restraining body at the center applies axial main power to the inner wall of the workpiece (not shown in the constrained reaction force diagram).
  • the workpiece is generated under the action of axial pressure.
  • the implementation of the method principle also includes the manners of FIGS. 7(b), (c), (d) and the like.
  • the combination of these different implementations such as the simultaneous application of axial main power to both constraints or the simultaneous application of active torque in opposite directions to the two constraints, will also achieve this principle.
  • the specific text description and schematic diagram are omitted.
  • the invention utilizes a tipping principle to realize a device for high-pressure shearing of a pipe, comprising a press having a constant pressure function and a die having a transmission pressure, a constraining deformation and a rotating function;
  • the mold comprises: a fixed or rotatable rigid mandrel 1 And a rigid sleeve 2 which can be rotated or fixed;
  • the rigid mandrel 1 and the rigid collar 2 are respectively connected to the upper and lower bottom plates (or the upper and lower pressing heads) on the central axis of the press, and the tapered tubular workpiece 3 is the same
  • the shaft is placed between the rigid mandrel 1 and the rigid cuff 2, and the outer wall of the rigid mandrel 1 and the inner wall of the rigid cuff 2 are respectively in contact with the inner and outer walls of the workpiece 3, and the taper of the contact surface is equal;
  • the inner surface of the rigid cuff 2 is
  • the outer surface of the rigid mandrel 1 is subjected to
  • At least one of the rigid mandrel 1 or the rigid cuff 2 is rotatable about a central axis, and the angle of rotation is not limited.
  • the tubular material high-pressure shear deformation device of the present invention can adopt a single-layer mold design, a pre-stress winding mold design or a pre-stress multi-layer mold design.
  • the method of realizing the high-pressure shear of the pipe by the tipping principle (also called the wedge effect or the principle of the beveling force) is composed of a part including a 1-rigid mandrel and a 2-rigid ring.
  • the mold combined with a press with a pressure holding function, is realized on a 3-cone tubular workpiece.
  • the 2-rigid ring is placed in the lower or lower head pad.
  • a 3-tapered tubular workpiece is placed concentrically in a rigid collar that is connected to the upper or upper ram at a centered position and passes through the center of the 3-tapered tubular workpiece.
  • 1- rigid mandrel, 3-workpiece and 2-rigid ring set are coaxially matched.
  • the outer surface of the rigid mandrel is in contact with the inner wall of the 3-workpiece, and the inner surface of the 2-rigid collar is in contact with the outer wall of the 3-workpiece.
  • the press then presses the 1-rigid mandrel and maintains the pressure constant at a certain value.
  • axial pressure is generated on the inner wall of the 3-workpiece.
  • small-angle inclined surface or wedge surface, tapered surface, tip
  • the workpiece is axially pressurized.
  • this principle can also be achieved by making certain changes to the equipment or mold and changing the pressure and rotating mold parts.
  • Figure 7(d) Applying axial compression to the outer wall of the 3-workpiece using a 2-rigid collar, rotating the 1-rigid mandrel and fixing the 3-rigid collar provides similar shear plasticity to the tapered tubular material. Deformation effect.
  • the principle of the method of using the tip of the tip to realize the high-pressure shearing of the pipe is omitted.
  • Fig. 8 the end is unconstrained; (b) the end semi-constraint; (c) the end full constraint.
  • the 3-workpiece end is unconstrained, as shown in Fig. 8(a)
  • the flow of the 3-workpiece end material will be completely limited by the frictional force in the opposite direction to the material flow tendency; for the 3-workpiece end
  • the annular shoulder on the 1-mandrel and the annular shoulder on the 2-rigid ring respectively constrain the upper and lower ends of the 3-workpiece.
  • Figure 9(a) is an exploded view of the device, detailing the composition of the device.
  • 90-upper head, 93-rigid mandrel, 95-tubular workpiece, 96-rigid ring sleeve, 97-ring sleeve gear, 98-thrust bearing, 100-mandrel base form the principle realization part of the whole device.
  • the 96-rigid ring is placed on the lower bottom plate of the press and connected to the 98-thrust bearing between the bottom plate of the press.
  • the 98-thrust bearing receives the axial pressure from the 96-rigid ring and reduces the axial pressure.
  • the tapered 95-tube workpiece is placed concentrically in the 96-rigid collar.
  • 93-Rigid mandrel, 96-rigid ring sleeve and 95-workpiece are coaxially assembled between the upper and lower plates of the press, and no displacement in the radial direction is allowed (no horizontal displacement is allowed).
  • the 93-rigid mandrel then transfers the axial pressure provided by the press to the 95-worker inner wall through a 90-upper head attached to the upper plate of the press.
  • 95-The inner wall of the workpiece is a small angle cone with respect to the axial direction. According to the principle of small angle inclined surface (or wedge surface, cone surface, tip), the 95-tubular workpiece will be produced perpendicular to the inner wall or outer wall of the 95-workpiece.
  • the servo motor is used to drive the reducer gear set (the power unit adopts the conventional motor and gear set or the worm gear of the appropriate power and speed, the schematic diagram is omitted) to drive the 97-ring sleeve gear, and rotate it under the action of the torque.
  • the rotation speed is 1 ⁇ 5rpm. Due to the friction, the material at the 95-work outer wall will have a tendency to rotate with the 97-rigid collar.
  • the concave hole of the square end section of the upper end of the 92-rigid mandrel is constrained by the square cross section of the upper end of the 91-upper head, and the square prism of the lower end of the 94-rigid mandrel is constrained by the concave hole of the upper end of the 99-core shaft base, 95-
  • the material at the inner wall of the workpiece will have a tendency to be fixed together with the 93-rigid mandrel; under high hydrostatic pressure conditions, the material will remain continuous, and the 95-tubular workpiece will rotate at different angular velocities along different layers of the radial thickness. That is, relative rotation occurs, and the material is shear-driven under the driving of friction.
  • the 93-rigid mandrel adopts a design in which the upper and lower ends simultaneously constrain the rotational freedom.
  • the constraining method adopts two sets of square-section quadrangular prisms and square-section recessed holes (91-, 92-, and 94-, 99-).
  • the clearance fit is achieved.
  • the F7/h6 base shaft clearance fit and the H7/g6 base hole clearance fit are used between the two sets of square-section quadrangular prisms and square-section recessed holes (91-, 92- and 94-, 99-).
  • the 93-core shaft is easy to fix, on the other hand, the 93-core shaft is simultaneously subjected to force at both ends, and the fracture is broken due to excessive torque.
  • the 90-upper head does not directly contact the 95-tubular workpiece, and the pressure is 93-rigid mandrel directly transmitted to the inner wall of the workpiece.
  • This design is because the part directly in contact with the end face of the workpiece is subjected to a very bad force. It is necessary to add an annular gasket made of cemented carbide to increase the cost; on the other hand, when the end of the 95-workpiece is directly pressurized, due to friction The presence of pressure does not pass evenly to the middle of the 95-workpiece, causing insufficient pressure in the middle, often limiting the height of the 95-workpiece.
  • the method for realizing high-pressure shearing of the pipe by using the tip principle of the patent can effectively overcome the above disadvantages.
  • the inner layer selects materials with high hardness and toughness, such as die steel; the wound layer uses high toughness materials, such as spring steel wire or spring steel strip; the outer layer adopts toughness. Higher material, such as medium carbon steel.
  • the inner layer selects materials with higher hardness and toughness, such as die steel; the other layers select materials with higher toughness, such as medium carbon alloy steel or die steel.
  • the 92-rigid mandrel is inlaid with hard alloy, and the rest is made of die steel.
  • the mold steel is Cr5Mo1V steel
  • the spring steel is 65Mn steel
  • the medium carbon steel is 45 steel
  • the medium carbon alloy steel is 45Mn steel
  • the hard alloy is YG6A.
  • the assembled effect of the device for achieving high pressure shear of the pipe using the tip principle is as shown in Fig. 9(b).
  • the radial microhardness distribution of the industrial pure aluminum tubular workpiece after 25° shear deformation is shown in Figure 10: from near the inner diameter to near the outer diameter, the hardness is changed from 48 HV (0.025 kg) to 33. HV (0.025kg), showing a decreasing distribution trend, but higher than the initial sample 31 without high-pressure shear deformation Hardness around HV (0.025kg).
  • FIG. 11 The cross-section optical microscopic metallographic phase of the sample is shown in Figure 11:
  • Figure 11 (a) The initial extruded pure aluminum sample is observed near the inner diameter of the anodic lamination, and the average grain size is about 40 ⁇ m; (b) high-pressure shear deformation After the pure aluminum sample is close to the bright field phase at the inner diameter, some grain boundaries are not shown in the bright field phase, and the average grain size is not given. However, it can be clearly seen that the grain is elongated, broken and refined. (c) The microstructure of the pure aluminum sample from the inner diameter to the outer diameter after high-pressure shear deformation.
  • the average grain size of 6063 aluminum alloy before high pressure shear is 80 ⁇ m, the compression test yield strength is 156.8MPa; the high pressure shear deformation of 60o is achieved by the tipping principle of 2.5GPa hydrostatic pressure at 1rpm.
  • the average strain reaches 3.1.
  • the average grain size reached 746 nm, and the compression test yield strength increased to 402.6 MPa.
  • the plasticity of AZ31 magnesium alloy is poor, and we heat the mold at 100 °C.
  • the average grain size before the high pressure shear was 27 ⁇ m, the compression test yield strength was 276.4 MPa; the high pressure shear deformation of the tubular material achieved by the tip principle of 90° at a rotational speed of 1 rpm at 3 MPa hydrostatic pressure, the average strain reached 4.7, the average grain size reached 640 nm, and the compression test yield strength increased to 396.5 MPa.

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Abstract

A method of achieving high-pressure shearing deformation in tube materials by the wedge principle and an apparatus therefor. The method involves: selecting a workpiece to be processed (3), and using constraining bodies to respectively constrain the inner wall and the outer wall of the workpiece (3); exerting an axial pressure on the constraining bodies, increasing the axial force by taking advantage of the force amplifying principle of the wedge, and converting to a positive pressure in a direction perpendicular to a contact surface with the workpiece (3), thereby obtaining a high hydrostatic pressure inside the workpiece (3); providing a torque to one of the constraining bodies such that the constraining body rotates around a central axis of the workpiece (3), while fixing the other constraining body; or providing a torque to the two constraining bodies at the same time in opposite directions, such that the two constraining bodies rotate relatively around the central axis of the workpiece (3); and under the action of a tangential frictional force between the constraining bodies and the inner and outer walls of the workpiece (3), materials inside of the workpiece (3) at different radial thicknesses rotate at different angular velocities, achieving shearing deformation of the workpiece (3). Using the completely new plastic processing method implemented by conventional pressure devices expands the function of the conventional pressure devices, the feasibility thereof is high, operation thereof has no specific requirements, and the required device is simple.

Description

利用劈尖原理实现管材高压切变的方法及其装置  Method and device for realizing high pressure shear of pipe by using tip principle 技术领域Technical field
本发明涉及材料加工工程领域,特别是一种利用劈尖原理实现管状材料高压剪切塑性变形的方法及其装置,主要应用于各种金属及合金材料、无机非金属材料及高分子材料等,以实现这些材料在高静水压力条件下的塑性变形,从而控制和优化其组织结构,提高其性能。 The invention relates to the field of material processing engineering, in particular to a method and a device for realizing high-pressure shear plastic deformation of a tubular material by using a tipping principle, which are mainly applied to various metal and alloy materials, inorganic non-metal materials and polymer materials, etc. To achieve plastic deformation of these materials under high hydrostatic pressure conditions, thereby controlling and optimizing its microstructure and improving its performance.
背景技术Background technique
剧烈塑性变形(severe plastic deformation,简称SPD)方法是一系列具有大变形量的塑性加工技术的总称。SPD方法细化晶粒效果明显,可以将材料内部组织细化到亚微米级、纳米级甚至非晶态[R. Z. Valiev. Nature materials. 2004 (3): 511-516.; R. Z. Valiev, A. K. Mukherjee. Scripta mater. 2001 (44): 1747–1750.]。近年来,采用SPD方法制备块体纳米结构材料的技术受到了材料科学领域专家、学者们的普遍关注。与此同时,大量的研究推动SPD技术在制备块体超细晶、纳米晶材料方面的不断发展。俄罗斯Ufa航空技术大学的R.Z. Valiev领导的研究小组认为,采用SPD方法制备超细晶材料应满足多项条件[R. Z. Valiev, R. K. Islamgaliev, I V. Alexandrov. Progress in Materials Science.2000 (45): 103-189.],主要包括:大塑性变形量、相对低的变形温度和变形材料内部高的静水压力。在这一原则指导下,人们提出并开发了各种SPD工艺和方法。Severe plastic deformation The method of deformation (SPD) is a general term for a series of plastic processing techniques with large deformation. The SPD method refines the grain effect obviously, and can refine the internal structure of the material to sub-micron, nano-scale or even amorphous [R. Z. Valiev. Nature materials. 2004 (3): 511-516.; R. Z. Valiev, A. K. Mukherjee. Scripta mater. 2001 (44): 1747–1750.]. In recent years, the technology of preparing bulk nanostructured materials by SPD method has received widespread attention from experts and scholars in the field of materials science. At the same time, a large number of researches have promoted the continuous development of SPD technology in the preparation of bulk ultrafine crystals and nanocrystalline materials. R.Z., Ufa Aviation Technical University, Russia The research team led by Valiev believes that the preparation of ultrafine grained materials by SPD method should satisfy a number of conditions [R. Z. Valiev, R. K. Islamgaliev, I V. Alexandrov. Progress in Materials Science. 2000 (45): 103-189.], mainly includes: large plastic deformation, relatively low deformation temperature and high hydrostatic pressure inside the deformed material. Under the guidance of this principle, various SPD processes and methods have been proposed and developed.
目前最受关注的SPD方法主要是,累积轧制 (accumulative roll-bonding,简称ARB) 技术,等径角变形 (equal-channel angular pressing,简称ECAP) 技术,以及高压扭转 (high-pressure torsion,简称HPT) 技术等。其中ARB技术如图1所示,可连续制备薄板类超细晶结构材料,且易于在传统轧机上实现,设备简单,实际应用意义重大。但是,在ARB技术加工过程中,为了实现良好的轧制复合,往往不能使用润滑剂,这对轧辊的服役寿命不利。同时,由于材料在轧制过程中受到变形条件限制所能达到的静水压力不够高,在加工过程中累积一定的变形量后会出现开裂问题 [N. Tsuji, Y. Saito, S. H. Lee, et al. Advanced Engineering Materials. 2003 (5) :338-344.]。ECAP技术如图2所示,采用该技术进行超细晶金属加工处理具有巨大潜力。但是,对于一些难加工合金(如镁合金等),进行ECAP经常发生开裂,如果提高变形温度,一方面会影响模具寿命,另一方面又会影响晶粒细化效果。再加上由于模具材料的限制,变形温度不可能无限制地提高。而且ECAP为实现大的累积塑性变形,需要多道次加工,操作复杂。背压ECAP (back pressure equal-channel angular pressing,简称BP-ECAP) 即在模具出口通道施加背压的ECAP技术,如图3所示,可以在一定程度上解决难变形金属ECAP的开裂问题,从而改善材料的微观组织和机械性能;所施加的背压有限,静水压力一般维持在几百兆帕[R. YE. Lapovok. Journal of materials science. 2005 (40) :341-346.]。施加的背压太高则由于摩擦力和模具强度等因素而无法实现ECAP。HPT技术如图4所示,是最符合前文中提到的SPD方法制备超细晶材料应满足的多项条件。在现有的SPD技术之中,HPT技术晶粒细化能力最强。然而,HPT所能加工的试样厚度方向尺寸很小[A. P. Zhilyaev, T. G. Langdon. Progress in Materials Science. 2008 (53) :893-979.],所加工的盘状试样,沿径向存在较大的应变梯度,变形不均匀,晶粒细化程度也不均匀。The most popular SPD method at present is mainly cumulative rolling (accumulative Roll-bonding (abbreviated ARB) technology, equal-channel angular pressing (ECAP) technology, and high-pressure torsion (high-pressure torsion, referred to as HPT) Technology, etc. The ARB technology is shown in Figure 1. It can continuously prepare thin-plate ultrafine-grained structural materials, and is easy to implement on traditional rolling mills. The equipment is simple and practical. However, in the ARB process, in order to achieve good rolling compounding, lubricants are often not used, which is detrimental to the service life of the rolls. At the same time, the hydrostatic pressure that can be achieved due to the deformation of the material during the rolling process is not high enough, and cracking will occur after a certain amount of deformation is accumulated during the processing. [N. Tsuji, Y. Saito, S. H. Lee, et al. Advanced Engineering Materials. 2003 (5) :338-344.]. The ECAP technology is shown in Figure 2. The use of this technology for ultra-fine grain metal processing has great potential. However, for some difficult-to-machine alloys (such as magnesium alloys), ECAP often cracks. If the deformation temperature is increased, the life of the mold will be affected on the one hand, and the grain refining effect will be affected on the other hand. In addition, due to the limitation of the mold material, the deformation temperature cannot be increased without limitation. Moreover, in order to achieve large cumulative plastic deformation, ECAP requires multiple passes and the operation is complicated. Back pressure ECAP (back pressure equal-channel angular pressing, BP-ECAP for short) That is, the ECAP technology of applying back pressure in the exit channel of the mold, as shown in FIG. 3, can solve the cracking problem of the difficult-to-deform metal ECAP to a certain extent, thereby improving the microstructure and mechanical properties of the material; the applied back pressure is limited, and the still water is The pressure is generally maintained at several hundred megapascals [R. YE. Lapovok. Journal of materials science. 2005 (40) :341-346.]. If the applied back pressure is too high, ECAP cannot be achieved due to factors such as friction and mold strength. The HPT technology shown in Figure 4 is the most suitable condition for the preparation of ultrafine grained materials in accordance with the SPD method mentioned in the previous section. Among the existing SPD technologies, HPT technology has the strongest grain refinement capability. However, the thickness of the specimen that HPT can process is small [A. P. Zhilyaev, T. G. Langdon. Progress in Materials Science. 2008 (53) : 893-979.], the processed disc-shaped sample has a large strain gradient in the radial direction, the deformation is uneven, and the degree of grain refinement is not uniform.
Tóth等人[L.S. Tóth, M. Arzaghi, J.J. Fundenberger, B. Beausir: Scr. Mater. Vol. 60 (2009), p. 175]提出了一种管状材料高压扭转方法(high-pressure tube twisting,HPTT),如图5所示,在管状工件内部安放弹性芯棒,外侧套置刚性圆盘(rigid disk),试样两端用挡板固定。对芯棒加压时,芯棒径向膨胀对管状工件内壁产生径向压力,同时刚性圆盘对管状工件外壁产生一个相反方向的径向压力,从而在管状工件中产生静水压力。此时转动环套,管状工件在表面摩擦力作用下实现剪切变形。这种方法思路很好,其最主要的问题是该方法对试样的加载方式是径向加载方式,也就是说,该方法直接对芯棒施加轴向压力,芯棒在对试样产生径向压力。在这种加载方式下,压力并没有直接加载在管状材料的轴向,试样所承受的静水压力来自芯棒受压后的弹性变形,由于芯棒弹性变形不可能很大,很难产生高的静水压力,因而能提供的摩擦力有限,仅适用于强度较低的纯金属等。对于强度较高的材料,由于所能产生的摩擦力达不到材料的屈服强度,容易出现打滑等现象,无法实现所需要的变形。Tóth et al [L.S. Tóth, M. Arzaghi, J.J. Fundenberger, B. Beausir: Scr. Mater. Vol. 60 (2009), p. 175] proposes a high-pressure tube method for tubular materials (high-pressure tube) Twisting, HPTT), as shown in Figure 5, the elastic core rod is placed inside the tubular workpiece, and the rigid disc is placed on the outer side (rigid Disk), both ends of the sample are fixed with a baffle. When the mandrel is pressurized, the radial expansion of the mandrel creates radial pressure on the inner wall of the tubular workpiece, while the rigid disk creates a radial pressure in the opposite direction to the outer wall of the tubular workpiece, thereby creating hydrostatic pressure in the tubular workpiece. At this time, the ring sleeve is rotated, and the tubular workpiece is sheared under the surface friction. This method is very good. The main problem is that the method of loading the sample is radial loading. That is to say, the method directly applies axial pressure to the mandrel, and the mandrel produces a diameter on the sample. To the pressure. In this loading mode, the pressure is not directly loaded in the axial direction of the tubular material, and the hydrostatic pressure of the specimen is derived from the elastic deformation of the mandrel after being pressed. Since the elastic deformation of the mandrel is unlikely to be large, it is difficult to produce high The hydrostatic pressure, therefore, provides limited friction and is only suitable for pure metals with lower strength. For materials with higher strength, the frictional force that can be generated does not reach the yield strength of the material, and slipping and the like are likely to occur, and the required deformation cannot be achieved.
该方法另一方面问题是位于管状工件两端的档板是悬臂梁式结构,对试样轴向变形的约束不够,试样承受的静水压力较高时,材料很容易从缝隙中挤出,影响加工过程。Another problem with the method is that the baffle at the two ends of the tubular workpiece is a cantilever beam structure, and the constraint on the axial deformation of the sample is insufficient. When the hydrostatic pressure of the sample is high, the material is easily extruded from the gap, affecting Processing process.
本发明提出了一种利用劈尖原理实现管状材料高压剪切变形的技术,该技术所应用的劈尖(wedge)原理,又称楔效应或者斜面增力原理。该原理可以用拉密定理(Lami's theorem)来进行解释:在同一平面内,当三个共点力的合力为零时,其中任一个力与其它两个力夹角正弦的比值相等[R.K. Bansal (2005). Laxmi Publications. p. 4.]。劈尖或者斜楔的小角度斜面可以看做力放大装置,如图5所示,当对劈尖相对的一端施加力时,与构成劈尖的斜面相接触的物体将会受到远大于施加力的正压力[Sybil P. Parker, ed., McGraw-Hill, Inc., 1992, p. 2041.]。这种设计与Tóth等人提出的一种管状材料高压扭转方法相比,能在试样中更加有效地产生高静水压力。The invention proposes a technology for realizing high-pressure shear deformation of a tubular material by using the tip principle, and the principle of the wedge applied by the technology is also called the wedge effect or the principle of the beveling force. This principle can be used with the Lamy's theorem (Lami's Theorem) to explain: in the same plane, when the resultant force of the three co-point forces is zero, the ratio of any one of the forces to the sine of the other two forces is equal [R.K. Bansal (2005). Laxmi Publications. p. 4.]. The small angled bevel of the tip or wedge can be seen as a force amplifying device. As shown in Figure 5, when a force is applied to the opposite end of the tip, the object in contact with the bevel forming the tip will be much larger than the applied force. Positive pressure [Sybil P. Parker, ed., McGraw-Hill, Inc., 1992, p. 2041.]. This design produces a higher hydrostatic pressure in the sample more effectively than the high pressure torsion method of the tubular material proposed by Tóth et al.
技术问题technical problem
本发明的目的在于提供一种新的剧烈塑性变形方法及其装置:利用劈尖原理实现管材高压切变的技术。本发明实现高静水压力利用了劈尖原理的力放大效应,使得该技术很好地满足了采用SPD方法制备超细晶材料应满足的多项条件,如大塑性变形量、相对低的变形温度和变形材料内部高的静水压力。该方法避免了ARB、ECAP以及背压ECAP等技术需要多道次操作的繁琐工艺过程,同时,由于加载方式本质上的不同,该方法也克服了Tóth等人HPTT法静水压力不足等问题,在加工材料时能提供类似HPT技术的高静水压力条件,从而适用于对难变形金属及合金的加工,达到控制和优化材料的组织结构、提高其性能的效果。 It is an object of the present invention to provide a new severe plastic deformation method and apparatus therefor: a technique for achieving high pressure shear of a pipe using a tip end principle. The high hydrostatic pressure of the invention utilizes the force amplification effect of the tip principle, so that the technology satisfies many conditions that should be satisfied by the SPD method for preparing the ultrafine grain material, such as large plastic deformation amount and relatively low deformation temperature. And the high hydrostatic pressure inside the deformed material. The method avoids the complicated process of multi-channel operation such as ARB, ECAP and back pressure ECAP. At the same time, due to the different nature of the loading method, the method also overcomes the problems of insufficient hydrostatic pressure of Tóth et al. When processing materials, it can provide high hydrostatic pressure conditions similar to HPT technology, which is suitable for the processing of difficult-to-deform metals and alloys, to achieve the effect of controlling and optimizing the structure of the material and improving its performance.
技术解决方案Technical solution
实现本发明目的的技术解决方案为:一种利用劈尖原理实现管材高压切变的方法,首先选择加工的工件,工件为带有锥度的管状,采用约束体分别约束工件的内壁和外壁;然后对约束体之一端部施加轴向压力,利用劈尖原理(也称楔效应或者斜面增力原理)的增压、增力特性,在垂直于工件内外壁的方向产生高压,使得工件发生弹性变形或微小塑性变形,工件的变形受到与变形趋势反向摩擦力的阻碍,从而,在工件内产生高静水压力;随后对与工件内、外壁接触的一个约束体提供扭矩,使其绕工件的中心轴转动,同时固定另一个约束体;或者同时对两个约束体提供方向相反的扭矩,在约束体与工件内外壁摩擦力的作用下,工件内部沿径向不同厚度处的材料以不同的角速度转动,从而实现工件的剪切变形。The technical solution for achieving the object of the present invention is: a method for realizing high-pressure shearing of a pipe by using a tipping principle, first selecting a machined workpiece, the workpiece is a tapered pipe, and the inner wall and the outer wall of the workpiece are respectively restrained by the restraining body; Applying axial pressure to one end of the restraining body, using the pressure-increasing and force-increasing characteristics of the tipping principle (also called the wedge effect or the principle of the beveling force), a high pressure is generated in a direction perpendicular to the inner and outer walls of the workpiece, so that the workpiece is elastically deformed. Or slight plastic deformation, the deformation of the workpiece is hindered by the reverse frictional force with the deformation trend, thereby generating a high hydrostatic pressure in the workpiece; then providing a torque to a restraining body in contact with the inner and outer walls of the workpiece to surround the center of the workpiece The shaft rotates while fixing the other restraint body; or the opposite direction torque is provided to the two restraint bodies at the same time. Under the action of the frictional force between the restraining body and the inner and outer walls of the workpiece, the materials at different thicknesses in the radial direction of the workpiece have different angular velocities. Rotate to achieve shear deformation of the workpiece.
一种利用劈尖原理实现管材高压切变的装置,包括具有恒压功能的压力机、提供扭矩的减速器和具有传递压力、约束形变以及实现部分旋转功能的模具;所述模具包括:固定或者可转动的刚性芯轴以及可转动或者固定的刚性环套;工件同轴放置于刚性环套内,刚性环套内表面与工件的外壁接触,工件的内部同轴设有刚性芯轴,刚性芯轴外表面与工件的内壁接触,刚性芯轴和刚性环套分别沿中轴线安装或放置在压力机的上底板和下底板上,并且刚性环套及刚性芯轴的位移被限制,只能沿轴向移动或者绕中心轴转动。A device for realizing high-pressure shearing of a pipe by using a tipping principle, comprising a press having a constant pressure function, a torque reducer providing torque, and a mold having a transfer pressure, a constraining deformation, and a partial rotation function; the mold includes: fixed or a rotatable rigid mandrel and a rotatable or fixed rigid collar; the workpiece is coaxially placed in the rigid collar, the inner surface of the rigid collar is in contact with the outer wall of the workpiece, and the interior of the workpiece is coaxially provided with a rigid mandrel, rigid core The outer surface of the shaft is in contact with the inner wall of the workpiece, and the rigid mandrel and the rigid ring sleeve are respectively mounted along the central axis or placed on the upper and lower bottom plates of the press, and the displacement of the rigid ring sleeve and the rigid mandrel is limited, only along Move axially or around the central axis.
有益效果Beneficial effect
本发明与现有技术相比,其显著优点:(1)加工工序简单。本发明提出的利用劈尖原理实现管材高压切变的方法是一种在常规的具有恒压功能的压力设备上单一道次即可实现的剧烈塑性变形方法。反观诸如累积轧制(ARB)方法、多向锻造、等径角挤压(ECAP)方法以及背压ECAP方法等,往往需要很多重复的工艺道次才能实现高应变量的塑性变形,人力消耗大。而本方法利用刚性环套、管状工件以及芯轴、管状工件之间摩擦力,使刚性环套与刚性芯轴发生相对转动,实现管状工件与刚性环套接触的外层区域相对于与芯轴接触的内层区域之间的剪切,从而实现单一工艺道次下的剧烈塑性变形。真应变为1~10,甚至更高。如前文技术方案所述,本发明提出的剧烈塑性变形方法原理简单,设备易得,在一般的压力加工工厂以及塑性成形实验室即可实现。Compared with the prior art, the invention has significant advantages: (1) the processing procedure is simple. The method for realizing high-pressure shearing of pipe by using the tip principle of the invention is a severe plastic deformation method which can be realized in a single pass on a conventional pressure device having a constant pressure function. In contrast, such as cumulative rolling (ARB) method, multi-directional forging, equal-angle extrusion (ECAP) method and back pressure ECAP method, etc., often require a lot of repeated process passes to achieve high strain plastic deformation, labor consumption . The method utilizes the friction between the rigid ring sleeve, the tubular workpiece and the mandrel and the tubular workpiece, so that the rigid ring sleeve and the rigid mandrel rotate relative to each other, and the outer layer region of the tubular workpiece contacting the rigid ring sleeve is opposite to the mandrel. Shearing between the inner regions of the contact, thereby achieving severe plastic deformation under a single process pass. The true strain is 1~10 or even higher. As described in the foregoing technical solution, the method of the severe plastic deformation proposed by the present invention is simple in principle and easy to obtain, and can be realized in a general pressure processing factory and a plastic forming laboratory.
(2)利用劈尖原理的斜面增力效果,很容易在管状工件内部产生高静水压力,因此可加工材料种类广,加工能力强。如前文背景技术所述,本发明提出的高压剪切方法,并没有直接对管状材料轴向加压,同时也没有对工件端部进行约束,因而,不存在工件过长后可能出现的中部压力不足、加压失稳等问题。可在材料内部较均匀地产生静水压力,可达15GPa。这是目前包括HPTT在内其它工艺无法达到的。而且,随着模具材料的发展,设计的改进,所能提供的静水压力会更高。在这种高静水压力条件下进行塑性变形,材料表面和内部裂纹的产生和发展被有效抑制,从而使得很多难加工材料(如塑性较差的镁合金等)的可加工性提高。众所周知,镁合金等材料由于晶体结构为密排六方,滑移系数量有限,往往塑性差。对镁合金等难变形材料进行ARB或者ECAP加工时,试样经常有开裂现象。为避免开裂,往往需要提高加工温度,势必增加加工成本,更重要的是,随着加工温度的升高,材料的晶粒细化效果变差,晶粒变得粗大,这与我们提高材料性能的初衷相左。相比之下,本方法在室温条件或者较低的加热温度下即可实现对铝、铜、镍、镁、钛、钨及其合金以及低碳钢等众多材料的塑性加工,从而控制和改善其组织结构,提高其性能。(2) It is easy to generate high hydrostatic pressure inside the tubular workpiece by using the beveling effect of the tipping principle, so that the material can be processed widely and the processing ability is strong. As described in the background art above, the high-pressure shearing method proposed by the present invention does not directly pressurize the tubular material axially, and does not restrain the end of the workpiece. Therefore, there is no central pressure that may occur after the workpiece is too long. Insufficient, pressure instability and other issues. Hydrostatic pressure can be generated more evenly inside the material up to 15 GPa. This is currently not possible with other processes including HPTT. Moreover, with the development of mold materials and the improvement of design, the hydrostatic pressure that can be provided will be higher. Plastic deformation under such high hydrostatic pressure conditions effectively suppresses the generation and development of material surfaces and internal cracks, thereby improving the workability of many difficult-to-machine materials such as magnesium alloys with poor plasticity. It is well known that materials such as magnesium alloys are densely packed due to the crystal structure, and the slip coefficient is limited, and the plasticity is often poor. When ARB or ECAP is processed on difficult-to-deform materials such as magnesium alloy, the sample often cracks. In order to avoid cracking, it is often necessary to increase the processing temperature, which will inevitably increase the processing cost. More importantly, as the processing temperature increases, the grain refining effect of the material becomes worse and the grains become coarser, which improves the material properties. The original intention is opposite. In contrast, the method can achieve plastic processing of many materials such as aluminum, copper, nickel, magnesium, titanium, tungsten and their alloys, and low carbon steel at room temperature or at a lower heating temperature, thereby controlling and improving. Its organizational structure improves its performance.
(3)能够获得的管状成品尺寸大。本发明提出的利用劈尖原理实现管材高压切变的方法选取的加工工件呈管状,其尺寸仅受设备规模限制。即便是在实验室,也可通过该方法制得~100mm高的管状材料,具有良好的性能,稍做后续处理即可在很多领域得到应用,此外获得的管状材料沿轴向剖开,经过轧制即可获得高性能板材。(3) The size of the tubular product that can be obtained is large. The method for realizing the high-pressure shearing of the pipe by using the tipping principle of the invention has a tubular shape, and the size thereof is limited only by the scale of the equipment. Even in the laboratory, the tubular material of ~100mm height can be obtained by this method, which has good performance and can be applied in many fields after a little subsequent treatment. In addition, the obtained tubular material is cut along the axial direction and is rolled. High performance sheeting is obtained.
附图说明DRAWINGS
图1是累积复合轧制(ARB)技术原理示意图。Figure 1 is a schematic diagram of the principle of cumulative composite rolling (ARB) technology.
图2是等径角挤压(ECAP)技术原理示意图。Figure 2 is a schematic diagram of the principle of equal channel angular extrusion (ECAP) technology.
图3是背压ECAP(BP-ECAP)技术原理示意图。Figure 3 is a schematic diagram of the principle of back pressure ECAP (BP-ECAP) technology.
图4是高压扭转(HPT)技术原理示意图。Figure 4 is a schematic diagram of the principle of high voltage torsion (HPT) technology.
图5是高压管扭转(high-pressure tube twisting-HPTT)技术原理示意图。Figure 5 is a high-pressure tube twist Twisting-HPTT) Schematic diagram of the technical principle.
图6是劈尖原理(或称楔效应、斜面力放大原理)示意图,所谓的劈尖原理如图2所示,输入力为P,输出力N+N'=P/sinθ,其中θ为半锥角,θ较小时,输出力N+N'≈P/θ。这种利用斜面增力原理对管状工件加压的方式,加载相对均匀,模具或者工件不易在加压的过程中失稳。Figure 6 is a schematic diagram of the tip principle (or wedge effect, ramping force amplification principle). The so-called tip principle is shown in Figure 2. The input force is P, and the output force is N+N'=P/sinθ, where θ is half. Cone angle, when θ is small, the output force N+N'≈P/θ. This method of pressing the tubular workpiece by the principle of the inclined surface force is relatively uniform in loading, and the mold or the workpiece is not easily destabilized during the pressurization process.
图7(a)至图7(d)是本发明利用劈尖原理实现管材高压切变的方法原理示意图,其中,1-刚性芯轴,2-刚性环套,3-带有锥度的管状工件;h为管状工件高度;ri、re分别为管状工件下端面的内、外半径;θ为半锥角;P为压力机提供的主动力;T为动力装置提供的主动扭矩。约束反力和约束反扭矩未标出;管状试样高压切变通过对刚性环套及芯轴施加图8所示的主动力及主动扭矩或者其组合方式实现(图中两种主动力方向相反,分别作用在刚性芯轴和环套上;两种主动扭矩方向相反,分别作用在刚性环套和芯轴上)。7(a) to 7(d) are schematic diagrams showing the principle of the method for realizing high-pressure shearing of pipes by using the tip principle of the present invention, wherein 1-rigid mandrel, 2-rigid ring sleeve, 3-tube workpiece with taper h is the height of the tubular workpiece; r i , r e are the inner and outer radii of the lower end surface of the tubular workpiece; θ is the half cone angle; P is the main power provided by the press; T is the active torque provided by the power unit. The constrained reaction force and the constrained counter torque are not marked; the high pressure shear of the tubular specimen is achieved by applying the main power and the active torque shown in Figure 8 to the rigid collar and the mandrel or a combination thereof (the two main power directions are opposite in the figure). , respectively, acting on the rigid mandrel and the collar; the two active torques are opposite in direction, acting on the rigid collar and the mandrel respectively).
图8(a)至图(c)是本发明工件端部的几种约束形式示意图:工件的内外壁始终被1-刚性芯轴和2-刚性环套约束,(a)端部无约束;(b)端部半约束;(c)端部全约束。8(a) to (c) are schematic views of several constraint forms of the end portion of the workpiece of the present invention: the inner and outer walls of the workpiece are always constrained by a 1-rigid mandrel and a 2-rigid cuff, and (a) the end is unconstrained; (b) end semi-constraint; (c) end full constraint.
图9是利用劈尖原理实现管材高压切变的方法具体实施案例的装置示意图,其中,(a)为爆炸视图:90-上压头, 93-刚性芯轴,95-管状工件,96-刚性环套,97-环套外套齿轮,98-推力轴承,100-芯轴底座;此外,还有以下特征:91-上压头下端方形截面四棱柱,92-刚性芯轴上端方形截面凹孔,94-刚性芯轴下端方形截面四棱柱,99-芯轴底座上端方形截面凹孔;(b)为装配效果图。9 is a schematic view of a device for implementing a method for realizing high-pressure shearing of a pipe by using a tipping principle, wherein (a) is an exploded view: 90-upper head, 93-rigid mandrel, 95-tubular workpiece, 96-rigid ring sleeve, 97-ring sleeve gear, 98-thrust bearing, 100-mandrel base; in addition, the following features: 91-upper head lower square section Quadrangular prism, 92-rigid mandrel at the upper end of the square mandrel, 94-rigid mandrel at the lower end of the square section quadrangular prism, 99-core shaft base upper end square section recessed hole; (b) for assembly effect diagram.
图10是尺寸为高30mm,半锥角10°,下端面半径ri=10mm,re=14mm,的工业纯铝管状工件经过25°剪切变形后的沿径向显微硬度分布图:从靠近内径处到靠近外径处,硬度由48 HV(0.025kg)变为33 HV(0.025kg),呈递减分布趋势,但均高于初始未经过高压剪切变形的试样31 HV(0.025kg)左右的硬度。Fig. 10 is a radial microhardness distribution diagram of an industrial pure aluminum tubular workpiece having a height of 30 mm, a half cone angle of 10°, a lower end surface radius r i = 10 mm, and r e = 14 mm after 25° shear deformation: From near the inner diameter to the outer diameter, the hardness changed from 48 HV (0.025kg) to 33 HV (0.025kg), showing a decreasing distribution trend, but higher than the sample 31 HV (0.025) which was not subjected to high-pressure shear deformation. Kg) hardness around.
图11为纯铝试样横截面光学显微金相图:(a)初始挤压态纯铝试样靠近内径处阳极复膜偏光金相,平均晶粒尺寸约40μm;(b)经过高压剪切变形后纯铝试样靠近内径处阳极复膜偏光金相,变形后的试样晶界未显示,没有给出平均晶粒尺寸的估算值,但可以明显看出晶粒被拉长、破碎、细化。Figure 11 is a cross-sectional optical microscopic metallographic diagram of a pure aluminum sample: (a) an initial extruded pure aluminum sample near the inner diameter of the anodic laminar polarized metallographic phase with an average grain size of about 40 μm; (b) high pressure shear After the deformation, the pure aluminum sample is close to the inner diameter of the anodic laminar polarized metallographic phase. The grain boundary of the deformed sample is not shown. No estimation of the average grain size is given, but it can be clearly seen that the grain is elongated and broken. Refined.
本发明的实施方式Embodiments of the invention
本发明的材料加工目的在传统的具有恒压功能的挤压机上即可实现:刚性环套居中放置在下底板或者下压头垫板上。带有锥度的管状工件同轴放置于的刚性环套中,刚性芯轴与上底板或者上压头在居中位置相连,并从带有锥度的管状工件的中心穿过。刚性芯轴、工件以及刚性环套三者同轴配合。刚性芯轴、刚性环套与工件同轴装配在压力机的上、下底板(或压头)之间后,不允许沿径向发生位移(不允许产生水平位移)。然后,通过与上、下底板(或压头)相连的刚性芯轴或刚性环套将压力机提供的轴向压力传递给工件内壁。工件内壁相对于轴向为小角度锥面,根据小角度斜面(或称楔、锥面、劈尖)力放大原理,管状工件在轴向压力的作用下产生垂直于工件内壁或外壁的巨大压力。刚性环套、芯轴对工件径向变形起到约束作用。同时,工件受压后有沿刚性环套与芯轴之间缝隙向外流动的趋势。此时,利用工件与刚性环套以及刚性芯轴接触面上产生的摩擦力,或者在工件端部添加约束,阻碍物质流动。这种对管状工件内、外壁施加高压,并同时限制其形变和流动的设计使得在工件内部累加了高静水压力(1GPa~15GPa)。高静水压力条件下,虽然管状工件形状改变被限制,但其有绕中心轴旋转的自由度。如果使与工件内壁或者外壁接触的约束体(分别为芯轴和刚性环套)中的一个绕工件的中心轴转动而另外一个固定,由于工件的内、外壁与设备约束体之间巨大摩擦力存在,工件内、外壁附近的材料有随约束体一起转动或者固定不动的趋势。高静水压力条件下,为了保持材料的连续性,管状工件沿径向不同厚度层的材料将以不同的角速度转动,即发生相对转动,材料在摩擦力的驱动下实现剪切变形。The material processing object of the present invention can be realized on a conventional extruder having a constant pressure function: the rigid ring is placed in the lower bottom plate or the lower pressing head plate. The tapered tubular workpiece is placed coaxially in a rigid collar that is connected to the upper or upper ram at a centered position and passes through the center of the tapered tubular workpiece. The rigid mandrel, the workpiece and the rigid ring sleeve are coaxially matched. After the rigid mandrel and rigid ring sleeve are coaxially assembled with the workpiece between the upper and lower plates (or indenters) of the press, displacement in the radial direction is not allowed (no horizontal displacement is allowed). The axial pressure provided by the press is then transmitted to the inner wall of the workpiece by a rigid mandrel or rigid collar attached to the upper and lower base plates (or rams). The inner wall of the workpiece is a small angle cone with respect to the axial direction. According to the principle of force amplification of the small angle slope (or wedge, cone, tip), the tubular workpiece generates a large pressure perpendicular to the inner or outer wall of the workpiece under the axial pressure. . The rigid ring sleeve and the mandrel constrain the radial deformation of the workpiece. At the same time, after the workpiece is pressed, there is a tendency to flow outward along the gap between the rigid collar and the mandrel. At this time, the friction generated by the contact surface between the workpiece and the rigid collar and the rigid mandrel, or the addition of a constraint at the end of the workpiece, hinders the flow of the substance. This design of applying high pressure to the inner and outer walls of the tubular workpiece while limiting its deformation and flow causes a high hydrostatic pressure (1 GPa to 15 GPa) to be accumulated inside the workpiece. Under high hydrostatic pressure conditions, although the shape change of the tubular workpiece is limited, it has a degree of freedom of rotation about the central axis. If one of the restraining bodies (the mandrel and the rigid collar, respectively) in contact with the inner wall or the outer wall of the workpiece is rotated about the central axis of the workpiece and the other is fixed, due to the large friction between the inner and outer walls of the workpiece and the device restraint There is a tendency for the material in the vicinity of the inner and outer walls of the workpiece to rotate or remain stationary with the binding body. Under high hydrostatic pressure conditions, in order to maintain the continuity of the material, the material of the tubular workpiece in different thickness layers in the radial direction will rotate at different angular velocities, that is, relative rotation occurs, and the material is sheared under the driving of friction.
本发明能使管状材料真正在高静水压力(可达~15GPa)条件下,发生剪切塑性变形(真应可达10~)。从而通过塑性变形,控制和优化材料的组织结构、提高其性能。The invention enables the tubular material to undergo shear plastic deformation under high hydrostatic pressure (up to ~15 GPa) (true should be up to 10~). Thereby, the plastic structure is controlled to control and optimize the structure of the material and improve its performance.
同时,本发明只需要在传统的具有恒压功能的挤压设备上安装一个由刚性芯轴以及刚性环套等关键要素构成的简单组合模具,即可在较低的温度(如室温或者较低的加热温度)实现一种全新的剧烈塑性变形(SPD)加工方法——利用劈尖原理(也称楔效应或者斜面增力原理)实现管材高压切变的技术。该技术可行性高,操作无特殊要求,所需设备简单易得。同时,由于本发明是依托传统挤压设备实现的新的塑性加工方法,因此扩展了传统挤压设备的功用。本发明适用于剧烈塑性变形制备块体超细晶、纳米晶材料的实验研究和工业生产。利用本发明,可以制备高性能金属、合金、无机非金属材料及高分子材料。利用劈尖原理实现管材高压切变的方法,起制得的样品形状为锥管状,具有很高的实际应用潜力和价值。At the same time, the present invention only needs to install a simple combined mold composed of a rigid mandrel and a rigid ring sleeve on a conventional pressing device having a constant pressure function, that is, at a lower temperature (such as room temperature or lower). The heating temperature) achieves a new method of severe plastic deformation (SPD) processing - the use of the tipping principle (also known as the wedge effect or the principle of beveling force) to achieve high-pressure shearing of the pipe. The technology is highly feasible, there are no special requirements for operation, and the required equipment is simple and easy to obtain. At the same time, since the present invention is a new plastic working method realized by a conventional extrusion apparatus, the function of the conventional extrusion apparatus is expanded. The invention is suitable for experimental research and industrial production of bulk ultrafine crystal and nanocrystalline materials prepared by vigorous plastic deformation. With the present invention, high-performance metals, alloys, inorganic non-metallic materials, and polymer materials can be prepared. The method of using the tip of the tip to realize the high-pressure shearing of the pipe has a shape of a cone-shaped tube, which has high practical application potential and value.
下面结合附图对本发明作进一步详细描述。The invention is further described in detail below with reference to the accompanying drawings.
结合图7(a),本发明利用劈尖原理实现管材高压切变的方法,首先选择加工的工件,其形状为带有锥度的管状,采用约束体分别约束工件的内壁和外壁;然后通过内壁处的约束体对工件内壁施加轴向主动力(约束反力图中未给出),根据小角度斜面(或称楔、锥面、劈尖)力放大原理,工件在轴向压力的作用下产生垂直于工件内壁的巨大压力;约束体对工件径向变形起到约束作用;同时,利用工件与刚性环套以及刚性芯轴接触面上产生的摩擦力,或者在工件端部添加约束,阻碍物质流动;这种对工件内壁施加高压,并同时限制其形变和流动的设计使得在工件内部累加了高静水压力(1GPa~15GPa);随后对与工件外壁接触的约束体提供主动扭矩(约束反扭矩图中未给出),使其绕工件的中心轴转动,同时使得与工件内壁接触的约束体不发生转动,在约束体与工件内外壁摩擦力的作用下,工件内部沿径向不同厚度处的材料以不同的角速度转动,从而实现工件的剪切变形。Referring to Fig. 7(a), the present invention utilizes the tipping principle to realize the method of high pressure shearing of the pipe. First, the workpiece is processed, and the shape is a tapered pipe, and the inner wall and the outer wall of the workpiece are respectively restrained by the restraining body; then the inner wall is passed through the inner wall. The restraining body at the center applies axial main power to the inner wall of the workpiece (not shown in the constrained reaction force diagram). According to the principle of force amplification of the small angle inclined surface (or wedge, cone surface, tip), the workpiece is generated under the action of axial pressure. A large pressure perpendicular to the inner wall of the workpiece; the restraining body acts to restrain the radial deformation of the workpiece; at the same time, the friction generated by the contact surface between the workpiece and the rigid collar and the rigid mandrel, or the constraint at the end of the workpiece, hinders the substance Flow; this design that applies high pressure to the inner wall of the workpiece while limiting its deformation and flow causes a high hydrostatic pressure (1GPa~15GPa) to be accumulated inside the workpiece; then the active torque is supplied to the constraining body in contact with the outer wall of the workpiece (constrained anti-torque) Not shown in the figure), it rotates around the central axis of the workpiece, and at the same time, the constraint body that is in contact with the inner wall of the workpiece does not rotate, in the constraint The inner and outer walls of the workpiece frictional force, along the inside of the workpiece material at a radially varying thickness in different angular speed, in order to achieve the shear deformation of the workpiece.
类似地,根据施加主动扭矩和轴向主动力的约束体不同,该方法原理的实现还包括图7(b)、(c)、(d)等方式。不仅如此,这些不同实现方式的组合方式,比如:同时对两个约束体都施加轴向主动力或者同时对两个约束体施加相反方向的主动扭矩等,也将实现本原理。具体文字描述及示意图从略。Similarly, depending on the constraint body to which the active torque and the axial main power are applied, the implementation of the method principle also includes the manners of FIGS. 7(b), (c), (d) and the like. Moreover, the combination of these different implementations, such as the simultaneous application of axial main power to both constraints or the simultaneous application of active torque in opposite directions to the two constraints, will also achieve this principle. The specific text description and schematic diagram are omitted.
本发明利用劈尖原理实现管材高压切变的装置,包括具有恒压功能的压力机和具有传递压力、约束形变以及实现旋转功能的模具;所述模具包括:固定或者可转动的刚性芯轴1以及可转动或者固定的刚性环套2;刚性芯轴1和刚性环套2在压力机的中轴线上分别与其上、下底板(或上、下压头)相联,锥管状的工件3同轴放置于刚性芯轴1和刚性环套2之间,刚性芯轴1的外壁和刚性环套2的内壁分别与工件3的内外壁接触,接触面的锥度相等;刚性环套2内表面与刚性芯轴1外表面经过特殊的毛化处理以控制与工件3之间的摩擦符合工艺要求。The invention utilizes a tipping principle to realize a device for high-pressure shearing of a pipe, comprising a press having a constant pressure function and a die having a transmission pressure, a constraining deformation and a rotating function; the mold comprises: a fixed or rotatable rigid mandrel 1 And a rigid sleeve 2 which can be rotated or fixed; the rigid mandrel 1 and the rigid collar 2 are respectively connected to the upper and lower bottom plates (or the upper and lower pressing heads) on the central axis of the press, and the tapered tubular workpiece 3 is the same The shaft is placed between the rigid mandrel 1 and the rigid cuff 2, and the outer wall of the rigid mandrel 1 and the inner wall of the rigid cuff 2 are respectively in contact with the inner and outer walls of the workpiece 3, and the taper of the contact surface is equal; the inner surface of the rigid cuff 2 is The outer surface of the rigid mandrel 1 is subjected to a special texturing treatment to control the friction with the workpiece 3 in accordance with the process requirements.
本发明管状材料高压剪切变形装置,所述刚性芯轴1或者刚性环套2之中至少有一个可绕中心轴转动,转动的角度无限制。In the tubular material high-pressure shear deformation device of the present invention, at least one of the rigid mandrel 1 or the rigid cuff 2 is rotatable about a central axis, and the angle of rotation is not limited.
本发明管状材料高压剪切变形装置,所述刚性环套2可采用单层模具设计、预应力缠绕模具设计或预应力多层模具设计。The tubular material high-pressure shear deformation device of the present invention can adopt a single-layer mold design, a pre-stress winding mold design or a pre-stress multi-layer mold design.
下面结合图7(a)说明依据本发明提出的剧烈塑性变形新方法具体实施细节及设备工作情况。The specific implementation details and equipment operation of the new method of severe plastic deformation proposed in accordance with the present invention will be described below with reference to FIG. 7(a).
如图7(a)所示,利用劈尖原理(也称楔效应或者斜面增力原理)实现管材高压切变的方法由一个包括1-刚性芯轴、2-刚性环套等几部分构成的模具,结合具有保压功能的压力机,在3-锥管状工件上实现。As shown in Fig. 7(a), the method of realizing the high-pressure shear of the pipe by the tipping principle (also called the wedge effect or the principle of the beveling force) is composed of a part including a 1-rigid mandrel and a 2-rigid ring. The mold, combined with a press with a pressure holding function, is realized on a 3-cone tubular workpiece.
首先,2-刚性环套居中放置在下底板或者下压头垫板上。将3-带有锥度的管状工件同心放置于的刚性环套中,1-刚性芯轴与上底板或者上压头在居中位置相连,并从3-带有锥度的管状工件的中心穿过。1-刚性芯轴、3-工件以及2-刚性环套三者同轴配合。1-刚性芯轴外表面与3-工件的内壁接触,2-刚性环套内表面与3-工件的外壁接触。First, the 2-rigid ring is placed in the lower or lower head pad. A 3-tapered tubular workpiece is placed concentrically in a rigid collar that is connected to the upper or upper ram at a centered position and passes through the center of the 3-tapered tubular workpiece. 1- rigid mandrel, 3-workpiece and 2-rigid ring set are coaxially matched. 1- The outer surface of the rigid mandrel is in contact with the inner wall of the 3-workpiece, and the inner surface of the 2-rigid collar is in contact with the outer wall of the 3-workpiece.
然后,压力机对1-刚性芯轴进行下压,并维持压力恒定于某一数值。1-刚性芯轴向下位移的过程中,对3-工件内壁产生轴向压力,根据小角度斜面(或称楔面、锥面、劈尖)力放大原理,3-工件在轴向压力的作用下产生垂直于内壁的巨大压力;1-刚性芯轴与2-刚性环套对3-工件径向变形起到约束作用;同时,3-工件有沿1-刚性芯轴、2-刚性环套之间缝隙向外流动的趋势;从而在3-工件与1-刚性芯轴以及2-刚性环套的接触面,会产生与物质流动趋势相反方向的摩擦力,阻碍物质流动;这种对3-工件内壁施加高压,并同时限制其形变和流动的设计使得在3-工件内部产生高静水压力(可高达15GPa)。对2-刚性环套施加切向推力,在扭矩的作用下使之旋转,与此同时,1-刚性芯轴不发生旋转,在2-刚性环套与3-工件以及1-芯轴与3-工件之间摩擦力的作用下,3-工件将沿切向发生剪切变形。随着旋转角度的增大,剪切变形量累积增大,从而有效地控制和优化材料的组织结构,提高其性能。The press then presses the 1-rigid mandrel and maintains the pressure constant at a certain value. 1-In the process of axially lower displacement of the rigid core, axial pressure is generated on the inner wall of the 3-workpiece. According to the principle of small-angle inclined surface (or wedge surface, tapered surface, tip), the workpiece is axially pressurized. Under the action, it generates a huge pressure perpendicular to the inner wall; 1- rigid mandrel and 2-rigid ring sleeve constrain the 3-piece radial deformation; at the same time, 3-worker has a 1-rigid mandrel, 2-rigid ring The tendency of the gap to flow outward between the sleeves; thus, at the contact surface of the 3-workpiece with the 1-rigid mandrel and the 2-rigid collar, a frictional force in the opposite direction to the tendency of the material flow is generated, hindering the flow of the substance; The design of the high pressure of the inner wall of the workpiece, while limiting its deformation and flow, creates a high hydrostatic pressure inside the 3-workpiece (up to 15 GPa). Applying a tangential thrust to the 2-rigid collar, rotating it under the action of torque, while the 1-rigid mandrel does not rotate, in the 2-rigid collar and 3-workpiece and 1-mandrel and 3 - Under the action of the friction between the workpieces, the 3-piece will undergo shear deformation along the tangential direction. As the angle of rotation increases, the amount of shear deformation increases cumulatively, thereby effectively controlling and optimizing the microstructure of the material and improving its performance.
此外,对设备或者模具进行一定的改动,改变施压及旋转的模具部件,同样也可以实现该原理。如图7(d)所示:利用2-刚性环套对3-工件的外壁施加轴向压力,旋转1-刚性芯轴而固定3-刚性环套可以使锥管状材料产生类似的剪切塑性变形效果。同理如7(b)、(c)情况下利用劈尖原理实现管材高压切变的方法原理文字说明从略。In addition, this principle can also be achieved by making certain changes to the equipment or mold and changing the pressure and rotating mold parts. As shown in Figure 7(d): Applying axial compression to the outer wall of the 3-workpiece using a 2-rigid collar, rotating the 1-rigid mandrel and fixing the 3-rigid collar provides similar shear plasticity to the tapered tubular material. Deformation effect. For the same reason, in the case of 7(b) and (c), the principle of the method of using the tip of the tip to realize the high-pressure shearing of the pipe is omitted.
另一方面,根据管状工件端部受约束情况,可以将其分成如图8所示三种情况:(a)端部无约束;(b)端部半约束;(c)端部全约束。对于3-工件端部无约束的情况,如图8(a)所示,3-工件端部物质的流动,将完全依靠与物质流动趋势相反方向的摩擦力进行限制;对于3-工件端部半约束的情况,如图8(b)所示,1-芯轴上的环形凸肩以及2-刚性环套上的环形凸肩分别对3-工件的上下端给予约束,采用这种约束时,环形凸肩与2-刚性环套之间留有较大间隙,避免刚性接触,同理,2-刚性环套上环形凸肩与1-刚性芯轴之间亦留有较大间隙,间隙处的物质流动同样依靠摩擦力进行限制;对于3-工件端部全约束的情况,如图8(c)所示,在3-工件上下端分别添加4-、5-环形垫圈,4-、5-垫圈采用固态传压介质,垫圈内外壁受压后的轴向膨胀将有效阻碍工件端部材料的物质流动。前文中对本发明原理详细描述时所,为了简洁起见,所用附图7中的4种原理图均采用端部无约束的简单设计。On the other hand, according to the constraint of the end of the tubular workpiece, it can be divided into three cases as shown in Fig. 8: (a) the end is unconstrained; (b) the end semi-constraint; (c) the end full constraint. For the case where the 3-workpiece end is unconstrained, as shown in Fig. 8(a), the flow of the 3-workpiece end material will be completely limited by the frictional force in the opposite direction to the material flow tendency; for the 3-workpiece end In the case of semi-constraint, as shown in Fig. 8(b), the annular shoulder on the 1-mandrel and the annular shoulder on the 2-rigid ring respectively constrain the upper and lower ends of the 3-workpiece. There is a large gap between the annular shoulder and the 2-rigid ring sleeve to avoid rigid contact. Similarly, there is a large gap between the annular shoulder on the 2-rigid ring and the 1-rigid mandrel. The material flow at the same place is also limited by friction; for the case where the 3-piece end is fully constrained, as shown in Fig. 8(c), 4-, 5-ring washers are added to the upper and lower ends of the 3-workpiece, respectively. The 5-gasket uses a solid-state pressure transmitting medium, and the axial expansion of the inner and outer walls of the gasket will effectively hinder the material flow of the material at the end of the workpiece. In the foregoing, a detailed description of the principles of the present invention, for the sake of brevity, the four schematics used in Figure 7 all employ a simple design with unconstrained ends.
下面结合具体实施例对本发明做进一步详细说明。The present invention will be further described in detail below in conjunction with specific embodiments.
如图9所示为利用劈尖原理(也称楔效应或者斜面增力原理)实现管材高压切变的方法原理实现装置。图9(a)为装置的爆炸视图,详细给出了装置的组成细节。As shown in Fig. 9, the method principle realization device for realizing high-pressure shearing of pipe by using the tipping principle (also called wedge effect or the principle of beveling force increase) is shown. Figure 9(a) is an exploded view of the device, detailing the composition of the device.
90-上压头, 93-刚性芯轴,95-管状工件,96-刚性环套,97-环套外套齿轮,98-推力轴承,100-芯轴底座组成了整个装置的原理实现部分。96-刚性环套居中放置在压力机下底板上,与压力机下底板之间靠98-推力轴承相连,98-推力轴承承受来自96-刚性环套的轴向压力,并减小轴向压力对96-刚性环套绕轴转动的阻碍作用。带有锥度的95-管状工件同心放置于的96-刚性环套中, 91-上压头下端方形截面四棱柱与92-刚性芯轴上端方形截面的凹陷实现间隙配合,使得90-上压头与93-刚性芯轴在压力机轴线位置相接触,并从带有锥度的95-管状工件的中心穿过,90-上压头与压力机上底板靠螺栓连接。93-刚性芯轴、95-工件以及96-刚性环套三者同轴配合。93-刚性芯轴、96-刚性环套与95-工件同轴装配在压力机的上、下底板之间后,不允许沿径向发生位移(不允许产生水平位移)。然后,93-刚性芯轴通过与压力机上底板连接的90-上压头将压力机提供的轴向压力传递给95-工件内壁。95-工件内壁相对于轴向为小角度锥面,根据小角度斜面(或称楔面、锥面、劈尖)力放大原理,95-管状工件在垂直于95-工件内壁或外壁处将产生远大于压力机提供的轴向载荷的正压力。96-刚性环套、93-芯轴对95-工件径向变形起到约束作用。同时,95-工件端部无约束,材料有沿96-刚性环套与93-芯轴之间缝隙向外流动的趋势,这种趋势被相反方向的摩擦力阻碍。这种设计使得在95-工件内部累加了高静水压力(1GPa~15GPa)。同时,采用伺服电机带动减速器齿轮组(动力装置采用常规的合适功率和转速的电机和齿轮组或者蜗轮蜗杆,其示意图从略)驱动97-环套外套齿轮,在扭矩的作用下使之旋转,转动速度1~5rpm。由于摩擦力,95-工件外壁处的材料将有跟97-刚性环套一起转动的趋势。而92-刚性芯轴上端方形截面的凹孔被91-上压头下端方形截面四棱柱约束,94-刚性芯轴下端方形截面四棱柱被99-芯轴底座上端方形截面凹孔约束,95-工件内壁处的材料将有跟93-刚性芯轴一起固定不动的趋势;高静水压力条件下,材料将保持连续性,95-管状工件沿径向不同厚度层的材料将以不同的角速度转动,即发生相对转动,材料在摩擦力的驱动下实现剪切变形。90-upper head, 93-rigid mandrel, 95-tubular workpiece, 96-rigid ring sleeve, 97-ring sleeve gear, 98-thrust bearing, 100-mandrel base form the principle realization part of the whole device. The 96-rigid ring is placed on the lower bottom plate of the press and connected to the 98-thrust bearing between the bottom plate of the press. The 98-thrust bearing receives the axial pressure from the 96-rigid ring and reduces the axial pressure. The obstruction of the rotation of the 96-rigid ring around the shaft. The tapered 95-tube workpiece is placed concentrically in the 96-rigid collar. 91-The lower end of the upper indenter square prismatic prism and the 92-rigid mandrel upper end square section of the recess to achieve clearance fit, so that the 90-upper head and 93-rigid mandrel in the press axis position contact, and from the taper The center of the 95-tubular workpiece passes through, and the 90-upper head is bolted to the upper plate of the press. 93-rigid mandrel, 95-workpiece and 96-rigid ring set are coaxially matched. 93-Rigid mandrel, 96-rigid ring sleeve and 95-workpiece are coaxially assembled between the upper and lower plates of the press, and no displacement in the radial direction is allowed (no horizontal displacement is allowed). The 93-rigid mandrel then transfers the axial pressure provided by the press to the 95-worker inner wall through a 90-upper head attached to the upper plate of the press. 95-The inner wall of the workpiece is a small angle cone with respect to the axial direction. According to the principle of small angle inclined surface (or wedge surface, cone surface, tip), the 95-tubular workpiece will be produced perpendicular to the inner wall or outer wall of the 95-workpiece. It is much larger than the positive pressure of the axial load provided by the press. The 96-rigid collar and the 93-core shaft constrain the 95-workpiece radial deformation. At the same time, the 95-end of the workpiece is unconstrained, and the material has a tendency to flow outward along the gap between the 96-rigid collar and the 93-mandrel. This tendency is hindered by the friction in the opposite direction. This design adds a high hydrostatic pressure (1GPa~15GPa) inside the 95-workpiece. At the same time, the servo motor is used to drive the reducer gear set (the power unit adopts the conventional motor and gear set or the worm gear of the appropriate power and speed, the schematic diagram is omitted) to drive the 97-ring sleeve gear, and rotate it under the action of the torque. The rotation speed is 1~5rpm. Due to the friction, the material at the 95-work outer wall will have a tendency to rotate with the 97-rigid collar. The concave hole of the square end section of the upper end of the 92-rigid mandrel is constrained by the square cross section of the upper end of the 91-upper head, and the square prism of the lower end of the 94-rigid mandrel is constrained by the concave hole of the upper end of the 99-core shaft base, 95- The material at the inner wall of the workpiece will have a tendency to be fixed together with the 93-rigid mandrel; under high hydrostatic pressure conditions, the material will remain continuous, and the 95-tubular workpiece will rotate at different angular velocities along different layers of the radial thickness. That is, relative rotation occurs, and the material is shear-driven under the driving of friction.
该实施方案中,93-刚性芯轴采用上下两端同时约束旋转自由度的设计,约束方式采用两组方形截面四棱柱和方形截面凹孔(91-、92-和94-、99-)的间隙配合实现。两组方形截面四棱柱和方形截面凹孔(91-、92-和94-、99-)之间分别采用F7/h6基轴制间隙配合和H7/g6基孔制间隙配合。一方面使得93-芯轴易于固定,另一方面,使93-芯轴两端同时受力,因扭矩过大而断裂失效。此外90-上压头并不直接接触95-管状工件,压力是93-刚性芯轴直接传递给工件内壁。这样设计是因为与工件端面直接接触的部位受力情况非常恶劣,需增设由硬质合金制成的环形垫圈,提高成本;另一方面,对95-工件端部直接加压时,由于摩擦力的存在,压力并不能均匀传递到95-工件的中部,造成中部压力不足,往往限制了95-工件的高度。采用本专利提出的利用劈尖原理实现管材高压切变的方法可有效克服以上不足。In this embodiment, the 93-rigid mandrel adopts a design in which the upper and lower ends simultaneously constrain the rotational freedom. The constraining method adopts two sets of square-section quadrangular prisms and square-section recessed holes (91-, 92-, and 94-, 99-). The clearance fit is achieved. The F7/h6 base shaft clearance fit and the H7/g6 base hole clearance fit are used between the two sets of square-section quadrangular prisms and square-section recessed holes (91-, 92- and 94-, 99-). On the one hand, the 93-core shaft is easy to fix, on the other hand, the 93-core shaft is simultaneously subjected to force at both ends, and the fracture is broken due to excessive torque. In addition, the 90-upper head does not directly contact the 95-tubular workpiece, and the pressure is 93-rigid mandrel directly transmitted to the inner wall of the workpiece. This design is because the part directly in contact with the end face of the workpiece is subjected to a very bad force. It is necessary to add an annular gasket made of cemented carbide to increase the cost; on the other hand, when the end of the 95-workpiece is directly pressurized, due to friction The presence of pressure does not pass evenly to the middle of the 95-workpiece, causing insufficient pressure in the middle, often limiting the height of the 95-workpiece. The method for realizing high-pressure shearing of the pipe by using the tip principle of the patent can effectively overcome the above disadvantages.
96-刚性环套采用预应力缠绕模具设计时,内层选择硬度和韧性都较高的材质,如模具钢;缠绕层采用韧性较高的材质,如弹簧钢丝或者弹簧钢带;外层采用韧性较高的材质,如中碳钢。96-刚性环套采用预应力多层环套设计时,内层选择硬度和韧性都较高的材质,如模具钢;其它层选择韧性较高的材质,如中碳合金钢或者模具钢。92-刚性芯轴镶嵌硬质合金,其余部位选择材质为模具钢。When the 96-rigid ring sleeve is designed with prestressed winding mold, the inner layer selects materials with high hardness and toughness, such as die steel; the wound layer uses high toughness materials, such as spring steel wire or spring steel strip; the outer layer adopts toughness. Higher material, such as medium carbon steel. When the 96-rigid ring sleeve is designed with prestressed multi-layer ring sleeve, the inner layer selects materials with higher hardness and toughness, such as die steel; the other layers select materials with higher toughness, such as medium carbon alloy steel or die steel. The 92-rigid mandrel is inlaid with hard alloy, and the rest is made of die steel.
具体选材如下:模具钢为Cr5Mo1V钢;弹簧钢为65Mn钢;中碳钢为45号钢;中碳合金钢为45Mn钢;硬质合金为YG6A。The specific materials are as follows: the mold steel is Cr5Mo1V steel; the spring steel is 65Mn steel; the medium carbon steel is 45 steel; the medium carbon alloy steel is 45Mn steel; the hard alloy is YG6A.
该实施方案中,装配好的利用劈尖原理实现管材高压切变的装置的效果图如图9(b)所示。In this embodiment, the assembled effect of the device for achieving high pressure shear of the pipe using the tip principle is as shown in Fig. 9(b).
通过该方案对工业纯铝、6063铝合金以及AZ31镁合金管状工件进行了初步实验研究。Through the scheme, preliminary experimental research on industrial pure aluminum, 6063 aluminum alloy and AZ31 magnesium alloy tubular workpiece was carried out.
工件尺寸为高30mm,半锥角10°,下端面半径ri=10mm,re=14mm。The workpiece has a height of 30 mm, a half cone angle of 10°, a lower end surface radius r i = 10 mm, and r e = 14 mm.
工业纯铝管状工件经过25°剪切变形后的沿径向显微硬度分布如图10所示:从靠近内径处到靠近外径处,硬度由48 HV(0.025kg)变为33 HV(0.025kg),呈递减分布趋势,但均高于初始未经过高压剪切变形的试样31 HV(0.025kg)左右的硬度。试样横截面光学显微金相如图11所示:图11(a)初始挤压态纯铝试样靠近内径处阳极复膜偏光观察,平均晶粒尺寸约40μm;(b)经过高压剪切变形后纯铝试样靠近内径处明场相观察,明场相下部分晶界未显示,没有给出平均晶粒尺寸的估算值,但可以明显看出晶粒被拉长、破碎、细化;(c)经过高压剪切变形后纯铝试样从内径到外径完整截面显微组织分布。The radial microhardness distribution of the industrial pure aluminum tubular workpiece after 25° shear deformation is shown in Figure 10: from near the inner diameter to near the outer diameter, the hardness is changed from 48 HV (0.025 kg) to 33. HV (0.025kg), showing a decreasing distribution trend, but higher than the initial sample 31 without high-pressure shear deformation Hardness around HV (0.025kg). The cross-section optical microscopic metallographic phase of the sample is shown in Figure 11: Figure 11 (a) The initial extruded pure aluminum sample is observed near the inner diameter of the anodic lamination, and the average grain size is about 40 μm; (b) high-pressure shear deformation After the pure aluminum sample is close to the bright field phase at the inner diameter, some grain boundaries are not shown in the bright field phase, and the average grain size is not given. However, it can be clearly seen that the grain is elongated, broken and refined. (c) The microstructure of the pure aluminum sample from the inner diameter to the outer diameter after high-pressure shear deformation.
此外,6063铝合金以及AZ31镁合金的实验结果简要总结如下:In addition, the experimental results of 6063 aluminum alloy and AZ31 magnesium alloy are briefly summarized as follows:
6063铝合金未进行高压切变前的平均晶粒尺寸为80μm,压缩试验屈服强度156.8MPa;在2.5GPa静水压力以1rpm的转动速度利用劈尖原理实现60º的高压剪切变形,平均应变达到3.1,平均晶粒尺寸达到746nm,压缩试验屈服强度增至402.6MPa。The average grain size of 6063 aluminum alloy before high pressure shear is 80μm, the compression test yield strength is 156.8MPa; the high pressure shear deformation of 60o is achieved by the tipping principle of 2.5GPa hydrostatic pressure at 1rpm. The average strain reaches 3.1. The average grain size reached 746 nm, and the compression test yield strength increased to 402.6 MPa.
AZ31镁合金塑性较差,我们对模具进行了100℃的加热。未进行高压切变前的平均晶粒尺寸为27μm,压缩试验屈服强度276.4MPa;在3GPa静水压力下以1rpm的转动速度经过90º的利用劈尖原理实现的管状材料高压剪切变形,平均应变达到4.7,平均晶粒尺寸达到640nm,压缩试验屈服强度增至396.5MPa。 The plasticity of AZ31 magnesium alloy is poor, and we heat the mold at 100 °C. The average grain size before the high pressure shear was 27 μm, the compression test yield strength was 276.4 MPa; the high pressure shear deformation of the tubular material achieved by the tip principle of 90° at a rotational speed of 1 rpm at 3 MPa hydrostatic pressure, the average strain reached 4.7, the average grain size reached 640 nm, and the compression test yield strength increased to 396.5 MPa.

Claims (8)

  1. 一种利用劈尖原理实现管材高压切变的方法,其特征在于:首先选择加工的工件,其形状为带有锥度的管状,采用约束体分别约束工件的内壁和外壁;然后对约束体施加轴向压力,利用劈尖的增力原理将这一轴向压力增大,并转变成与工件接触面垂直方向的正压力,从而在工件内获得高静水压力;然后对一个约束体提供扭矩,使其绕工件的中心轴转动,并且固定另一个约束体;或者同时对两个约束体提供方向相反的扭矩,使得它们绕工件的中心轴相对转动;在约束体与工件内外壁切向摩擦力的作用下,工件内部沿径向不同厚度处的材料以不同的角速度转动,从而实现工件的剪切变形。 The invention relates to a method for realizing high-pressure shearing of a pipe by using a tipping principle, which is characterized in that: firstly, the processed workpiece is selected to have a tapered tubular shape, and the inner wall and the outer wall of the workpiece are respectively restrained by the binding body; then the shaft is applied to the binding body To the pressure, the axial pressure is increased by the force-increasing principle of the tip and converted into a positive pressure perpendicular to the contact surface of the workpiece to obtain a high hydrostatic pressure in the workpiece; then a torque is provided to a restraining body so that Rotating around the central axis of the workpiece and fixing the other binding body; or simultaneously providing the opposite directions to the two binding bodies such that they rotate relative to each other about the central axis of the workpiece; the tangential friction between the binding body and the inner and outer walls of the workpiece Under the action, the materials at different thicknesses in the radial direction of the workpiece rotate at different angular velocities, thereby achieving shear deformation of the workpiece.
  2. 根据权利要求1所述的利用劈尖原理实现管材高压切变的方法,其特征在于:所述高静水压力为1~15GPa。The method for realizing high pressure shearing of a pipe using the tip principle according to claim 1, wherein the high hydrostatic pressure is 1 to 15 GPa.
  3. 一种利用劈尖原理实现管材高压切变的装置,其特征在于:包括具有恒压功能的压力机和具有传递压力、约束形变以及实现部分旋转功能的模具;该模具包括可轴向移动或者可转动的刚性芯轴(1)以及可转动或者可轴向移动的刚性环套(2);刚性芯轴(1)和刚性环套(2)分别设置在压力机的上底板和下底板上,工件(3)同轴放置于刚性环套(2)内,刚性环套(2)内表面与工件(3)的外壁接触,工件(3)的内部同轴设有刚性芯轴(1),刚性芯轴(1)外表面与工件(3)的内壁接触。A device for realizing high-pressure shearing of a pipe by using a tipping principle, comprising: a press having a constant pressure function and a die having a transmitting pressure, a constraining deformation, and a partial rotating function; the die includes an axially movable or a rotating rigid mandrel (1) and a rotatable or axially moveable rigid collar (2); the rigid mandrel (1) and the rigid collar (2) are respectively disposed on the upper and lower plates of the press, The workpiece (3) is coaxially placed in the rigid ring sleeve (2), the inner surface of the rigid ring sleeve (2) is in contact with the outer wall of the workpiece (3), and the inner portion of the workpiece (3) is coaxially provided with a rigid core shaft (1). The outer surface of the rigid mandrel (1) is in contact with the inner wall of the workpiece (3).
  4. 根据权利要求3所述的利用劈尖原理实现管材高压切变的装置,其特征在于:刚性环套(2)内表面与刚性芯轴(1)外表面进行毛化处理。The apparatus for realizing high-pressure shearing of a pipe by the tipping principle according to claim 3, characterized in that the inner surface of the rigid collar (2) and the outer surface of the rigid mandrel (1) are subjected to texturing treatment.
  5. 根据权利要求3所述的利用劈尖原理实现管材高压切变的装置,其特征在于:所述刚性芯轴(1)和刚性环套(2)之中至少有一个可沿轴向移动,完成加压动作。The apparatus for realizing high-pressure shearing of a pipe by using a tipping principle according to claim 3, wherein at least one of the rigid mandrel (1) and the rigid collar (2) is axially movable to complete Pressurize action.
  6. 根据权利要求3所述的利用劈尖原理实现管材高压切变的装置,其特征在于:刚性环套和刚性芯轴二者之一可转动,或二者可同时沿相反方向转动,转动的角度无限制。The apparatus for realizing high-pressure shearing of a pipe by using a tipping principle according to claim 3, wherein one of the rigid collar and the rigid mandrel is rotatable, or both can be rotated in opposite directions at the same time, the angle of rotation No limit.
  7. 根据权利要求3所述的利用劈尖原理实现管材高压切变的装置,其特征在于:所述刚性环套(2)采用单层模具设计、预应力缠绕模具设计或预应力多层模具设计。The apparatus for realizing high-pressure shearing of a pipe using the tip principle according to claim 3, wherein the rigid ring sleeve (2) adopts a single-layer mold design, a pre-stressed winding mold design or a pre-stressed multilayer mold design.
  8. 根据权利要求3所述的利用劈尖原理实现管材高压切变的装置,其特征在于:所述工件(3)的端部约束可采用无约束、半约束或全约束设计。The device for realizing high pressure shearing of a pipe using the tip principle according to claim 3, characterized in that the end constraint of the workpiece (3) can adopt an unconstrained, semi-constrained or fully constrained design.
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