WO2012100673A1 - High pressure shear deformation method for tubular material and device thereof - Google Patents

High pressure shear deformation method for tubular material and device thereof Download PDF

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Publication number
WO2012100673A1
WO2012100673A1 PCT/CN2012/070156 CN2012070156W WO2012100673A1 WO 2012100673 A1 WO2012100673 A1 WO 2012100673A1 CN 2012070156 W CN2012070156 W CN 2012070156W WO 2012100673 A1 WO2012100673 A1 WO 2012100673A1
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Prior art keywords
workpiece
anvil
rigid
pressure
shear deformation
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PCT/CN2012/070156
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French (fr)
Chinese (zh)
Inventor
王经涛
李政
王进
刘金强
尹德良
刘冉
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南京理工大学
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Publication of WO2012100673A1 publication Critical patent/WO2012100673A1/en

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21CMANUFACTURE OF METAL SHEETS, WIRE, RODS, TUBES OR PROFILES, OTHERWISE THAN BY ROLLING; AUXILIARY OPERATIONS USED IN CONNECTION WITH METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL
    • B21C23/00Extruding metal; Impact extrusion
    • B21C23/001Extruding metal; Impact extrusion to improve the material properties, e.g. lateral extrusion
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21JFORGING; HAMMERING; PRESSING METAL; RIVETING; FORGE FURNACES
    • B21J1/00Preparing metal stock or similar ancillary operations prior, during or post forging, e.g. heating or cooling
    • B21J1/02Preliminary treatment of metal stock without particular shaping, e.g. salvaging segregated zones, forging or pressing in the rough
    • B21J1/025Preliminary treatment of metal stock without particular shaping, e.g. salvaging segregated zones, forging or pressing in the rough affecting grain orientation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21JFORGING; HAMMERING; PRESSING METAL; RIVETING; FORGE FURNACES
    • B21J5/00Methods for forging, hammering, or pressing; Special equipment or accessories therefor
    • B21J5/008Incremental forging
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21KMAKING FORGED OR PRESSED METAL PRODUCTS, e.g. HORSE-SHOES, RIVETS, BOLTS OR WHEELS
    • B21K1/00Making machine elements
    • B21K1/76Making machine elements elements not mentioned in one of the preceding groups
    • B21K1/761Making machine elements elements not mentioned in one of the preceding groups rings

Definitions

  • the invention relates to the field of material processing engineering, in particular to a method and a device for realizing circumferential shear plastic deformation of a tubular material, which are mainly applied to various metal and alloy materials, inorganic non-metal materials and polymer materials, etc., to realize these The material is plastically deformed at high hydrostatic pressure, thereby controlling and optimizing its structural structure and improving its performance.
  • Background technique
  • the severe plastic deformation (SPD) method is a general term for a series of plastic processing techniques with large deformation.
  • the SPD method refines the grain effect clearly, and can refine the internal structure of the material to sub-micron, nano-scale or even amorphous [RZ Valiev. Nature materials. 2004 (3): 511-516.; RZ Valiev, AK Mukheq' Ee. Scripta mater. 2001 (44): 1747-1750.].
  • SPD method refines the grain effect clearly, and can refine the internal structure of the material to sub-micron, nano-scale or even amorphous [RZ Valiev. Nature materials. 2004 (3): 511-516.; RZ Valiev, AK Mukheq' Ee. Scripta mater. 2001 (44): 1747-1750.].
  • SPD method refines the grain effect clearly, and can refine the internal structure of the material to sub-micron, nano-scale or even amorphous [RZ Valiev. Nature materials. 2004 (3): 511-516.
  • the most popular SPD methods are mainly accumulative roll-bonding (ARB) technology, equal-channel angular pressing (ECAP) technology, and high-pressure torsion (referred to as high-pressure torsion). HPT) technology, etc.
  • ARB accumulative roll-bonding
  • ECAP equal-channel angular pressing
  • HPT high-pressure torsion
  • the ARB technology is shown in Figure 1. It can continuously prepare thin-plate ultrafine-grained structural materials, and is easy to implement on traditional rolling mills. The equipment is simple and practical. However, in the ARB process, in order to achieve good rolling compounding, lubricants are often not used, which is detrimental to the service life of the rolls.
  • the hydrostatic pressure that can be achieved due to the deformation of the material during the rolling process is not high enough, and the cracking problem occurs after a certain amount of deformation is accumulated in the process [N. Tsuji, Y. Saito, SH Lee, et Al. Advanced Engineering Materials. 2003 (5): 338-344.].
  • the ECAP technology is shown in Figure 2. The use of this technology for ultra-fine grain metal processing has great potential. However, for some difficult-to-machine alloys (such as magnesium alloys), ECAP often cracks. If the deformation temperature is increased, it will affect the life of the mold, and on the other hand, it will affect the grain refining effect.
  • back pressure ECAP back pressure Equal-channel angular pressing (BP-ECAP) is the ECAP technology that applies back pressure to the die exit channel.
  • BP-ECAP back pressure Equal-channel angular pressing
  • Figure 3 the cracking problem of the difficult-to-deform metal ECAP can be solved to some extent, thereby improving the microstructure and material.
  • HPT technology shown in Figure 3 is the most suitable condition for the preparation of ultrafine grained materials in accordance with the SPD method mentioned in the previous section.
  • SPD technology has the strongest grain refinement capability.
  • the thickness of the specimen that HPT can process is small [AP Zhilyaev, TG Langdon. Progress in Materials Science. 2008 (53): 893-979.], the processed disc specimens are radially present. Large strain gradient, uneven deformation, and uneven grain refinement.
  • the ring sleeve is rotated, and the tubular sample is subjected to the circumferential shear deformation under the action of the surface ring friction.
  • This method is very good.
  • the main problem is that the method of loading the sample is radial loading. That is to say, the method directly applies axial pressure to the mandrel, and the mandrel produces a diameter on the sample. To the pressure. In this loading mode, the pressure is not directly loaded in the axial direction of the tubular material, and the hydrostatic pressure of the sample is derived from the elastic deformation of the mandrel after being pressed.
  • baffle at the ends of the tubular sample is a cantilever beam structure, which has insufficient constraint on the axial deformation of the sample.
  • hydrostatic pressure of the sample is high, the material is easily extruded from the gap. , affecting the processing process.
  • the technique satisfies a number of conditions for the preparation of ultrafine grained materials by the SPD method, such as large plastic deformation, relatively low deformation temperature and high hydrostatic pressure inside the deformed material.
  • This method avoids the cumbersome process that requires multiple operations such as AB, ECAP, and back pressure ECAP.
  • the method due to the nature of the loading method, the method also overcomes the hydrostatic pressure of T0th et al. Problems such as insufficient force can provide high hydrostatic pressure conditions similar to HPT technology when processing materials, which is suitable for processing difficult metals and alloys, achieving the effect of controlling and optimizing the structure of materials and improving their performance.
  • the technical solution for achieving the object of the present invention is: a high-pressure shear deformation method for a tubular material, first selecting a machined workpiece, the workpiece is tubular, and constraining the inner and outer walls of the workpiece respectively; then directly applying an axial direction to the end of the workpiece The pressure causes the workpiece to undergo elastic deformation or slight plastic deformation, accumulating high hydrostatic pressure in the workpiece; then providing a torque to a constraining body in contact with the inner or outer wall of the workpiece to rotate around the central axis of the workpiece while fixing another binding body Under the action of the frictional force between the restraining body and the inner and outer walls of the workpiece, the materials at different thicknesses in the radial direction of the workpiece rotate at different angular velocities, thereby achieving the circumferential shear deformation of the workpiece.
  • a high-pressure shear deformation device for a tubular material comprising a press having a constant pressure function and a mold having a transfer pressure, a constraining deformation, and a partial rotation function;
  • the mold comprising: an upper anvil, a lower anvil, fixed or rotatable a rigid mandrel and a rigid or fixed rigid collar;
  • the upper anvil and the lower anvil are respectively mounted on the upper pressing head and the base of the press, and the workpiece is placed between the upper anvil and the lower anvil, the upper anvil
  • the upper end and the upper end of the lower anvil are in contact with the upper and lower end faces of the workpiece through a boss provided, and the cross section of the boss is a ring which completely conforms to the upper and lower end faces of the workpiece;
  • the inner part of the workpiece is concentrically provided with a rigid mandrel, a rigid mandrel
  • the outer surface is in contact with the inner wall of the workpiece, and the outer portion of the workpiece
  • the processing procedure is simple.
  • the t-HPS method proposed by the present invention is a severe plastic deformation method which can be realized in a single pass on a conventional extruder having a constant pressure function.
  • methods such as cumulative rolling (ARB), multi-directional forging, equal-cavity extrusion (ECAP), and back-pressure ECAP often require many repetitive process passes to achieve high strain plastic deformation, and high labor consumption. .
  • the method utilizes a rigid collar, a tubular workpiece, and a friction between the mandrel and the tubular workpiece, rotates the rigid collar and fixes the mandrel such that the outer region of the tubular workpiece in contact with the rigid collar is in contact with the inner core
  • the zone region is circumferentially sheared to achieve severe plastic deformation under a single process pass.
  • the true strain is 1 to 10, or even higher.
  • the t-HPS method proposed by the present invention has a simple principle and is easy to obtain, and can be realized in a general plastic forming laboratory.
  • the hydrostatic pressure that can be supplied is high, so the wide range of materials that can be processed and the processing ability are strong.
  • the t-HPS method proposed by the present invention directly pressurizes the tubular material axially while restraining its radial deformation, so that a hydrostatic pressure of up to 15 ⁇ GPa can be generated inside the material. This is currently not possible with other processes including HPTT.
  • the hydrostatic pressure that can be provided will be higher. Plastic deformation under such high hydrostatic pressure conditions effectively suppresses the generation and development of the surface and internal cracks of the material, thereby improving the workability of many difficult-to-machine materials (such as magnesium alloys with poor plasticity).
  • the tubular product that can be obtained is large in size.
  • the workpiece processed by the t-HPS method proposed by the present invention is tubular, and its size is limited only by the scale of the equipment. Even in the laboratory, the tubular material of ⁇ 100mm height can be obtained by this method, which has good performance and can be applied in many fields after a little subsequent treatment. In addition, the obtained tubular material is axially cut and rolled. High performance sheeting is obtained.
  • Figure 1 is a schematic diagram of the principle of cumulative composite rolling (ARB) technology.
  • FIG. 2 is a schematic diagram of the principle of equal channel angular extrusion (ECAP) technology.
  • FIG. 3 is a schematic diagram of the principle of back pressure ECAP (BP-ECAP) technology.
  • FIG. 4 is a schematic diagram of the principle of high voltage torsion (HPT) technology.
  • FIG. 5 is a schematic diagram of the principle of high-pressure tube twisting (HPTT) technology.
  • Figure 6 is a schematic diagram of the t-HPS technology of the present invention, wherein: 61-upper anvil, 62-rigid collar, 63-tubular workpiece, 64-lower anvil, 65-rigid mandrel; h is the height of the tubular workpiece; The inner radius of the tubular workpiece; the outer radius of the R tubular workpiece; P is the pressure; T is the torque.
  • Figure 8 is a schematic view of the apparatus for the t-HPS severe plastic deformation method embodiment, wherein (a) is an exploded view: 1- support column, 2-upper anvil connection sleeve, 3-upper anvil connection bolt, 4-connection Sleeve square pin, 5-connected sleeve cylindrical pin, 6-lower anvil, 7-tubular workpiece, 8-rigid ring sleeve, 9-lower annular washer, 10-upper annular washer, 11-integrated upper anvil With mandrel, 12-core bushing plate, 13-lower anvil connecting bolt, 14-servo motor, 15-hollow shaft reducer gearbox, 16-belt, 17-thrust bearing, 18-rigid ring sleeve, 19-sleeve connecting bolt; (b) main view.
  • (a) is an exploded view: 1- support column, 2-upper anvil connection sleeve, 3-upper anvil connection bolt, 4-connection Sleeve square pin, 5-connected sleeve cylindrical pin, 6-lower anvil, 7-tub
  • the material processing object of the present invention can be realized on a conventional extruder having a constant pressure function: a tubular workpiece is placed on the lower anvil, and a rectangular outer sleeve is provided with a rotatable rigid ring sleeve, and the rigid mandrel is worn from the center of the tubular workpiece. Over, on The anvil directly transmits axial pressure to the workpiece, and the tubular workpiece has a tendency to expand radially under the action of a large axial pressure. The rigid disc and the mandrel constrain the radial deformation of the tubular workpiece.
  • the design of the end of the workpiece while applying high pressure while limiting its deformation causes a high hydrostatic pressure (lGPa ⁇ 15 GPa) to be accumulated inside the workpiece. Under high hydrostatic pressure conditions, a large amount of friction will be generated on the inner and outer walls of the tubular workpiece.
  • the shape change of the tubular workpiece is limited, it has the degree of freedom of rotation in the axial direction, and the upper and lower anvils are respectively mounted on the upper and lower bottom plates of the extruder, so that the binding bodies (the mandrel and the respectively respectively are in contact with the inner wall or the outer wall of the workpiece)
  • One of the rigid ring sleeves rotates around the central axis of the tubular workpiece and the other one is fixed.
  • the material near the inner and outer walls of the workpiece rotates or fixes with the binding body.
  • the trend of not moving Under high hydrostatic pressure conditions, in order to maintain the continuity of the material, the material of the tubular workpiece in different thickness layers in the radial direction will rotate at different angular velocities, that is, relative rotation occurs, and the material is driven by friction to achieve circumferential shearing.
  • Deformation it is important that the deformation is the shear of the material inside the workpiece and does not change the macroscopic shape of the tubular workpiece.
  • the invention enables the tubular material to undergo a circumferential shear plastic deformation under the condition of high hydrostatic pressure (up to 15 ⁇ GPa) (it should be up to 10 ⁇ ). Thereby controlling and optimizing the structure of the material and improving its performance through plastic deformation.
  • the present invention only needs to install a combined mold composed of key elements such as an upper anvil, a mandrel, a lower anvil and a rigid disc on a conventional extrusion device having a constant pressure function, which can be at a lower temperature. (such as room temperature or lower heating temperature) to achieve a new severe plastic deformation (SPD) processing method - tubular workpiece high pressure shear (t-HPS) technology.
  • SPD severe plastic deformation
  • t-HPS tubular workpiece high pressure shear
  • the t-HPS technology is highly feasible, with no special requirements for operation, and the required equipment is simple and easy to obtain.
  • the present invention is a new plastic working method realized by a conventional extrusion apparatus, the function of the conventional extrusion apparatus is expanded.
  • the invention is suitable for experimental research and industrial production of bulk ultrafine crystal and nanocrystalline materials for severe plastic deformation.
  • high-performance metals, alloys, inorganic non-metallic materials, and polymer materials can be prepared.
  • the sample prepared by the t-HPS method has a tubular shape and has high practical application potential and value.
  • the high-pressure shear deformation method of the tubular material of the present invention first selects the workpiece to be processed, the workpiece is tubular, and the inner and outer walls of the workpiece are respectively restrained by the restraining body; then the axial pressure is directly applied to the end of the workpiece to make the workpiece elastic.
  • Deformation or microplastic deformation accumulating hydrostatic pressure up to 1 ⁇ 15 GPa in the workpiece; then providing a torque to a constraining body in contact with the inner or outer wall of the workpiece, rotating it around the central axis of the workpiece while fixing another constraint, Under the action of the frictional force between the restraining body and the inner and outer walls of the workpiece, the materials at different thicknesses in the radial direction of the workpiece rotate at different angular velocities, thereby achieving the circumferential shear deformation of the workpiece.
  • the tubular material high-pressure shear deformation device of the present invention comprises a press having a constant pressure function and a mold having a transfer pressure, a constraining deformation and a partial rotation function;
  • the mold comprises: an upper anvil 61, a lower anvil 64, a fixed or a rotatable rigid mandrel 65 and a rotatable or fixed rigid collar 62; an upper anvil 61 and a lower anvil 64 are respectively mounted on the upper pressing head and the base of the press, and the workpiece 63 is placed on the upper anvil 61 and Between the lower anvils 64, the lower end of the upper anvil 61 and the upper end of the lower anvil 64 are in contact with the upper and lower end faces of the workpiece 63 through the boss provided, and the cross section of the boss is a ring which completely conforms to the upper and lower end faces of the workpiece 63.
  • the inner portion of the workpiece 63 is concentrically provided with a rigid mandrel 65.
  • the outer surface of the rigid mandrel 65 is in contact with the inner wall of the workpiece 63.
  • the outer portion of the workpiece 63 is concentrically provided with a rigid collar, and the inner surface of the rigid collar 62 is in contact with the outer wall of the workpiece 63.
  • the inner surface of the rigid collar 62 and the outer surface of the rigid mandrel 65 are textured to increase friction with the workpiece 63.
  • a clearance fit is used between the upper anvil 61 and the rigid collar 62; a clearance fit is used between the rigid mandrel 65 and the lower anvil 64.
  • one of the rigid mandrel 65 or the rigid cuff 62 is rotatable, and the other is fixed, and the angle of rotation is not limited.
  • the tubular material high-pressure shear deformation device of the present invention may adopt a single-layer mold design, a pre-stressed winding mold design or a pre-stressed multilayer mold design.
  • the upper anvil 61 and the rigid mandrel 65 are two independent parts or are integrated into a part; the upper anvil 61 is designed as a whole or in combination, and when the overall design is used, the upper anvil 61 and the lower part
  • the ends of the anvil 64 have annular bosses respectively conforming to the shape of the upper and lower end faces of the workpiece 63.
  • the anvil comprises two parts, an anvil main body and an annular washer, and the annular gasket cross-section conforms to the shape of the end face of the work 63.
  • the t-HPS method consists of a mold consisting of a 61-upper anvil, a 62-rigid annulus, a 64-lower anvil and a 65-rigid mandrel, combined with a pressure-holding pressure.
  • Machine implemented on a 63-tubular workpiece.
  • the 61-upper anvil and the 64-lower anvil are respectively mounted on the upper and lower bottom plates (or the workbench) of the press, and the 63-tubular workpiece is placed on the 61-upper anvil and the 64-lower anvil.
  • the upper end of the 61-upper anvil and the upper end of the 64-lower anvil are in contact with the upper and lower end faces of the 63-tubular workpiece through a boss provided, and the cross section of the boss is completely coincident with the upper and lower end faces of the 63-tubular workpiece.
  • Ring-shaped; 63- tubular workpiece is internally concentrically provided with a 65-rigid mandrel, 65-rigid mandrel outer surface is in contact with the inner wall of the 63-tubular workpiece, and 63-tubular workpiece is concentrically provided with a 62-rigid collar, 62- The inner surface of the rigid collar is in contact with the outer wall of the 63-tubular workpiece.
  • the 63-tubular workpiece is in a closed cavity composed of a 61-upper anvil, a 62-rigid annulus, a 64-lower anvil, and a 65-rigid mandrel. Then, the press presses the 61-upper anvil and maintains the pressure constant at a certain value.
  • the 61-upper anvil will also exert downward pressure on the 3-tubular workpiece, since the 63-tubular workpiece is subjected to a 61-upper anvil, a 62-rigid collar, 64 - a closed cavity formed by a lower anvil and a 65-rigid mandrel
  • the bundle therefore, produces a high hydrostatic pressure inside it (can be as high as ⁇ 15GPa).
  • the circumferential thrust is applied to the 62-rigid collar, which is rotated in the direction of the torque.
  • the 61-upper anvil, the 64-lower anvil and the 65-rigid mandrel do not rotate, at 62-
  • the 63-tubular workpiece will undergo circumferential shear deformation.
  • the angle of rotation increases, the amount of shear deformation becomes large, thereby effectively controlling and optimizing the structure of the material and improving its performance.
  • the two-dimensional and three-dimensional finite element simulation analysis of the method was carried out.
  • the 2219T62 aluminum alloy workpiece was selected.
  • the material properties of the aluminum alloy are shown in Table 1.
  • the simulated temperature is room temperature and does not take into account the temperature rise and strain rate sensitivity of the material during deformation.
  • the results show that the t-HPS method can accumulate very high strains in large-sized workpieces. As shown in Fig. 7, a tubular workpiece with an inner diameter of 20 mm and an outer diameter of 22 mm undergoes only a 90-degree circumferential shear, and the highest strain is up to 10.78, the minimum strain is 8.41, and the average strain statistics can reach 9.45.
  • the device consists of three parts: t-HPS severe plastic deformation principle realization part, power unit and connection part.
  • Figure 8(a) is an exploded view of the device, detailing the composition of the device.
  • 6-lower anvil, 7-tubular workpiece, 8-rigid ring sleeve, 9-lower annular washer, 10-upper annular washer, 11-integrated upper anvil and mandrel and 12-core bushing plate Principle implementation of the device.
  • 7-Tubular workpiece passes through the 11-integrated upper anvil and mandrel, with an annular gasket (9-, 10-) placed on the upper and lower end faces, and the workpiece is surrounded by an 8-rigid ring, upper and lower anvils (11 -, 6-)
  • the 11-mandrel and the 8-rigid collar constrain its radial expansion and accumulate inside the workpiece.
  • the end of the 11-mandrel is a hexagonal prism. Same as the shape of the hole in the 12-core bushing. After the mandrel is inserted into the hole in the sleeve, its rotation will be constrained. Applying a circumferential thrust to the 8-rigid collar, rotating it under the action of torque, the rotation speed is l ⁇ 5rpm, at the same time, the 11-integrated upper anvil and mandrel are constrained without rotation, at 8 - Under the action of the friction between the rigid collar and the 7-tubular workpiece and the 11-mandrel and the 7-tube workpiece, the 7-tubular workpiece will undergo circumferential shear deformation.
  • the upper anvil and the mandrel are integrally designed to facilitate the fixing of the mandrel on the one hand and the demolding of the tubular workpiece on the other hand.
  • the upper and lower anvils (11-, 6-) do not directly contact the 7-tubular workpiece, and the pressure is transmitted to the workpiece through the upper and lower annular gaskets (9-, 10-).
  • This design is because the part that is in direct contact with the workpiece section is subjected to severe stress.
  • the addition of an annular gasket made of cemented carbide can increase the service life of the anvil and reduce the cost of mold replacement.
  • the 6-lower anvil and the 11-core shaft need to be axially owned.
  • the 11-integrated upper anvil, the mandrel and the 8-rigid ring are made of F7/h6 base shaft clearance fit; 11- integrated upper anvil
  • the head, mandrel and 6-lower anvil are made of H7/g6 base hole clearance fit. This choice of clearance fit is also advantageous from the standpoint of demolding.
  • the rigid ring rotates and causes the tubular workpiece to be circumferentially sheared under the action of friction.
  • the torque required for this action is achieved by the power device.
  • the power unit drives the 15-hollow shaft reducer output torque through a 16-belt through a 14-servo motor.
  • the 11-integrated upper anvil and mandrel are connected by a 2-upper anvil connection sleeve, a 3-upper anvil connection bolt, a 4-connection sleeve square pin, and a 5-connection sleeve cylindrical pin.
  • the upper platen of the press is connected.
  • the connection made up of 1-support column, 13- lower anvil connection bolt, 17-thrust bearing, 18-rigid collar sleeve and 19-sleeve connection bolt will
  • the 6-lower anvil is connected to the lower bottom plate of the press through the 1-support column, while the 18-rigid ring sleeve and the 19-sleeve connection bolt are connected to the 15-hollow shaft reducer and the 8-rigid ring sleeve for torque. transfer.
  • the 17-thrust bearing reduces the axial frictional resistance to the rotation of the 8-rigid ring.
  • the inner layer selects materials with higher hardness and toughness, such as die steel; the wound layer is made of high toughness material, such as spring steel wire or spring steel strip; Higher material, such as medium carbon steel.
  • the inner layer selects materials with higher hardness and toughness, such as die steel; the other layer selects materials with higher toughness, such as medium carbon alloy steel or die steel.
  • 11-Integral The upper anvil and the mandrel and the lower anvil are inlaid with hard alloy at the working part, and the other parts are made of die steel.
  • the 9-lower ring washer and the 10-upper ring washer are made of hard alloy or steel-bonded carbide.
  • the specific materials are as follows:
  • the mold steel is Cr5MolV steel; the spring steel is 65Mn steel; the medium carbon steel is 45 steel; the medium carbon alloy steel is 45Mn steel; the hard alloy is YG6A.
  • the front view of the assembled t-HPS device is shown in Figure 8(b).
  • the tubular workpiece has an inner diameter of 40 mm, an outer diameter of 46 mm and a height of 40 mm. Before and after the deformation, the macro size and shape of the workpiece remain unchanged.
  • the average grain size of industrial pure aluminum before t-HPS is 24 ⁇ , and the yield strength of compression test is 73.7MPa. Under the hydrostatic pressure of 1.5GPa, the t-HPS deformation is 30° at a rotation speed of 1rpm, and the average strain reaches 4, The average grain size reached 633 nm and the compression test yield strength increased to 261.3 MPa.
  • the average grain size of 6063 aluminum alloy before t-HPS is 80 ⁇ , compression test yield strength is 156.8MPa; at 2.5GPa hydrostatic pressure, the t-HPS deformation at 60° is rotated at 60°, the average strain reaches 8, average The grain size reached 561 nm, and the compression test yield strength increased to 447.6 MPa.
  • the AZ31 magnesium alloy is inferior in plasticity, and we heat the mold at 100 °C.
  • the average grain size before t-HPS was 27 ⁇ , the compression yield strength was 276.4 MPa; the t-HPS deformation at 90° at a rotational speed of 1 MPa under a hydrostatic pressure of 1 GP, the average strain reached 9, the average grain size At 335 nm, the compression test yield strength increased to 590.2 MPa.

Abstract

Disclosed are a high pressure shear deformation method for tubular material and a device thereof. Firstly, a workpiece (63, 7) to be machined is selected, with the workpiece (63, 7) being of a tubular shape and with the inner wall and the outer wall of the workpiece (63, 7) being respectively restrained by restraining bodies; then axial pressure is applied directly to the ends of the workpiece (63, 7) so that the workpiece (63, 7) experiences elastic deformation or slight plastic deformation, with hydrostatic pressure of up to 1 to 15 GPa accumulated within the workpiece (63, 7); after that, a torque is provided to one restraining body in contact with the inner wall or the outer wall of the workpiece (63, 7) so as to make it rotate about the central axis of the workpiece (63, 7) while the other restraining body is fixed; under the action of an annular friction force between the restraining body and the inner wall of the workpiece (63, 7), the interior materials of the workpiece (63, 7), at different thicknesses along the radial direction are rotated at different angular velocities so as to achieve an annular shear deformation of the workpiece (63, 7). The high pressure shear deformation method for tubular material and the device thereof is of high technological feasibility without special requirements for operation, and the required equipment is simple and easy to obtain.

Description

管状材料高压剪切变形方法及其装置 技术领域  High-pressure shear deformation method of tubular material and device thereof
本发明涉及材料加工工程领域, 特别是一种实现管状材料环向剪切塑性变形的方法 及其装置, 主要应用于各种金属及合金材料、 无机非金属材料及高分子材料等, 以实现 这些材料在高静水压力的塑性变形, 从而控制和优化其组织结构, 提高其性能。 背景技术  The invention relates to the field of material processing engineering, in particular to a method and a device for realizing circumferential shear plastic deformation of a tubular material, which are mainly applied to various metal and alloy materials, inorganic non-metal materials and polymer materials, etc., to realize these The material is plastically deformed at high hydrostatic pressure, thereby controlling and optimizing its structural structure and improving its performance. Background technique
剧烈塑性变形 (severe plastic deformation, 简称 SPD)方法是一系列具有大变形量的塑 性加工技术的总称。 SPD方法细化晶粒效果明显, 可以将材料内部组织细化到亚微米级、 纳米级甚至非晶态 [R. Z. Valiev. Nature materials. 2004 (3): 511-516.; R. Z. Valiev, A. K. Mukheq'ee. Scripta mater. 2001 (44): 1747-1750.]。近年来, 采用 SPD方法制备块体纳米结 构材料的技术受到了材料科学领域专家、 学者们的普遍关注。 与此同时, 大量的研究推 动 SPD技术在制备块体超细晶、 纳米晶材料方面的不断发展。 俄罗斯 Ufa航空技术大学 的 R.Z. Valiev领导的研究小组认为,采用 SPD方法制备超细晶材料应满足多项条件 [R. Z. Valiev, R. K. Islamgaliev, I V. Alexandrov. Progress in Materials Science.2000 (45): 103-189.], 主要包括: 大塑性变形量、 相对低的变形温度和变形材料内部高的静水压力。 在这一原 则指导下, 人们提出并开发了各种 SPD工艺和方法。  The severe plastic deformation (SPD) method is a general term for a series of plastic processing techniques with large deformation. The SPD method refines the grain effect clearly, and can refine the internal structure of the material to sub-micron, nano-scale or even amorphous [RZ Valiev. Nature materials. 2004 (3): 511-516.; RZ Valiev, AK Mukheq' Ee. Scripta mater. 2001 (44): 1747-1750.]. In recent years, the technology of preparing bulk nanostructure materials by SPD method has received widespread attention from experts and scholars in the field of materials science. At the same time, a large number of studies have pushed the development of SPD technology in the preparation of bulk ultrafine crystals and nanocrystalline materials. The research team led by RZ Valiev of Ufa Aviation Technology University in Russia believes that the preparation of ultrafine grained materials by SPD method should satisfy a number of conditions [RZ Valiev, RK Islamgaliev, I V. Alexandrov. Progress in Materials Science. 2000 (45): 103 -189.], mainly includes: large plastic deformation, relatively low deformation temperature and high hydrostatic pressure inside the deformed material. Under the guidance of this principle, various SPD processes and methods have been proposed and developed.
目前最受关注的 SPD方法主要是, 累积轧制 (accumulative roll-bonding, 简称 ARB) 技术, 等径角变形 (equal-channel angular pressing, 简称 ECAP) 技术, 以及高压扭转 (high-pressure torsion, 简称 HPT) 技术等。 其中 ARB技术如图 1所示, 可连续制备薄板 类超细晶结构材料, 且易于在传统轧机上实现, 设备简单, 实际应用意义重大。 但是, 在 ARB技术加工过程中, 为了实现良好的轧制复合, 往往不能使用润滑剂, 这对轧辊的 服役寿命不利。 同时, 由于材料在轧制过程中受到变形条件限制所能达到的静水压力不 够高, 在加工过程中的累积一定的变形量后会出现开裂问题 [N. Tsuji, Y. Saito, S. H. Lee, et al. Advanced Engineering Materials. 2003 (5) :338-344.]。 ECAP技术如图 2所示, 采用该 技术进行超细晶金属加工处理具有巨大潜力。但是,对于一些难加工合金(如镁合金等), 进行 ECAP经常发生开裂, 如果提高变形温度, 一方面会影响模具寿命, 另一方面又会 影响晶粒细化效果。 再加上由于模具材料的限制, 变形温度不可能无限制地提高。 而且 ECAP为实现大的累积塑性变形, 需要多道次加工, 操作复杂。背压 ECAP (back pressure equal-channel angular pressing, 简称 BP-ECAP) 即在模具出口通道施加背压的 ECAP技 术, 如图 3所示, 可以在一定程度上解决难变形金属 ECAP的开裂问题, 从而改善材料 的微观组织和机械性能; 所施加的背压有限, 静水压力一般维持在几百兆帕 [R. YE. Lapovok. Journal of materials science. 2005 (40) :341-346.]。 施加的背压太高则由于摩擦力 和模具强度等因素而无法实现 ECAP。 HPT技术如图 3所示,是最符合前文中提到的 SPD 方法制备超细晶材料应满足的多项条件。 在现有的 SPD技术之中, HPT技术晶粒细化能 力最强。 然而, HPT 所能加工的试样厚度方向尺寸很小 [A. P. Zhilyaev, T. G. Langdon. Progress in Materials Science. 2008 (53) :893-979.],所加工的盘状试样,沿径向存在较大的 应变梯度, 变形不均匀, 晶粒细化程度也不均匀。 At present, the most popular SPD methods are mainly accumulative roll-bonding (ARB) technology, equal-channel angular pressing (ECAP) technology, and high-pressure torsion (referred to as high-pressure torsion). HPT) technology, etc. The ARB technology is shown in Figure 1. It can continuously prepare thin-plate ultrafine-grained structural materials, and is easy to implement on traditional rolling mills. The equipment is simple and practical. However, in the ARB process, in order to achieve good rolling compounding, lubricants are often not used, which is detrimental to the service life of the rolls. At the same time, the hydrostatic pressure that can be achieved due to the deformation of the material during the rolling process is not high enough, and the cracking problem occurs after a certain amount of deformation is accumulated in the process [N. Tsuji, Y. Saito, SH Lee, et Al. Advanced Engineering Materials. 2003 (5): 338-344.]. The ECAP technology is shown in Figure 2. The use of this technology for ultra-fine grain metal processing has great potential. However, for some difficult-to-machine alloys (such as magnesium alloys), ECAP often cracks. If the deformation temperature is increased, it will affect the life of the mold, and on the other hand, it will affect the grain refining effect. In addition, due to the limitation of the mold material, the deformation temperature cannot be increased without limitation. Moreover, in order to achieve large cumulative plastic deformation, ECAP requires multiple passes and is complicated to operate. Back pressure ECAP (back pressure Equal-channel angular pressing (BP-ECAP) is the ECAP technology that applies back pressure to the die exit channel. As shown in Figure 3, the cracking problem of the difficult-to-deform metal ECAP can be solved to some extent, thereby improving the microstructure and material. Mechanical properties; The applied back pressure is limited, and the hydrostatic pressure is generally maintained at several hundred megapascals [R. YE. Lapovok. Journal of materials science. 2005 (40): 341-346.]. If the applied back pressure is too high, ECAP cannot be achieved due to factors such as friction and mold strength. The HPT technology shown in Figure 3 is the most suitable condition for the preparation of ultrafine grained materials in accordance with the SPD method mentioned in the previous section. Among the existing SPD technologies, HPT technology has the strongest grain refinement capability. However, the thickness of the specimen that HPT can process is small [AP Zhilyaev, TG Langdon. Progress in Materials Science. 2008 (53): 893-979.], the processed disc specimens are radially present. Large strain gradient, uneven deformation, and uneven grain refinement.
T0th等人 [L.S. Toth, M. Arzaghi, J.J. Fundenberger, B. Beausir: Scr. Mater. Vol. 60 (2009), p. 175]提出了一种管状材料高压扭转方法 (high-pressure tube twisting, HPTT) , 如图 5所示, 在管状试样内部安放弹性芯轴, 外侧套置刚性圆盘 (rigid disk) , 试样两 端用挡板固定。 对芯轴加压时, 芯轴径向膨胀对管状试样内壁产生径向压力, 同时刚性 圆盘对管状试样外壁产生一个相反方向的径向压力, 从而在管状试样中产生静水压力。 此时转动环套, 管状试样在表面环向摩擦力作用下实现环向剪切变形。 这种方法思路很 好, 其最主要的问题是该方法对试样的加载方式是径向加载方式, 也就是说, 该方法直 接对芯棒施加轴向压力, 芯棒在对试样产生径向压力。 在这种加载方式下, 压力并没有 直接加载在管状材料的轴向, 试样所承受的静水压力来自芯棒受压后的弹性变形, 由于 材料弹性变形不可能很大, 很难产生高的静水压力, 因而能提供的环向摩擦力有限, 仅 适用于强度较低的纯金属等。 对于强度较高的材料, 由于所能产生的摩擦力达不到材料 的屈服强度, 容易出现打滑等现象, 无法实现所需要的变形。  T0th et al. [LS Toth, M. Arzaghi, JJ Fundenberger, B. Beausir: Scr. Mater. Vol. 60 (2009), p. 175] proposed a high-pressure tube twisting (HPTT) method for tubular materials. As shown in Fig. 5, an elastic mandrel is placed inside the tubular sample, and a rigid disk is placed on the outer side, and both ends of the sample are fixed by a baffle. When the mandrel is pressurized, the radial expansion of the mandrel produces radial pressure on the inner wall of the tubular sample, while the rigid disk creates a radial pressure in the opposite direction to the outer wall of the tubular sample, thereby creating hydrostatic pressure in the tubular sample. At this time, the ring sleeve is rotated, and the tubular sample is subjected to the circumferential shear deformation under the action of the surface ring friction. This method is very good. The main problem is that the method of loading the sample is radial loading. That is to say, the method directly applies axial pressure to the mandrel, and the mandrel produces a diameter on the sample. To the pressure. In this loading mode, the pressure is not directly loaded in the axial direction of the tubular material, and the hydrostatic pressure of the sample is derived from the elastic deformation of the mandrel after being pressed. Since the elastic deformation of the material is unlikely to be large, it is difficult to produce high Hydrostatic pressure, therefore, provides limited hoop friction and is only suitable for pure metals with lower strength. For materials with higher strength, the frictional force that can be generated does not reach the yield strength of the material, and it is prone to slippage and the like, and the required deformation cannot be achieved.
该方法另一方面问题是位于管状试样两端的档板是一悬臂梁式结构, 对试样轴向变 形的约束不够, 试样承受的静水压力较高时, 材料很容易从缝隙中挤出, 影响加工过程。 发明内容  Another problem with this method is that the baffle at the ends of the tubular sample is a cantilever beam structure, which has insufficient constraint on the axial deformation of the sample. When the hydrostatic pressure of the sample is high, the material is easily extruded from the gap. , affecting the processing process. Summary of the invention
本发明的目的在于提供一种新的剧烈塑性变形方法及其装置: 管状材料高压剪切 (tube-High Pressure Shearing,简称 t-HPS) 技术。该技术很好地满足了采用 SPD方法制备 超细晶材料应满足多项条件, 如大塑性变形量、 相对低的变形温度和变形材料内部高的 静水压力。 该方法避免了 A B、 ECAP以及背压 ECAP等技术需要多道次操作的繁琐工 艺过程, 同时, 由于加载方式本质上的不同, 该方法也克服了 T0th等人 HPTT法静水压 力不足等问题, 在加工材料时能提供类似 HPT技术的高静水压力条件, 从而适用于对难 变形金属及合金的加工, 达到控制和优化材料的组织结构、 提高其性能的效果。 It is an object of the present invention to provide a new severe plastic deformation method and apparatus therefor: Tube-High Pressure Shearing (t-HPS) technology. The technique satisfies a number of conditions for the preparation of ultrafine grained materials by the SPD method, such as large plastic deformation, relatively low deformation temperature and high hydrostatic pressure inside the deformed material. This method avoids the cumbersome process that requires multiple operations such as AB, ECAP, and back pressure ECAP. At the same time, due to the nature of the loading method, the method also overcomes the hydrostatic pressure of T0th et al. Problems such as insufficient force can provide high hydrostatic pressure conditions similar to HPT technology when processing materials, which is suitable for processing difficult metals and alloys, achieving the effect of controlling and optimizing the structure of materials and improving their performance.
实现本发明目的的技术解决方案为: 一种管状材料高压剪切变形方法, 首先选择加 工的工件, 工件为管状, 采用约束体分别约束工件的内壁和外壁; 然后直接对工件端部 施加轴向压力, 使得工件发生弹性变形或微小塑性变形, 在工件内累加高静水压力; 随 后对与工件内壁或外壁接触的一个约束体提供扭矩, 使其绕工件的中心轴转动, 同时固 定另一个约束体, 在约束体与工件内外壁环向摩擦力的作用下, 工件内部沿径向不同厚 度处的材料以不同的角速度转动, 从而实现工件的环向剪切变形。  The technical solution for achieving the object of the present invention is: a high-pressure shear deformation method for a tubular material, first selecting a machined workpiece, the workpiece is tubular, and constraining the inner and outer walls of the workpiece respectively; then directly applying an axial direction to the end of the workpiece The pressure causes the workpiece to undergo elastic deformation or slight plastic deformation, accumulating high hydrostatic pressure in the workpiece; then providing a torque to a constraining body in contact with the inner or outer wall of the workpiece to rotate around the central axis of the workpiece while fixing another binding body Under the action of the frictional force between the restraining body and the inner and outer walls of the workpiece, the materials at different thicknesses in the radial direction of the workpiece rotate at different angular velocities, thereby achieving the circumferential shear deformation of the workpiece.
一种管状材料高压剪切变形装置, 包括具有恒压功能的压力机和具有传递压力、 约 束形变以及实现部分旋转功能的模具; 所述模具包括: 上砧头、 下砧头、 固定或者可转 动的刚性芯轴以及可转动或者固定的刚性环套; 上砧头、 下砧头分别安装在压力机的上 压头和底座上, 工件放置于上砧头和下砧头之间, 上砧头下端与下砧头上端通过设置的 凸台与工件的上、 下端面接触, 凸台的截面是与工件的上、 下端面完全吻合的环形; 工 件的内部同心设有刚性芯轴, 刚性芯轴外表面与工件的内壁接触, 工件的外部同心设有 刚性环套, 刚性环套内表面与工件的外壁接触。  A high-pressure shear deformation device for a tubular material, comprising a press having a constant pressure function and a mold having a transfer pressure, a constraining deformation, and a partial rotation function; the mold comprising: an upper anvil, a lower anvil, fixed or rotatable a rigid mandrel and a rigid or fixed rigid collar; the upper anvil and the lower anvil are respectively mounted on the upper pressing head and the base of the press, and the workpiece is placed between the upper anvil and the lower anvil, the upper anvil The upper end and the upper end of the lower anvil are in contact with the upper and lower end faces of the workpiece through a boss provided, and the cross section of the boss is a ring which completely conforms to the upper and lower end faces of the workpiece; the inner part of the workpiece is concentrically provided with a rigid mandrel, a rigid mandrel The outer surface is in contact with the inner wall of the workpiece, and the outer portion of the workpiece is concentrically provided with a rigid collar, and the inner surface of the rigid collar is in contact with the outer wall of the workpiece.
本发明与现有技术相比, 其显著优点: (1 )加工工序简单。 本发明提出的 t-HPS方 法是一种在传统的具有恒压功能的挤压机上单一道次即可实现的剧烈塑性变形方法。 反 观诸如累积轧制 (ARB) 方法、 多向锻造、 等径角挤压 (ECAP) 方法以及背压 ECAP 等方法, 往往需要很多重复的工艺道次才能实现高应变量的塑性变形, 人力消耗大。 而 本方法利用刚性环套、 管状工件以及芯轴、 管状工件之间摩擦力, 转动刚性环套并固定 芯轴, 使得管状工件与刚性环套接触的外层区域相对于与芯轴接触的内层区域发生环向 剪切, 从而实现单一工艺道次下的剧烈塑性变形。 真应变为 1〜10, 甚至更高。 如前文技 术方案所述, 本发明提出的 t-HPS方法原理简单, 设备易得, 在一般的塑性成形实验室 即可实现。  Compared with the prior art, the present invention has significant advantages: (1) The processing procedure is simple. The t-HPS method proposed by the present invention is a severe plastic deformation method which can be realized in a single pass on a conventional extruder having a constant pressure function. In contrast, methods such as cumulative rolling (ARB), multi-directional forging, equal-cavity extrusion (ECAP), and back-pressure ECAP often require many repetitive process passes to achieve high strain plastic deformation, and high labor consumption. . The method utilizes a rigid collar, a tubular workpiece, and a friction between the mandrel and the tubular workpiece, rotates the rigid collar and fixes the mandrel such that the outer region of the tubular workpiece in contact with the rigid collar is in contact with the inner core The zone region is circumferentially sheared to achieve severe plastic deformation under a single process pass. The true strain is 1 to 10, or even higher. As described in the foregoing technical scheme, the t-HPS method proposed by the present invention has a simple principle and is easy to obtain, and can be realized in a general plastic forming laboratory.
(2) 能够提供的静水压力高, 因此可加工材料种类广, 加工能力强。 本发明提出的 t-HPS方法直接对管状材料轴向加压, 同时约束其径向变形, 因而可在材料内部产生静水 压力高达 15〜GPa。 这是目前包括 HPTT在内其它工艺无法达到的。 而且, 随着模具材料 的发展, 设计的改进, 所能提供的静水压力会更高。 在这种高静水压力条件进行塑性变 形, 材料表面和内部裂纹的产生和发展被有效抑制, 从而使得很多难加工材料 (如塑性 较差的镁合金等) 的可加工性提高。 众所周知, 镁合金等材料由于晶体结构为密排六方, 滑移系数量有限, 往往塑性差。对镁合金等难变形材料进行 ARB或者 ECAP加工时, 试 样经常有开裂现象。 为避免开裂, 往往需要提高加工温度, 势必增加加工成本, 更重要 的是, 随着加工温度的升高, 材料的晶粒细化效果变差, 晶粒变得粗大, 这与我们提高 材料性能的初衷相左。 相比之下, 本方法在室温条件或者较低的加热温度下即可实现对 铝、 铜、 镍、 镁、 钛、 钨及其合金以及低碳钢等众多材料的塑性加工, 从而控制和改善 其组织结构, 提高其性能。 (2) The hydrostatic pressure that can be supplied is high, so the wide range of materials that can be processed and the processing ability are strong. The t-HPS method proposed by the present invention directly pressurizes the tubular material axially while restraining its radial deformation, so that a hydrostatic pressure of up to 15~GPa can be generated inside the material. This is currently not possible with other processes including HPTT. Moreover, with the development of mold materials and the improvement of design, the hydrostatic pressure that can be provided will be higher. Plastic deformation under such high hydrostatic pressure conditions effectively suppresses the generation and development of the surface and internal cracks of the material, thereby improving the workability of many difficult-to-machine materials (such as magnesium alloys with poor plasticity). It is well known that materials such as magnesium alloys are arranged in a hexagonal shape due to the crystal structure. The slip coefficient is limited and often has poor plasticity. When ARB or ECAP is processed on difficult-to-deform materials such as magnesium alloy, the sample often cracks. In order to avoid cracking, it is often necessary to increase the processing temperature, which will inevitably increase the processing cost. More importantly, as the processing temperature increases, the grain refining effect of the material becomes worse and the grains become coarser, which improves the material properties. The original intention is opposite. In contrast, the method can achieve plastic processing of many materials such as aluminum, copper, nickel, magnesium, titanium, tungsten and their alloys, and low carbon steel at room temperature or at a lower heating temperature, thereby controlling and improving Its organizational structure enhances its performance.
(3 )能够获得的管状成品尺寸大。本发明提出的 t-HPS方法选取的加工工件呈管状, 其尺寸仅受设备规模限制。 即便是在实验室, 也可通过该方法制得〜 100mm 高的管状材 料, 具有良好的性能, 稍做后续处理即可在很多领域得到应用, 此外获得的管状材料沿 轴向剖开, 经过轧制即可获得高性能板材。 附图说明  (3) The tubular product that can be obtained is large in size. The workpiece processed by the t-HPS method proposed by the present invention is tubular, and its size is limited only by the scale of the equipment. Even in the laboratory, the tubular material of ~100mm height can be obtained by this method, which has good performance and can be applied in many fields after a little subsequent treatment. In addition, the obtained tubular material is axially cut and rolled. High performance sheeting is obtained. DRAWINGS
图 1是累积复合轧制 (ARB)技术原理示意图。  Figure 1 is a schematic diagram of the principle of cumulative composite rolling (ARB) technology.
图 2是等径角挤压 (ECAP)技术原理示意图。  Figure 2 is a schematic diagram of the principle of equal channel angular extrusion (ECAP) technology.
图 3是背压 ECAP(BP-ECAP)技术原理示意图。  Figure 3 is a schematic diagram of the principle of back pressure ECAP (BP-ECAP) technology.
图 4是高压扭转 (HPT)技术原理示意图。  Figure 4 is a schematic diagram of the principle of high voltage torsion (HPT) technology.
图 5是高压管扭转 (high-pressure tube twisting-HPTT)技术原理示意图。  Figure 5 is a schematic diagram of the principle of high-pressure tube twisting (HPTT) technology.
图 6是本发明 t-HPS技术原理示意图, 其中, 61-上砧头, 62-刚性环套, 63-管状工 件, 64-下砧头, 65-刚性芯轴; h为管状工件高度; r为管状工件内半径; R管状工件外 半径; P为压力; T为扭矩。  Figure 6 is a schematic diagram of the t-HPS technology of the present invention, wherein: 61-upper anvil, 62-rigid collar, 63-tubular workpiece, 64-lower anvil, 65-rigid mandrel; h is the height of the tubular workpiece; The inner radius of the tubular workpiece; the outer radius of the R tubular workpiece; P is the pressure; T is the torque.
图 7是有限元模拟尺寸为 r=10mm, R=llmm 的 2219T62铝合金管状工件经过 90° 环向剪切变形后的应变分布情况:沿径向最大应变 10.79,最小应变 8.41,统计平均值 9.45。  Fig. 7 is the strain distribution of a 2219T62 aluminum alloy tubular workpiece with a finite element simulation size of r=10mm and R=llmm after 90° hoop shear deformation: maximum radial strain 10.79, minimum strain 8.41, statistical average 9.45 .
图 8是 t-HPS剧烈塑性变形方法实施方案的装置示意图, 其中, (a)为爆炸视图: 1- 支撑柱, 2-上砧头连接套筒, 3-上砧头连接螺栓, 4-连接套筒方形插销, 5-连接套筒圆柱 插销, 6-下砧头, 7-管状工件, 8-刚性环套, 9-下环形垫圈, 10-上环形垫圈, 11-一体化 的上砧头与芯轴, 12-芯轴套板, 13-下砧头连接螺栓, 14-伺服电机, 15-空心轴减速器齿 轮箱, 16-皮带, 17-推力轴承, 18-刚性环套套筒, 19-套筒连接螺栓; (b)为主视图。 具体实施方式  Figure 8 is a schematic view of the apparatus for the t-HPS severe plastic deformation method embodiment, wherein (a) is an exploded view: 1- support column, 2-upper anvil connection sleeve, 3-upper anvil connection bolt, 4-connection Sleeve square pin, 5-connected sleeve cylindrical pin, 6-lower anvil, 7-tubular workpiece, 8-rigid ring sleeve, 9-lower annular washer, 10-upper annular washer, 11-integrated upper anvil With mandrel, 12-core bushing plate, 13-lower anvil connecting bolt, 14-servo motor, 15-hollow shaft reducer gearbox, 16-belt, 17-thrust bearing, 18-rigid ring sleeve, 19-sleeve connecting bolt; (b) main view. Detailed ways
本发明的材料加工目的在传统的具有恒压功能的挤压机上即可实现: 管状工件被放 置在下砧头上, 工件外侧套有可转动的刚性环套, 刚性芯轴从管状工件的中心穿过, 上 砧头直接将轴向压力传递给工件, 管状工件在巨大轴向压力的作用下产生沿径向膨胀的 趋势, 刚性圆盘、 芯轴对管状工件径向变形起到约束作用, 这种对管状工件端部施加高 压的同时限制其形变的设计使得在工件内部累加了高静水压力 (lGPa〜15GPa)。 高静水压 力条件下, 将会在管状工件的内外壁都产生很大的摩擦力。 虽然管状工件形状改变被限 制, 但其有沿轴向旋转的自由度, 而上下砧头分别安装在挤压机的上下底板上, 使与工 件内壁或者外壁接触的约束体 (分别为芯轴和刚性环套) 中的一个绕管状工件的中心轴 转动而另外一个固定, 由于管状工件的内外壁与设备约束体之间摩擦力存在, 工件内、 外壁附近的材料有随约束体一起转动或者固定不动的趋势。 高静水压力条件下, 为了保 持材料的连续性, 管状工件沿径向不同厚度层的材料将以不同的角速度转动, 即发生相 对转动, 材料在摩擦力的驱动下实现环向剪切 (circumferential shearing)变形, 很重要的一 点是该变形是工件内部材料的切变, 并未改变管状工件的宏观尺寸形状。 The material processing object of the present invention can be realized on a conventional extruder having a constant pressure function: a tubular workpiece is placed on the lower anvil, and a rectangular outer sleeve is provided with a rotatable rigid ring sleeve, and the rigid mandrel is worn from the center of the tubular workpiece. Over, on The anvil directly transmits axial pressure to the workpiece, and the tubular workpiece has a tendency to expand radially under the action of a large axial pressure. The rigid disc and the mandrel constrain the radial deformation of the tubular workpiece. The design of the end of the workpiece while applying high pressure while limiting its deformation causes a high hydrostatic pressure (lGPa~15 GPa) to be accumulated inside the workpiece. Under high hydrostatic pressure conditions, a large amount of friction will be generated on the inner and outer walls of the tubular workpiece. Although the shape change of the tubular workpiece is limited, it has the degree of freedom of rotation in the axial direction, and the upper and lower anvils are respectively mounted on the upper and lower bottom plates of the extruder, so that the binding bodies (the mandrel and the respectively respectively are in contact with the inner wall or the outer wall of the workpiece) One of the rigid ring sleeves rotates around the central axis of the tubular workpiece and the other one is fixed. Due to the friction between the inner and outer walls of the tubular workpiece and the device binding body, the material near the inner and outer walls of the workpiece rotates or fixes with the binding body. The trend of not moving. Under high hydrostatic pressure conditions, in order to maintain the continuity of the material, the material of the tubular workpiece in different thickness layers in the radial direction will rotate at different angular velocities, that is, relative rotation occurs, and the material is driven by friction to achieve circumferential shearing. ) Deformation, it is important that the deformation is the shear of the material inside the workpiece and does not change the macroscopic shape of the tubular workpiece.
本发明能使管状材料真正在高静水压力 (可达 15〜GPa)条件下, 发生环向剪切塑性 变形 (真应可达 10〜)。 从而通过塑性变形, 控制和优化材料的组织结构、 提高其性能。  The invention enables the tubular material to undergo a circumferential shear plastic deformation under the condition of high hydrostatic pressure (up to 15~GPa) (it should be up to 10~). Thereby controlling and optimizing the structure of the material and improving its performance through plastic deformation.
同时, 本发明只需要在传统的具有恒压功能的挤压设备上安装一个由上砧头、 芯轴、 下砧头以及刚性圆盘等关键要素构成的组合模具, 即可在较低的温度 (如室温或者较低 的加热温度)实现一种全新的剧烈塑性变形 (SPD)加工方法——管状工件高压剪切 (t-HPS) 技术。 t-HPS技术可行性高, 操作无特殊要求, 所需设备简单易得。 同时, 由于本发明是 依托传统挤压设备实现的新的塑性加工方法, 因此扩展了传统挤压设备的功用。 本发明 适用于剧烈塑性变形制备块体超细晶、 纳米晶材料的实验研究和工业生产。利用本发明, 可以制备高性能金属、合金、无机非金属材料及高分子材料。 t-HPS方法制得的样品形状 为管状, 具有很高的实际应用潜力和价值。  At the same time, the present invention only needs to install a combined mold composed of key elements such as an upper anvil, a mandrel, a lower anvil and a rigid disc on a conventional extrusion device having a constant pressure function, which can be at a lower temperature. (such as room temperature or lower heating temperature) to achieve a new severe plastic deformation (SPD) processing method - tubular workpiece high pressure shear (t-HPS) technology. The t-HPS technology is highly feasible, with no special requirements for operation, and the required equipment is simple and easy to obtain. At the same time, since the present invention is a new plastic working method realized by a conventional extrusion apparatus, the function of the conventional extrusion apparatus is expanded. The invention is suitable for experimental research and industrial production of bulk ultrafine crystal and nanocrystalline materials for severe plastic deformation. With the present invention, high-performance metals, alloys, inorganic non-metallic materials, and polymer materials can be prepared. The sample prepared by the t-HPS method has a tubular shape and has high practical application potential and value.
下面结合附图对本发明作进一步详细描述。  The invention is further described in detail below with reference to the accompanying drawings.
结合图 6, 本发明管状材料高压剪切变形方法, 首先选择加工的工件, 工件为管状, 采用约束体分别约束工件的内壁和外壁; 然后直接对工件端部施加轴向压力, 使得工件 发生弹性变形或微小塑性变形, 在工件内累加高达 l〜15GPa的静水压力; 随后对与工件 内壁或外壁接触的一个约束体提供扭矩, 使其绕工件的中心轴转动, 同时固定另一个约 束体, 在约束体与工件内外壁环向摩擦力的作用下, 工件内部沿径向不同厚度处的材料 以不同的角速度转动, 从而实现工件的环向剪切变形。  Referring to Figure 6, the high-pressure shear deformation method of the tubular material of the present invention first selects the workpiece to be processed, the workpiece is tubular, and the inner and outer walls of the workpiece are respectively restrained by the restraining body; then the axial pressure is directly applied to the end of the workpiece to make the workpiece elastic. Deformation or microplastic deformation, accumulating hydrostatic pressure up to 1~15 GPa in the workpiece; then providing a torque to a constraining body in contact with the inner or outer wall of the workpiece, rotating it around the central axis of the workpiece while fixing another constraint, Under the action of the frictional force between the restraining body and the inner and outer walls of the workpiece, the materials at different thicknesses in the radial direction of the workpiece rotate at different angular velocities, thereby achieving the circumferential shear deformation of the workpiece.
本发明管状材料高压剪切变形装置, 包括具有恒压功能的压力机和具有传递压力、 约束形变以及实现部分旋转功能的模具; 所述模具包括: 上砧头 61、 下砧头 64、 固定或 者可转动的刚性芯轴 65以及可转动或者固定的刚性环套 62; 上砧头 61、 下砧头 64分别 安装在压力机的上压头和底座上,工件 63放置于上砧头 61和下砧头 64之间,上砧头 61 下端与下砧头 64上端通过设置的凸台与工件 63的上、 下端面接触, 凸台的截面是与工 件 63的上、 下端面完全吻合的环形; 工件 63的内部同心设有刚性芯轴 65, 刚性芯轴 65 外表面与工件 63的内壁接触, 工件 63的外部同心设有刚性环套, 刚性环套 62内表面与 工件 63的外壁接触。刚性环套 62内表面与刚性芯轴 65外表面经过毛化处理以增大与工 件 63之间的摩擦。 上砧头 61与刚性环套 62之间采用间隙配合; 刚性芯轴 65与下砧头 64之间采用间隙配合。 The tubular material high-pressure shear deformation device of the present invention comprises a press having a constant pressure function and a mold having a transfer pressure, a constraining deformation and a partial rotation function; the mold comprises: an upper anvil 61, a lower anvil 64, a fixed or a rotatable rigid mandrel 65 and a rotatable or fixed rigid collar 62; an upper anvil 61 and a lower anvil 64 are respectively mounted on the upper pressing head and the base of the press, and the workpiece 63 is placed on the upper anvil 61 and Between the lower anvils 64, the lower end of the upper anvil 61 and the upper end of the lower anvil 64 are in contact with the upper and lower end faces of the workpiece 63 through the boss provided, and the cross section of the boss is a ring which completely conforms to the upper and lower end faces of the workpiece 63. The inner portion of the workpiece 63 is concentrically provided with a rigid mandrel 65. The outer surface of the rigid mandrel 65 is in contact with the inner wall of the workpiece 63. The outer portion of the workpiece 63 is concentrically provided with a rigid collar, and the inner surface of the rigid collar 62 is in contact with the outer wall of the workpiece 63. The inner surface of the rigid collar 62 and the outer surface of the rigid mandrel 65 are textured to increase friction with the workpiece 63. A clearance fit is used between the upper anvil 61 and the rigid collar 62; a clearance fit is used between the rigid mandrel 65 and the lower anvil 64.
本发明管状材料高压剪切变形装置, 所述刚性芯轴 65或者刚性环套 62之中有一个 可转动, 另一个则为固定, 转动的角度无限制。  In the tubular material high-pressure shear deformation device of the present invention, one of the rigid mandrel 65 or the rigid cuff 62 is rotatable, and the other is fixed, and the angle of rotation is not limited.
本发明管状材料高压剪切变形装置, 所述刚性环套 62可采用单层模具设计、预应力 缠绕模具设计或预应力多层模具设计。所述上砧头 61、刚性芯轴 65为独立的两部分或者 采用一体化设计使其成为一部分; 所述上砧头 61为整体设计或者组合设计, 采用整体设 计时, 上砧头 61、 下砧头 64端部分别有与工件 63的上、 下端面形状吻合的环形凸台, 采用组合设计时, 砧头包括砧头主体和环形垫圈两部分, 环形垫圈截面与工 63端面形状 吻合。  The tubular material high-pressure shear deformation device of the present invention may adopt a single-layer mold design, a pre-stressed winding mold design or a pre-stressed multilayer mold design. The upper anvil 61 and the rigid mandrel 65 are two independent parts or are integrated into a part; the upper anvil 61 is designed as a whole or in combination, and when the overall design is used, the upper anvil 61 and the lower part The ends of the anvil 64 have annular bosses respectively conforming to the shape of the upper and lower end faces of the workpiece 63. When the combination is designed, the anvil comprises two parts, an anvil main body and an annular washer, and the annular gasket cross-section conforms to the shape of the end face of the work 63.
下面结合图 6说明依据本发明提出的剧烈塑性变形新方法具体实施细节及设备工作 情况。  The specific implementation details and equipment operation of the new method of severe plastic deformation proposed in accordance with the present invention will be described below with reference to FIG.
如图 6所示, t-HPS方法由一个包括 61-上砧头, 62-刚性环套, 64-下砧头和 65-刚性 芯轴等四部分构成的模具, 结合具有保压功能的压力机, 在 63-管状工件上实现。  As shown in Fig. 6, the t-HPS method consists of a mold consisting of a 61-upper anvil, a 62-rigid annulus, a 64-lower anvil and a 65-rigid mandrel, combined with a pressure-holding pressure. Machine, implemented on a 63-tubular workpiece.
首先, 将 61-上砧头、 64-下砧头分别安装在压力机的上底板和下底板 (或工作台) 上, 63-管状工件放置于 61-上砧头和 64-下砧头之间, 61-上砧头下端与 64-下砧头上端通 过设置的凸台与 63-管状工件的上、 下端面接触, 凸台的截面是与 63-管状工件的上、 下 端面完全吻合的环形; 63-管状工件的内部同心设有 65-刚性芯轴, 65-刚性芯轴外表面与 63-管状工件的内壁接触, 63-管状工件的外部同心设有 62-刚性环套, 62-刚性环套内表面 与 63-管状工件的外壁接触。  First, the 61-upper anvil and the 64-lower anvil are respectively mounted on the upper and lower bottom plates (or the workbench) of the press, and the 63-tubular workpiece is placed on the 61-upper anvil and the 64-lower anvil. The upper end of the 61-upper anvil and the upper end of the 64-lower anvil are in contact with the upper and lower end faces of the 63-tubular workpiece through a boss provided, and the cross section of the boss is completely coincident with the upper and lower end faces of the 63-tubular workpiece. Ring-shaped; 63- tubular workpiece is internally concentrically provided with a 65-rigid mandrel, 65-rigid mandrel outer surface is in contact with the inner wall of the 63-tubular workpiece, and 63-tubular workpiece is concentrically provided with a 62-rigid collar, 62- The inner surface of the rigid collar is in contact with the outer wall of the 63-tubular workpiece.
此时, 63-管状工件处在由 61-上砧头、 62-刚性环套、 64-下砧头和 65-刚性芯轴构成 的密闭空腔中。 然后, 压力机对 61-上砧头进行下压, 并维持压力恒定于某一数值。 61- 上砧头向下位移的过程中, 61-上砧头同样会对 3-管状工件产生向下的压力, 由于 63-管 状工件受到由 61-上砧头、 62-刚性环套、 64-下砧头和 65-刚性芯轴构成的密闭空腔的约 束, 因此其内部产生高的静水压力 (可高达〜 15GPa)。 对 62-刚性环套施加环向推力, 在扭 矩的作用下使之环向旋转, 与此同时, 61-上砧头、 64-下砧头和 65-刚性芯轴不发生旋转, 在 62-刚性环套与 63-管状工件以及 65-芯轴与 63-管状工件之间摩擦力的作用下, 63-管状 工件将发生环向剪切变形。 随着旋转角度的增大, 剪切变形量变得很大, 从而有效地控 制和优化材料的组织结构, 提高其性能。 At this time, the 63-tubular workpiece is in a closed cavity composed of a 61-upper anvil, a 62-rigid annulus, a 64-lower anvil, and a 65-rigid mandrel. Then, the press presses the 61-upper anvil and maintains the pressure constant at a certain value. 61- During the downward displacement of the upper anvil, the 61-upper anvil will also exert downward pressure on the 3-tubular workpiece, since the 63-tubular workpiece is subjected to a 61-upper anvil, a 62-rigid collar, 64 - a closed cavity formed by a lower anvil and a 65-rigid mandrel The bundle, therefore, produces a high hydrostatic pressure inside it (can be as high as ~15GPa). The circumferential thrust is applied to the 62-rigid collar, which is rotated in the direction of the torque. At the same time, the 61-upper anvil, the 64-lower anvil and the 65-rigid mandrel do not rotate, at 62- Under the action of the friction between the rigid ring sleeve and the 63-tubular workpiece and the 65-core shaft and the 63-tube workpiece, the 63-tubular workpiece will undergo circumferential shear deformation. As the angle of rotation increases, the amount of shear deformation becomes large, thereby effectively controlling and optimizing the structure of the material and improving its performance.
此外, 其它条件不变的情况下, 环向旋转 65-刚性芯轴而固定 62-刚性环套可以使管 状材料产生类似的环向剪切塑性变形效果。 这种情况的 t-HPS技术原理示意图从略。  In addition, the other conditions are the same, the circumferential rotation of the 65-rigid mandrel and the fixing of the 62-rigid ring can produce a similar hoop shear plastic deformation effect on the tubular material. The schematic diagram of the t-HPS technology in this case is omitted.
为了考察 t-HPS工艺过程中管状工件的力学行为, 特别是应变的分布情况, 而对该 方法进行了二维和三维的有限元模拟分析。有限元模拟时, 选用了 2219T62铝合金工件, 该铝合金的材料性能参数如表 1所示,该材料的流变规律可以用 Crussard-Jaoul应变硬化 模型 二 + ^^加以描述。 其中为流变应力, = 290 Mpa为屈服强度, K=248MPa为 强度系数, ^为塑性应变, n=0.36为应变硬化指数。 In order to investigate the mechanical behavior of the tubular workpiece during the t-HPS process, especially the distribution of strain, the two-dimensional and three-dimensional finite element simulation analysis of the method was carried out. In the finite element simulation, the 2219T62 aluminum alloy workpiece was selected. The material properties of the aluminum alloy are shown in Table 1. The rheological law of the material can be described by the Crussard-Jaoul strain hardening model II + ^^. Among them, the rheological stress, = 290 Mpa is the yield strength, K = 248 MPa is the strength coefficient, ^ is the plastic strain, and n = 0.36 is the strain hardening index.
简便起见, 模拟温度为室温, 并且不考虑变形过程中材料的温升和应变速率敏感性。 结果表明 t-HPS方法能够在尺寸较大的工件中累加非常高的应变量, 如图 7所示, 内径 20mm, 外径 22mm的管状工件仅仅经过 90度的环向剪切, 其最高应变达 10.78, 最低应 变达 8.41, 应变统计平均值可达到 9.45。 For simplicity, the simulated temperature is room temperature and does not take into account the temperature rise and strain rate sensitivity of the material during deformation. The results show that the t-HPS method can accumulate very high strains in large-sized workpieces. As shown in Fig. 7, a tubular workpiece with an inner diameter of 20 mm and an outer diameter of 22 mm undergoes only a 90-degree circumferential shear, and the highest strain is up to 10.78, the minimum strain is 8.41, and the average strain statistics can reach 9.45.
Figure imgf000009_0001
下面结合实施例对本发明做进一步详细说明。
Figure imgf000009_0001
The present invention will be further described in detail below with reference to the embodiments.
如图 8所示装置由 t-HPS剧烈塑性变形法原理实现部、 动力装置和连接部等三部分 组成。 图 8(a)为装置的爆炸视图, 详细给出了装置的组成细节。  As shown in Figure 8, the device consists of three parts: t-HPS severe plastic deformation principle realization part, power unit and connection part. Figure 8(a) is an exploded view of the device, detailing the composition of the device.
6-下砧头、 7-管状工件、 8-刚性环套、 9-下环形垫圈、 10-上环形垫圈、 11-一体化的 上砧头与芯轴和 12-芯轴套板组成了整个装置的原理实现部。 7-管状工件穿过 11-一体化 的上砧头与芯轴, 其上下端面各放置一个环形垫圈 (9-、 10-) , 工件被 8-刚性环套包围, 上、 下砧头 (11-、 6-)通过上、 下垫圈 (9-、 10-)对 7-管状工件轴向施压时, 11-芯轴和 8-刚性环套约束了其径向膨胀, 在工件内部累积的高静水压力。 11-芯轴末端为六棱柱, 与 12-芯轴套板中孔形状尺寸相同。芯轴插入套板中孔后, 其转动将受到约束。对 8-刚性 环套施加环向推力, 在扭矩的作用下使之旋转, 转动速度 l〜5rpm, 与此同时, 11-一体化 的上砧头和芯轴受约束而不发生旋转, 在 8-刚性环套与 7-管状工件以及 11-芯轴与 7-管 状工件之间摩擦力的作用下, 7-管状工件将发生环向剪切变形。 6-lower anvil, 7-tubular workpiece, 8-rigid ring sleeve, 9-lower annular washer, 10-upper annular washer, 11-integrated upper anvil and mandrel and 12-core bushing plate Principle implementation of the device. 7-Tubular workpiece passes through the 11-integrated upper anvil and mandrel, with an annular gasket (9-, 10-) placed on the upper and lower end faces, and the workpiece is surrounded by an 8-rigid ring, upper and lower anvils (11 -, 6-) When the 7-tubular workpiece is axially pressed by the upper and lower washers (9-, 10-), the 11-mandrel and the 8-rigid collar constrain its radial expansion and accumulate inside the workpiece. High hydrostatic pressure. The end of the 11-mandrel is a hexagonal prism. Same as the shape of the hole in the 12-core bushing. After the mandrel is inserted into the hole in the sleeve, its rotation will be constrained. Applying a circumferential thrust to the 8-rigid collar, rotating it under the action of torque, the rotation speed is l~5rpm, at the same time, the 11-integrated upper anvil and mandrel are constrained without rotation, at 8 - Under the action of the friction between the rigid collar and the 7-tubular workpiece and the 11-mandrel and the 7-tube workpiece, the 7-tubular workpiece will undergo circumferential shear deformation.
该实施方案中, 上砧头与芯轴采用一体化设计, 一方面使得芯轴易于固定, 另一方 面, 对管状工件脱模有利。 此外上、 下砧头 (11-、 6-) 并不直接接触 7-管状工件, 压力 是通过上、 下环形垫圈 (9-、 10-) 传递给工件。 这样设计是因为与工件断面直接接触的 部位受力情况非常恶劣, 增设由硬质合金制成的环形垫圈, 可提高砧头的使用寿命, 降 低模具更换成本。考虑到 8-刚性环套与 11-芯轴之间既需要沿轴向自有移动又需要沿周向 自由转动, 而 6-下砧头与 11-芯轴之间只要求沿轴向自有移动, 因此在选取孔与轴之间的 配合时, 11-一体化的上砧头、 芯轴与 8-刚性环套之间采用 F7/h6 基轴制间隙配合; 11- 一体化的上砧头、 芯轴与 6-下砧头采用 H7/g6基孔制间隙配合。 这种间隙配合的选择, 从脱模的角度考虑, 也是有利的。  In this embodiment, the upper anvil and the mandrel are integrally designed to facilitate the fixing of the mandrel on the one hand and the demolding of the tubular workpiece on the other hand. In addition, the upper and lower anvils (11-, 6-) do not directly contact the 7-tubular workpiece, and the pressure is transmitted to the workpiece through the upper and lower annular gaskets (9-, 10-). This design is because the part that is in direct contact with the workpiece section is subjected to severe stress. The addition of an annular gasket made of cemented carbide can increase the service life of the anvil and reduce the cost of mold replacement. Considering that the 8-rigid ring sleeve and the 11-core shaft need to move both in the axial direction and in the circumferential direction, the 6-lower anvil and the 11-core shaft only need to be axially owned. Move, so when selecting the fit between the hole and the shaft, the 11-integrated upper anvil, the mandrel and the 8-rigid ring are made of F7/h6 base shaft clearance fit; 11- integrated upper anvil The head, mandrel and 6-lower anvil are made of H7/g6 base hole clearance fit. This choice of clearance fit is also advantageous from the standpoint of demolding.
刚性环套旋转并在摩擦力作用下使管状工件发生环向剪切, 该动作所需扭矩依靠动 力装置实现。该动力装置通过一个 14-伺服电机通过 16-皮带轮带动 15-空心轴减速器输出 扭矩。  The rigid ring rotates and causes the tubular workpiece to be circumferentially sheared under the action of friction. The torque required for this action is achieved by the power device. The power unit drives the 15-hollow shaft reducer output torque through a 16-belt through a 14-servo motor.
由 2-上砧头连接套筒、 3-上砧头连接螺栓、 4-连接套筒方形插销和 5-连接套筒圆柱 插销组成的连接部将 11-一体化的上砧头和芯轴与压力机的上压板相连。由 1-支撑柱、 13- 下砧头连接螺栓、 17-推力轴承、 18-刚性环套套筒和 19-套筒连接螺栓组成的连接部将 The 11-integrated upper anvil and mandrel are connected by a 2-upper anvil connection sleeve, a 3-upper anvil connection bolt, a 4-connection sleeve square pin, and a 5-connection sleeve cylindrical pin. The upper platen of the press is connected. The connection made up of 1-support column, 13- lower anvil connection bolt, 17-thrust bearing, 18-rigid collar sleeve and 19-sleeve connection bolt will
6-下砧头通过 1-支撑柱与压力机的下底板相连, 同时 18-刚性环套套筒和 19-套筒连 接螺栓连接 15-空心轴减速器和 8-刚性环套, 实现扭矩的传递。 17-推力轴承降低了轴向 摩擦力对 8-刚性环套旋转的阻碍。 The 6-lower anvil is connected to the lower bottom plate of the press through the 1-support column, while the 18-rigid ring sleeve and the 19-sleeve connection bolt are connected to the 15-hollow shaft reducer and the 8-rigid ring sleeve for torque. transfer. The 17-thrust bearing reduces the axial frictional resistance to the rotation of the 8-rigid ring.
18-刚性环套采用预应力缠绕模具设计时, 内层选择硬度和韧性都较高的材质, 如模 具钢; 缠绕层采用韧性较高的材质, 如弹簧钢丝或者弹簧钢带; 外层采用韧性较高的材 质, 如中碳钢。 18-刚性环套采用预应力多层环套设计时, 内层选择硬度和韧性都较高的 材质, 如模具钢; 其它层选择韧性较高的材质, 如中碳合金钢或者模具钢。 11-一体化的 上砧头与芯轴、 下砧头在工作部位镶嵌硬质合金, 其余部位选择材质为模具钢。 9-下环 形垫圈、 10-上环形垫圈选用硬质合金或者钢结硬质合金。  When the 18-rigid ring sleeve is designed with prestressed winding mold, the inner layer selects materials with higher hardness and toughness, such as die steel; the wound layer is made of high toughness material, such as spring steel wire or spring steel strip; Higher material, such as medium carbon steel. When the 18-rigid ring sleeve is designed with prestressed multi-layer ring sleeve, the inner layer selects materials with higher hardness and toughness, such as die steel; the other layer selects materials with higher toughness, such as medium carbon alloy steel or die steel. 11-Integral The upper anvil and the mandrel and the lower anvil are inlaid with hard alloy at the working part, and the other parts are made of die steel. The 9-lower ring washer and the 10-upper ring washer are made of hard alloy or steel-bonded carbide.
具体选材如下: 模具钢为 Cr5MolV钢; 弹簧钢为 65Mn钢; 中碳钢为 45号钢; 中 碳合金钢为 45Mn钢; 硬质合金为 YG6A。 该实施方案中, 装配好的 t-HPS装置的主视图如图 8(b)所示。 The specific materials are as follows: The mold steel is Cr5MolV steel; the spring steel is 65Mn steel; the medium carbon steel is 45 steel; the medium carbon alloy steel is 45Mn steel; the hard alloy is YG6A. In this embodiment, the front view of the assembled t-HPS device is shown in Figure 8(b).
通过该方案对工业纯铝、 6063铝合金以及 AZ31镁合金管状工件进行了初步实验研 究。 管状工件的内径 40mm, 外径 46mm, 高 40mm。 变形前后, 工件的宏观尺寸、 形状 保持不变。  Through the scheme, preliminary experimental research on industrial pure aluminum, 6063 aluminum alloy and AZ31 magnesium alloy tubular workpiece was carried out. The tubular workpiece has an inner diameter of 40 mm, an outer diameter of 46 mm and a height of 40 mm. Before and after the deformation, the macro size and shape of the workpiece remain unchanged.
工业纯铝未进行 t-HPS前的平均晶粒尺寸为 24μηι, 压縮试验屈服强度 73.7MPa; 在 1.5GPa静水压力下以 lrpm的转动速度经过 30°的 t-HPS变形, 平均应变达到 4, 平均晶 粒尺寸达到 633nm, 压縮试验屈服强度增至 261.3MPa。  The average grain size of industrial pure aluminum before t-HPS is 24μηι, and the yield strength of compression test is 73.7MPa. Under the hydrostatic pressure of 1.5GPa, the t-HPS deformation is 30° at a rotation speed of 1rpm, and the average strain reaches 4, The average grain size reached 633 nm and the compression test yield strength increased to 261.3 MPa.
6063铝合金未进行 t-HPS前的平均晶粒尺寸为 80μηι,压縮试验屈服强度 156.8MPa; 在 2.5GPa静水压力以 lrpm的转动速度经过 60°的 t-HPS变形, 平均应变达到 8, 平均晶 粒尺寸达到 561nm, 压縮试验屈服强度增至 447.6MPa。  The average grain size of 6063 aluminum alloy before t-HPS is 80μηι, compression test yield strength is 156.8MPa; at 2.5GPa hydrostatic pressure, the t-HPS deformation at 60° is rotated at 60°, the average strain reaches 8, average The grain size reached 561 nm, and the compression test yield strength increased to 447.6 MPa.
AZ31镁合金塑性较差, 我们对模具进行了 100°C的加热。 未进行 t-HPS前的平均晶粒尺 寸为 27μηι, 压縮试验屈服强度 276.4MPa; 在 3GPa静水压力下以 lrpm的转动速度经过 90°的 t-HPS变形, 平均应变达到 9, 平均晶粒尺寸达到 335nm, 压縮试验屈服强度增至 590.2MPa。 The AZ31 magnesium alloy is inferior in plasticity, and we heat the mold at 100 °C. The average grain size before t-HPS was 27 μηι, the compression yield strength was 276.4 MPa; the t-HPS deformation at 90° at a rotational speed of 1 MPa under a hydrostatic pressure of 1 GP, the average strain reached 9, the average grain size At 335 nm, the compression test yield strength increased to 590.2 MPa.

Claims

权利要求书 Claim
1、 一种管状材料高压剪切变形方法, 其特征在于: 首先选择加工的工件, 工件为管 状, 采用约束体分别约束工件的内壁和外壁; 然后直接对工件端部施加轴向压力, 使得 工件发生弹性变形或微小塑性变形, 在工件内累加高静水压力; 随后对与工件内壁或外 壁接触的一个约束体提供扭矩, 使其绕工件的中心轴转动, 同时固定另一个约束体, 在 约束体与工件内外壁环向摩擦力的作用下, 工件内部沿径向不同厚度处的材料以不同的 角速度转动, 从而实现工件的环向剪切变形。 A method for high-pressure shear deformation of a tubular material, characterized in that: firstly, the workpiece is machined, the workpiece is tubular, and the inner wall and the outer wall of the workpiece are respectively restrained by the binding body; then the axial pressure is directly applied to the end of the workpiece, so that the workpiece Elastic deformation or slight plastic deformation occurs, accumulating high hydrostatic pressure in the workpiece; then providing a torque to a constraining body that is in contact with the inner or outer wall of the workpiece, rotating it around the central axis of the workpiece while fixing another binding body, in the binding body Under the action of the circumferential frictional force between the inner and outer walls of the workpiece, the materials at different thicknesses in the radial direction of the workpiece are rotated at different angular velocities, thereby achieving the circumferential shear deformation of the workpiece.
2、 根据权利要求 1 所述的管状材料高压剪切变形方法, 其特征在于: 所述工件内累 加的静水压力高达 l~15GPa。  2. The high-pressure shear deformation method of tubular material according to claim 1, wherein: the accumulated hydrostatic pressure in the workpiece is as high as l~15 GPa.
3、 一种管状材料高压剪切变形装置, 其特征在于: 包括具有恒压功能的压力机和具 有传递压力、 约束形变以及实现部分旋转功能的模具; 所述模具包括: 上砧头 [61]、 下砧 头 [64]、 固定或者可转动的刚性芯轴 [65]以及可转动或者固定的刚性环套 [62] ; 上砧头 [61]、 下砧头 [64]分别安装在压力机的上压头和底座上, 工件 [63]放置于上砧头 [61]和下砧 头 [64]之间, 上砧头 [61]下端与下砧头 [64]上端通过设置的凸台与工件 [63]的上、 下端面接 触, 凸台的截面是与工件 [63]的上、 下端面完全吻合的环形; 工件 [63]的内部同心设有刚 性芯轴 [65], 刚性芯轴 [65]外表面与工件 [63]的内壁接触, 工件 [63]的外部同心设有刚性环 套 [62], 刚性环套 [62]内表面与工件 [63]的外壁接触。  3. A tubular material high-pressure shear deformation device, comprising: a press having a constant pressure function and a mold having a transfer pressure, a constraining deformation, and a partial rotation function; the mold comprising: an upper anvil [61] , the lower anvil [64], the fixed or rotatable rigid mandrel [65] and the rotatable or fixed rigid collar [62]; the upper anvil [61] and the lower anvil [64] are respectively mounted on the press On the upper head and the base, the workpiece [63] is placed between the upper anvil [61] and the lower anvil [64], and the upper end of the upper anvil [61] and the upper end of the lower anvil [64] are passed through the provided bosses. In contact with the upper and lower end faces of the workpiece [63], the cross section of the boss is a ring that perfectly matches the upper and lower end faces of the workpiece [63]; the inner portion of the workpiece [63] is concentrically provided with a rigid mandrel [65], a rigid core The outer surface of the shaft [65] is in contact with the inner wall of the workpiece [63], and the outer portion of the workpiece [63] is concentrically provided with a rigid collar [62], and the inner surface of the rigid collar [62] is in contact with the outer wall of the workpiece [63].
4、 根据权利要求 2 所述的管状材料高压剪切变形装置, 其特征在于: 刚性环套 [62] 内表面与刚性芯轴 [65]外表面经过毛化处理以增大与工件 [63]之间的摩擦。  4. The tubular material high-pressure shear deformation device according to claim 2, wherein: the inner surface of the rigid collar [62] and the outer surface of the rigid core shaft [65] are subjected to texturing treatment to increase the workpiece [63]. The friction between.
5、 根据权利要求 2 所述的管状材料高压剪切变形装置, 其特征在于: 上砧头 [61]与 刚性环套 [62]之间采用间隙配合; 刚性芯轴 [65]与下砧头 [64]之间采用间隙配合。  5. The tubular material high-pressure shear deformation device according to claim 2, wherein: a clearance fit is used between the upper anvil [61] and the rigid collar [62]; the rigid mandrel [65] and the lower anvil A gap fit is used between [64].
6、 根据权利要求 2所述的管状材料高压剪切变形装置, 其特征在于: 所述刚性芯轴 [65]或者刚性环套 [62]之中有一个可转动, 另一个则为固定, 转动的角度无限制。  6. The tubular material high-pressure shear deformation device according to claim 2, wherein: one of the rigid mandrel [65] or the rigid collar [62] is rotatable, and the other is fixed, rotating. The angle is unlimited.
7、 根据权利要求 2所述的管状材料高压剪切变形装置, 其特征在于: 所述刚性环套 [62]可采用单层模具设计、 预应力缠绕模具设计或预应力多层模具设计。  7. The tubular material high pressure shear deformation device according to claim 2, wherein: the rigid ring sleeve [62] can adopt a single layer mold design, a prestressed winding mold design or a prestressed multilayer mold design.
8、 根据权利要求 2 所述的管状材料高压剪切变形装置, 其特征在于: 所述上砧头 [61]、 刚性芯轴 [65]为独立的两部分或者采用一体化设计使其成为一部分; 所述上砧头 [61] 为整体设计或者组合设计, 采用整体设计时, 上砧头 [61]、 下砧头 [64]端部分别有与工件 [63]的上、 下端面形状吻合的环形凸台, 采用组合设计时, 砧头包括砧头主体和环形垫圈 两部分, 环形垫圈截面与工件 [63]端面形状吻合。  8. The tubular material high-pressure shear deformation device according to claim 2, wherein: the upper anvil [61] and the rigid mandrel [65] are two independent parts or are integrated into a part. The upper anvil [61] is an overall design or a combined design. When the overall design is adopted, the ends of the upper anvil [61] and the lower anvil [64] respectively conform to the shape of the upper and lower end faces of the workpiece [63]. The annular boss has a combined design, the anvil includes an anvil body and an annular washer, and the annular gasket cross-section conforms to the shape of the end surface of the workpiece [63].
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