WO2012128510A3 - 이온성 액체를 용매로 이용한 푸르푸라놀계 화합물과 2-푸란카르복시산계 화합물의 제조방법 - Google Patents

이온성 액체를 용매로 이용한 푸르푸라놀계 화합물과 2-푸란카르복시산계 화합물의 제조방법 Download PDF

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Publication number
WO2012128510A3
WO2012128510A3 PCT/KR2012/001914 KR2012001914W WO2012128510A3 WO 2012128510 A3 WO2012128510 A3 WO 2012128510A3 KR 2012001914 W KR2012001914 W KR 2012001914W WO 2012128510 A3 WO2012128510 A3 WO 2012128510A3
Authority
WO
WIPO (PCT)
Prior art keywords
based compound
solvent
furfuranol
preparing
ionic liquid
Prior art date
Application number
PCT/KR2012/001914
Other languages
English (en)
French (fr)
Other versions
WO2012128510A2 (ko
Inventor
김백진
조진구
김상용
김영규
강은실
채다원
Original Assignee
한국생산기술연구원
서울대학교산학협력단
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 한국생산기술연구원, 서울대학교산학협력단 filed Critical 한국생산기술연구원
Priority to US14/000,500 priority Critical patent/US8889891B2/en
Publication of WO2012128510A2 publication Critical patent/WO2012128510A2/ko
Publication of WO2012128510A3 publication Critical patent/WO2012128510A3/ko

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/42—Singly bound oxygen atoms
    • C07D307/44—Furfuryl alcohol
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C07D307/48—Furfural
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/56—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D307/64—Sulfur atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/56—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D307/68—Carbon atoms having three bonds to hetero atoms with at the most one bond to halogen

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Furan Compounds (AREA)

Abstract

본 발명은 푸르푸랄계 화합물을 이온성 액체(ionic liquid)를 용매로 사용하고 알칼리 금속 또는 알칼리 토금속의 수산화물과 반응시켜 푸르푸라놀계 화합물과 2-푸란카르복시산계 화합물을 제조하는 것을 특징으로 하는 푸르푸라놀계 화합물과 2-푸란카르복시산계 화합물의 제조방법에 관한 것으로서, 반응용매로 물을 사용하지 않으므로 반응폐수가 발생하지 않고, 용매로 사용후 회수와 재사용이 용이한 이온성 액체를 반응용매로 이용하는 친환경적인 푸르푸라놀계 화합물과 2-푸란카르복시산계 화합물의 제조방법을 제공할 수 있다.
PCT/KR2012/001914 2011-03-23 2012-03-19 이온성 액체를 용매로 이용한 푸르푸라놀계 화합물과 2-푸란카르복시산계 화합물의 제조방법 WO2012128510A2 (ko)

Priority Applications (1)

Application Number Priority Date Filing Date Title
US14/000,500 US8889891B2 (en) 2011-03-23 2012-03-19 Method for preparing a furfuranol-based compound and 2-furancarboxylic acid-based compound using an ionic liquid as a solvent

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
KR1020110025675A KR101306277B1 (ko) 2011-03-23 2011-03-23 이온성 액체를 용매로 이용한 푸르푸라놀계 화합물과 2-푸란카르복시산계 화합물의 제조방법
KR10-2011-0025675 2011-03-23

Publications (2)

Publication Number Publication Date
WO2012128510A2 WO2012128510A2 (ko) 2012-09-27
WO2012128510A3 true WO2012128510A3 (ko) 2012-12-27

Family

ID=46879867

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/KR2012/001914 WO2012128510A2 (ko) 2011-03-23 2012-03-19 이온성 액체를 용매로 이용한 푸르푸라놀계 화합물과 2-푸란카르복시산계 화합물의 제조방법

Country Status (3)

Country Link
US (1) US8889891B2 (ko)
KR (1) KR101306277B1 (ko)
WO (1) WO2012128510A2 (ko)

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20080033187A1 (en) * 2006-08-07 2008-02-07 Haibo Zhao Methods for conversion of carbohydrates in ionic liquids to value-added chemicals
US20100058650A1 (en) * 2007-09-07 2010-03-11 Furanix Technologies B.V. Hydroxymethylfurfural ethers from sugars or hmf and mixed alcohols
US20100081833A1 (en) * 2007-09-07 2010-04-01 Furanix Technologies B.V. Hydroxymethylfurfural ethers and esters prepared in ionic liquids

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20080033187A1 (en) * 2006-08-07 2008-02-07 Haibo Zhao Methods for conversion of carbohydrates in ionic liquids to value-added chemicals
US20100058650A1 (en) * 2007-09-07 2010-03-11 Furanix Technologies B.V. Hydroxymethylfurfural ethers from sugars or hmf and mixed alcohols
US20100081833A1 (en) * 2007-09-07 2010-04-01 Furanix Technologies B.V. Hydroxymethylfurfural ethers and esters prepared in ionic liquids

Also Published As

Publication number Publication date
US20130345446A1 (en) 2013-12-26
WO2012128510A2 (ko) 2012-09-27
US8889891B2 (en) 2014-11-18
KR101306277B1 (ko) 2013-09-09
KR20120108114A (ko) 2012-10-05

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